BR0200464A - Continuous adiabatic process for the preparation of nitrochlorobenzene - Google Patents
Continuous adiabatic process for the preparation of nitrochlorobenzeneInfo
- Publication number
- BR0200464A BR0200464A BR0200464-0A BR0200464A BR0200464A BR 0200464 A BR0200464 A BR 0200464A BR 0200464 A BR0200464 A BR 0200464A BR 0200464 A BR0200464 A BR 0200464A
- Authority
- BR
- Brazil
- Prior art keywords
- preparation
- nitrochlorobenzene
- adiabatic process
- continuous adiabatic
- continuous
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 4
- BFCFYVKQTRLZHA-UHFFFAOYSA-N 1-chloro-2-nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC=C1Cl BFCFYVKQTRLZHA-UHFFFAOYSA-N 0.000 title abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 2
- 238000006396 nitration reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
Abstract
"PROCESSO ADIABáTICO CONTìNUO PARA A PREPARAçãO DE NITROCLOROBENZENO". A presente invenção refere-se a um processo adiabático para a preparação de nitrociorobenzeno, em que o ácido sulfúrico residual obtido na execução do processo é concentrado e reconduzido na reação de nitração."CONTINUOUS ADIABATIC PROCESS FOR THE PREPARATION OF NITROCHLOROBENZENE". The present invention relates to an adiabatic process for the preparation of nitrociorobenzene, in which the residual sulfuric acid obtained in the execution of the process is concentrated and returned to the nitration reaction.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10108979A DE10108979C1 (en) | 2001-02-23 | 2001-02-23 | Continuous production of nitrochlorobenzene, used as intermediates for dye, pharmaceutical and pesticide production, uses specified adiabatic conditions and acid composition in nitration of chlorobenzene |
Publications (1)
Publication Number | Publication Date |
---|---|
BR0200464A true BR0200464A (en) | 2002-10-29 |
Family
ID=7675382
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR0200464-0A BR0200464A (en) | 2001-02-23 | 2002-02-21 | Continuous adiabatic process for the preparation of nitrochlorobenzene |
Country Status (13)
Country | Link |
---|---|
US (1) | US6586645B2 (en) |
EP (1) | EP1234814B1 (en) |
JP (1) | JP4257891B2 (en) |
KR (1) | KR100777517B1 (en) |
CN (1) | CN1219746C (en) |
AT (1) | ATE265416T1 (en) |
BR (1) | BR0200464A (en) |
CA (1) | CA2372767A1 (en) |
CZ (1) | CZ299615B6 (en) |
DE (2) | DE10108979C1 (en) |
HK (1) | HK1049828B (en) |
PL (1) | PL205525B1 (en) |
RU (1) | RU2301221C2 (en) |
Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10205855A1 (en) | 2002-02-13 | 2003-08-21 | Bayer Ag | Continuous production of nitrochlorobenzene, useful e.g. in pharmaceuticals or dyestuffs production, comprises nitration of chlorobenzene with a mixture of sulfuric, phosphoric and nitric acids and water, with recycling of acids |
CN100368377C (en) * | 2006-06-19 | 2008-02-13 | 常州市佳森化工有限公司 | Tech. of producing ortho nitro methyl-phenoxide para nitro methyl-phenoxide and meta nitro chlorobenzene from chlorobenzene |
DE102008048713A1 (en) * | 2008-09-24 | 2010-03-25 | Bayer Materialscience Ag | Process for the continuous production of nitrobenzene |
CN101602561B (en) * | 2009-07-07 | 2011-08-17 | 扬州大学 | Process for comprehensive use and treatment of wastewater from chlorobenzene adiabatic nitration material separation |
CN101607910B (en) * | 2009-07-07 | 2012-10-17 | 扬州大学 | Removal technology of nitrogen oxides generated in chlorobenzene thermal insulation nitration |
CN102070457B (en) * | 2011-02-15 | 2013-07-17 | 连云港地浦化工有限公司 | Method for continuously preparing dinitrochlorobenzene |
WO2012110839A1 (en) | 2011-02-17 | 2012-08-23 | Noram International Limited | Removal of non-aromatic impurities from a nitration process |
CN102093223A (en) * | 2011-03-03 | 2011-06-15 | 安徽省怀远县虹桥化工有限公司 | Improved production process of 2,4-dinitrochlorbenzene |
KR101906168B1 (en) * | 2012-09-06 | 2018-10-10 | 코오롱인더스트리 주식회사 | Method of manufacturing para-phenylenediamine |
CN104478731B (en) * | 2014-12-31 | 2016-04-13 | 浙江永太科技股份有限公司 | One utilizes micro passage reaction to synthesize the method for the chloro-3-fluoronitrobenzene of 2,4-bis- |
DE102018217955B4 (en) * | 2018-10-19 | 2020-06-04 | Plinke Gmbh | Process for working up mixed acid and waste water from the nitration of aromatics and device for carrying out the process |
CN113045427A (en) * | 2021-03-19 | 2021-06-29 | 宁夏华御化工有限公司 | Nitrochlorobenzene preparation method and system capable of reducing nitrate content in wastewater |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19808748A1 (en) * | 1997-11-03 | 1999-05-06 | Bayer Ag | Process for the preparation of aromatic nitro compounds |
US4021498A (en) * | 1975-12-09 | 1977-05-03 | American Cyanamid Company | Adiabatic process for nitration of nitratable aromatic compounds |
US4453027A (en) * | 1982-12-10 | 1984-06-05 | Monsanto Company | Adiabatic process for the nitration of halobenzenes |
DE3409717C2 (en) * | 1984-03-16 | 1994-03-31 | Bayer Ag | Process for the preparation of nitrobenzene |
DE4411064A1 (en) * | 1994-03-30 | 1995-10-05 | Bayer Ag | Process for the adiabatic production of mononitrohalobenzenes |
US5763687A (en) | 1995-12-15 | 1998-06-09 | Mitsui Chemicals, Inc. | Preparation process for aromatic mononitro compounds |
HUP0100200A3 (en) * | 1997-11-03 | 2002-03-28 | Bayer Ag | Method for producing aromatic nitro compounds |
-
2001
- 2001-02-23 DE DE10108979A patent/DE10108979C1/en not_active Expired - Fee Related
-
2002
- 2002-02-11 DE DE50200376T patent/DE50200376D1/en not_active Expired - Lifetime
- 2002-02-11 EP EP02002074A patent/EP1234814B1/en not_active Expired - Lifetime
- 2002-02-11 AT AT02002074T patent/ATE265416T1/en not_active IP Right Cessation
- 2002-02-19 JP JP2002041539A patent/JP4257891B2/en not_active Expired - Fee Related
- 2002-02-19 US US10/078,655 patent/US6586645B2/en not_active Expired - Fee Related
- 2002-02-20 KR KR1020020008986A patent/KR100777517B1/en not_active IP Right Cessation
- 2002-02-21 CZ CZ20020648A patent/CZ299615B6/en not_active IP Right Cessation
- 2002-02-21 CA CA002372767A patent/CA2372767A1/en not_active Abandoned
- 2002-02-21 PL PL352396A patent/PL205525B1/en not_active IP Right Cessation
- 2002-02-21 BR BR0200464-0A patent/BR0200464A/en not_active Application Discontinuation
- 2002-02-22 RU RU2002104565/04A patent/RU2301221C2/en not_active IP Right Cessation
- 2002-02-25 CN CNB021051674A patent/CN1219746C/en not_active Expired - Fee Related
-
2003
- 2003-03-17 HK HK03101943.3A patent/HK1049828B/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
CN1371902A (en) | 2002-10-02 |
EP1234814A1 (en) | 2002-08-28 |
CZ2002648A3 (en) | 2002-10-16 |
CN1219746C (en) | 2005-09-21 |
JP2002255904A (en) | 2002-09-11 |
PL205525B1 (en) | 2010-04-30 |
ATE265416T1 (en) | 2004-05-15 |
EP1234814B1 (en) | 2004-04-28 |
DE50200376D1 (en) | 2004-06-03 |
HK1049828B (en) | 2006-05-12 |
US6586645B2 (en) | 2003-07-01 |
HK1049828A1 (en) | 2003-05-30 |
KR20020069122A (en) | 2002-08-29 |
RU2301221C2 (en) | 2007-06-20 |
CZ299615B6 (en) | 2008-09-24 |
US20020161269A1 (en) | 2002-10-31 |
KR100777517B1 (en) | 2007-11-20 |
CA2372767A1 (en) | 2002-08-23 |
DE10108979C1 (en) | 2002-05-08 |
JP4257891B2 (en) | 2009-04-22 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B25A | Requested transfer of rights approved |
Owner name: LANXESS DEUTSCHLAND GMBH (DE) Free format text: TRANSFERIDO DE: BAYER AKTIENGESELLSCHAFT |
|
B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
B09B | Patent application refused [chapter 9.2 patent gazette] | ||
B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: MANTIDO O INDEFERIMENTO UMA VEZ QUE NAO FOI APRESENTADO RECURSO DENTRO DO PRAZO LEGAL. |