BR112018008405A2 - method for preparing polymer microparticles with a mesh structure, and polymer microparticles with a mesh structure. - Google Patents
method for preparing polymer microparticles with a mesh structure, and polymer microparticles with a mesh structure.Info
- Publication number
- BR112018008405A2 BR112018008405A2 BR112018008405A BR112018008405A BR112018008405A2 BR 112018008405 A2 BR112018008405 A2 BR 112018008405A2 BR 112018008405 A BR112018008405 A BR 112018008405A BR 112018008405 A BR112018008405 A BR 112018008405A BR 112018008405 A2 BR112018008405 A2 BR 112018008405A2
- Authority
- BR
- Brazil
- Prior art keywords
- solid content
- polymer
- solvent mixture
- mesh structure
- polymer microparticles
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
- C08L67/04—Polyesters derived from hydroxycarboxylic acids, e.g. lactones
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Biological Depolymerization Polymers (AREA)
- Medicinal Preparation (AREA)
Abstract
a presente invenção refere-se a um método para produzir micropartículas de polímero tendo uma estrutura de rede por injeção de uma solução polimérica, obtida por dissolução de um polímero à base de poliéster, em uma mistura de solventes de carbonato de etileno (daqui em diante, chamado de ?ec?) e dimetilsulfóxido (daqui em diante, chamado de ?dmso?), em hidrocarbonetos com uma temperatura inferior à do ponto de congelamento da mistura de solventes para obter um conteúdo sólido contendo o ec/dmso/polímero e depois colocando o conteúdo sólido em água para remover a mistura de solventes do conteúdo sólido. o método compreende: (1) uma etapa de preparação da solução polimérica por dissolução de um polímero em uma mistura de solventes contendo ec e dmso para preparar uma solução polimérica; (2) uma etapa de preparação de conteúdos sólidos para colocar a solução polimérica obtida na etapa de preparação da solução polimérica em hidrocarboneto líquido com uma temperatura igual ou inferior ao ponto de congelamento da mistura de solventes para preparar conteúdos sólidos; e (3) uma etapa de remoção do solvente para separar os conteúdos sólidos obtidos na etapa de preparação de conteúdos sólidos e colocar os conteúdos sólidos separados em água para remover a mistura de solventes nos conteúdos sólidos.The present invention relates to a method for producing polymer microparticles having a mesh structure by injecting a polymeric solution obtained by dissolving a polyester-based polymer in a mixture of ethylene carbonate solvents (hereafter , called "ec") and dimethyl sulfoxide (hereinafter "dmso"), in hydrocarbons having a temperature below the freezing point of the solvent mixture to obtain a solid content containing the ec / dmso / polymer and then placing the solid content in water to remove the solvent mixture from the solid content. the method comprises: (1) a step of preparing the polymer solution by dissolving a polymer in a solvent mixture containing ec and dmso to prepare a polymer solution; (2) a solid content preparation step for placing the polymer solution obtained in the liquid hydrocarbon polymer solution preparation step at or below the freezing point of the solvent mixture to prepare solid content; and (3) a solvent removal step for separating the solid contents obtained in the solid content preparation step and placing the separated solid contents in water to remove the solvent mixture in the solid contents.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020150149151A KR101725279B1 (en) | 2015-10-27 | 2015-10-27 | Manufacturing method of polymeric microparticles having network structure |
KR10-2015-0149151 | 2015-10-27 | ||
PCT/KR2016/011862 WO2017073963A1 (en) | 2015-10-27 | 2016-10-21 | Method for producing polymer microparticles having network structure |
Publications (2)
Publication Number | Publication Date |
---|---|
BR112018008405A2 true BR112018008405A2 (en) | 2018-10-30 |
BR112018008405B1 BR112018008405B1 (en) | 2022-01-25 |
Family
ID=58581020
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR112018008405-0A BR112018008405B1 (en) | 2015-10-27 | 2016-10-21 | Method for preparing polymer microparticles with a lattice structure |
Country Status (4)
Country | Link |
---|---|
KR (1) | KR101725279B1 (en) |
CN (1) | CN108350180B (en) |
BR (1) | BR112018008405B1 (en) |
WO (1) | WO2017073963A1 (en) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR102012441B1 (en) | 2017-11-29 | 2019-08-20 | 주식회사 울트라브이 | The fabrication method of fine particle of biodegradable polymer, the fabrication method of injection including the same, and reactor for manufacturing fine particle of biodegradable polymer |
KR20230171675A (en) * | 2022-06-14 | 2023-12-21 | 주식회사 바임 | Complex, method for manufacturing the same, and filler composition for plastic surgery using the same |
KR102587872B1 (en) * | 2022-06-14 | 2023-10-12 | 주식회사 바임 | Complex, method for manufacturing the same, and filler composition for plastic surgery using the same |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20010002589A (en) * | 1999-06-16 | 2001-01-15 | 김윤 | Process for preparing biodegradable microspheres containing physiologically active agents |
KR100429000B1 (en) * | 2001-08-14 | 2004-04-28 | 한국과학기술원 | Process for Preparing Drug-embeded Biodegradable Porous Polymeric Scaffold |
CN101214947B (en) * | 2008-01-18 | 2010-06-09 | 中国科学技术大学 | Method for preparing carbon nano-tube by catalyzing and carbonizing polymer and /or asphalt |
KR101105292B1 (en) * | 2009-06-05 | 2012-01-17 | 주식회사 리젠 바이오텍 | Biodegradable polymeric microparticles and their preparation method |
KR20140094119A (en) * | 2013-01-21 | 2014-07-30 | 주식회사 바임 | A process for the preparation of polymeric microparticles |
KR101481441B1 (en) * | 2013-02-22 | 2015-01-13 | 주식회사 바임 | A process for the preparation of polylactic acid microparticles by a spray method |
KR101831079B1 (en) * | 2013-08-09 | 2018-02-21 | 킴벌리-클라크 월드와이드, 인크. | Microparticles having a multimodal pore distribution |
-
2015
- 2015-10-27 KR KR1020150149151A patent/KR101725279B1/en active IP Right Review Request
-
2016
- 2016-10-21 BR BR112018008405-0A patent/BR112018008405B1/en active IP Right Grant
- 2016-10-21 WO PCT/KR2016/011862 patent/WO2017073963A1/en active Application Filing
- 2016-10-21 CN CN201680062806.0A patent/CN108350180B/en active Active
Also Published As
Publication number | Publication date |
---|---|
CN108350180B (en) | 2021-01-01 |
KR101725279B1 (en) | 2017-04-10 |
WO2017073963A1 (en) | 2017-05-04 |
CN108350180A (en) | 2018-07-31 |
WO2017073963A9 (en) | 2018-09-13 |
BR112018008405B1 (en) | 2022-01-25 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B06U | Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 21/10/2016, OBSERVADAS AS CONDICOES LEGAIS. |