CA1163022A - Apparatus for recording pulse height distribution in a fluorescent x-ray film thickness meter - Google Patents

Apparatus for recording pulse height distribution in a fluorescent x-ray film thickness meter

Info

Publication number
CA1163022A
CA1163022A CA000395563A CA395563A CA1163022A CA 1163022 A CA1163022 A CA 1163022A CA 000395563 A CA000395563 A CA 000395563A CA 395563 A CA395563 A CA 395563A CA 1163022 A CA1163022 A CA 1163022A
Authority
CA
Canada
Prior art keywords
staircase
signal
discriminator
pulse height
fluorescent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA000395563A
Other languages
French (fr)
Inventor
Toshiyuki Koga
Hiroshi Ishijima
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Seiko Instruments Inc
Original Assignee
Seiko Instruments Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Seiko Instruments Inc filed Critical Seiko Instruments Inc
Application granted granted Critical
Publication of CA1163022A publication Critical patent/CA1163022A/en
Expired legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01BMEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS; MEASURING ANGLES; MEASURING AREAS; MEASURING IRREGULARITIES OF SURFACES OR CONTOURS
    • G01B15/00Measuring arrangements characterised by the use of electromagnetic waves or particle radiation, e.g. by the use of microwaves, X-rays, gamma rays or electrons
    • G01B15/02Measuring arrangements characterised by the use of electromagnetic waves or particle radiation, e.g. by the use of microwaves, X-rays, gamma rays or electrons for measuring thickness
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01DMEASURING NOT SPECIALLY ADAPTED FOR A SPECIFIC VARIABLE; ARRANGEMENTS FOR MEASURING TWO OR MORE VARIABLES NOT COVERED IN A SINGLE OTHER SUBCLASS; TARIFF METERING APPARATUS; MEASURING OR TESTING NOT OTHERWISE PROVIDED FOR
    • G01D1/00Measuring arrangements giving results other than momentary value of variable, of general application
    • G01D1/14Measuring arrangements giving results other than momentary value of variable, of general application giving a distribution function of a value, i.e. number of times the value comes within specified ranges of amplitude
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/22Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
    • G01N23/223Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material by irradiating the sample with X-rays or gamma-rays and by measuring X-ray fluorescence
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R31/00Arrangements for testing electric properties; Arrangements for locating electric faults; Arrangements for electrical testing characterised by what is being tested not provided for elsewhere
    • G01R31/26Testing of individual semiconductor devices
    • G01R31/265Contactless testing
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2223/00Investigating materials by wave or particle radiation
    • G01N2223/07Investigating materials by wave or particle radiation secondary emission
    • G01N2223/076X-ray fluorescence

Landscapes

  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Electromagnetism (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)
  • Length-Measuring Devices Using Wave Or Particle Radiation (AREA)

Abstract

ABSTRACT
An apparatus for recording pulse height distribution of X-rays detected in a fluorescent X-ray apparatus in which a basically single channel analysis circuit is switched by means of an analog staircase signal so as to produce an output for each step of the staircase and thereby effectively give multi-channel analysis of pulse heights.

Description

APPARATUS FOR R~CORDING PULSE HEIGHT DISTRIB~TION IN A FLUORESCENT
X-RAY FILM THICRNESS METER
The present device relates to an apparatus for recording pulse helght distribution in a fluorescent X-ray f~lm thickness me~er, and more particularly to an i~proved and novel device in which the analysis of the pulse height distribution can be performed in a single channel circuit by applying a stalrcase signal, In the prior art, analysi~ of pulse height distribu~ion has required scannlng and the provision of a variable resistor at the input of a single channel circuit. Alternatively, a multi-channel device has been u3ed.
In the conventional single channel circuit arrangement, since the variable resistor i8 controlled either manually or by a motor, it is difficult to carry out the measurement accurately or to increase such accuracy.
An ob~ect of the present disclosure is to provide an effective means for eliminating the above described drawbacks. The device here disclosed applies a respective analog ~taircase signal to respective input~ of upper limlt and lower limit discrlminators connected to a comparator gate circuit to carry out the multi-channel analysis.
Specific embodiments of the invention will now be described having reference to the accompanying drawings in which:
Fig. 1 is a diagrammatic side view of an X-ray apparatus for measuring film thickness by X-ray fluorescence, Fig, 2 i8 an electrical circuit diagram for obtalning a pulse height information from the detector of the apparatus oP Fig. 1, Fig. 3 is a graph showing a curve of pulse height distribution obtained in a typical observation, and Figs. 4 (A), 4 (B), 4 (C), and 4 (D) illustrates signals obtained in various parts of the circuit of Fig. 2.

. ~

3~
An apparatus for recording pulse height distribution ln a fluorescent X-ray film thlckness meter wlll now be described in more detail in con~unction with the at~ached drawings. An X-ray tube 1 delivers X-radiation (shown by the broken line in Fig. 1) through a collimator 2 to a sample 3. Fluorescing X-rays from the sample 3 are reused in a detector 4. An output signal from the detector 4 i8 applied to the input terminal 5 shown in Fig. 2 which feeds the input of an upper limit discriminator 6 and a lower limit discriminator 7. A
staircase analog signal from respective signal generators 8 and 9 is applied to each other input terminal of the discriminators 6 and 7. The outputs from the discriminators 6 and 7 are applied to the inputs of comparator gate circuit 10, whose output in ~urn is fed to a counter 11 and a display device 12. The output from the analog signal generator 9 is applied to the display 12.
The operation of the apparatus is as follows.
The signal from the detector 4 is shown in Fig. 4 ~A)~ When this signal is applied to the differential amplifiers 6 and 7 (which act as level discriminators), each pulse which has a level equal to or greater than LL
(lower llmit) shown at (B) in Fig. 4 is passed to the comparator ate circuit 10 by the lower limit discriminator 6, and each pulse having a level equal to or greater than UL (upper limit) shown at (C) Ln Fig. 4 is passed to the comparator gate circuit 10 by the upper Limit discrimlnator 7. The upper and lower limlts are determined in each instance by the level of the staircase signal present on the respective other input terminalc of di6criminators 6 and 7 at that timaO
The signal shown at (D) in Fig. 4 is produced by the comparator gate circuit 10 which suppresses all pulses exceeding the upper limit and passes there~ore only those of amplitude between the lower and upper limits. The output of circult 10 is passed to the counter 11 and also to the display 12.

1~3~2 Let us assume that this first reading has been taken with the staircase signals synchronized and at their first ~teps. At a later time instant the staircase signals will present their second steps to the respectlve discrimlnators 6 and 7, thus setting new lower and uppar limits. A second pulse spectrum will be obtained. Later the third steps of the staircases will determine the next lower and upper limlts and so on. By feeding at least one of the synchronized staircases to the display 12 the pulse amplitude range belng measured at each instant can be lndlcated.
Thus by switchlng this single channel apparatus using the stalrcase signals, multi-channel analysis is performed and the pulse height distribution curve shown in Fig. 3 can be obtalned.
The pulse height distributlon curve shown in Fig. 3 ls the result of analysis for a sample of copper plated with silver. In this curve, the lower lntensity portion is due to X-ray fluorescence of Cu and that at high intensity is due to X-ray fluorescence of Ag.
Thls apparatus therefore allows the productlon of a pulse height dlstribution record automatically from a circuit of little greater complexity than a slngle channel device.

Claims

THE EMBODIMENTS OF THE INVENTION IN WHICH AN EXCLUSIVE PROPERTY
OR PRIVILEGE IS CLAIMED ARE DEFINED AS FOLLOWS:
1. An apparatus for recording pulse height distribution of fluorescing X-rays in a film thickness meter, comprising:
a pair of analog signal generators for generating a staircase signal;
an upper limit discriminator and a lower limit discriminator, each having a first input terminal for a respective staircase signal from a respective said signal generator;
input means for receiving a detected signal from a fluorescent X-ray detector for applying said detected signal to a respective second input terminal of said upper limit discriminator and said lower limit discriminator, respectively;
a comparator gate circuit for output signals from said upper limit discriminator and said lower limit discriminator;
a counter connected to said comparator circuit;
a display device connected to said counter;
an input means on said display device for one of said staircase signals from its respective generator device; and said discriminators passing only pulses from said detected signal of amplitude exceeding respective lower and upper limits determined by aid staircase signals, said comparator gate passing only pulses exceeding said lower limit but suppressing pulses exceeding said upper limit, whereby a count and display of pulses falling between said lower and upper limits for each step of said staircase signals is obtained.
CA000395563A 1981-02-04 1982-02-04 Apparatus for recording pulse height distribution in a fluorescent x-ray film thickness meter Expired CA1163022A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP1467881U JPS57129111U (en) 1981-02-04 1981-02-04
JP14678/81 1981-02-04

Publications (1)

Publication Number Publication Date
CA1163022A true CA1163022A (en) 1984-02-28

Family

ID=11867869

Family Applications (1)

Application Number Title Priority Date Filing Date
CA000395563A Expired CA1163022A (en) 1981-02-04 1982-02-04 Apparatus for recording pulse height distribution in a fluorescent x-ray film thickness meter

Country Status (6)

Country Link
JP (1) JPS57129111U (en)
CA (1) CA1163022A (en)
DE (1) DE3203746A1 (en)
FR (1) FR2499240A1 (en)
GB (1) GB2096313A (en)
NL (1) NL8200300A (en)

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3440537A (en) * 1963-08-20 1969-04-22 Non Linear Systems Inc Bar-graph display instrument
JPS5810098Y2 (en) * 1973-05-07 1983-02-24 株式会社小松製作所 Yuatsu Sokutei Souchi
US4129827A (en) * 1976-05-20 1978-12-12 Southwick R Amplitude probability detector

Also Published As

Publication number Publication date
DE3203746A1 (en) 1982-09-02
JPS57129111U (en) 1982-08-12
FR2499240A1 (en) 1982-08-06
NL8200300A (en) 1982-09-01
GB2096313A (en) 1982-10-13

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