BR112016028479A2 - process for operating a simulated moving bed reactor - Google Patents

process for operating a simulated moving bed reactor

Info

Publication number
BR112016028479A2
BR112016028479A2 BR112016028479A BR112016028479A BR112016028479A2 BR 112016028479 A2 BR112016028479 A2 BR 112016028479A2 BR 112016028479 A BR112016028479 A BR 112016028479A BR 112016028479 A BR112016028479 A BR 112016028479A BR 112016028479 A2 BR112016028479 A2 BR 112016028479A2
Authority
BR
Brazil
Prior art keywords
reagent
smbr
cycle
injection
bed reactor
Prior art date
Application number
BR112016028479A
Other languages
Portuguese (pt)
Other versions
BR112016028479B1 (en
Inventor
Bommarius Andreas
Sreedhar Balamurali
Agrawal Gaurav
Oh Jungmin
Kawajiri Yoshiaki
Original Assignee
Dow Global Technologies Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Global Technologies Llc filed Critical Dow Global Technologies Llc
Publication of BR112016028479A2 publication Critical patent/BR112016028479A2/en
Publication of BR112016028479B1 publication Critical patent/BR112016028479B1/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/10Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1814Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns recycling of the fraction to be distributed
    • B01D15/1857Reactive simulated moving beds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/08Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/56Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Sustainable Development (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

a presente divulgação fornece um processo para fornecer um primeiro reagente e um segundo reagente (reagentes) a um reator de leito móvel simulado (smbr) em cada etapa de um ciclo de injeção de repetição sequencial, em que o smbr inclui zonas, tendo cada uma um ponto de injeção e cada uma contendo um meio de separação de sólido; reagir o primeiro reagente e o segundo reagente no smbr durante o ciclo de injeção de repetição sequencial (ciclo) para formar um primeiro produto; separar o primeiro produto no smbr com o meio de separação de sólido; e alterar uma quantidade de um ou ambos do primeiro reagente e do segundo reagente injetado a um ou mais dos pontos de injeção do smbr durante uma etapa do ciclo de injeção de repetição sequencial. a alteração da quantidade de reagentes pode ser feita em cada etapa do ciclo de injeção de repetição sequencial. a alteração da quantidade pode incluir a mudança de uma concentração de entrada dos reagentes injetados em um ou mais dos pontos de injeção durante cada etapa do ciclo.The present disclosure provides a process for providing a first reagent and a second reagent (reactants) to a simulated moving bed reactor (smbr) at each step of a sequential repeat injection cycle, wherein smbr includes zones, each having an injection point and each containing a solid separation means; reacting the first reagent and the second reagent on smbr during the sequential repeat injection cycle (cycle) to form a first product; separating the first product in the smbr with the solid separation medium; and altering an amount of one or both of the first reagent and the second reagent injected at one or more of the smbr injection points during one step of the sequential repeat injection cycle. The amount of reagents may be changed at each step of the sequential repeat injection cycle. Changing the amount may include changing an input concentration of injected reagents at one or more of the injection points during each step of the cycle.

BR112016028479-8A 2014-06-06 2015-06-04 Process for operating a simulated moving bed reactor BR112016028479B1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201462008560P 2014-06-06 2014-06-06
US62/008,560 2014-06-06
PCT/US2015/034175 WO2015187931A1 (en) 2014-06-06 2015-06-04 Process for operating a simulated moving bed reactor

Publications (2)

Publication Number Publication Date
BR112016028479A2 true BR112016028479A2 (en) 2017-08-22
BR112016028479B1 BR112016028479B1 (en) 2022-04-19

Family

ID=53539910

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112016028479-8A BR112016028479B1 (en) 2014-06-06 2015-06-04 Process for operating a simulated moving bed reactor

Country Status (8)

Country Link
US (1) US9914072B2 (en)
EP (1) EP3151940B1 (en)
JP (1) JP6588476B2 (en)
CN (1) CN106794390B (en)
BR (1) BR112016028479B1 (en)
CA (1) CA2952149C (en)
ES (1) ES2870601T3 (en)
WO (1) WO2015187931A1 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109408841A (en) * 2017-09-08 2019-03-01 吉林中粮生化有限公司 Simulated Moving Bed Chromatography process simulation

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0720521B2 (en) * 1986-07-10 1995-03-08 オルガノ株式会社 Control method for simulated moving bed
JP2888667B2 (en) * 1991-05-17 1999-05-10 オルガノ株式会社 Method and apparatus for producing useful substance by product inhibition reaction or reversible reaction
JP3258513B2 (en) * 1995-02-28 2002-02-18 オルガノ株式会社 Method for producing useful substance using simulated moving bed type chromatographic separation operation
JP3614279B2 (en) * 1997-08-07 2005-01-26 塩水港精糖株式会社 Method for producing galactosyl sucrose
JP2002153295A (en) * 2000-11-22 2002-05-28 Ensuiko Sugar Refining Co Ltd METHOD FOR CONTINUOUSLY PRODUCING beta-1,4- GALACTOSYLMALTOSE
US6518454B1 (en) 2001-10-12 2003-02-11 Eastman Chemical Company Preparation of esters of carboxylic acids
CN1169595C (en) * 2002-03-13 2004-10-06 浙江大学 Analogue mobile bed chromatic reactor
DE10235385B4 (en) * 2002-08-02 2006-10-05 MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. Method for the chromatographic separation of components
CN1884523A (en) * 2006-06-13 2006-12-27 南京工业大学 Method for separating and preparing 5'-nucleotide using emulated moving bed
US9085499B2 (en) * 2011-11-09 2015-07-21 Uop Llc Energy efficiency in adsorptive separation

Also Published As

Publication number Publication date
JP6588476B2 (en) 2019-10-09
US20170216740A1 (en) 2017-08-03
BR112016028479B1 (en) 2022-04-19
US9914072B2 (en) 2018-03-13
CA2952149A1 (en) 2015-12-10
CA2952149C (en) 2022-09-13
JP2017523905A (en) 2017-08-24
EP3151940A1 (en) 2017-04-12
CN106794390A (en) 2017-05-31
ES2870601T3 (en) 2021-10-27
CN106794390B (en) 2019-07-09
EP3151940B1 (en) 2021-04-07
WO2015187931A1 (en) 2015-12-10

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Legal Events

Date Code Title Description
B06U Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 04/06/2015, OBSERVADAS AS CONDICOES LEGAIS.