BR9507325A - Process for the manufacture of free flowing detergent granules - Google Patents

Process for the manufacture of free flowing detergent granules

Info

Publication number
BR9507325A
BR9507325A BR9507325A BR9507325A BR9507325A BR 9507325 A BR9507325 A BR 9507325A BR 9507325 A BR9507325 A BR 9507325A BR 9507325 A BR9507325 A BR 9507325A BR 9507325 A BR9507325 A BR 9507325A
Authority
BR
Brazil
Prior art keywords
paste
manufacture
free flowing
detergent granules
flowing detergent
Prior art date
Application number
BR9507325A
Other languages
Portuguese (pt)
Inventor
Achille Jules Edmond Doumen
Lucas Goovaerts
Jose Luis Vega
Original Assignee
Procter & Gamble
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Procter & Gamble filed Critical Procter & Gamble
Publication of BR9507325A publication Critical patent/BR9507325A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06Powder; Flakes; Free-flowing mixtures; Sheets
    • C11D17/065High-density particulate detergent compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0082Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00Special methods for preparing compositions containing mixtures of detergents
    • C11D11/04Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/37Polymers
    • C11D3/3746Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3757(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
    • C11D3/3761(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions in solid compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/37Polymers
    • C11D3/3746Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3769(Co)polymerised monomers containing nitrogen, e.g. carbonamides, nitriles or amines
    • C11D3/3776Heterocyclic compounds, e.g. lactam

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

The present invention provides a process for the manufacture of free flowing detergent granules having a bulk density of at least 600 g/l, comprising the steps of: a) neutralising anionic surfactant acid or acids in an excess of alkali to form a paste, and optionally mixing other surfactants with the paste, to give a total surfactant level in the paste of at least 40% by weight; b) mixing said paste with one or more powders to form a granular product; and c) optionally drying the granular product, wherein at least one of the powders in step b) is spray dried and comprises anionic polymer and cationic surfactant.
BR9507325A 1994-04-20 1995-04-20 Process for the manufacture of free flowing detergent granules BR9507325A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP94201090A EP0678573B1 (en) 1994-04-20 1994-04-20 Process for the manufacture of free-flowing detergent granules
PCT/US1995/004798 WO1995029215A1 (en) 1994-04-20 1995-04-20 Process for the manufacture of free-flowing detergent granules

Publications (1)

Publication Number Publication Date
BR9507325A true BR9507325A (en) 1997-09-30

Family

ID=8216814

Family Applications (1)

Application Number Title Priority Date Filing Date
BR9507325A BR9507325A (en) 1994-04-20 1995-04-20 Process for the manufacture of free flowing detergent granules

Country Status (12)

Country Link
EP (1) EP0678573B1 (en)
JP (1) JP2763403B2 (en)
CN (1) CN1078246C (en)
AT (1) ATE197811T1 (en)
AU (1) AU2389295A (en)
BR (1) BR9507325A (en)
CA (1) CA2187516C (en)
DE (1) DE69426356T2 (en)
ES (1) ES2152286T3 (en)
PE (1) PE4996A1 (en)
PH (1) PH31632A (en)
WO (1) WO1995029215A1 (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0745662B1 (en) * 1994-12-15 2004-06-16 Nippon Shokubai Co., Ltd. Detergent builder, process for producing the same, and detergent composition containing said builder
DE19721885A1 (en) 1997-05-26 1998-12-03 Henkel Kgaa Process for the production of granules containing cationic surfactants
DE19844523A1 (en) 1998-09-29 2000-03-30 Henkel Kgaa Granulation process
DE10163603B4 (en) 2001-12-21 2006-05-04 Henkel Kgaa Process for the preparation of builder-containing surfactant granules
DE102008059447A1 (en) * 2008-11-27 2010-06-02 Henkel Ag & Co. Kgaa Detergents and cleaning agents containing proteases from Bacillus pumilus
DE102012217877A1 (en) 2012-10-01 2013-08-14 Henkel Ag & Co. Kgaa Producing detergent composition, comprises dry neutralizing anionic surfactant and optionally other acidic components with solid neutralizing agent in free-fall mixer, and mixing product with additional particulate and/or liquid components

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3521498A1 (en) * 1984-06-20 1986-01-16 Lion Corp., Tokio/Tokyo ADDITIVE FOR DETERGENT GRANULES
JPS6272799A (en) * 1985-09-26 1987-04-03 ライオン株式会社 Granular detergent additive
JPS62146998A (en) * 1985-12-19 1987-06-30 ライオン株式会社 Granular detergent additive and its production
US4704221A (en) * 1986-10-22 1987-11-03 The Procter & Gamble Company Granular detergents which contain high levels of anionic surfactant that forms a middle-phase, surface treated with a water soluble cationic surfactant
IN170991B (en) * 1988-07-21 1992-06-27 Lever Hindustan Ltd
CA2017922C (en) * 1989-06-09 1995-07-11 Frank Joseph Mueller Formation of discrete, high active detergent granules using a continuous neutralization system
GB9001285D0 (en) * 1990-01-19 1990-03-21 Unilever Plc Detergent compositions and process for preparing them
US5066425A (en) * 1990-07-16 1991-11-19 The Procter & Gamble Company Formation of high active detergent particles
DE69221357T2 (en) * 1991-04-12 1998-03-12 Procter & Gamble Chemical structuring of surface-active pastes for the production of highly effective surfactant granules

Also Published As

Publication number Publication date
WO1995029215A1 (en) 1995-11-02
CN1078246C (en) 2002-01-23
EP0678573A1 (en) 1995-10-25
ES2152286T3 (en) 2001-02-01
DE69426356T2 (en) 2001-06-21
PH31632A (en) 1999-01-12
AU2389295A (en) 1995-11-16
ATE197811T1 (en) 2000-12-15
CN1150449A (en) 1997-05-21
CA2187516C (en) 2000-02-15
DE69426356D1 (en) 2001-01-04
PE4996A1 (en) 1996-04-01
EP0678573B1 (en) 2000-11-29
JPH09512299A (en) 1997-12-09
JP2763403B2 (en) 1998-06-11
CA2187516A1 (en) 1995-11-02

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Legal Events

Date Code Title Description
FB36 Technical and formal requirements: requirement - article 36 of industrial property law
FF Decision: intention to grant
FG9A Patent or certificate of addition granted
B24C Patent annual fee: request for for restoration

Free format text: REFERENTE 14A., 15A. E 16A. ANUIDADE(S)

B24H Lapse because of non-payment of annual fees (definitively: art 78 iv lpi)
B24F Patent annual fee: publication cancelled

Free format text: ANULADA A PUBLICACAO CODIGO 24.8 NA RPI NO 2257 DE 08/04/2014 POR TER SIDO INDEVIDA.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: REFERENTE AS 14A, 15A E 16A ANUIDADES.

B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2606 DE 15-12-2020 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.