BRPI0909427A2 - loaded resins and method for the production of loaded resins - Google Patents

loaded resins and method for the production of loaded resins

Info

Publication number
BRPI0909427A2
BRPI0909427A2 BRPI0909427A BRPI0909427A BRPI0909427A2 BR PI0909427 A2 BRPI0909427 A2 BR PI0909427A2 BR PI0909427 A BRPI0909427 A BR PI0909427A BR PI0909427 A BRPI0909427 A BR PI0909427A BR PI0909427 A2 BRPI0909427 A2 BR PI0909427A2
Authority
BR
Brazil
Prior art keywords
loaded resins
production
resins
loaded
Prior art date
Application number
BRPI0909427A
Other languages
Portuguese (pt)
Inventor
Brant U Kolb
James M Nelson
Matthew N Archibald
Steven C Hackett
Wendy L Thompson
William J Schultz
Original Assignee
3M Innovative Proferties Company
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 3M Innovative Proferties Company filed Critical 3M Innovative Proferties Company
Publication of BRPI0909427A2 publication Critical patent/BRPI0909427A2/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/20—Compounding polymers with additives, e.g. colouring
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/04—Ingredients treated with organic substances
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/002—Methods
    • B29B7/005—Methods for mixing in batches
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/02—Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type
    • B29B7/06—Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type with movable mixing or kneading devices
    • B29B7/10—Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type with movable mixing or kneading devices rotary
    • B29B7/18—Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type with movable mixing or kneading devices rotary with more than one shaft
    • B29B7/20—Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type with movable mixing or kneading devices rotary with more than one shaft with intermeshing devices, e.g. screws
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/80—Component parts, details or accessories; Auxiliary operations
    • B29B7/82—Heating or cooling
    • B29B7/826—Apparatus therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/80—Component parts, details or accessories; Auxiliary operations
    • B29B7/86—Component parts, details or accessories; Auxiliary operations for working at sub- or superatmospheric pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00—Mixing; Kneading
    • B29B7/80—Component parts, details or accessories; Auxiliary operations
    • B29B7/88—Adding charges, i.e. additives
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/005—Reinforced macromolecular compounds with nanosized materials, e.g. nanoparticles, nanofibres, nanotubes, nanowires, nanorods or nanolayered materials
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L101/00—Compositions of unspecified macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2323/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
    • C08J2323/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
    • C08J2323/04—Homopolymers or copolymers of ethene
BRPI0909427A 2008-03-28 2009-03-26 loaded resins and method for the production of loaded resins BRPI0909427A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US4032908P 2008-03-28 2008-03-28
PCT/US2009/038408 WO2009120868A2 (en) 2008-03-28 2009-03-26 Filled resins and method for making filled resins

Publications (1)

Publication Number Publication Date
BRPI0909427A2 true BRPI0909427A2 (en) 2015-11-03

Family

ID=41114717

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0909427A BRPI0909427A2 (en) 2008-03-28 2009-03-26 loaded resins and method for the production of loaded resins

Country Status (7)

Country Link
US (1) US8487019B2 (en)
EP (1) EP2265669B1 (en)
JP (1) JP5711111B2 (en)
KR (2) KR20160093114A (en)
CN (1) CN102037066B (en)
BR (1) BRPI0909427A2 (en)
WO (1) WO2009120868A2 (en)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BRPI0910033A2 (en) 2008-03-28 2015-12-29 3M Innovative Properties Co process for modifying particle surfaces
KR20150143864A (en) 2008-04-25 2015-12-23 쓰리엠 이노베이티브 프로퍼티즈 컴파니 Process for the surface modification of particles
WO2010138440A1 (en) * 2009-05-26 2010-12-02 3M Innovative Properties Company Process for making filled resins
DE102009045503A1 (en) 2009-10-08 2011-04-14 Wacker Chemie Ag Crosslinkable compositions based on organosilicon compounds
DE102009053965B4 (en) * 2009-11-19 2016-06-02 Siemens Aktiengesellschaft With a potting compound poured gradient coil
JP5798129B2 (en) 2010-02-11 2015-10-21 スリーエム イノベイティブ プロパティズ カンパニー Resin system containing dispersed multimode surface modified nanoparticles
JP5809241B2 (en) 2010-04-20 2015-11-10 スリーエム イノベイティブ プロパティズ カンパニー Pressure sensitive adhesive containing polymer surface modified nanoparticles
DE102010022523B4 (en) 2010-06-02 2017-09-14 Siemens Healthcare Gmbh Gradient coil with cast in a potting coil windings
CN103261086B (en) * 2010-12-13 2016-08-03 3M创新有限公司 The surface-modified nano calcite being dried
DE102011009433A1 (en) * 2011-01-26 2012-07-26 Gneuß Kunststofftechnik GmbH Method and device for introducing nanoparticles in plastic melts
JP6148241B2 (en) * 2011-10-24 2017-06-14 スリーエム イノベイティブ プロパティズ カンパニー Nanosilica-containing bismaleimide-containing composition
BR112014011936A2 (en) 2011-11-16 2017-05-30 3M Innovative Properties Co nanosilic containing polycyanate ester compositions
US8840996B2 (en) 2011-12-19 2014-09-23 Exxonmobil Research And Engineering Company Processes for making polyolefin nanocomposites
JP5440968B1 (en) * 2012-07-20 2014-03-12 三菱瓦斯化学株式会社 Method for producing resin composition containing active particles
CN103263360B (en) * 2012-12-07 2015-09-30 璨圆光电股份有限公司 Dentistry composite resin of matching nature tooth and preparation method thereof
US10011699B2 (en) 2014-08-29 2018-07-03 3M Innovative Properties Company Inductively curable composition
JP5858311B1 (en) 2015-01-23 2016-02-10 富田製薬株式会社 Hygroscopic inorganic filler-containing polyolefin composition and molded body using the same
TWI671364B (en) 2015-12-30 2019-09-11 美商聖高拜陶器塑膠公司 Modified nitride particles, oligomer functionalized nitride particles and polymer based composites
US11015040B2 (en) 2016-11-07 2021-05-25 3M Innovative Properties Company Curable resin including nanoparticles including surface-bonded hydrophobically-modifying alkyl groups
CN109593151B (en) * 2017-09-30 2022-04-08 中国石油化工股份有限公司 Process and system for producing polyalphaolefin, polyalphaolefin and continuous reactor
CN108084501A (en) * 2017-12-22 2018-05-29 贺州市星辉科技有限公司 A kind of pearl filler and preparation method thereof
KR102020146B1 (en) 2018-03-06 2019-09-09 지경수 Body Correction Machine
CN109043702B (en) * 2018-08-25 2020-07-10 威海迪尚医疗科技有限公司 Medical washable antibacterial isolation clothes
GB2605646A (en) * 2021-04-09 2022-10-12 Landa Labs 2012 Ltd Dispersion of nanoparticles in a polymeric matrix
CN115850913B (en) * 2022-12-02 2024-03-08 西南石油大学 Preparation method of environment-friendly nano intumescent flame retardant mBN@LDH@PATP and epoxy resin nanocomposite

Family Cites Families (54)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2801185A (en) * 1952-05-16 1957-07-30 Du Pont Silica hydrosol powder
US3018262A (en) * 1957-05-01 1962-01-23 Shell Oil Co Curing polyepoxides with certain metal salts of inorganic acids
US3298998A (en) * 1961-03-07 1967-01-17 Eastman Kodak Co Bisglycidyl ethers of bisphenols
FR1536946A (en) * 1967-02-28 1968-09-02 Rhodiaceta New bis-maleamic compounds
FR1555564A (en) * 1967-07-13 1969-01-31
DE1694348C3 (en) * 1967-11-21 1975-09-25 Enka Glanzstoff Ag, 5600 Wuppertal Process for continuously mixing a pigment dispersion into a polyamide melt
BE754723A (en) * 1969-08-12 1971-02-11 Rhone Poulenc Sa PROCESS FOR PREPARING
US4076550A (en) * 1971-08-17 1978-02-28 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler Reinforcing additive
CH615935A5 (en) * 1975-06-19 1980-02-29 Ciba Geigy Ag
US4157360A (en) * 1978-04-26 1979-06-05 Allied Chemical Corporation Thermoformable compositions comprising a crosslinked polycyanurate polymer and a thermoplastic polymer
US4468497A (en) * 1981-03-30 1984-08-28 Hitco Elastomer modified bis-maleimide resin
US4522958A (en) * 1983-09-06 1985-06-11 Ppg Industries, Inc. High-solids coating composition for improved rheology control containing chemically modified inorganic microparticles
US5453262A (en) * 1988-12-09 1995-09-26 Battelle Memorial Institute Continuous process for production of ceramic powders with controlled morphology
DE4012457C2 (en) 1990-04-19 2003-12-04 Zinkweiss Forschungsgmbh Surface treated zinc oxide and process for its manufacture
CA2050612A1 (en) * 1990-09-21 1992-03-22 Keith Gannon Addition of additives to polymeric materials
US5648407A (en) * 1995-05-16 1997-07-15 Minnesota Mining And Manufacturing Company Curable resin sols and fiber-reinforced composites derived therefrom
JP3353552B2 (en) * 1995-06-21 2002-12-03 信越化学工業株式会社 Method for producing liquid silicone rubber base
GB9927431D0 (en) * 1999-11-22 2000-01-19 Ciba Sc Holding Ag Casting resin and process for the fabrication of resin molds
EP1110696A3 (en) * 1999-12-21 2001-11-21 General Electric Company Continuous process to prepare silicone compositions
US6388001B1 (en) * 1999-12-21 2002-05-14 General Electric Company Compounding filled silicone compositions
KR100818964B1 (en) * 2000-09-21 2008-04-04 롬 앤드 하스 캄파니 Aqueous nanocomposite dispersions: processes, compositions, and uses thereof
JP4149648B2 (en) * 2000-09-29 2008-09-10 富士フイルム株式会社 Magnetic recording medium
US7514263B2 (en) * 2001-04-02 2009-04-07 3M Innovative Properties Company Continuous process for the production of combinatorial libraries of materials
DE10117804A1 (en) * 2001-04-10 2002-10-17 Pku Pulverkautschuk Union Gmbh Powdered, siliceous filler-containing rubber powders based on rubbers present in organic solvents, process for their preparation and use
JP4164789B2 (en) * 2001-12-28 2008-10-15 日本アエロジル株式会社 Method for producing filler for resin
JP2003286306A (en) * 2002-03-28 2003-10-10 Tama Tlo Kk Manufacturing method of nano composite resin composition
EP2045439B1 (en) * 2002-05-24 2010-07-21 3M Innovative Properties Company Use of surface-modified nanoparticles for oil recovery
US7244498B2 (en) * 2002-06-12 2007-07-17 Tda Research, Inc. Nanoparticles modified with multiple organic acids
JP4456798B2 (en) 2002-07-17 2010-04-28 タマティーエルオー株式会社 Nano-composite transparent resin composition, molded article using the same, automotive part, and production method thereof
JP2004155942A (en) * 2002-11-07 2004-06-03 Nissan Motor Co Ltd Resin composition, manufacturing method therefor, molded article therewith, and automobile part
US20040102529A1 (en) * 2002-11-22 2004-05-27 Campbell John Robert Functionalized colloidal silica, dispersions and methods made thereby
JP2004331883A (en) 2003-05-09 2004-11-25 Nissan Motor Co Ltd Intermediate of composite resin composition, composite resin composition, method for producing intermediate of composite resin composition and method for producing composite resin composition
KR20060028414A (en) 2003-06-17 2006-03-29 시바 스페셜티 케미칼스 홀딩 인크. A process for the preparation of a pigment comprising a core material and at least one dielectric layer
US7169375B2 (en) * 2003-08-29 2007-01-30 General Electric Company Metal oxide nanoparticles, methods of making, and methods of use
GB0321703D0 (en) * 2003-09-16 2003-10-15 Imerys Minerals Ltd Surface modified fillers for polymer resin compositions
US7803347B2 (en) * 2005-07-01 2010-09-28 Tohoku Techno Arch Co., Ltd. Organically modified fine particles
DE102004007456A1 (en) * 2004-02-13 2005-09-01 Degussa Ag Highly filled polyolefin compounds
US7691932B2 (en) * 2004-09-27 2010-04-06 3M Innovative Properties Company Method of making a composition and nanocomposites therefrom
DE102004048230A1 (en) 2004-10-04 2006-04-06 Institut für Neue Materialien Gemeinnützige GmbH Process for the preparation of nanoparticles with customized surface chemistry and corresponding colloids
JP2008523224A (en) * 2004-12-10 2008-07-03 スリーエム イノベイティブ プロパティズ カンパニー Filled polymer composites
US7264874B2 (en) * 2004-12-22 2007-09-04 Aps Laboratory Preparation of metal chalcogenide nanoparticles and nanocomposites therefrom
US7241437B2 (en) * 2004-12-30 2007-07-10 3M Innovative Properties Company Zirconia particles
JP2007063117A (en) * 2005-08-02 2007-03-15 Nissan Chem Ind Ltd Silica sol dispersed in organic solvent and process for producing the same
JP5541864B2 (en) 2005-08-25 2014-07-09 コーティングス フォーリン アイピー カンパニー， エルエルシー Modified nanoparticles
GB2431173B (en) 2005-09-15 2010-01-13 Alexium Ltd Method for attachment of silicon-containing compounds to a surface
WO2007119993A1 (en) 2006-04-14 2007-10-25 Amorepacific Corporation Reforming method of the surface of inorganic particles
DE102006039638B3 (en) * 2006-08-24 2007-11-15 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Production of nano-composite for use e.g. in coating materials and adhesives, involves surface-modifying nano-filler with a silane, titanate or zirconate in presence of strong non-ionic base and then mixing with binder
WO2008027979A2 (en) 2006-08-29 2008-03-06 3M Innovative Properties Company Resin systems including reactive surface-modified nanoparticles
US7834083B2 (en) * 2006-10-11 2010-11-16 Samsung Electro-Mechanics Co., Ltd. Nanocomposite composition comprising transparent nanoparticles
EP2234922B1 (en) 2007-12-28 2011-08-31 3M Innovative Properties Company Acicular boehmite nanoparticles
BRPI0910033A2 (en) 2008-03-28 2015-12-29 3M Innovative Properties Co process for modifying particle surfaces
KR20150143864A (en) 2008-04-25 2015-12-23 쓰리엠 이노베이티브 프로퍼티즈 컴파니 Process for the surface modification of particles
CN102317361B (en) 2008-12-19 2014-07-02 3M创新有限公司 Nanocalcite composites
WO2010138440A1 (en) * 2009-05-26 2010-12-02 3M Innovative Properties Company Process for making filled resins

Also Published As

Publication number Publication date
EP2265669B1 (en) 2018-02-21
EP2265669A4 (en) 2012-12-19
KR20110003504A (en) 2011-01-12
EP2265669A2 (en) 2010-12-29
WO2009120868A2 (en) 2009-10-01
KR20160093114A (en) 2016-08-05
JP5711111B2 (en) 2015-04-30
JP2011516638A (en) 2011-05-26
WO2009120868A3 (en) 2009-12-17
CN102037066B (en) 2014-11-19
KR101857805B1 (en) 2018-05-14
CN102037066A (en) 2011-04-27
US8487019B2 (en) 2013-07-16
US20110028605A1 (en) 2011-02-03

Similar Documents

Publication Publication Date Title
BRPI0909427A2 (en) loaded resins and method for the production of loaded resins
BRPI0907654A2 (en) method for producing an article and article
BRPI0719843A2 (en) METHOD FOR THE PRODUCTION OF BISBENZOXAZOIS
BRPI0915208A2 (en) method and apparatus for the manufacture of torrified lignocellulosic material
BRPI0906906A2 (en) Method for preparing a compound and compound
BR112012015322A2 (en) proppant and method for forming the proppant
BR112013012801A2 (en) method for the production of footwear and footwear
BRPI1014911A2 (en) process for manufacturing loaded resins
BRPI0810718A2 (en) METHOD AND APPARATUS FOR THE FORMATION OF MULTIPLE MICROCONDUCTS
BRPI0815138A2 (en) METHODS AND BODIES FOR THE GROWTH-COUPLED PRODUCTION OF 1,4-BUTANODIOL
BRPI0923748A2 (en) Method for the preparation of diols
BR112012003365A2 (en) method and device for the manufacture of titanium objects.
BRPI0922710A8 (en) method for the production of platelets
BRPI0908323A2 (en) method for producing an overmolded article
BRPI0910916A2 (en) Process for the production of a dianidroacúcar
BRPI0822518A2 (en) Method and arrangement for the manufacture of a laminated structure
BRPI0915572A2 (en) process for the manufacture of epichloroidrin
BRPI1014514A2 (en) solid powder cosmetics and method for the production thereof
BRPI0913074A2 (en) tire and method for its manufacture
BRPI0922490A2 (en) Method for beta-santalene production
BRPI1012237A2 (en) method for the production of aromatic hydrocarbons
BRPI0923299A8 (en) method for the production of sintered ore
EP2269818A4 (en) Cured film and method for production thereof
BR112012009974A2 (en) method for producing granules comprising a perticide
BRPI0923109A2 (en) method for the production of diamine derivatives

Legal Events

Date Code Title Description
B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]
B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]