AU2016260101B2 - Method for producing steel material, apparatus for cooling steel material, and steel material - Google Patents

Method for producing steel material, apparatus for cooling steel material, and steel material Download PDF

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Publication number
AU2016260101B2
AU2016260101B2 AU2016260101A AU2016260101A AU2016260101B2 AU 2016260101 B2 AU2016260101 B2 AU 2016260101B2 AU 2016260101 A AU2016260101 A AU 2016260101A AU 2016260101 A AU2016260101 A AU 2016260101A AU 2016260101 B2 AU2016260101 B2 AU 2016260101B2
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Australia
Prior art keywords
cooling
steel material
rail
longitudinal direction
headers
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AU2016260101B9 (en
AU2016260101A1 (en
Inventor
Hiroyuki Fukuda
Hiroshi Ishikawa
Hideo Kijima
Sadanori Nakano
Kenji Okushiro
Yoshikazu Yoshida
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JFE Steel Corp
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JFE Steel Corp
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C21—METALLURGY OF IRON
    • C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/04—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for rails
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21B—ROLLING OF METAL
    • B21B1/00—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
    • B21B1/08—Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling structural sections, i.e. work of special cross-section, e.g. angle steel
    • B21B1/085—Rail sections
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21B—ROLLING OF METAL
    • B21B45/00—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
    • B21B45/02—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills for lubricating, cooling, or cleaning
    • B21B45/0203—Cooling
    • C—CHEMISTRY; METALLURGY
    • C21—METALLURGY OF IRON
    • C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/002—Ferrous alloys, e.g. steel alloys containing In, Mg, or other elements not provided for in one single group C22C38/001 - C22C38/60
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/02—Ferrous alloys, e.g. steel alloys containing silicon
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/04—Ferrous alloys, e.g. steel alloys containing manganese
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/06—Ferrous alloys, e.g. steel alloys containing aluminium
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/14—Ferrous alloys, e.g. steel alloys containing titanium or zirconium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21B—ROLLING OF METAL
    • B21B45/00—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
    • B21B45/02—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills for lubricating, cooling, or cleaning
    • B21B45/0203—Cooling
    • B21B45/0209—Cooling devices, e.g. using gaseous coolants
    • B21B2045/0212—Cooling devices, e.g. using gaseous coolants using gaseous coolants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21B—ROLLING OF METAL
    • B21B45/00—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
    • B21B45/02—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills for lubricating, cooling, or cleaning
    • B21B45/0203—Cooling
    • B21B45/0209—Cooling devices, e.g. using gaseous coolants
    • B21B45/0215—Cooling devices, e.g. using gaseous coolants using liquid coolants, e.g. for sections, for tubes
    • B21B2045/0221—Cooling devices, e.g. using gaseous coolants using liquid coolants, e.g. for sections, for tubes for structural sections, e.g. H-beams
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/60—Ferrous alloys, e.g. steel alloys containing lead, selenium, tellurium, or antimony, or more than 0.04% by weight of sulfur

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Heat Treatment Of Articles (AREA)
  • Heat Treatments In General, Especially Conveying And Cooling (AREA)
  • Heat Treatment Of Steel (AREA)
  • Metal Rolling (AREA)

Abstract

The present invention provides a method for producing a steel material that is uniform in material quality in the longitudinal direction, an apparatus for cooling a steel material and a steel material. The method for producing a steel material according to the present invention is characterized in that when a hot-worked or cooled and re-heated steel material is cooled with a cooling apparatus (2) comprising a plurality of cooling units (head-section cooling headers (21a) to (21c), foot-section cooling headers (22)) arranged in the longitudinal direction of the steel material, the steel material is transported in the cooling device (2) in the longitudinal direction of the steel material for a transport distance L

Description

(57) Abstract: The present invention provides a method for producing a steel material that is uniform in material quality in the longitudinal direction, an apparatus for cooling a steel material and a steel material. The method for producing a steel material according to the present invention is characterized in that when a hot-worked or cooled and re-heated steel material is cooled with a cooling apparatus (2) comprising a plurality of cooling units (head-section cooling headers (21a) to (21c), foot-section cooling headers (22)) arranged in the longitudinal direction of the steel material, the steel material is transported in the cooling device (2) in the longitudinal direction of the steel material for a transport distance L0(m) that satisfies formula (1) wherein Lo is the transport distance (m) of the steel material, m is a natural number, and Lh is the length (m) of the cooling units in the longitudinal direction of the steel material, (m - 0.20) x Lh < Lo < (m + 0.20) xLb (1) (57)
Figure AU2016260101B2_D0001
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- 21 £(3)) (2 1a) ~ (21c) , £ SlJftiIJ'N'yy (2 2) ) (2) ICT, (2) λτ\ cd (m) as
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METHOD FOR PRODUCING STEEL MATERIAL, APPARATUS FOR COOLING
STEEL MATERIAL, AND STEEL MATERIAL
Technical Field [0001]
The present disclosure relates to a method for producing a steel material, an apparatus for cooling a steel material, and a steel material.
Background Art [0002]
One of the longest steel materials is a rail for railways.
In particular, a rail where a rail head section has a pearlite 15 structure high in hardness is, for example, produced as follows .
First, bloom cast by continuous casting is reheated to
1100°C or more, and thereafter hot rolled by rough rolling and finish rolling so as to have a predetermined rail shape. The 20 rolling method in each rolling step is performed by a combination of caliber rolling and universal rolling, or by only caliber rolling, and such rough rolling is performed for a plurality of passes and such finish rolling is performed for a plurality of passes or a single pass. The rail here usually 25 has a length of about 50 m to 200 m by hot rolling.
[0003]
Next, an unsteady section at an end of the rail hot rolled is hot sawn (hot sawing step). In the case where a heat treatment apparatus is here limited with respect to the length, further sawing is performed so that a predetermined length (for example, 25 m) is achieved.
After the hot sawing step, a coolant (air, water, mist, or the like) is sprayed to the rail in a cooling apparatus, thereby performing forced cooling (heat treatment step) . In the heat treatment step, the rail is restricted by a restraint apparatus such as a clamp, and the coolant is sprayed to a head section, a foot section, and also, if necessary, a web. The cooling apparatus usually performs cooling until the temperature of the head section of the rail reaches 650°C or less. After such forced cooling is completed, the rail is released from the restraint apparatus, and is further conveyed to a cooling bed and cooled to 100°C or less. [0004]
In the case where the rail for railways is, for example, a rail for use in a severe environment where heavy goods such as coal and iron ore are transported from any mine of natural resources such as coal, such a rail is demanded to have high wear resistance and high toughness, and therefore the heat treatment step is required. The heat treatment is performed, thereby enabling the rail to be high in hardness and decreasing the amount of wear in use, and therefore the effects of increasing the rail replacement period and decreasing the life-time cost are achieved. A case where the variation in hardness is large in the longitudinal direction of the rail, however, is not preferable because the amount of wear is larger at a low-hardness section than a high-hardness section, thereby not only increasing the vibration in train running, but also decreasing the replacement period. Thus, there is demanded a heat treatment method which allows the rail to be small in the variation in hardness and high in hardness.
[0005]
For example, PTL 1 discloses a method for suppressing a cooling rate to 7°C/sec or less, as a method for decreasing the variation in hardness of a rail.
Moreover, PTL 2 discloses a method for oscillating an H-shaped steel in an amount obtained by an Equation with the pitch between nozzles being adopted as a parameter in accelerated cooling of the H-shaped steel, as a method for uniformly cooling a steel material. Furthermore, PTL 3 discloses a method for oscillating a steel material at a distance 5 times to 10 times the distance in the longitudinal direction of the material of a guide roller, as a method for uniformly cooling a steel material.
Citation List
Patent Literature [0006]
PTL 1 : JP H03-166318 A
PTL 2 : JP 2003-193126 A
PTL 3: JP 2006-55864 A
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-4Summary of Invention [0007]
The method described in PTL 1 can decrease the influence of the variation in temperature at the start of a heat 5 treatment in the longitudinal direction of a steel material on the variation in hardness. In the heat treatment, however, in the case where the variation in cooling rate is caused in the longitudinal direction of a steel material, uniform hardness is not achieved. Therefore, it is difficult to produce a steel 10 material uniform in material properties in the longitudinal direction .
While the methods described in PTLs 2 and 3 can alleviate the reduction in cooling rate due to a weak cooling section generated in cooling equipment, it is difficult to provide a 15 uniform cooling rate in the case where the variation in cooling rate is caused between cooling headers in the longitudinal direction of a steel material. Therefore, it is difficult to produce a steel material uniform in material properties such as hardness in the longitudinal direction.
The present invention has been then made in consideration of the above and seeks to provide a method for producing a steel material uniform in material properties in the longitudinal direction, an apparatus for cooling a steel material, and a steel material.
[0008]
One aspect of the present invention provides a method for producing a steel material, wherein, when a cooling apparatus having a plurality of cooling headers disposed side by side in 30 the longitudinal direction of a steel material cools the steel material hot worked or cooled/reheated, the steel material is conveyed at a conveyance distance Lo (m) satisfying Equation
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-5 (1), in one direction along with the longitudinal direction of the steel material, in the cooling apparatus:
(m - 0.20) x Lh < Lo < (m + 0.20) x Lh ... (1)
Lo: conveyance distance (m) of steel material m: natural number
Lh: length (m) of cooling headers in longitudinal direction of steel material.
[0009]
One aspect of the present invention provides an apparatus for cooling a steel material hot worked or cooled/reheated, including: a plurality of cooling headers disposed side by side in the longitudinal direction of the steel material; and a conveyance section that conveys the steel material at a conveyance distance Lo (m) satisfying Equation (1), in one direction along with the longitudinal direction of the steel material in the cooling apparatus, during cooling of the steel material using the cooling headers.
[0010]
One aspect of the present invention provides a steel material produced by hot working or cooling/reheating and thereafter cooling in a cooling apparatus having a plurality of cooling headers disposed side by side in a longitudinal direction, wherein, during cooling in the cooling apparatus, the steel material is produced with being conveyed at a conveyance distance Lo (m) satisfying Equation (1), in one direction along with the longitudinal direction of the steel material using the cooling headers.
[0011]
One or more embodiments of the present invention may seek
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-βίο provide a method for producing a steel material uniform in material properties in the longitudinal direction, an apparatus for cooling a steel material, and a steel material.
Brief Description of Drawings [0012]
Various embodiments of the present invention are described herein, by way of example only, with reference to the following drawings .
FIG. 1 is a schematic view illustrating a cooling apparatus according to one embodiment of the present invention;
FIG. 2 is a cross-section view illustrating each section of a rail;
FIG. 3 is a plan view illustrating peripheral equipment of 15 the cooling apparatus;
FIG. 4A and FIG. 4B are schematic views illustrating a conveyance operation of the cooling apparatus;
FIG. 5 is a plan view illustrating peripheral equipment of a cooling apparatus in Examples; and
FIG. 6 is a schematic view illustrating a conveyance state on a discharge table in Examples.
Description of Embodiments [0013]
In the following detailed description, many particular details are described so as to provide a complete understanding of embodiments of the present invention. It, however, will be apparent that one or more aspects can be carried out even without such particular details. Additionally, well-known configurations and apparatuses are schematically illustrated in order to simplify the drawings.
<Configuration of cooling apparatus>
First, an apparatus 2 for cooling a steel material according to one embodiment of the present invention is described with reference to FIG. 1 to FIG. 3. Herein, a rail 1 is produced as a steel material in the present embodiment. The cooling apparatus 2 is used in a heat treatment step performed after a hot rolling step or a hot sawing step described below, and forcedly cools a rail 1 having a high temperature. The rail 1, when viewed cross-sectionally perpendicular to the longitudinal direction, includes a head section 11 and a foot section 13 which extend in the width direction and which are opposite to each other in the vertical direction, and a web section 12 which connects the head section 11 disposed above and the foot section 13 disposed below and which extends in the vertical direction, as illustrated in FIG. 2.
[0014]
As illustrated in FIG. 1, the cooling apparatus 2 includes head section-cooling headers 21a to 21c, a foot section-cooling header 22, a pair of clamps 23a and 23b, a thermometer 24 in the apparatus, and a conveyance section 25. The head section-cooling headers 21a to 21c, and the foot section-cooling header 22 serve as cooling sections for cooling the rail 1, and a plurality of the respective headers are provided continuously side by side in the y-axis direction serving as the longitudinal direction of the rail 1. In the following description, the head section-cooling headers 21a to 21c, and the foot section-cooling header 22 are also collectively called cooling headers.
The head section-cooling headers 21a to 21c have coolant-spraying outlets arranged at pitches of several mm to 100 mm, and the coolant-spraying outlets of each of the head section-cooling headers 21a to 21c are provided oppositely on each of the head top surface (end surface in the z-axis positive direction) and the head side surfaces (both end surfaces in the x-axis positive direction) of the head section 11. The head section-cooling headers 21a to 21c each spray a coolant supplied from a supply section not illustrated, to the head top surface and the head side surface of the head section 11, thereby subjecting the head section 11 to forced cooling. The coolant to be used is air, spray water, mist, or the like. Respective pressure measurement apparatuses 211a to 211c are also provided on coolant supply
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-9pathways of the head section-cooling headers 21a to 21c, and the coolant spray pressure is monitored.
[0015]
The foot section-cooling header 22 has coolant-spraying outlets arranged at pitches of several mm to 100 mm, and the coolant-spraying outlets are provided opposite to the lower surface (end surface in the z-axis negative direction) of the foot section 13. The foot section-cooling header 22 sprays a coolant supplied from a supply section not illustrated, to the 10 lower surface of the foot section 13, thereby subjecting the foot section 13 to forced cooling, as in the head sectioncooling headers 21a to 21c. The coolant to be used is air, spray water, mist, or the like, as in the head section-cooling headers 21a to 21c. A pressure apparatus 221 is also provided 15 on a coolant supply pathway of the foot section-cooling header
22, and the coolant spray pressure is monitored.
[0016]
The head section-cooling headers 21a to 21c and the foot section-cooling header 22 each have the same length in the y20 axis direction. The cooling headers are heated from the rail 1 and thus thermally deformed, thereby causing warpage (the generation mechanism of such warpage is described below) to be generated. The amount of warpage of the cooling headers, generated at the same curvature, increases with the square of 25 the length of the cooling headers in the y-axis direction.
Therefore, the length of the cooling headers in the y-axis direction is preferably shorter. On the other hand, an increase in the number of the cooling headers provided in the y-axis direction for a decrease in the length of the cooling 30 headers is not preferable because there are required many feed ports of the coolant as well as many measurement devices and control devices of the amount of coolant spray (for example, a
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-10pressure gauge, a flow meter, and a flow regulator) which are mounted to the cooling headers and a pipe arrangement. Accordingly, the length of the cooling headers in the y-axis direction is needed to be a proper length, and is preferably
0.5 m or more and 4 m or less. The head section-cooling headers 21a to 21c and the foot section-cooling header 22 provided side by side in the y-axis direction are preferably provided as close as possible so that any cooling irregularity is not caused.
[0017]
The pair of clamps 23a and 23b is an instrument for sandwiching each of both ends of the foot section 13 in the xaxis direction to thereby support and restrain the rail 1. The pair of clamps 23a and 23b is plurally provided over the entire 15 length in the longitudinal direction of the rail 1 with being several meters apart.
The thermometer 24 in the apparatus is a non-contact thermometer such as a radiation thermometer, and measures the surface temperature of at least one point on the head top 20 surface of the head section 11.
[0018]
The conveyance section 25 is a conveyance mechanism connected to the pair of clamps 23a and 23b, and is an apparatus that conveys the pair of clamps 23a and 23b in the y-axis direction, thereby conveying the rail 1 in the cooling apparatus 2. The detail of a conveyance operation of the conveyance section 25 is described below.
In the cooling apparatus 2 configured above, the amount of the coolant sprayed from each of the head section-cooling headers 21a to 21c and the foot section-cooling header 22 is adjusted by a control section not illustrated. The control section here acquires the temperature measurement result of the thermometer 24 in the apparatus, and the amount sprayed is adjusted, as needed, based on the temperature measurement result acquired.
[0019]
As illustrated in FIG. 3, a carrying-in table 3 and a discharge table 4 are provided on the periphery of the cooling apparatus 2. The carrying-in table 3 is a table that conveys the rail 1 from a preceding step such as the hot rolling step to the cooling apparatus 2. The discharge table 4 is a table that conveys the rail 1 heat-treated in the cooling apparatus 2, to a next step such as a cooling bed or an examination instrument. An exit side thermometer 5 is a non-contact thermometer that measures the surface temperature of the head section 11 of the rail 1, as in the thermometer 24 in the apparatus, and that measures the temperature of the rail 1 discharged from the cooling apparatus 2 after the heat treatment.
[0020] <Method for producing steel material>
Next, a method for producing a steel material according to the present embodiment is described. In the present embodiment, a perlite-based rail 1 is produced as a steel material. The rail 1 that can be used is, for example, steel including the following chemical component composition. Herein, Equation by % with respect to each chemical component means % by mass, unless especially noted.
C: 0.60% or more and 1.05% or less
C (carbon) is an important element that forms cementite in a perlite-based rail, resulting in increases in hardness and strength and enhancement in wear resistance. If the C content is less than 0.60%, however, such effects are less exerted. The C content is thus preferably 0.60% or more, more preferably 0.70% or more. On the other hand, if C is excessively contained, an increase in the amount of the cementite can be achieved to result in increases in hardness and strength, but deterioration in ductility is conversely caused. Moreover, an increase in the C content expands the temperature range of the γ + Θ region, and promotes softening of a welded heat affected zone. In consideration of such adverse effects, the C content is preferably 1.05% or less, more preferably 0.97% or less.
[0021]
Si: 0.1% or more and 1.5% or less
Si (silicon) is added for enhancing a deoxidizer and a pearlite structure in a rail material, but such an effect is less exerted if the content is less than 0.1%. Therefore, the Si content is preferably 0.1% or more, more preferably
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- 13 0.2% or more. On the other hand, if Si is excessively contained, decarburization is promoted and generation of surface defects of the rail 1 is promoted. Therefore, the Si content is preferably 1.5% or less, more preferably 1.3% or 5 less.
[0022]
Mn: 0.01% or more and 1.5% or less
Mn (manganese) has the effects of decreasing the temperature of perlite transformation and fining the perlite 10 lamellar spacing, and therefore is an element effective for maintaining high hardness inside the rail 1. If the Mn content is less than 0.01%, however, the effects are less exerted. Therefore, the Mn content is preferably 0.01% or more, more preferably 0.3% or more. If the Mn content is more than 1.5%, 15 the eguilibrium transformation temperature (TE) of perlite is lowered, and martensitic transformation easily occurs in the structure. Therefore, the Mn content is preferably 1.5% or less, more preferably 1.3% or less.
[0023]
P: 0.035% or less
P (phosphorus) causes deterioration in toughness and ductility, if the content thereof is more than 0.035%. Therefore, the P content is preferably made lower. Specifically, the P content is preferably 0.035% or less, more 25 preferably 0.025% or less. If special refining or the like is here performed in order to decrease the P content as much as possible, cost rise is caused in smelting. Therefore, the P content is preferably 0.001% or more.
[0024]
S: 0.030% or less
S (sulfur) forms coarse MnS which extends in the rolling direction and which results in deterioration in ductility and
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- 14toughness. Therefore, the S content is preferably made lower. Specifically, the S content is preferably 0.030% or less, more preferably 0.015% or less. If the S content is here decreased as much as possible, cost rise in smelting is remarkably caused due to increases in smelting treatment time and the amount of a solvent. Therefore, the S content is preferably 0.0005% or more .
[0025]
Cr: 0.1% or more and 2.0% or less
Cr (chromium) increases the equilibrium transformation temperature (TE), contributes to fining of the perlite lamellar spacing, and increases hardness and strength. Cr, when used in combination with Sb, is also effective for inhibiting a decarburization layer from being generated. Therefore, the Cr content is preferably 0.1% or more, more preferably 0.2% or more. If the Cr content is more than 2.0%, not only the possibility of the occurrence of welding defects is increased, but also hardenability is increased, and generation of martensite is promoted. Therefore, the Cr content is preferably 2.0% or less, more preferably 1.5% or less.
The total content of Si and Cr is desirably 2.0% or less.
The reason is because, if the total content of Si and Cr is more than 2.0%, an excessive increase in scale adhesiveness can inhibit scale peeling and promote decarburization.
[0026]
Sb: 0.005% or more and 0.5% or less
Sb (antimony) has a remarkable effect of preventing decarburization during heating of a rail steel material in a heating furnace. In particular, Sb is added together with Cr, to thereby have the effect of reducing generation of a decarburization layer, when the Sb content is 0.005% or more . Therefore, the Sb content is preferably 0.005% or more, more preferably 0.01% or more . If the Sb content is more than 0.5%, the effect is saturated. Therefore, the Sb content is preferably 0.5% or less, more preferably 0.3% or less.
The steel for use as the rail 1 may further contain, in addition to the chemical composition, one or more elements of Cu: 0.01% or more and 1.0% or less, Ni: 0.01% or more and 0.5% or less, Mo: 0.01% or more and 0.5% or less, V: 0.001% or more and 0.15% or less, and Nb: 0.001% or more and 0.030% or less.
[0027]
Cu: 0.01% or more and 1.0% or less
Cu (copper) is an element that can provide much higher hardness by solid solution strengthening. Cu also has the effect of suppressing decarburization. In order to expect such an effect, the Cu content is preferably 0.01% or more, more preferably 0.05% or more . If the Cu content is more than 1.0%, surface cracking due to embrittlement in continuous casting and/or rolling easily occurs. Therefore, the Cu content is preferably 1.0% or less, more preferably 0.6% or less .
[0028]
Ni: 0.01% or more and 0.5% or less
Ni (nickel) is an element effective for enhancements in toughness and ductility. Moreover, Ni is an element also effective for suppressing Cu cracking by addition as a composite with Cu . Therefore, in the case where Cu is added, Ni is desirably added, and the Ni content is more preferably 0.05% or mo re. If the Ni content is less than 0.01%, however, such effects are not exerted. Therefore, the Ni content is preferably 0.01% or more. If the Ni content is more than 0.5%, hardenability is increased, and generation of martensite is promoted. Therefore, the Ni content is preferably 0.5% or less, more preferably 0.3% or less.
[0029]
Mo: 0.01% or more and 0.5% or less
Mo (molybdenum) is an element effective for an increase in strength, but such an effect is less exerted if the content is less than 0.01%. Therefore, the Mo content is preferably 0.01% or more, more preferably 0.05% or more. If the Mo content is more than 0.5%, an increase in hardenability causes martensite to be generated, resulting in extreme deterioration in toughness and ductility. Therefore, the Mo content is preferably 0.5% or less, more preferably 0.3% or less .
[0030]
V: 0.001% or more and 0.15% or less
V (vanadium) is an element that forms VC, VN or the like and is finely precipitated in ferrite, and that contributes to an increase in strength through precipitation strengthening. V can also be expected to have the effects of serving as a trap site of hydrogen and suppressing delayed fracture. In order to exert such effects, the V content is preferably 0.001% or more, more preferably 0.005% or more. If V is added in a rate of more than 0.15%, an increase in alloy cost is remarkable relative to saturation of such effects. Therefore, the V content is preferably 0.15% or less, more preferably 0.12% or less.
[0031]
Nb: 0.001% or more and 0.030% or less
Nb (niobium) is effective for allowing the unrecrystallized temperature region of austenite to be in a higher temperature region and promoting introduction of processing strain into austenite in rolling, thereby miniaturizing the sizes of perlite colony and block. Thus, Nb is an element effective for enhancements in ductility and toughness. In order to exert such effects, the Nb content is preferably 0.001% or more, more preferably 0.003% or more. If the Nb content is more than 0.030%, Nb carbonitride is crystalized in the course of solidification in casting of a rail steel material such as bloom, resulting in deterioration in cleanliness. Therefore, the Nb content is preferably 0.030% or less, more preferably 0.025% or less.
[0032]
The balance other than the above components is configured from Fe (iron) and inevitable impurities. Up to 0.015% of N (nitrogen), up to 0.004% of 0 (oxygen), and up to 0.0003% of H (hydrogen) can be allowed to be incorporated as such inevitable impurities. In order to suppress deterioration in rolling fatigue characteristics due to hard AIN and TiN, the Al content is desirably 0.001% or less and the Ti content is desirably 0.001% or less.
[0033]
In a method for producing the rail 1 according to the present embodiment, first, for example, the bloom of the chemical component composition, serving as the material of the rail 1 cast by a continuous casting method, is carried in a heating furnace, and heated to 1100°C or more.
Next, the bloom heated is rolled in each of a break-down roller, a rough roller and a finish roller for one or more passes, and finally rolled to the rail 1 having a shape illustrated in FIG. 2 (hot rolling step) . The length in the longitudinal direction of the rail 1 rolled is here about 50 m to 200 m, and is, if necessary, hot sawn so as to have a length of, for example, 25 m (hot sawing step). A shorter length in the longitudinal direction of the rail 1 here causes the subseguent heat treatment step to be involuntarily affected by the coolant sprayed onto the end surface in the longitudinal direction during cooling. Therefore, the length in the longitudinal direction of the rail 1 for use in the heat treatment step is three times or more the height from the head top surface of the head section 11 of the rail
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- 191 to the lower surface of the foot section 13 thereof. On the other hand, the upper limit of the length in the longitudinal direction of the rail 1 for use in the heat treatment step is defined as the length of rolling (the maximum rolling length in the hot rolling step).
[0034]
The rail 1 hot rolled or hot sawn is conveyed to the cooling apparatus 2 by the carrying-in table 3, and cooled in the cooling apparatus 2 (heat treatment step).
The temperature of the rail 1 here conveyed to the cooling apparatus 2 is desirably in the austenite temperature region. A rail for use in mine or a curved section is needed to have high hardness, and therefore rapid acceleration is needed in the cooling apparatus 2 after rolling. Such acceleration is for fining the perlite lamellar spacing, thereby providing a high-hardness structure, and an increase in the degree of supercooling in transformation, namely, an increase in the cooling rate in transformation can provide such a high-hardness structure. If the structure of the rail 1, however, is transformed before cooling in the cooling apparatus 2, such transformation progresses at an extremely low cooling rate in spontaneous cooling, and therefore cannot provide a highhardness structure. Accordingly, when the temperature of the rail 1 is equal to or lower than the lowest temperature in the austenite temperature region at the start of cooling in the cooling apparatus 2, the rail 1 is preferably reheated to any temperature in the austenite temperature region and thereafter subjected to the heat treatment step.
[0035]
In the heat treatment step, the rail 1 is conveyed to the cooling apparatus 2, and thereafter the rail 1 is restrained by the clamps 23a and 23b. Thereafter, the rail 1 is rapidly cooled by spraying the coolant from each of the head section-cooling headers 21a to 21c and the foot section-cooling header 22. The cooling rate in the heat treatment is preferably changed depending on the desired hardness, and furthermore, the cooling rate may be excessively increased, thereby causing martensitic transformation to occur and impairing toughness. Therefore, the control section monitors the cooling rate based on the result of the temperature measured by the thermometer 24 in the apparatus during cooling, and changes the amount of the coolant to be sprayed. The control section may also be here, if necessary, set so as to stop spraying of the coolant and to perform cooling by spontaneous cooling.
[0036]
In the heat treatment step, in the case where a plurality of the cooling headers serving as the cooling sections of the cooling apparatus 2 have been provided in portions in the longitudinal direction of the rail, temperature variation has occurred in the longitudinal direction of the rail 1 in some cases. The present inventors have investigated the cause for the occurrence of the temperature variation, and thus describe the investigation result. The cooling headers may be close to the rail 1 in order to achieve a high cooling rate in cooling of the rail 1 having a high temperature. In such
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-21 a case, the cooling headers are heated by radiation from the rail 1 and/or heat conduction of air, and therefore thermally deformed. Only surfaces of the cooling headers, the surfaces being closer to the steel material, are heated and thermally expanded, and therefore, the cooling headers are usually warped so that end portions thereof are away from the rail 1. When the cooling headers are thus deformed, the end portions are away from the rail 1 against the center portion of the cooling headers, thereby resulting in a reduction in the cooling rate 10 at the end portions as compared with the center portion.
Therefore, a strong cooling section and a weak cooling section are repeatedly present in the longitudinal direction of the rail 1 at an interval where each of the cooling headers is provided, thereby causing the temperature variation in the 15 longitudinal direction of the rail 1.
[0037]
The present inventors have found that such temperature variation can be eliminated by oscillating the rail 1 in the cooling apparatus 2 along with the longitudinal direction of 20 the rail 1 at a predetermined amplitude and conveying it. In the heat treatment step of the present embodiment, the conveyance section 25 conveys the clamps 23a and 23b together with the rail 1 restrained, with oscillation at a predetermined amplitude, in cooling. Such oscillation here means an operation that conveys the rail 1 alternately in the y-axis positive direction and in the y-axis negative direction by a predetermined conveyance distance Lo. The conveyance distance Lo serving as the amplitude of oscillation corresponds to the distance (m) satisfying the following Equation (1). In Equation (1) , m represents a natural number, and Lh represents the length (m) of the cooling headers, being the length of the cooling sections in the longitudinal direction of the rail 1 (y-axis direction), respectively.
(m - 0.20) x Lh < Lo < (m + 0.20) x Lh ... (1) [0038]
The conveyance operation of the rail 1 by the conveyance section 25 is described with reference to FIG. 4. In the example illustrated in FIG. 4, the conveyance distance Lo in the heat treatment step is a length twice the length Lh of the cooling headers (head section-cooling header 21a and foot section-cooling header 22) serving as the cooling sections. The conveyance section 25 then conveys the rail 1 in the state illustrated in FIG. 4A at the conveyance distance Lo in the y-axis negative direction. Thus, the rail 1 is in the state illustrated in FIG. 4B from the state illustrated in FIG. 4A. Next, the conveyance section 25 conveys the rail 1 in the state illustrated in FIG. 4B at the conveyance distance Lo in the y-axis positive direction. Thus, the rail 1 is again in the state illustrated in FIG. 4A from the state illustrated in FIG. 4B. Such operations are repeated to perform the conveyance operation.
[0039]
Furthermore, the conveyance operation of the rail 1 in the cooling apparatus 2 by the conveyance section 25 is preferably performed continuously during cooling of the rail
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-23 1. In other words, when the cooling time of the rail 1 in the heat treatment step is defined as T (min) , the conveyance velocity V (mm/min) of the rail 1 is set so that a relationship of Equation (2) is satisfied. In Equation (2), n represents a 5 natural number.
V = Lh/ (T x n) ... (2) [0040]
Furthermore, cooling is performed in the heat treatment step until a final structure made of 100% of perlite, or a 10 final structure having 5% or less of pro-eutectoid ferrite and pro-eutectoid cementite and the balance being perlite or a final structure where perlite and bainite are mixed is obtained. The bainite phase and the cementite phase are impaired in toughness, therefore a structure made of 100% of 15 the perlite phase is preferable in order not to generate any failures caused by deterioration in toughness, such as sharing, and a final structure is determined depending on the intended use .
[0041]
As described above, a high-hardness structure is obtained by allowing transformation to occur in the heat treatment, and therefore the heat treatment completion temperature is needed to be achieved after completion of transformation. While the depth necessary for such a high-hardness structure, however, varies depending on the intended use of the rail 1 and the heat treatment completion temperature cannot be thus clearly limited, cooling is needed to be performed at least until the temperature of the surface of the head section 11 reaches 650°C or less.
[0042]
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-24After the heat treatment step, the rail 1 is conveyed to the cooling bed by the discharge table 4, and is cooled thereon to a temperature ranging from room temperature to 100°C. Thereafter, the rail 1 is straightened by roller straightening 5 in order to decrease warpage. The rail 1 then undergoes an examination and thereafter is shipped. Since a nonstraightened section is generated at an end in the longitudinal direction of the rail 1 in straightening by roller straightening, cold sawing may also be performed after 10 straightening by roller straightening, without sawing to the length of a final product in hot sawing. The end in the longitudinal direction of the rail 1, in cold sawing, here corresponds to each of both ends in the rolling length, and therefore any non-straightened section is decreased and warpage 15 is decreased.
A rail 1 uniform in material properties in the longitudinal direction can be produced through the above steps. [0043] <Modifications>
Although the present invention is described above with reference to particular embodiments, the present invention is not intended to be limited by such description. Not only various modifications of the embodiments disclosed, but also other embodiments of the present invention are also apparent to 25 those skilled in the art with reference to the detailed description of the present invention. Accordingly, it is to be understood that claims also cover such modifications or embodiments encompassed in the scope and gist of the present invention .
[0044]
For example, the rail 1 is used as the steel material in the embodiment, but the present invention is not limited to such an embodiment. For example, the steel material to be produced may be any other steel material product such as a thick plate or a shaped steel. In such a case, the chemical component composition of the steel material product, the configuration of the cooling apparatus 2, and the like are not limited to the cases of the embodiments. Even when the steel material to be produced is the rail 1, any steel having a different chemical component composition from that in the embodiment may be used. As described above, an end surface is involuntarily affected by the coolant sprayed, during cooling, and therefore the minimum length in the longitudinal direction of the steel material product is three times or more the thickness of the thickest portion of a steel material such as a shaped steel, or three times or more the thickness of a plate material representative of a thick plate, and the maximum length thereof is the rolling length.
[0045]
While the conveyance distance Lo satisfies Equation (1) in the embodiment, the conveyance distance Lo is preferably a value closer to the integral multiple of the length L of the cooling sections, and preferably satisfies the following
Equation (3).
(m - 0.10) x Lh < Lo < (m + 0.10) x Lh ... (3)
Thus, the variation in cooling rate, caused in each header unit of the cooling sections, can be more decreased.
While the conveyance section 25 conveys the rail 1 with the rail 1 being oscillated in the heat treatment step in the embodiment, the present invention is not limited to such an embodiment. For example, the conveyance section 25 may be configured so as to convey the rail 1 at the conveyance distance Lo in only any one direction of the y-axis positive direction and the y-axis negative direction with the rail 1 being not oscillated.
[0046]
While the conveyance operation of the rail 1 in the cooling apparatus 2 by the conveyance section 25 in the heat treatment step is continuously performed during cooling of the rail 1 in the embodiment, the present invention is not limited to such an embodiment. For example, the conveyance operation of the rail 1 in the embodiment may be performed for a time more than half of the cooling time T, after cooling of the rail 1. The conveyance operation is here performed at the conveyance distance Lo satisfying Equation (1), for a predetermined time (time more than half of the cooling time T) from the start of cooling of the rail 1. Thereafter, the conveyance operation is preferably continuously performed for the remaining time of the cooling time T, but the conveyance distance Lo does not necessarily satisfy Equation (1) . Thus, the time for which uniform cooling can be made can be at least half of the heat treatment time, thereby decreasing the variation in cooling rate. In such a case, the conveyance velocity V does not necessarily satisfy Equation (2), and therefore application to a cooling apparatus 2 that cannot be changed in the conveyance velocity V can also be made.
[0047] <Effects of embodiment>
(1) In a method for producing a steel material according to one aspect of the present invention, when a cooling apparatus 2 having a plurality of cooling sections (head section-cooling headers 21a to 21c, and a foot section-cooling header 22) disposed side by side in the longitudinal direction of a steel material cools a steel material hot worked or cooled/reheated, the steel material is conveyed at the conveyance distance Lo (m) satisfying Equation (1), in the longitudinal direction of the steel material, in the cooling apparatus 2.
[0048]
While the steel material is needed to be cooled at a high cooling rate in order to provide a high-hardness steel material, as described above, the cooling headers of the cooling apparatus 2 are needed therefor to be cooled with being closer to the steel material. The cooling headers are here heated by radiation or the like from the steel material, and the cooling headers are deformed so as to be warped in the longitudinal direction. If cooling is performed in such a state, the difference in distance from the steel material is caused in the longitudinal direction of the cooling headers, and thus the variation in the cooling rate (in a strong cooling section and a weak cooling section) is caused in each cooling header unit, resulting in the occurrence of the variation in hardness of the steel material. For example, in production of the rail 1 as the steel material, the rail 1 may be usually cooled with being oscillated at a lower amplitude than that in the embodiment, in the longitudinal direction. The cooling rate is here higher at a position immediately below each coolant-spraying outlet and lower at a position away from the position immediately below each coolant-spraying outlet, and therefore the rail can be at least conveyed at a distance (several mm to 100 mm) between coolant-spraying outlets, thereby uniformly passing through the position immediately below each coolant-spraying outlet, higher in the cooling rate, and the position away therefrom, lower in the cooling rate. Such conventional oscillation (conveyance operation), however, has not be able to eliminate cooling irregularity caused in each cooling header unit.
[0049]
On the other hand, the above configuration can allow the steel material to be conveyed at a distance substantially integral multiple of the length Lh of the cooling headers in the longitudinal direction during cooling, thereby allowing respective times, at which the steel material passes through the strong cooling section and the weak cooling section, to be the same at each position in a region corresponding to the conveyance distance Lo in the longitudinal direction of the steel material. Therefore, the variation in cooling rate, caused in each cooling header unit, can be decreased, thereby allowing a steel material uniform in material properties such as hardness in the longitudinal direction to be obtained. Furthermore, the distance between the cooling headers and the steel material can be shorter, and therefore a high cooling rate can be achieved and the steel material can have high hardness .
[0050] (2) In conveyance of the steel material in configuration (1) above, the steel material is conveyed with being oscillated, and the amplitude of such oscillation is set at the conveyance distance Lo satisfying Equation (1) .
Such a configuration can allow a long total conveyance distance to be achieved even in the case where the length of the cooling apparatus does not have sufficient margin relative to the length in the longitudinal direction of the steel material.
(3) In configuration (1) or (2), the steel material is a rail material.
Such a configuration can allow a rail material less in the variation in material properties in the longitudinal direction to be obtained as a rail material being a long steel material. For example, when the rail material is a high-hardness rail 1, the variation in cooling in the heat treatment step can be suppressed within 20°C or less, and as a result, the variation in hardness can be suppressed within an HV of 13 or less at a depth position of 1 mm from the surface and within an HV of 10 or less at a depth position of 5 mm therefrom.
[0051] (4) An apparatus 2 for cooling a steel material according to one aspect of the present invention is a cooling apparatus 2 for cooling a steel material hot worked or cooled/reheated, including a plurality of cooling sections (head section-cooling headers 21a to 21c, and a foot section-cooling header 22) disposed side by side in the longitudinal direction of the steel material, and a conveyance section 25 that conveys the steel material at the conveyance distance Lo (m) satisfying Equation (1), in the longitudinal direction of the steel material in the cooling apparatus 2, during cooling of the steel material in the cooling sections.
Such a configuration can allow the same effect as in configuration (1) above to be obtained.
[0052] (5) A steel material according to one aspect of the present invention is a steel material produced by hot working or cooling/reheating and thereafter cooling in a cooling apparatus 2 having a plurality of cooling sections (head section-cooling headers 21a to 21c, and a foot section-cooling header 22) disposed side by side in the longitudinal direction, wherein, during cooling in the cooling apparatus 2, the steel material is produced with being conveyed at the conveyance distance Lo (m) satisfying Equation (1), in one direction along with the longitudinal direction of the steel material in the cooling apparatus 2.
Such a configuration can allow the steel material to be uniformly cooled in the longitudinal direction, thereby providing a steel material uniform in material properties in the longitudinal direction.
Example 1 [0053]
Next, Example 1 performed by the inventors is described. First, before Example 1, a rail 1 being a steel material was produced in a different conveyance distance Lo condition from the embodiment, as Conventional Examples, and the material properties thereof were evaluated.
In Conventional Examples, first, bloom of a chemical component composition in Condition A represented in Table 1 was cast by using a continuous casting method. The balance of the chemical component composition of the bloom was here substantially Fe, specifically Fe and inevitable impurities. [0054] [Table 1]
Condition Chemical component composition (% by mass)
C Si Mn P S Al Ti
A 0.83 0.52 0.51 0.015 0.008 0.0005 0.001
B 0.83 0.52 1.11 0.015 0.008 0.0005 0.001
C 1.03 0.52 1.11 0.015 0.008 0.0005 0.001
[0055]
Next, the bloom cast was reheated to 1100°C or more in a heating furnace, thereafter taken out from the heating furnace, and hot rolled through a break-down roller, a rough roller and a finish roller so that the cross-sectional shape was the final shape (rail shape illustrated in FIG. 2). In such hot rolling, the rail 1 was rolled at an inverted position where a head section 11 and a foot section 13 were in contact with a conveyance stage.
Furthermore, the rail 1 hot rolled was conveyed to a cooling apparatus 2, and the rail 1 was cooled (heat treatment step) . Since the rail 1 was here rolled at the inverted position as a rolling position, the rail 1, when carried in the cooling apparatus 2, was inverted, and was allowed to be at an erect position illustrated in FIG. 2, where the foot section 13 was located below in the vertical direction and the head section 11 was located above in the vertical direction, and the rail 1 was restrained by clamps 23a and 23b. Cooling was then performed by spraying of a coolant from each cooling header. During such cooling, the coolant was air, and the distance between the cooling headers and the rail was 20 mm or 50 mm. As disclosed in PTL 1, the spray pressure of the coolant was set at 1.3 kPa to 130 kPa so that the cooling rate at 670°C to 770°C at a depth position of 5 mm from the surface layer was 3°C/sec to 7°C/sec, and cooling was performed until the surface temperature of the head section 11 reached 530°C or less, while temperature measurement was performed by a thermometer 24 in the apparatus.
[0056]
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-33 During cooling in the cooling apparatus 2, such cooling was performed in a condition where the rail 1 was not conveyed at all and in a condition where the rail 1 was conveyed at a conveyance distance Lo of 1 m, in Conventional Examples. The 5 length Lh of the cooling headers was 4 m, and the rail 1 was conveyed at only a total distance of 4 m with being oscillated in the cooling apparatus 2, in the condition where the rail 1 was conveyed.
After completion of the heat treatment, the rail 1 was 10 taken out from the cooling apparatus 2 onto a discharge table 4, and the surface temperature of the head section 11 of the rail 1 after cooling was measured by use of an exit side thermometer 5 provided on the discharge table 4 as illustrated in FIG. 5 and FIG. 6. The exit side thermometer 5 was here 15 used to measure the temperature at a plurality of positions over the entire length in the longitudinal direction of the rail 1, and the variation in temperature after cooling was calculated from the maximum value and the minimum value of the measurement results.
[0057]
Thereafter, the rail 1 was conveyed to a cooling bed and cooled in the cooling bed until the temperature reached room temperature to 100°C, and thereafter straightening was performed by a roller straightening machine to produce a rail 1 25 being a final product. Thereafter, the rail 1 produced was cold sawn to thereby take a sample, and the hardness of the sample taken was measured. The sample was here taken at a pitch of 1 m relative to the total length of the rail 1, and the Vickers hardness test was performed as hardness measurement at depth positions of 1 mm and 5 mm from the surface at the center in the width direction of the head section 11 of the rail 1.
[0058]
The cooling conditions and the evaluation results of material properties in Conventional Examples are represented in Table 2 . In Conventional Examples 1 to 3 where the distance between the cooling headers and the rail was 50 mm, the variation in temperature in the entire length was within 20°C and the variation in hardness at each position where the sample was taken was also within an HV of 20 at a depth of 1 mm and within an HV of 10 at a depth of 5 mm. In Conventional Examples 4 to 9 where the distance between the headers and the rail was 20 mm, the variation in temperature in the entire length was within 120°C, the variation in hardness was within an HV of 120 at a depth of 1 mm and within an HV of 60 at a depth of 5 mm, and material properties were confirmed not to be uniform. The reason for this was considered because, in the case where the distance between the cooling headers and the rail was 50 mm, the influence of radiation from the rail 1 was smaller and therefore the amount of warpage of the cooling headers was smaller, and the variations in temperature and hardness were smaller. On the other hand, it was considered with respect to the condition where the distance between the cooling headers and the rail was 20 mm that the cooling headers were heated by radiation of the rail 1 and thus the cooling headers were thermally deformed considerably, and therefore the variations in temperature and hardness were larger.
In the case where the distance between the cooling headers and the rail was 50 mm, however, a high pressure of
130 kPa exceeding 1 atm was reguired when the cooling rate is 7°C/sec in order to obtain a high-hardness structure.
Therefore, such a case is not preferable in terms of facility cost and energy cost. It is confirmed from the foregoing that material properties uniform in the longitudinal direction 10 were difficult to obtain, while a high cooling rate was obtained, in the conditions of Conventional Examples 1 to 9.
[0059] [Table 2]
Condition Component Colling header length Lh [m] Conveyance distance Lo [m] Coolant Distance between cooling headers and rail [mm] Spray pressure [kPa] Target cooling rate at 5 mm depth position [°C/sec] Variation in temperature after completion of heat treatment (Maximum - Minimum) [°C] Hardness at 1 mm depth position Hardness at 5 mm depth position
Average Maximum Minimum Average Maximum Minimum
[HV] [HV] [HV] [HV] [HV] [HV]
Conventional Example 1 A 4 0 Air 50 130 7 20 393 400 387 375 380 370
Conventional Example 2 A 4 0 Air 50 30 5 15 375 380 370 356 360 353
Conventional Example 3 A 4 0 Air 50 5 3 10 357 360 353 338 340 335
Conventional Example 4 A 4 0 Air 20 30 7 120 360 400 320 350 380 320
Conventional Example 5 A 4 0 Air 20 7 5 110 343 380 307 333 360 305
Conventional Example 6 A 4 0 Air 20 1.3 3 100 327 360 293 315 340 290
Conventional Example Ί A 4 1 Air 20 30 7 80 373 400 347 360 380 340
Conventional Example 8 A 4 1 Air 20 7 5 60 360 380 340 345 360 330
Conventional Example 9 A 4 1 Air 20 1.3 3 40 347 360 333 330 340 320
[0060]
Next, a rail 1 was produced by the inventors in a condition where the conveyance distance Lo of the embodiment was adopted, as Example 1, and the material properties thereof were evaluated.
In Example 1, first, bloom of each of chemical component compositions with respect to A to C represented in Table 1 was cast by using a continuous casting method. Herein, the balance of the chemical component composition of the bloom was substantially Fe, and specifically Fe and inevitable impurities .
Next, the bloom cast was reheated to 1100°C or more in a heating furnace, and thereafter taken out from the heating furnace and hot rolled through a break-down roller, a rough roller and a finish roller so that the cross-sectional shape was the final shape, in the same manner as in Conventional Examples. In the hot rolling, the rail 1 was rolled at an inverted position where the head section 11 and the foot section 13 were in contact with a conveyance stage.
[0061]
Furthermore, the rail 1 hot rolled was conveyed to the cooling apparatus 2, and the rail 1 was cooled in the same manner as in the embodiment (heat treatment step) . Since the rail 1 was here rolled at the inverted position as a rolling position, the rail 1, when carried in the cooling apparatus 2, was inverted, and was allowed to be at an erect position illustrated in FIG. 2, where the foot section 13 was located below in the vertical direction and the head section 11 was located above in the vertical direction, and the rail 1 was restrained by clamps 23a and 23b. Cooling was then performed by spraying of a coolant from each cooling header. During such cooling, the coolant was any of air, mist or spray water, and the distance between the cooling headers and the rail was 20 mm. When the coolant was air, the spray pressure of the coolant was 5 kPa to 50 kPa, and when the coolant was mist or spray water, 15% of a spray outlet was changed to a mist nozzle or a spray nozzle, and the coolant was sprayed through such a nozzle at a spray pressure of 500 kPa or 300 kPa. When the coolant was mist or spray water, air was sprayed through 85% of the remaining outlet, and the pressure of air was 30 kPa. Cooling was performed with the spray pressure of the coolant being changed depending on the condition in the heat treatment step. Furthermore, cooling was performed in the heat treatment step until the surface temperature of the head section 11 reached 530°C or less, while temperature measurement was performed by the thermometer 24 in the apparatus, in the same manner as in Conventional Examples. [0062]
Furthermore, cooling was performed in the heat treatment step in conditions of the length Lh of the cooling headers, where the conveyance distance Lo and the total conveyance distance (m) serving as the total distance of conveyance in cooling were changed within the scope of the embodiment.
After completion of the heat treatment, the rail 1 was taken out from the cooling apparatus 2 onto the discharge table 4, and the surface temperature of the head section 11
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-39of the rail 1 after cooling was measured by use of the exit side thermometer 5 provided on the discharge table 4, as illustrated in FIG. 5 and FIG. 6. The exit side thermometer 5 was here used to measure the temperature at a plurality of positions over the entire length in the longitudinal direction of the rail 1, and the variation in temperature after cooling was calculated from the maximum value and the minimum value of the measurement results.
[0063]
Thereafter, the rail 1 was conveyed to a cooling bed and cooled in the cooling bed until the temperature reached room temperature to 100°C, and thereafter straightening was performed by a roller straightening machine to produce a rail 1 being a final product. Thereafter, the rail 1 produced was cold sawn to thereby take a sample, and the hardness of the sample taken was measured. Herein, the sample was taken at a pitch of 1 m relative to the total length of the rail 1, and the Vickers hardness test was performed as hardness measurement at depth positions of 1 mm and 5 mm from the surface at the 20 center in the width direction of the head section 11 of the rail 1.
The same manner was also conducted in Comparative Example where the condition of the conveyance distance Lo was different from that of the embodiment, for comparison with
Example 1, and material properties of a rail 1 produced were evaluated.
[0064]
The cooling conditions and the evaluation results of material properties in Example 1 and Comparative Example 1 are represented in Table 3. In Table 3, the pressure as the spray pressure condition of the coolant in Example 1-14 was changed from 10 to 30 at a position of 1/3 of the total conveyance distance, and the pressure as the spray pressure condition of the coolant in Example 1-15 was changed from 30 to 10 at a position of 1/3 of the total conveyance distance and the spray pressure was changed from 10 to 30 at a position of 2/3 of the total conveyance distance. While the conveyance distance Lo was set to 4 m in the condition of Comparative Example 1-3, conveyance was made by only up to 3.0 m during cooling of the rail 1, and while the conveyance distance Lo was set to 2 m in the condition of Comparative Example 1-4, conveyance was made by only up to 1.0 m during cooling of the rail 1.
[0065]
The variation in temperature in the entire length was within 20°C in the conditions of Examples 1-1 to 1-17, and the variation in temperature in the entire length was smaller and was within 5°C in the condition where the oscillation distance Lo was n times the cooling header length Lh. The variation in temperature, however, was within 20°C or more in the condition where the oscillation distance Lo indicated in Comparative Examples 1-1 to 1-4 was shorter than the cooling header length Lh or in the condition where the total conveyance distance in the heat treatment was less than the cooling header length Lh.
[0066] [Table 3]
Condition Component Dooling headei length Lh [m] Conveyance distance Lo [m] Total conveyance distance [m] Coolant Spray pressure [kPa] Variation in temperature after completion of heat treatment (Maximum - Minimum) [°C] Hardness at 1 mm depth position Hardness at 5 mm depth position
Average [HV] Maximum [HV] Minimum [HV] Average [HV] Maximum [HV] Minimum [HV]
Example 1-1 A 0.5 0.5 4.0 Air 30 3 405 406 404 385 386 385
Example 1-2 A 1 1 4.0 Air 30 3 400 401 399 380 381 380
Example 1-3 A 2 2 4.0 Air 30 4 390 391 388 370 371 369
Example 1-4 A 4 4 4.0 Air 30 5 360 362 359 350 351 349
Example 1-5 A 2 4 4.0 Air 30 4 390 391 388 370 371 369
Example 1-6 A 2 8 8.0 Air 30 4 390 391 388 370 371 369
Example 1-7 A 2 2 2.0 Air 30 4 390 391 388 370 371 369
Example 1-8 A 2 2 5.0 Air 30 17 385 391 380 367 371 363
Example 1-9 A 2 2 2.5 Air 30 9 388 391 385 369 371 367
Example 1-10 B 1 1 3.0 Air 30 19 434 440 427 415 420 411
Example 1-11 C 1 1 5.0 Air 30 19 444 450 437 425 430 421
Example 1-12 A 2 2 6.0 Air 5 4 370 371 368 350 351 349
Example 1-13 A 2 2 8.0 Air 50 4 410 411 408 390 391 389
Example 1-14 A 2 2 10.0 Air 10—>30 4 375 376 373 370 371 369
Example 1-15 A 2 2 12.0 Air 30-^10—>30 4 395 396 393 390 391 389
Example 1-16 A 4 4 8.0 Mist 500 4 450 451 448 430 431 429
Example 1-17 A 4 4 8.0 Spray water 300 4 450 451 448 430 431 429
Comparative Example 1-1 A 4 1 8.0 Air 30 80 344 371 318 331 351 311
Comparative Example 1-2 A 2 1 8.0 Air 30 40 378 391 364 361 371 351
Comparative Example 1-3 A 4 4 3.0 Air 30 35 359 371 348 342 351 334
Comparative Example 1-4 A 2 2 1.0 Air 30 25 383 391 374 365 371 359
[0067]
It was confirmed from the evaluation results of material properties that the variation in temperature was suppressed within 20°C or less, and the variation in hardness was an HV of 13 or less at a depth position of 1 mm from the surface and an HV of 10 or less at a depth position of 5 mm therefrom in the conditions of Examples 1-1 to 1-17. On the other hand, the variation in temperature was not suppressed within 20°C or less, and the variation in hardness was as large as an HV of 15 or more at a depth position of 1 mm from the surface and as large as an HV of 13 or more at a depth position of 5 mm therefrom in the conditions of Comparative Examples 1-1 to 1-4 .
[0068]
In comparison of the conditions indicated in Examples 1-1 to 1-9 where Component A was adopted, the spray pressure was constant and 30 kPa and the coolant was air, it was confirmed that the average hardness was as very high as an HV of 391 or more at a depth position of 1 mm and was as very high as an HV of 367 or more at a depth position of 5 mm in the condition where the cooling header length Lh was 3 m or less. The average hardness, however, was as low as an HV of 398 at a depth position of 1 mm and as low as an HV of 379 at a depth position of 5 mm, while the variation in hardness could be reduced, in the condition where the cooling header length Lh was 4 m, as compared with the condition where the cooling header length Lh was shorter.
[0069]
It could also be confirmed in Examples 1-10 and 1-11 where the component was changed, in Examples 1-12 and 1-13 where the spray pressure was changed, and in Examples 1-14 and 1-15 where the spray pressure was changed halfway that the variations in temperature and hardness were reduced as in Examples 1-1 to 1-9. The average cooling rate in cooling was 4°C/sec in Example 1-12 where the spray pressure was the lowest, and the average cooling rate in cooling was 8.5°C/sec in Example 1-13 where the spray pressure was the highest. Therefore, it has been able to be confirmed that, when the coolant is air, the effects of the present invention can be exerted at least in the range from 4°C/sec to 8.5°C/sec. It was also confirmed that the variations in temperature and hardness were smaller, furthermore the average hardness at a depth position of 1 mm was an HV of 479 and the average hardness at a depth position of 5 mm was an HV of 459, and the hardness was thus very high regardless of a long cooling header length Lh of 4 m, in Examples 1-16 and 1-17 where the coolant was spray water or mist.
Example 2 [0070]
Next, Example 2 performed by the inventors is described. In Example 2, bloom of a different chemical component composition from that in Example 1 was used to produce a rail 1 in the same manner as in Example 1 in the condition where the conveyance distance Lo in the embodiment was adopted, and material properties of the rail 1 were evaluated. In Example 2, first, bloom of each chemical component composition of
Conditions D to F represented in Table 4 was cast by using a continuous casting method. The balance of the chemical component composition of the bloom was here substantially Fe, specifically Fe and inevitable impurities.
[0071] [Table 4]
Condition
Chemical component composition (% by mass)
Si
Mn
0.84
0.54
0.55
0.82
0.23
1.26
0.83
0.66
0.26
0.82
0.55
1.13
P
0.018
0.018
0.015
0.012
S
0.004
0.005
0.005
0.002
Cr
0.784
0.155
0.896
0.224
Sb Al
Ti
0.002
Others
V: 0.058
0.0360 0.0001 0.001
0.1200 0.0005 0.001
Cu: 0.11, Ni: 0.12, Mo: 0.11
Nb: 0.009
C:\Interwoven\NRPortbl\DCC\KZI I\l 7791059_ I .docx-2/l 0/2018
2016260101 02 Oct 2018
-46[0072]
Next, the bloom cast was reheated to 1100°C or more in a heating furnace, thereafter hot rolled, and subseguently cooled (heat treatment step) in the same manner as in Example 1 described above. Measurement of the surface temperature of the rail 1 and cooling in the cooling bed after completion of the heat treatment, and furthermore straightening with a roller straightening machine, sampling and hardness measurement were also in the same conditions as in Example 1. The same manner 10 was also conducted in Comparative Example 2 where the condition of the conveyance distance Lo was different from that of the embodiment, for comparison with Example 2, and material properties of a rail 1 produced were evaluated.
The cooling conditions and the evaluation results of 15 material properties in Example 2 and Comparative Example 2 are represented in Table 5.
[0073] [Table 5]
Condition Component Dooling headei length Lh [m] Conveyance distance Lo [m] Total conveyance distance [m] Coolant Spray pressure [kPa] Variation in temperature after completion of heat treatment (Maximum - Minimum) [°C] Hardness at 1 mm depth position Hardness at 5 mm depth position
Average [Hvf Maximum [HV] Minimum [HV] Average [HV] Maximum [HV] Minimum [HV]
Example 2-1 D 2 2 4.0 Air 30 4 479 480 478 409 410 409
Example 2-2 E 1 1 4.0 Air 30 3 406 407 405 474 475 474
Example 2-3 F 4 4 4.0 Air 30 5 415 416 414 378 379 378
Example 2-4 G 2 8 8.0 Air 30 4 430 431 429 383 384 382
Comparative Example 2-1 D 4 1 8.0 Air 30 81 481 508 455 410 430 390
Comparative Example 2-2 G 2 1 8.0 Air 30 39 432 455 409 382 392 372
[0074]
The conveyance distance Lo was n times the cooling header length Lh in the conditions of Examples 2-1 to 2-4, and therefore the variation in temperature in the entire length was within 5°C and was smaller. As a result, it was confirmed that the variation in hardness was an HV of 2 or less at a depth position of 1 mm from the surface and an HV of 2 at a depth position of 5 mm therefrom in the conditions of Examples 2-1 to 2-4.
On the other hand, it was confirmed that the variation in temperature was not suppressed within 20°C or less, and the variation in hardness was as large as an HV of 40 or more at a depth position of 1 mm from the surface and as large as an HV of 20 or more at a depth position of 5 mm therefrom, in the conditions indicated in Comparative Example 2-1 to 2-2 where the oscillation distance Lo was shorter than the cooling header length Lh.
Reference Signs List [0075] rail head section web section foot section cooling apparatus
21a to 21c head section-cooling header foot section-cooling header
23a, 23b clamp
C:\Interwoven\NRPortbl\DCC\KZI I\l 7791059_ I .docx-2/l 0/2018
2016260101 02 Oct 2018
-4924 thermometer in apparatus conveyance section carrying-in table
4 discharge table exit side thermometer [0076]
The reference in this specification to any prior publication (or information derived from it), or to any matter which is known, is not, and should not be taken as an acknowledgment or admission or any form of suggestion that that prior publication (or information derived from it) or known 15 matter forms part of the common general knowledge in the field of endeavour to which this specification relates.
[0077]
Throughout this specification and the claims which follow, unless the context requires otherwise, the word comprise, and 20 variations such as comprises and comprising, will be understood to imply the inclusion of a stated integer or step or group of integers or steps but not the exclusion of any other integer or step or group of integers or steps.
C:\Interwoven\NRPortbl\DCC\KZI I\l 7624585_ 1 .docx-2/l 0/2018
2016260101 02 Oct 2018

Claims (5)

1. A method for producing a steel material, wherein when a cooling apparatus having a plurality of cooling headers disposed side by side in the longitudinal direction of a steel material cools the steel material hot worked or cooled/reheated, the steel material is conveyed at a conveyance distance Lo (m) satisfying Equation (1), in one direction along with the longitudinal direction of the steel material, in the cooling apparatus, wherein Lo is defined as conveyance distance (m) of steel material, m is defined as natural number, and Lh is defined as length (m) of cooling headers in longitudinal direction of steel material.
(m - 0.20) x Lh < Lo < (m + 0.20) x Lh ... (1)
2. The method for producing a steel material according to claim 1, wherein, in conveyance of the steel material, the steel material is conveyed with being oscillated in both directions of one direction and other direction along with the longitudinal direction of the steel material, and the amplitude of the oscillation is set to the conveyance distance Lo satisfying Equation (1).
3. The method for producing a steel material according to claim 1 or claim 2, wherein the steel material is a rail material.
4. An apparatus for cooling a steel material for cooling a steel material hot worked or cooled/reheated, comprising:
C:\Interwoven\NRPortbl\DCC\KZI I\l 7624585_ I .docx-2/| 0/2018
2016260101 02 Oct 2018 a plurality of cooling headers disposed side by side in the longitudinal direction of the steel material; and a conveyance section configured to convey the steel material at a conveyance distance Lo (m) satisfying Eguation (1), in one direction along with the longitudinal direction of the steel material in the cooling apparatus, during cooling of the steel material using the cooling headers, wherein Lo is defined as conveyance distance (m) of steel material, m is defined as natural number, and Lh is defined as length (m) of cooling headers in longitudinal direction of steel material.
(m - 0.20) x Lh < Lo < (m + 0.20) x Lh ... (1)
5. A steel material produced by hot working or cooling/reheating and thereafter cooling in a cooling apparatus having a plurality of cooling headers disposed side by side in a longitudinal direction, wherein, during cooling in the cooling apparatus, the steel material is produced with being conveyed at a conveyance distance Lo (m) satisfying Eguation (1), in one direction along with the longitudinal direction of the steel material in the cooling apparatus, wherein Lo is defined as conveyance distance (m) of steel material, m is defined as natural number, and Lh is defined as length (m) of cooling headers in longitudinal direction of steel material.
(m - 0.20) x Lh < Lo < (m + 0.20) x Lh ... (1)
FIG. 1
SECTION
1/4
FIG. 2
FIG. 3
2/4
FIG. 4A
FIG.4B V
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