CA1066484A - Method for heavy-water production by the h2s-h2o chemical exchange process - Google Patents
Method for heavy-water production by the h2s-h2o chemical exchange processInfo
- Publication number
- CA1066484A CA1066484A CA242,154A CA242154A CA1066484A CA 1066484 A CA1066484 A CA 1066484A CA 242154 A CA242154 A CA 242154A CA 1066484 A CA1066484 A CA 1066484A
- Authority
- CA
- Canada
- Prior art keywords
- liquid
- tower
- cold
- pressure
- cold tower
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims abstract description 20
- 230000008569 process Effects 0.000 title claims abstract description 10
- XLYOFNOQVPJJNP-ZSJDYOACSA-N Heavy water Chemical compound [2H]O[2H] XLYOFNOQVPJJNP-ZSJDYOACSA-N 0.000 title abstract description 20
- 238000004519 manufacturing process Methods 0.000 title abstract description 7
- 239000000126 substance Substances 0.000 title 1
- 239000007788 liquid Substances 0.000 claims abstract description 41
- 238000000926 separation method Methods 0.000 claims abstract description 14
- 239000007791 liquid phase Substances 0.000 claims abstract description 4
- 230000006872 improvement Effects 0.000 claims description 2
- 239000002518 antifoaming agent Substances 0.000 abstract description 5
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 55
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 14
- 239000007789 gas Substances 0.000 description 11
- 238000013461 design Methods 0.000 description 7
- 230000008901 benefit Effects 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- 239000012071 phase Substances 0.000 description 4
- 230000007480 spreading Effects 0.000 description 4
- 238000003892 spreading Methods 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- 238000005187 foaming Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- YZCKVEUIGOORGS-OUBTZVSYSA-N Deuterium Chemical compound [2H] YZCKVEUIGOORGS-OUBTZVSYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 229910052805 deuterium Inorganic materials 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 238000010793 Steam injection (oil industry) Methods 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000001143 conditioned effect Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 230000004001 molecular interaction Effects 0.000 description 1
- 238000010587 phase diagram Methods 0.000 description 1
- BALXUFOVQVENIU-KXNXZCPBSA-N pseudoephedrine hydrochloride Chemical compound [H+].[Cl-].CN[C@@H](C)[C@@H](O)C1=CC=CC=C1 BALXUFOVQVENIU-KXNXZCPBSA-N 0.000 description 1
- 230000003134 recirculating effect Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 238000009966 trimming Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B5/00—Water
- C01B5/02—Heavy water; Preparation by chemical reaction of hydrogen isotopes or their compounds, e.g. 4ND3 + 7O2 ---> 4NO2 + 6D2O, 2D2 + O2 ---> 2D2O
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Water Treatments (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA242,154A CA1066484A (en) | 1975-12-19 | 1975-12-19 | Method for heavy-water production by the h2s-h2o chemical exchange process |
| US05/721,113 US4125598A (en) | 1975-12-19 | 1976-09-07 | Method for heavy-water production by H2 S-H2 O chemical exchange process |
| GB42183/76A GB1500887A (en) | 1975-12-19 | 1976-10-11 | Heavy water production |
| AU18753/76A AU506021B2 (en) | 1975-12-19 | 1976-10-15 | Heavy-water production by h2s-h20 chemical |
| DE19762647193 DE2647193A1 (de) | 1975-12-19 | 1976-10-19 | Verfahren und vorrichtung zur herstellung von schwerem wasser mit hilfe eines chemischen h tief 2 s-h tief 2 o- austausches |
| RO7688736A RO72136A (ro) | 1975-12-19 | 1976-12-15 | Procedeu de obtinere a apei grele |
| JP51150408A JPS5277895A (en) | 1975-12-19 | 1976-12-16 | Method of operating heavy water producing plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA242,154A CA1066484A (en) | 1975-12-19 | 1975-12-19 | Method for heavy-water production by the h2s-h2o chemical exchange process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1066484A true CA1066484A (en) | 1979-11-20 |
Family
ID=4104788
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA242,154A Expired CA1066484A (en) | 1975-12-19 | 1975-12-19 | Method for heavy-water production by the h2s-h2o chemical exchange process |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US4125598A (index.php) |
| JP (1) | JPS5277895A (index.php) |
| AU (1) | AU506021B2 (index.php) |
| CA (1) | CA1066484A (index.php) |
| DE (1) | DE2647193A1 (index.php) |
| GB (1) | GB1500887A (index.php) |
| RO (1) | RO72136A (index.php) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB202214710D0 (en) | 2022-10-06 | 2022-11-23 | Nacamed As | New methods for production of deuterium oxide and deuterium gas |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2954279A (en) * | 1954-02-23 | 1960-09-27 | Rensselaer Polytech Inst | Method of manufacturing heavy water |
| US2952525A (en) * | 1955-10-20 | 1960-09-13 | Rensselaer Polytech Inst | Method of manufacturing heavy water |
| US2967089A (en) * | 1955-11-25 | 1961-01-03 | Houdry Process Corp | Process for making heavy water |
-
1975
- 1975-12-19 CA CA242,154A patent/CA1066484A/en not_active Expired
-
1976
- 1976-09-07 US US05/721,113 patent/US4125598A/en not_active Expired - Lifetime
- 1976-10-11 GB GB42183/76A patent/GB1500887A/en not_active Expired
- 1976-10-15 AU AU18753/76A patent/AU506021B2/en not_active Expired
- 1976-10-19 DE DE19762647193 patent/DE2647193A1/de not_active Withdrawn
- 1976-12-15 RO RO7688736A patent/RO72136A/ro unknown
- 1976-12-16 JP JP51150408A patent/JPS5277895A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| DE2647193A1 (de) | 1977-06-23 |
| JPS5277895A (en) | 1977-06-30 |
| AU506021B2 (en) | 1979-12-13 |
| AU1875376A (en) | 1978-04-20 |
| JPS5526891B2 (index.php) | 1980-07-16 |
| GB1500887A (en) | 1978-02-15 |
| US4125598A (en) | 1978-11-14 |
| RO72136A (ro) | 1982-02-26 |
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