BE537123A - - Google Patents
Info
- Publication number
- BE537123A BE537123A BE537123DA BE537123A BE 537123 A BE537123 A BE 537123A BE 537123D A BE537123D A BE 537123DA BE 537123 A BE537123 A BE 537123A
- Authority
- BE
- Belgium
- Prior art keywords
- water
- solution
- polymers
- parts
- nitrogen
- Prior art date
Links
- 229920000642 polymer Polymers 0.000 claims description 70
- HKLHGHHKGCTLRS-UHFFFAOYSA-N N#[P]CO Chemical compound N#[P]CO HKLHGHHKGCTLRS-UHFFFAOYSA-N 0.000 claims description 9
- 238000002360 preparation method Methods 0.000 claims description 2
- 239000000243 solution Substances 0.000 claims 60
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 59
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 44
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 34
- -1 trimethylene phosphine oxide Chemical compound 0.000 claims 28
- 229920000877 Melamine resin Polymers 0.000 claims 27
- XSQUKJJJFZCRTK-UHFFFAOYSA-N urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims 24
- 150000002830 nitrogen compounds Chemical class 0.000 claims 23
- 229910052757 nitrogen Inorganic materials 0.000 claims 22
- JDSHMPZPIAZGSV-UHFFFAOYSA-N Melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 claims 21
- 229910052698 phosphorus Inorganic materials 0.000 claims 21
- 239000011574 phosphorus Substances 0.000 claims 21
- 238000006243 chemical reaction Methods 0.000 claims 20
- 239000000203 mixture Substances 0.000 claims 19
- 239000002244 precipitate Substances 0.000 claims 18
- 239000000047 product Substances 0.000 claims 17
- 229920005989 resin Polymers 0.000 claims 17
- 239000011347 resin Substances 0.000 claims 17
- QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 16
- 238000000034 method Methods 0.000 claims 16
- 239000004202 carbamide Substances 0.000 claims 12
- 235000013877 carbamide Nutrition 0.000 claims 12
- 239000004744 fabric Substances 0.000 claims 11
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Tris Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims 10
- 239000007788 liquid Substances 0.000 claims 10
- OAICVXFJPJFONN-UHFFFAOYSA-N phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims 10
- 150000003018 phosphorus compounds Chemical class 0.000 claims 10
- 239000000843 powder Substances 0.000 claims 10
- 238000003860 storage Methods 0.000 claims 10
- 238000001914 filtration Methods 0.000 claims 9
- 238000006116 polymerization reaction Methods 0.000 claims 9
- 150000001875 compounds Chemical class 0.000 claims 8
- RTZKZFJDLAIYFH-UHFFFAOYSA-N diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 8
- 238000002955 isolation Methods 0.000 claims 8
- 239000012429 reaction media Substances 0.000 claims 8
- 239000007787 solid Substances 0.000 claims 8
- VMHLLURERBWHNL-UHFFFAOYSA-M sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims 7
- 239000001632 sodium acetate Substances 0.000 claims 7
- 235000017281 sodium acetate Nutrition 0.000 claims 7
- 229960000583 Acetic Acid Drugs 0.000 claims 6
- 229920000742 Cotton Polymers 0.000 claims 6
- 239000007864 aqueous solution Substances 0.000 claims 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-M chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims 6
- WSFSSNUMVMOOMR-UHFFFAOYSA-N formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims 6
- 238000010438 heat treatment Methods 0.000 claims 6
- 239000004753 textile Substances 0.000 claims 6
- MRVZORUPSXTRHD-UHFFFAOYSA-N bis(hydroxymethyl)phosphorylmethanol Chemical compound OCP(=O)(CO)CO MRVZORUPSXTRHD-UHFFFAOYSA-N 0.000 claims 5
- 229920000591 gum Polymers 0.000 claims 5
- 150000002829 nitrogen Chemical group 0.000 claims 5
- AKXUUJCMWZFYMV-UHFFFAOYSA-M tetrakis(hydroxymethyl)phosphanium;chloride Chemical compound [Cl-].OC[P+](CO)(CO)CO AKXUUJCMWZFYMV-UHFFFAOYSA-M 0.000 claims 5
- 229920001187 thermosetting polymer Polymers 0.000 claims 5
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 claims 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 4
- HRPVXLWXLXDGHG-UHFFFAOYSA-N acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims 4
- 238000004458 analytical method Methods 0.000 claims 4
- 238000005119 centrifugation Methods 0.000 claims 4
- 238000001816 cooling Methods 0.000 claims 4
- QGBSISYHAICWAH-UHFFFAOYSA-N cyanoguanidine Chemical compound NC(N)=NC#N QGBSISYHAICWAH-UHFFFAOYSA-N 0.000 claims 4
- 238000001035 drying Methods 0.000 claims 4
- 125000004435 hydrogen atoms Chemical group [H]* 0.000 claims 4
- 239000000463 material Substances 0.000 claims 4
- 239000004033 plastic Substances 0.000 claims 4
- 239000011780 sodium chloride Substances 0.000 claims 4
- 239000002904 solvent Substances 0.000 claims 4
- 238000003756 stirring Methods 0.000 claims 4
- 239000004640 Melamine resin Substances 0.000 claims 3
- VGGLHLAESQEWCR-UHFFFAOYSA-N N-(hydroxymethyl)urea Chemical compound NC(=O)NCO VGGLHLAESQEWCR-UHFFFAOYSA-N 0.000 claims 3
- MBHRHUJRKGNOKX-UHFFFAOYSA-N [(4,6-diamino-1,3,5-triazin-2-yl)amino]methanol Chemical class NC1=NC(N)=NC(NCO)=N1 MBHRHUJRKGNOKX-UHFFFAOYSA-N 0.000 claims 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims 3
- 239000007795 chemical reaction product Substances 0.000 claims 3
- 239000000460 chlorine Substances 0.000 claims 3
- 229910052801 chlorine Inorganic materials 0.000 claims 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 3
- 238000001704 evaporation Methods 0.000 claims 3
- 239000000706 filtrate Substances 0.000 claims 3
- ZRALSGWEFCBTJO-UHFFFAOYSA-N guanidine Chemical compound NC(N)=N ZRALSGWEFCBTJO-UHFFFAOYSA-N 0.000 claims 3
- 150000002897 organic nitrogen compounds Chemical class 0.000 claims 3
- 125000004437 phosphorous atoms Chemical group 0.000 claims 3
- 238000001556 precipitation Methods 0.000 claims 3
- 239000000376 reactant Substances 0.000 claims 3
- 150000003839 salts Chemical class 0.000 claims 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N Butanol Natural products CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 2
- 238000007792 addition Methods 0.000 claims 2
- 125000000217 alkyl group Chemical group 0.000 claims 2
- 150000001450 anions Chemical class 0.000 claims 2
- 239000002585 base Substances 0.000 claims 2
- 230000015572 biosynthetic process Effects 0.000 claims 2
- 238000009835 boiling Methods 0.000 claims 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims 2
- 239000003153 chemical reaction reagent Substances 0.000 claims 2
- 239000003795 chemical substances by application Substances 0.000 claims 2
- 238000000748 compression moulding Methods 0.000 claims 2
- ZHNUHDYFZUAESO-UHFFFAOYSA-N formamide Chemical compound NC=O ZHNUHDYFZUAESO-UHFFFAOYSA-N 0.000 claims 2
- 238000005755 formation reaction Methods 0.000 claims 2
- DHMQDGOQFOQNFH-UHFFFAOYSA-N glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 claims 2
- FJLUATLTXUNBOT-UHFFFAOYSA-N hexadecan-1-amine Chemical compound CCCCCCCCCCCCCCCCN FJLUATLTXUNBOT-UHFFFAOYSA-N 0.000 claims 2
- 125000004029 hydroxymethyl group Chemical group [H]OC([H])([H])* 0.000 claims 2
- 238000001746 injection moulding Methods 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- 150000007974 melamines Chemical class 0.000 claims 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N methanol Chemical class OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 2
- 239000003607 modifier Substances 0.000 claims 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 2
- 239000004014 plasticizer Substances 0.000 claims 2
- 230000000379 polymerizing Effects 0.000 claims 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims 2
- 150000003512 tertiary amines Chemical class 0.000 claims 2
- FAUOSXUSCVJWAY-UHFFFAOYSA-N tetrakis(hydroxymethyl)phosphanium Chemical class OC[P+](CO)(CO)CO FAUOSXUSCVJWAY-UHFFFAOYSA-N 0.000 claims 2
- 238000001721 transfer moulding Methods 0.000 claims 2
- 238000005406 washing Methods 0.000 claims 2
- PIICEJLVQHRZGT-UHFFFAOYSA-N 1,2-ethanediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 claims 1
- BBMCTIGTTCKYKF-UHFFFAOYSA-N 1-Heptanol Chemical class CCCCCCCO BBMCTIGTTCKYKF-UHFFFAOYSA-N 0.000 claims 1
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N 1-Hexanol Chemical class CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 claims 1
- VVJKKWFAADXIJK-UHFFFAOYSA-N Allylamine Chemical compound NCC=C VVJKKWFAADXIJK-UHFFFAOYSA-N 0.000 claims 1
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims 1
- 239000004475 Arginine Substances 0.000 claims 1
- 240000008564 Boehmeria nivea Species 0.000 claims 1
- DNSISZSEWVHGLH-UHFFFAOYSA-N Butyramide Chemical compound CCCC(N)=O DNSISZSEWVHGLH-UHFFFAOYSA-N 0.000 claims 1
- 229960003563 Calcium Carbonate Drugs 0.000 claims 1
- 240000000491 Corchorus aestuans Species 0.000 claims 1
- 235000011777 Corchorus aestuans Nutrition 0.000 claims 1
- 235000010862 Corchorus capsularis Nutrition 0.000 claims 1
- 239000004471 Glycine Substances 0.000 claims 1
- 239000004472 Lysine Substances 0.000 claims 1
- ODGAOXROABLFNM-UHFFFAOYSA-N Polynoxylin Chemical compound O=C.NC(N)=O ODGAOXROABLFNM-UHFFFAOYSA-N 0.000 claims 1
- 229920000297 Rayon Polymers 0.000 claims 1
- LPXPTNMVRIOKMN-UHFFFAOYSA-M Sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 claims 1
- 241000779819 Syncarpia glomulifera Species 0.000 claims 1
- 229940036248 Turpentine Drugs 0.000 claims 1
- 229920001807 Urea-formaldehyde Polymers 0.000 claims 1
- 210000002268 Wool Anatomy 0.000 claims 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K [O-]P([O-])([O-])=O Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims 1
- 238000005299 abrasion Methods 0.000 claims 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims 1
- 230000001476 alcoholic Effects 0.000 claims 1
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 229910000288 alkali metal carbonate Inorganic materials 0.000 claims 1
- 150000008041 alkali metal carbonates Chemical class 0.000 claims 1
- 125000003545 alkoxy group Chemical group 0.000 claims 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 1
- 150000001408 amides Chemical class 0.000 claims 1
- 150000001413 amino acids Chemical class 0.000 claims 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims 1
- 235000011114 ammonium hydroxide Nutrition 0.000 claims 1
- 239000012431 aqueous reaction media Substances 0.000 claims 1
- 150000007514 bases Chemical class 0.000 claims 1
- 229910000019 calcium carbonate Inorganic materials 0.000 claims 1
- 125000004432 carbon atoms Chemical group C* 0.000 claims 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 238000009833 condensation Methods 0.000 claims 1
- 230000005494 condensation Effects 0.000 claims 1
- 230000000875 corresponding Effects 0.000 claims 1
- 238000010908 decantation Methods 0.000 claims 1
- 238000006297 dehydration reaction Methods 0.000 claims 1
- 230000001934 delay Effects 0.000 claims 1
- 238000007865 diluting Methods 0.000 claims 1
- 238000010790 dilution Methods 0.000 claims 1
- 239000006185 dispersion Substances 0.000 claims 1
- 239000012153 distilled water Substances 0.000 claims 1
- QUSNBJAOOMFDIB-UHFFFAOYSA-N ethyl amine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 claims 1
- 238000000605 extraction Methods 0.000 claims 1
- 150000002194 fatty esters Chemical class 0.000 claims 1
- 239000000835 fiber Substances 0.000 claims 1
- 239000000945 filler Substances 0.000 claims 1
- 239000010419 fine particle Substances 0.000 claims 1
- 238000007701 flash-distillation Methods 0.000 claims 1
- IVJISJACKSSFGE-UHFFFAOYSA-N formaldehyde;1,3,5-triazine-2,4,6-triamine Chemical compound O=C.NC1=NC(N)=NC(N)=N1 IVJISJACKSSFGE-UHFFFAOYSA-N 0.000 claims 1
- SLGWESQGEUXWJQ-UHFFFAOYSA-N formaldehyde;phenol Chemical compound O=C.OC1=CC=CC=C1 SLGWESQGEUXWJQ-UHFFFAOYSA-N 0.000 claims 1
- 238000007710 freezing Methods 0.000 claims 1
- 239000012362 glacial acetic acid Substances 0.000 claims 1
- RDBMUARQWLPMNW-UHFFFAOYSA-O hydroxymethylphosphanium Chemical class OC[PH3+] RDBMUARQWLPMNW-UHFFFAOYSA-O 0.000 claims 1
- 238000011065 in-situ storage Methods 0.000 claims 1
- 239000006193 liquid solution Substances 0.000 claims 1
- 239000000314 lubricant Substances 0.000 claims 1
- BDAGIHXWWSANSR-UHFFFAOYSA-M methanoate Chemical compound [O-]C=O BDAGIHXWWSANSR-UHFFFAOYSA-M 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- 238000000465 moulding Methods 0.000 claims 1
- 230000001264 neutralization Effects 0.000 claims 1
- 125000004433 nitrogen atoms Chemical group N* 0.000 claims 1
- 150000004027 organic amino compounds Chemical class 0.000 claims 1
- 150000002894 organic compounds Chemical class 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- ZFLIKDUSUDBGCD-UHFFFAOYSA-N parabanic acid Chemical compound O=C1NC(=O)C(=O)N1 ZFLIKDUSUDBGCD-UHFFFAOYSA-N 0.000 claims 1
- 239000002245 particle Substances 0.000 claims 1
- 229920001568 phenolic resin Polymers 0.000 claims 1
- 239000010452 phosphate Substances 0.000 claims 1
- 239000001739 pinus spp. Substances 0.000 claims 1
- DNIAPMSPPWPWGF-UHFFFAOYSA-N propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims 1
- 238000009877 rendering Methods 0.000 claims 1
- 229910000029 sodium carbonate Inorganic materials 0.000 claims 1
- 239000001187 sodium carbonate Substances 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- QAOWNCQODCNURD-UHFFFAOYSA-L sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims 1
- 239000000725 suspension Substances 0.000 claims 1
- 230000002522 swelling Effects 0.000 claims 1
- 150000003672 ureas Chemical class 0.000 claims 1
- 239000000080 wetting agent Substances 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G79/00—Macromolecular compounds obtained by reactions forming a linkage containing atoms other than silicon, sulfur, nitrogen, oxygen, and carbon with or without the latter elements in the main chain of the macromolecule
- C08G79/02—Macromolecular compounds obtained by reactions forming a linkage containing atoms other than silicon, sulfur, nitrogen, oxygen, and carbon with or without the latter elements in the main chain of the macromolecule a linkage containing phosphorus
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Phenolic Resins Or Amino Resins (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BE537123A true BE537123A (no) |
Family
ID=167572
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BE537123D BE537123A (no) |
Country Status (1)
| Country | Link |
|---|---|
| BE (1) | BE537123A (no) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1226309B (de) * | 1958-07-15 | 1966-10-06 | Albright & Wilson Mfg Ltd | Verfahren zur Herstellung von monomeren oder polymeren Kondensationsprodukten, die P-CH-N-Bindungen enthalten |
-
0
- BE BE537123D patent/BE537123A/fr unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1226309B (de) * | 1958-07-15 | 1966-10-06 | Albright & Wilson Mfg Ltd | Verfahren zur Herstellung von monomeren oder polymeren Kondensationsprodukten, die P-CH-N-Bindungen enthalten |
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