BE589471A - - Google Patents
Info
- Publication number
- BE589471A BE589471A BE589471DA BE589471A BE 589471 A BE589471 A BE 589471A BE 589471D A BE589471D A BE 589471DA BE 589471 A BE589471 A BE 589471A
- Authority
- BE
- Belgium
- Prior art keywords
- magnesium
- vessel
- reaction vessel
- reaction
- organic halide
- Prior art date
Links
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 44
- 229910052749 magnesium Inorganic materials 0.000 claims description 44
- 239000011777 magnesium Substances 0.000 claims description 44
- 238000006243 chemical reaction Methods 0.000 claims description 42
- 238000000034 method Methods 0.000 claims description 29
- 150000004820 halides Chemical class 0.000 claims description 22
- -1 organomagnesium halides Chemical class 0.000 claims description 20
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 16
- 239000002904 solvent Substances 0.000 claims description 15
- 238000002360 preparation method Methods 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 9
- RDHPKYGYEGBMSE-UHFFFAOYSA-N bromoethane Chemical compound CCBr RDHPKYGYEGBMSE-UHFFFAOYSA-N 0.000 claims description 6
- 238000004821 distillation Methods 0.000 claims description 5
- 239000000047 product Substances 0.000 description 5
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 238000005303 weighing Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- GZUXJHMPEANEGY-UHFFFAOYSA-N bromomethane Chemical compound BrC GZUXJHMPEANEGY-UHFFFAOYSA-N 0.000 description 2
- 230000000977 initiatory effect Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 2
- ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 description 1
- 238000003747 Grignard reaction Methods 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 150000001350 alkyl halides Chemical class 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 238000001739 density measurement Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 229960003750 ethyl chloride Drugs 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- ULYZAYCEDJDHCC-UHFFFAOYSA-N isopropyl chloride Chemical compound CC(C)Cl ULYZAYCEDJDHCC-UHFFFAOYSA-N 0.000 description 1
- FRIJBUGBVQZNTB-UHFFFAOYSA-M magnesium;ethane;bromide Chemical compound [Mg+2].[Br-].[CH2-]C FRIJBUGBVQZNTB-UHFFFAOYSA-M 0.000 description 1
- 229940102396 methyl bromide Drugs 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
- C07F3/02—Magnesium compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BE589471A true BE589471A (en:Method) |
Family
ID=191846
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BE589471D BE589471A (en:Method) |
Country Status (1)
| Country | Link |
|---|---|
| BE (1) | BE589471A (en:Method) |
-
0
- BE BE589471D patent/BE589471A/fr unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| FR2549825A1 (fr) | Procede pour la recuperation de butene-1 de qualite appropriee pour la polymerisation | |
| CA2032355C (fr) | Procede de preparation de (meth)acrylate d'alkylimidazolidone | |
| CA1091894A (fr) | Procede de preparation de solutions concentrees d'hydrate d'hydrazine | |
| EP0461096A1 (fr) | Procédé de fabrication de N-phénylmaléimide | |
| EP2203405A1 (fr) | Procede de recuperation d'acides fluorocarboxyliques | |
| BE589471A (en:Method) | ||
| CA1198736A (fr) | Procede de decomposition d'un complexe ortho-benzoyl- benzoique de fluorure d'hydrogene et de trifluorure de bore | |
| JPH0147454B2 (en:Method) | ||
| EP4584238A1 (fr) | Procede ameliore de fabrication d'acides carboxyliques alpha-beta insatures a partir de poly(3-hydroxyalcanoate) | |
| EP3632850A1 (en) | Production method for aqueous solution of zinc halide | |
| FR2508460A1 (fr) | Procede de production d'acyloxysilanes | |
| BE597880A (en:Method) | ||
| EP0889871B1 (fr) | Procede de preparation d'acide acetique et/ou d'acetate de methyle par isomerisation et carbonylation | |
| CA2017650C (fr) | Procede de separation de deux isomeres, son application a la purification du phenyl-1 bromo-2 ethane | |
| EP0210694B1 (fr) | Compositions stabilisées de 1,1,1-trichloréthane | |
| EP0912485B1 (fr) | Procede d'hydroxycarbonylation des acides pentenoiques | |
| EP0892776B1 (fr) | Procede de preparation d'acide acetique et/ou d'acetate de methyle par isomerisation de formiate de methyle | |
| Mohammadi et al. | Separation and encapsulation of Persian red rose oil by eutectic compounds | |
| EP0465294A1 (fr) | Procédé de fabrication de bromures insaturés | |
| FR2726824A1 (fr) | Composition d'alcoxysilanes protegee de la reaction de dismutation | |
| FR1463200A (fr) | Procédé de fabrication d'esters aliphatiques | |
| WO2020079281A1 (fr) | Adduits de triphenylphosphine et de triphenylphosphite et leur utilisation pour la bromation d'alcools primaires | |
| FR2693456A1 (fr) | Réactif de perfluoroalcoylation et procédé utilisant ce réactif. | |
| EP0110761A1 (fr) | Procédé de préparation de chlorures d'acides alpha-chlores | |
| BE683976A (en:Method) |