AU2001278456A1 - Process for the preparation of nitroalkenes - Google Patents

Process for the preparation of nitroalkenes

Info

Publication number
AU2001278456A1
AU2001278456A1 AU2001278456A AU7845601A AU2001278456A1 AU 2001278456 A1 AU2001278456 A1 AU 2001278456A1 AU 2001278456 A AU2001278456 A AU 2001278456A AU 7845601 A AU7845601 A AU 7845601A AU 2001278456 A1 AU2001278456 A1 AU 2001278456A1
Authority
AU
Australia
Prior art keywords
nitroalkenes
preparation
alkenes
agent
nitration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2001278456A
Inventor
Aldo Belli
Maurizio Paiocchi
Francesco Ponzini
Marco Villa
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zambon Group SpA
Original Assignee
Zambon Group SpA
Zambon SpA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zambon Group SpA, Zambon SpA filed Critical Zambon Group SpA
Publication of AU2001278456A1 publication Critical patent/AU2001278456A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
    • C07D311/58—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/02—Systems containing two condensed rings the rings having only two atoms in common
    • C07C2602/14—All rings being cycloaliphatic
    • C07C2602/26—All rings being cycloaliphatic the ring system containing ten carbon atoms
    • C07C2602/28—Hydrogenated naphthalenes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pyrane Compounds (AREA)

Abstract

A process for the nitration of conjugated alkenes of formula (I) wherein R, R1, R2, R3 and R4 have the meanings reported in the description, which allows to obtain the corresponding beta-nitro-alkenes, characterised in that the nitrating agent is a mixture of an inorganic nitrite and iodine in the presence of an oxidising agent is described.
AU2001278456A 2000-06-28 2001-06-19 Process for the preparation of nitroalkenes Abandoned AU2001278456A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP00830453 2000-06-28
EP00830453 2000-06-28
PCT/EP2001/006902 WO2002000575A1 (en) 2000-06-28 2001-06-19 Process for the preparation of nitroalkenes

Publications (1)

Publication Number Publication Date
AU2001278456A1 true AU2001278456A1 (en) 2002-01-08

Family

ID=8175386

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2001278456A Abandoned AU2001278456A1 (en) 2000-06-28 2001-06-19 Process for the preparation of nitroalkenes

Country Status (12)

Country Link
US (2) US20040006248A1 (en)
EP (1) EP1294658B1 (en)
JP (1) JP4705307B2 (en)
CN (1) CN1232480C (en)
AT (1) ATE289986T1 (en)
AU (1) AU2001278456A1 (en)
CA (1) CA2412232C (en)
DE (1) DE60109163T2 (en)
DK (1) DK1294658T3 (en)
ES (1) ES2239155T3 (en)
PT (1) PT1294658E (en)
WO (1) WO2002000575A1 (en)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7776916B2 (en) 2004-04-28 2010-08-17 The Uab Research Foundation Nitrated lipids and methods of making and using thereof
EP2679224A1 (en) 2007-08-01 2014-01-01 University of Pittsburgh of the Commonwealth System of Higher Education Nitro oleic acid modulation of type II diabetes
ES2692291T3 (en) 2008-05-01 2018-12-03 Complexa Inc. Vinyl substituted fatty acids
US20140024713A1 (en) 2008-06-19 2014-01-23 University Of Utah Research Foundation Use of nitrated lipids for treatment of side effects of toxic medical therapies
US8686038B2 (en) 2008-06-19 2014-04-01 The Univsersity of Utah Research Foundation Use of nitrated lipids for treatment of side effects of toxic medical therapies
EP2459189A4 (en) 2009-07-31 2013-01-16 Univ Pittsburgh Fatty acids as anti-inflammatory agents
CA2781276A1 (en) 2009-10-02 2011-04-07 Complexa, Inc. Heteroatom containing substituted fatty acids
CN102574768B (en) * 2009-10-20 2015-07-08 安格斯化学公司 Process for nitroalkane recovery by aqueous phase recycle to nitration reactor
JP2013526865A (en) 2010-05-13 2013-06-27 ニトロメガ コーポレーション Nitro fatty acids, neuroprotection and / or suppression of cognitive decline
EP2744491B1 (en) 2011-08-19 2020-07-29 The University of Utah Research Foundation Combination therapy with nitrated lipids and inhibitors of the renin-angiotensin-aldosterone system
FR2985999B1 (en) 2012-01-23 2014-01-31 Arkema France PROCESS FOR THE PRODUCTION OF 2-OCTYL ACRYLATE BY TRANSESTERIFICATION
SI3865484T1 (en) 2015-07-07 2024-05-31 H. Lundbeck A/S Pde9 inhibitor with imidazo pyrazinone backbone for treatment of peripheral diseases
CN105152935A (en) * 2015-09-06 2015-12-16 安徽理工大学 Method for preparing beta-nitrostyrolene compound
BR112018006687A2 (en) 2015-10-02 2018-10-09 Complexa Inc disease prevention, treatment and reversal using therapeutically effective amounts of active fatty acids
CN106995373B (en) * 2017-05-17 2019-01-11 沅江华龙催化科技有限公司 Using ammonium iodide as nitro source one-pot synthesis α, β-unsaturation nitroolefin derivative method
CN107032939B (en) * 2017-05-17 2020-09-11 沅江华龙催化科技有限公司 Synthetic method of alpha, beta-unsaturated nitroolefin derivative
CN107098811B (en) * 2017-05-17 2019-03-26 沅江华龙催化科技有限公司 (E)-beta-nitrostyrene synthetic method
CN106995372B (en) * 2017-05-17 2018-12-18 沅江华龙催化科技有限公司 A method of (E)-beta-nitrostyrene derivative is catalyzed and synthesized based on tetaraary porphyrin iron
JP2021526134A (en) 2018-05-25 2021-09-30 イマラ インク． 6-[(3S, 4S) -4-methyl-l- (pyrimidine-2-ylmethyl) pyrrolidine-3-yl] -3-tetrahydropyran-4-yl-7H-imidazole [l, 5-A] pyrazine- 8-one monohydrate and crystalline form
CN109970701B (en) * 2019-04-02 2021-05-04 常州大学 By using I2O5/NaNO2Process for nitrating electron-rich aromatic compounds

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE9701438D0 (en) * 1997-04-17 1997-04-17 Astra Ab A new process

Also Published As

Publication number Publication date
EP1294658B1 (en) 2005-03-02
CN1438977A (en) 2003-08-27
JP4705307B2 (en) 2011-06-22
DK1294658T3 (en) 2005-06-27
US20060063953A1 (en) 2006-03-23
PT1294658E (en) 2005-07-29
CA2412232A1 (en) 2002-01-03
CA2412232C (en) 2010-03-30
US20040006248A1 (en) 2004-01-08
WO2002000575A1 (en) 2002-01-03
EP1294658A1 (en) 2003-03-26
JP2004501878A (en) 2004-01-22
DE60109163D1 (en) 2005-04-07
CN1232480C (en) 2005-12-21
ES2239155T3 (en) 2005-09-16
DE60109163T2 (en) 2006-04-13
ATE289986T1 (en) 2005-03-15
US7265251B2 (en) 2007-09-04

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