AU2003293841A1 - Method for producing chlorine by oxidising hydrogen chlorine in a gaseous phase - Google Patents

Method for producing chlorine by oxidising hydrogen chlorine in a gaseous phase

Info

Publication number
AU2003293841A1
AU2003293841A1 AU2003293841A AU2003293841A AU2003293841A1 AU 2003293841 A1 AU2003293841 A1 AU 2003293841A1 AU 2003293841 A AU2003293841 A AU 2003293841A AU 2003293841 A AU2003293841 A AU 2003293841A AU 2003293841 A1 AU2003293841 A1 AU 2003293841A1
Authority
AU
Australia
Prior art keywords
chlorine
gaseous phase
reactor
producing
tubes
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2003293841A
Inventor
Martin Fiene
Klaus Harth
Gerhard Olbert
Eckhard Strofer
Christian Walsdorff
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of AU2003293841A1 publication Critical patent/AU2003293841A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/01—Chlorine; Hydrogen chloride
    • C01B7/03—Preparation from chlorides
    • C01B7/04—Preparation of chlorine from hydrogen chloride
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/01—Chlorine; Hydrogen chloride
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B01J2208/00221—Plates; Jackets; Cylinders comprising baffles for guiding the flow of the heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00823—Mixing elements
    • B01J2208/00831—Stationary elements
    • B01J2208/00849—Stationary elements outside the bed, e.g. baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/00038—Processes in parallel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)

Abstract

Preparation of chlorine involves passing hydrogen chloride and molecular oxygen in a reactor (1) having parallel catalyst tubes (2) charged with fixed-bed catalyst aligned in longitudinal direction of reactor; and alternatively arranged annular and disk-shaped deflection plates (6 and 7) which leave annular passage (9) free. A liquid heat transfer medium circulates between tubes.
AU2003293841A 2002-12-12 2003-12-11 Method for producing chlorine by oxidising hydrogen chlorine in a gaseous phase Abandoned AU2003293841A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10258180.0 2002-12-12
DE10258180A DE10258180A1 (en) 2002-12-12 2002-12-12 Preparation of chlorine involves oxidation of hydrogen chloride and gas stream comprising molecular oxygen in presence of fixed-bed catalyst is carried out in reactor having annular and disk-shaped deflection plates between catalyst tubes
PCT/EP2003/014075 WO2004052777A1 (en) 2002-12-12 2003-12-11 Method for producing chlorine by oxidising hydrogen chlorine in a gaseous phase

Publications (1)

Publication Number Publication Date
AU2003293841A1 true AU2003293841A1 (en) 2004-06-30

Family

ID=32336261

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2003293841A Abandoned AU2003293841A1 (en) 2002-12-12 2003-12-11 Method for producing chlorine by oxidising hydrogen chlorine in a gaseous phase

Country Status (12)

Country Link
US (1) US20040115119A1 (en)
EP (1) EP1581457B1 (en)
JP (1) JP4330537B2 (en)
KR (1) KR101057049B1 (en)
CN (1) CN1317182C (en)
AT (1) ATE502896T1 (en)
AU (1) AU2003293841A1 (en)
DE (2) DE10258180A1 (en)
ES (1) ES2362093T3 (en)
MX (1) MXPA05005935A (en)
PT (1) PT1581457E (en)
WO (1) WO2004052777A1 (en)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MXPA04010691A (en) * 2002-05-15 2005-03-31 Basf Ag Methods for producing chlorine from hydrogen chloride.
DE102005001952A1 (en) * 2005-01-14 2006-07-27 Man Dwe Gmbh Tube bundle reactor for carrying out exothermic or endothermic gas phase reactions
NL2000030C2 (en) * 2005-03-17 2007-06-14 Sasol Tech Pty Ltd Process for operating a fluidized bed reactor and fluidized bed reactor.
JP4341591B2 (en) * 2005-06-22 2009-10-07 住友化学株式会社 Chlorine production reactor and chlorine production method
DE102006024515A1 (en) * 2006-05-23 2007-11-29 Bayer Materialscience Ag Procedure for carrying out an optionally catalyst-supported hydrogen chloride oxidation process, comprises: cooling a process gas; separating non-reacted hydrogen chloride, drying product gases and separating chlorine from the mixture
US7897813B2 (en) * 2006-07-19 2011-03-01 Nippon Shokubai Co., Ltd. Reactor for gas phase catalytic oxidation and a process for producing acrylic acid using it
JP5171031B2 (en) * 2006-07-19 2013-03-27 株式会社日本触媒 Reactor for catalytic gas phase oxidation and method for producing acrylic acid using the same
DE102007024934B4 (en) * 2007-05-29 2010-04-29 Man Dwe Gmbh Tube bundle reactors with pressure fluid cooling
EP2237869B1 (en) * 2008-01-25 2011-08-31 Basf Se Reactor for carrying out high pressure reactions, method for starting and method for carrying out a reaction
JP5130155B2 (en) * 2008-08-28 2013-01-30 住友化学株式会社 Chlorine production method
CN102076411B (en) * 2008-09-30 2013-02-13 株式会社日本触媒 Catalyst for acrolein and/or acrylic acid production and process for producing acrolein and/or acrylic acid using the catalyst
WO2010038676A1 (en) * 2008-09-30 2010-04-08 株式会社日本触媒 Catalyst for acrylic acid production and process for producing acrylic acid using the catalyst
DE202011102549U1 (en) * 2011-06-29 2012-10-01 Boa Balg- Und Kompensatoren-Technologie Gmbh metal bellows
CN102784596B (en) * 2012-07-12 2014-12-17 天津大学 Shell side structure and shell and tube vinyl acetate synthesis reactor with same
US9440903B2 (en) * 2012-09-24 2016-09-13 Arkema Inc. Shell and tube oxidation reactor with improved resistance to fouling
WO2015018963A2 (en) * 2013-08-07 2015-02-12 Abengoa Hidrógeno, S. A. Multitube reformer for a hydrocarbon- and alcohol-reforming system and hydrocarbon- and alcohol-reforming system comprising same, and associated method
WO2017127681A1 (en) * 2016-01-22 2017-07-27 Fulton Group N.A., Inc. Tube configuration for a heat exchanger, heat exchanger including the tube configuration, fluid heating system including the same, and methods of manufacture thereof
CA3082520A1 (en) * 2017-12-20 2019-06-27 Nova Chemicals Corporation Corrosion resistant heat exchanger
CN111569790B (en) * 2020-05-22 2022-04-22 万华化学集团股份有限公司 Gas distributor for organosilicon fluidized bed and organosilicon fluidized bed reactor
CN114212233A (en) * 2021-10-29 2022-03-22 中国船舶重工集团公司第七一九研究所 Inter-board cooler and ship centralized cooling system
WO2023196946A2 (en) * 2022-04-08 2023-10-12 Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College Methods for oxidation of methane to methanol, systems for oxidation of methane to methanol, and devices for oxidation of methane to methanol
CN116899249B (en) * 2023-09-13 2024-01-02 山西诚宏福得一化工有限公司 Light benzene separation processing device and processing technology thereof

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BE793928A (en) * 1972-01-13 1973-05-02 Deggendorfer Werft Eisenbau APPARATUS FOR IMPLEMENTING EXOTHERMAL AND ENDOTHERMAL CHEMICAL PROCESSES
AU529228B2 (en) * 1977-07-13 1983-06-02 Nippon Shokubai Kagaku Kogyo Co. Ltd. Catalytic vapour phase oxidation
US4475588A (en) * 1981-09-28 1984-10-09 Mcquay Inc. Heat exchanger with tubes fixed at baffles
WO1987000081A1 (en) * 1985-06-27 1987-01-15 Stone & Webster Engineering Corporation Production of synthesis gas using convective reforming
US5615738A (en) * 1994-06-29 1997-04-01 Cecebe Technologies Inc. Internal bypass valve for a heat exchanger
US5480620A (en) * 1994-08-17 1996-01-02 Cameron; Gordon M. Catalytic converter
CN2210372Y (en) * 1994-12-08 1995-10-18 顾广瑞 Corrugated tube heat exchanger of rotational flow type
DE19505664C2 (en) * 1995-02-20 1996-12-12 Hoechst Ag Device and its use for oxychlorination
US5908607A (en) * 1996-08-08 1999-06-01 Sumitomo Chemical Co., Ltd. Process for producing chlorine
DE19748299A1 (en) * 1996-10-31 1998-05-07 Sumitomo Chemical Co Production of chlorine@
JP3559456B2 (en) * 1998-09-18 2004-09-02 株式会社日本触媒 Catalytic gas phase oxidation method and multitubular reactor
BR0007634A (en) * 1999-01-22 2001-12-18 Sumitomo Chemical Co Chlorine production process
US6167951B1 (en) * 1999-01-26 2001-01-02 Harold Thompson Couch Heat exchanger and method of purifying and detoxifying water
EP1080780B1 (en) * 1999-08-31 2007-08-01 Nippon Shokubai Co., Ltd. Reactor for catalytic gas phase oxidation
KR101513299B1 (en) * 2000-01-19 2015-04-17 스미또모 가가꾸 가부시끼가이샤 Method for producing chlorine
DE10134026A1 (en) * 2000-07-12 2002-01-24 Basf Ag Countercurrent reactor, for use in oxidative preparation of (meth)acrylic acid, comprising contact tube bundle and having system for improving flow of circulating heat exchange medium
JP3961254B2 (en) * 2001-09-28 2007-08-22 株式会社日本触媒 Multi-tube heat exchanger and method for producing (meth) acrylic acid using the heat exchanger

Also Published As

Publication number Publication date
ES2362093T3 (en) 2011-06-28
EP1581457A1 (en) 2005-10-05
MXPA05005935A (en) 2005-08-18
JP2006509706A (en) 2006-03-23
JP4330537B2 (en) 2009-09-16
CN1726164A (en) 2006-01-25
US20040115119A1 (en) 2004-06-17
ATE502896T1 (en) 2011-04-15
DE50313571D1 (en) 2011-05-05
DE10258180A1 (en) 2004-06-24
PT1581457E (en) 2011-04-29
KR101057049B1 (en) 2011-08-16
WO2004052777A1 (en) 2004-06-24
EP1581457B1 (en) 2011-03-23
CN1317182C (en) 2007-05-23
KR20050089821A (en) 2005-09-08

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Legal Events

Date Code Title Description
MK6 Application lapsed section 142(2)(f)/reg. 8.3(3) - pct applic. not entering national phase