BR9812909A - Process and micro-reactor for rapid classification of potential catalyst collections for catalytic properties - Google Patents

Process and micro-reactor for rapid classification of potential catalyst collections for catalytic properties

Info

Publication number
BR9812909A
BR9812909A BR9812909-0A BR9812909A BR9812909A BR 9812909 A BR9812909 A BR 9812909A BR 9812909 A BR9812909 A BR 9812909A BR 9812909 A BR9812909 A BR 9812909A
Authority
BR
Brazil
Prior art keywords
plumes
product
classification
collections
micro
Prior art date
Application number
BR9812909-0A
Other languages
Portuguese (pt)
Inventor
Martins Philip Atkins
Mehmet Senkan
Original Assignee
Bp Chemical Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from GBGB9807836.3A external-priority patent/GB9807836D0/en
Application filed by Bp Chemical Ltd filed Critical Bp Chemical Ltd
Publication of BR9812909A publication Critical patent/BR9812909A/en

Links

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00Particle spectrometers or separator tubes
    • H01J49/02Details
    • H01J49/10Ion sources; Ion guns
    • H01J49/16Ion sources; Ion guns using surface ionisation, e.g. field-, thermionic- or photo-emission
    • H01J49/161Ion sources; Ion guns using surface ionisation, e.g. field-, thermionic- or photo-emission using photoionisation, e.g. by laser
    • H01J49/162Direct photo-ionisation, e.g. single photon or multi-photon ionisation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0046Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N31/00Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
    • G01N31/10Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using catalysis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277Apparatus
    • B01J2219/00279Features relating to reactor vessels
    • B01J2219/00306Reactor vessels in a multiple arrangement
    • B01J2219/00313Reactor vessels in a multiple arrangement the reactor vessels being formed by arrays of wells in blocks
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277Apparatus
    • B01J2219/00497Features relating to the solid phase supports
    • B01J2219/00527Sheets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583Features relative to the processes being carried out
    • B01J2219/00585Parallel processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583Features relative to the processes being carried out
    • B01J2219/00596Solid-phase processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583Features relative to the processes being carried out
    • B01J2219/00603Making arrays on substantially continuous surfaces
    • B01J2219/00605Making arrays on substantially continuous surfaces the compounds being directly bound or immobilised to solid supports
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583Features relative to the processes being carried out
    • B01J2219/00603Making arrays on substantially continuous surfaces
    • B01J2219/00659Two-dimensional arrays
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068Means for controlling the apparatus of the process
    • B01J2219/00702Processes involving means for analysing and characterising the products
    • B01J2219/00707Processes involving means for analysing and characterising the products separated from the reactor apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718Type of compounds synthesised
    • B01J2219/00745Inorganic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718Type of compounds synthesised
    • B01J2219/00745Inorganic compounds
    • B01J2219/00747Catalysts
    • CCHEMISTRY; METALLURGY
    • C40COMBINATORIAL TECHNOLOGY
    • C40BCOMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B30/00Methods of screening libraries
    • C40B30/08Methods of screening libraries by measuring catalytic activity
    • CCHEMISTRY; METALLURGY
    • C40COMBINATORIAL TECHNOLOGY
    • C40BCOMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B40/00Libraries per se, e.g. arrays, mixtures
    • C40B40/18Libraries containing only inorganic compounds or inorganic materials
    • CCHEMISTRY; METALLURGY
    • C40COMBINATORIAL TECHNOLOGY
    • C40BCOMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B60/00Apparatus specially adapted for use in combinatorial chemistry or with libraries
    • C40B60/14Apparatus specially adapted for use in combinatorial chemistry or with libraries for creating libraries

Abstract

"PROCESSO E MICROREATOR PARA CLASSIFICAçãO RáPIDA DE COLETâNEAS DE CATALISADOR EM POTENCIAL QUANTO AS PROPRIEDADES CATALìTICAS". A classificação rápida das atividades e seletividades das coletâneas de catalisadores possuindo sítios de teste endereçáveis é obtida por contato de catalisadores em potencial nos sítios de teste, com correntes de reatância, formando plumas de produto nos sítios de teste endereçáveis. As plumas de produto são classificadas por passagem do feixe de radiação de um nível de energia para promover a formação de fotoíons e fotoelétrons específicos que são detectados por coletânea do microeletrodo in situ, nas proximidades do respectivo sítio de teste endereçável. Plumas de produto podem ser classificadas fileira a fileira ou todas as plumas de produto emanando de uma coletânea de catalisador total podem ser simultaneamente classificadas. São revelados reatores apropriados e microreatores para classificação de ativação de radiação."PROCESS AND MICROREATOR FOR QUICK CLASSIFICATION OF CATALYST COLLECTORS IN POTENTIAL AS CATALYTIC PROPERTIES". The rapid classification of the activities and selectivities of the collections of catalysts having addressable test sites is obtained by contacting potential catalysts at the test sites, with reactance currents, forming plumes of product at the addressable test sites. The product plumes are classified by passing the radiation beam of an energy level to promote the formation of specific photons and photoelectrons that are detected by the collection of the microelectrode in situ, in the vicinity of the respective addressable test site. Product plumes can be classified row by row or all product plumes emanating from a total catalyst collection can be classified simultaneously. Appropriate reactors and micro-reactors are revealed for the classification of radiation activation.

BR9812909-0A 1997-10-10 1998-10-08 Process and micro-reactor for rapid classification of potential catalyst collections for catalytic properties BR9812909A (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US94920397A 1997-10-10 1997-10-10
GBGB9807836.3A GB9807836D0 (en) 1998-04-14 1998-04-14 Reactors
US8741798A 1998-05-29 1998-05-29
PCT/GB1998/003023 WO1999019724A1 (en) 1997-10-10 1998-10-08 Radiation activation and screening of catalyst libraries for catalyst evaluation and reactors therefor

Publications (1)

Publication Number Publication Date
BR9812909A true BR9812909A (en) 2002-02-05

Family

ID=27269278

Family Applications (1)

Application Number Title Priority Date Filing Date
BR9812909-0A BR9812909A (en) 1997-10-10 1998-10-08 Process and micro-reactor for rapid classification of potential catalyst collections for catalytic properties

Country Status (12)

Country Link
EP (1) EP1019713A1 (en)
JP (1) JP2001520380A (en)
KR (1) KR20010031021A (en)
CN (1) CN1281551A (en)
AU (1) AU736438B2 (en)
BR (1) BR9812909A (en)
CA (1) CA2306256A1 (en)
ID (1) ID24631A (en)
NO (1) NO20001787L (en)
NZ (1) NZ503731A (en)
PL (1) PL339834A1 (en)
WO (1) WO1999019724A1 (en)

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DE19822077A1 (en) * 1998-05-16 1999-11-18 Studiengesellschaft Kohle Mbh Preparation of library of spatially separted solids by wet-chemical methods on a removable reaction plate, used e.g. to screen for new catalysts or materials
US6240790B1 (en) * 1998-11-09 2001-06-05 Agilent Technologies, Inc. Device for high throughout sample processing, analysis and collection, and methods of use thereof
BR9915268A (en) * 1998-11-12 2001-08-07 Bp Chem Int Ltd Method and apparatus for separating catalyst libraries
US7491677B2 (en) 1999-01-15 2009-02-17 Basf Catalysts Llc Combinatorial synthesis
US6749814B1 (en) 1999-03-03 2004-06-15 Symyx Technologies, Inc. Chemical processing microsystems comprising parallel flow microreactors and methods for using same
DE19913076A1 (en) * 1999-03-23 2000-10-19 Hahn Schickard Ges Device and method for applying microdroplets to a substrate
WO2001034291A2 (en) 1999-11-09 2001-05-17 Sri International High-throughput synthesis, screening and characterization of combinatorial libraries
DE19959974A1 (en) * 1999-12-13 2001-06-21 Basf Ag Process for the production of material libraries by electrochemical deposition
US6776963B1 (en) 1999-12-15 2004-08-17 Uop Llc Multiple parallel catalytic reactor assembly
US6368865B1 (en) 1999-12-15 2002-04-09 Uop Llc Combinatorial process for performing catalytic chemical reactions
US6627445B1 (en) 1999-12-15 2003-09-30 Uop Llc Process for simultaneously evaluating a plurality of catalysts
CA2327419C (en) 1999-12-15 2009-01-13 Uop Llc Combinatorial catalytic reactor
US6576196B1 (en) 1999-12-15 2003-06-10 Uop Llc Multiple parallel catalytic reactor assembly
US6770245B2 (en) 1999-12-15 2004-08-03 Uop Llc Multiple parallel processing assembly
US6342185B1 (en) 1999-12-15 2002-01-29 Uop Llc Combinatorial catalytic reactor
DE10004816A1 (en) 2000-02-04 2001-08-09 Hte Gmbh Method and device for the combinatorial production and testing of material libraries using photoacoustic analysis methods
US6627571B1 (en) 2000-03-01 2003-09-30 Symyx Technologies, Inc. Method and system for the situ synthesis of a combinatorial library of supported catalyst materials
DE10012847A1 (en) 2000-03-16 2001-09-27 Hte Gmbh Combinatorial properties inspection method for building blocks of material libraries, e.g. catalyst, involves measuring different parameters of two building blocks by infrared thermography and mass spectrometry
EP1299182A2 (en) 2000-07-07 2003-04-09 Symyx Technologies, Inc. Methods for analysis of heterogeneous catalysts in a multi-variable screening reactor
DE10036633B4 (en) * 2000-07-27 2005-03-10 Hte Ag The High Throughput Exp Arrangement in a modular design and method for the parallel testing of a plurality of components of a material library
AU2001283076A1 (en) * 2000-08-14 2002-02-25 Chevron U.S.A. Inc. Use of microchannel reactors in combinatorial chemistry
GB2366793B (en) * 2000-09-13 2005-03-09 Imperial College Chemical processing system and method
US6923939B1 (en) 2001-07-05 2005-08-02 Uop Llc Heat activated membrane introduction apparatus and method for screening materials
US6974665B2 (en) 2001-09-06 2005-12-13 University Of Nebraska In situ screening to optimize variables in organic reactions
US6808685B2 (en) 2001-09-17 2004-10-26 Uop Llc Apparatus and method for generating a plurality of isolated effluents
US20030173205A1 (en) 2002-03-12 2003-09-18 Arne Karlsson Process vessel with integral evaporator
US6989131B2 (en) 2002-03-12 2006-01-24 Uop Llc Catalytic reactor with integral evaporator
US7063982B1 (en) 2002-03-12 2006-06-20 Uop Llc Process of vaporizing and reacting a liquid feed
US6949267B2 (en) 2002-04-08 2005-09-27 Engelhard Corporation Combinatorial synthesis
ES2199080B1 (en) * 2002-07-16 2005-02-16 Universidad Politecnica De Valencia ROTARY SUPPORT AND APPARATUS FOR SPECTROSCOPIC MULTIPLE CHARACTERIZATION OF SAMPLES OF SOLID MATERIALS.
DE10234564B4 (en) * 2002-07-25 2005-06-02 Senslab-Gesellschaft Zur Entwicklung Und Herstellung Bioelektrochemischer Sensoren Mbh biosensor
US7141217B2 (en) 2002-12-05 2006-11-28 Uop Llc Elevated pressure apparatus and method for generating a plurality of isolated effluents
US7267987B2 (en) 2003-01-06 2007-09-11 Uop Llc Process and assembly for simultaneously evaluating a plurality of catalysts
JP4630264B2 (en) * 2006-11-27 2011-02-09 古河電気工業株式会社 Manufacturing method of micro chemical reaction apparatus
JP4532458B2 (en) * 2006-11-27 2010-08-25 古河電気工業株式会社 Micro chemical reactor
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Also Published As

Publication number Publication date
CA2306256A1 (en) 1999-04-22
NZ503731A (en) 2001-05-25
KR20010031021A (en) 2001-04-16
EP1019713A1 (en) 2000-07-19
ID24631A (en) 2000-07-27
JP2001520380A (en) 2001-10-30
NO20001787L (en) 2000-06-09
CN1281551A (en) 2001-01-24
NO20001787D0 (en) 2000-04-06
PL339834A1 (en) 2001-01-02
WO1999019724A1 (en) 1999-04-22
AU736438B2 (en) 2001-07-26
AU9449498A (en) 1999-05-03

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Legal Events

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B08F Application fees: application dismissed [chapter 8.6 patent gazette]

Free format text: REFERENTE A 5A,6A,7A E 8A ANUIDADES

B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]

Free format text: REFERENTE AO DESPACHO 8.6 PUBLICADO NA RPI 1909 DE 07/08/2007.