BE516048A - - Google Patents

Info

Publication number

BE516048A

BE516048A BE516048DA BE516048A BE 516048 A BE516048 A BE 516048A BE 516048D A BE516048D A BE 516048DA BE 516048 A BE516048 A BE 516048A

Authority

BE

Belgium

Prior art keywords

molecules

products

formula

molecule

temperature

Prior art date

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• 239000000047 product Substances 0.000 claims description 28
• 238000000034 method Methods 0.000 claims description 9
• 150000001412 amines Chemical class 0.000 claims description 7
• 125000004432 carbon atom Chemical group C* 0.000 claims description 5
• IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 4
• 125000000217 alkyl group Chemical group 0.000 claims description 4
• 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 4
• 239000004215 Carbon black (E152) Substances 0.000 claims description 3
• 230000002378 acidificating effect Effects 0.000 claims description 3
• 229940100198 alkylating agent Drugs 0.000 claims description 3
• 239000002168 alkylating agent Substances 0.000 claims description 3
• RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 3
• 150000002170 ethers Chemical class 0.000 claims description 3
• 229930195733 hydrocarbon Natural products 0.000 claims description 3
• 125000003710 aryl alkyl group Chemical group 0.000 claims description 2
• 230000007935 neutral effect Effects 0.000 claims description 2
• 229910052757 nitrogen Inorganic materials 0.000 claims description 2
• 238000002360 preparation method Methods 0.000 claims description 2
• 239000007859 condensation product Substances 0.000 claims 1
• 229920000151 polyglycol Polymers 0.000 claims 1
• 239000010695 polyglycol Substances 0.000 claims 1
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 17
• RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 description 15
• 150000001875 compounds Chemical class 0.000 description 15
• 238000003756 stirring Methods 0.000 description 13
• IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 12
• -1 octadecenyl oxy propenes Chemical class 0.000 description 12
• SJEYSFABYSGQBG-UHFFFAOYSA-M Patent blue Chemical compound [Na+].C1=CC(N(CC)CC)=CC=C1C(C=1C(=CC(=CC=1)S([O-])(=O)=O)S([O-])(=O)=O)=C1C=CC(=[N+](CC)CC)C=C1 SJEYSFABYSGQBG-UHFFFAOYSA-M 0.000 description 9
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
• 239000000980 acid dye Substances 0.000 description 9
• VAYGXNSJCAHWJZ-UHFFFAOYSA-N dimethyl sulfate Chemical compound COS(=O)(=O)OC VAYGXNSJCAHWJZ-UHFFFAOYSA-N 0.000 description 8
• GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 6
• BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 description 4
• 239000007795 chemical reaction product Substances 0.000 description 4
• 239000003795 chemical substances by application Substances 0.000 description 4
• 239000004698 Polyethylene Substances 0.000 description 3
• FOCAUTSVDIKZOP-UHFFFAOYSA-N chloroacetic acid Chemical compound OC(=O)CCl FOCAUTSVDIKZOP-UHFFFAOYSA-N 0.000 description 3
• 239000000470 constituent Substances 0.000 description 3
• IUNMPGNGSSIWFP-UHFFFAOYSA-N dimethylaminopropylamine Chemical compound CN(C)CCCN IUNMPGNGSSIWFP-UHFFFAOYSA-N 0.000 description 3
• 150000002118 epoxides Chemical class 0.000 description 3
• 239000000203 mixture Substances 0.000 description 3
• 235000011121 sodium hydroxide Nutrition 0.000 description 3
• KSVYTTKMILZAKH-UHFFFAOYSA-N 2-methyl-3-octadec-1-enoxyoxirane Chemical compound C(=CCCCCCCCCCCCCCCCC)OC1C(C)O1 KSVYTTKMILZAKH-UHFFFAOYSA-N 0.000 description 2
• VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 2
• 239000005977 Ethylene Substances 0.000 description 2
• PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
• FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
• KCXMKQUNVWSEMD-UHFFFAOYSA-N benzyl chloride Chemical compound ClCC1=CC=CC=C1 KCXMKQUNVWSEMD-UHFFFAOYSA-N 0.000 description 2
• 229940073608 benzyl chloride Drugs 0.000 description 2
• 229910052804 chromium Inorganic materials 0.000 description 2
• 239000011651 chromium Substances 0.000 description 2
• 239000000975 dye Substances 0.000 description 2
• 229920000768 polyamine Polymers 0.000 description 2
• 229920000573 polyethylene Polymers 0.000 description 2
• 239000000243 solution Substances 0.000 description 2
• FAGUFWYHJQFNRV-UHFFFAOYSA-N tetraethylenepentamine Chemical compound NCCNCCNCCNCCN FAGUFWYHJQFNRV-UHFFFAOYSA-N 0.000 description 2
• 238000005292 vacuum distillation Methods 0.000 description 2
• BZQIOJCTHFYLNC-UHFFFAOYSA-N 1-chloro-1-hydroxypropane-1-sulfonic acid Chemical compound CCC(O)(Cl)S(O)(=O)=O BZQIOJCTHFYLNC-UHFFFAOYSA-N 0.000 description 1
• PFJOTFSIBVZGPK-UHFFFAOYSA-N 1-ethyl-2-methylhydrazine Chemical compound CCNNC PFJOTFSIBVZGPK-UHFFFAOYSA-N 0.000 description 1
• MVTYCOHHPZPWKY-UHFFFAOYSA-N 2-dodecoxy-3-methyloxirane Chemical compound C(CCCCCCCCCCC)OC1C(C)O1 MVTYCOHHPZPWKY-UHFFFAOYSA-N 0.000 description 1
• GKAJGEHMEPPBAY-UHFFFAOYSA-N 2-methyl-2,3-dipentyl-3-phenoxyoxirane Chemical compound C(CCCC)C1(C(OC2=CC=CC=C2)(CCCCC)O1)C GKAJGEHMEPPBAY-UHFFFAOYSA-N 0.000 description 1
• JFTHCMSPGRQMBB-UHFFFAOYSA-N 2-methyl-3-octoxyoxirane Chemical compound CCCCCCCCOC1OC1C JFTHCMSPGRQMBB-UHFFFAOYSA-N 0.000 description 1
• 229940105325 3-dimethylaminopropylamine Drugs 0.000 description 1
• GDZRQEDYIXQKLQ-UHFFFAOYSA-N 3-methyl-2-(6-methylheptyl)-2-phenoxyoxirane Chemical compound C(CCCCC(C)C)C1(C(C)O1)OC1=CC=CC=C1 GDZRQEDYIXQKLQ-UHFFFAOYSA-N 0.000 description 1
• SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 1
• VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
• PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 1
• 239000004743 Polypropylene Substances 0.000 description 1
• 238000010521 absorption reaction Methods 0.000 description 1
• 239000003377 acid catalyst Substances 0.000 description 1
• 239000002671 adjuvant Substances 0.000 description 1
• 238000013019 agitation Methods 0.000 description 1
• 150000001298 alcohols Chemical class 0.000 description 1
• 230000029936 alkylation Effects 0.000 description 1
• 238000005804 alkylation reaction Methods 0.000 description 1
• 239000007864 aqueous solution Substances 0.000 description 1
• 239000003518 caustics Substances 0.000 description 1
• 238000006243 chemical reaction Methods 0.000 description 1
• 229940106681 chloroacetic acid Drugs 0.000 description 1
• DENRZWYUOJLTMF-UHFFFAOYSA-N diethyl sulfate Chemical compound CCOS(=O)(=O)OCC DENRZWYUOJLTMF-UHFFFAOYSA-N 0.000 description 1
• 229940008406 diethyl sulfate Drugs 0.000 description 1
• 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 1
• 238000004821 distillation Methods 0.000 description 1
• WNAHIZMDSQCWRP-UHFFFAOYSA-N dodecane-1-thiol Chemical compound CCCCCCCCCCCCS WNAHIZMDSQCWRP-UHFFFAOYSA-N 0.000 description 1
• 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
• 238000001035 drying Methods 0.000 description 1
• 238000004043 dyeing Methods 0.000 description 1
• 239000000835 fiber Substances 0.000 description 1
• 235000011187 glycerol Nutrition 0.000 description 1
• 229910052736 halogen Inorganic materials 0.000 description 1
• 150000002367 halogens Chemical class 0.000 description 1
• 239000007788 liquid Substances 0.000 description 1
• QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
• 229910052753 mercury Inorganic materials 0.000 description 1
• WGYKZJWCGVVSQN-UHFFFAOYSA-N mono-n-propyl amine Natural products CCCN WGYKZJWCGVVSQN-UHFFFAOYSA-N 0.000 description 1
• KFDIDIIKNMZLRZ-UHFFFAOYSA-N n'-propan-2-ylpropane-1,3-diamine Chemical compound CC(C)NCCCN KFDIDIIKNMZLRZ-UHFFFAOYSA-N 0.000 description 1
• 125000004433 nitrogen atom Chemical group N* 0.000 description 1
• 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
• 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
• 235000014594 pastries Nutrition 0.000 description 1
• 230000035515 penetration Effects 0.000 description 1
• 229920001281 polyalkylene Polymers 0.000 description 1
• 239000000843 powder Substances 0.000 description 1
• 239000011780 sodium chloride Substances 0.000 description 1
• 159000000000 sodium salts Chemical class 0.000 description 1
• 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
• 239000004753 textile Substances 0.000 description 1
• 239000000984 vat dye Substances 0.000 description 1