AU2001269120A1 - Method for the production of trioxime derivatives - Google Patents

Method for the production of trioxime derivatives

Info

Publication number
AU2001269120A1
AU2001269120A1 AU2001269120A AU6912001A AU2001269120A1 AU 2001269120 A1 AU2001269120 A1 AU 2001269120A1 AU 2001269120 A AU2001269120 A AU 2001269120A AU 6912001 A AU6912001 A AU 6912001A AU 2001269120 A1 AU2001269120 A1 AU 2001269120A1
Authority
AU
Australia
Prior art keywords
sup
formula
line
formulae
derivatives
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2001269120A
Inventor
Michael Henningsen
Matthias Kiefer
Andreas Kramer Dr
Jochen Schroder
Wolfgang Siegel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of AU2001269120A1 publication Critical patent/AU2001269120A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/06—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by nitrosation of hydrocarbons or substituted hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)

Abstract

The present invention relates to a process for preparing trioxime derivatives of the formula I in which the substituents R<SUP>1 </SUP>and R<SUP>2 </SUP>are identical or different and each is cyano, alkyl, haloalkyl or cycloalkyl, and R<SUP>3 </SUP>and R<SUP>4 </SUP>are identical or different and each is alkyl, haloalkyl, cycloalkyl, alkylcarbonyl or arylalkyl, by the following reaction steps in water without isolation of the intermediates: A) nitrosation of 1,3-diketones of the formula II to give monooximes of the formula III, B) oximation of III with hydroxylamine derivatives of the formula IV <?in-line-formulae description="In-line Formulae" end="lead"?>H<SUB>2</SUB>N-OR<SUP>3'</SUP> IV<?in-line-formulae description="In-line Formulae" end="tail"?> in which R<SUP>3'</SUP> is hydrogen or a group R<SUP>3 </SUP>to give bisoximes of the formula V, C) alkylation of V with alkylating agents or acylation of V with acylating agents to give compounds of the formula VI and D) subsequent oximation of VI with hydroxylamine to give compounds of the formula I.
AU2001269120A 2000-07-05 2001-07-04 Method for the production of trioxime derivatives Abandoned AU2001269120A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10032031 2000-07-05
DE10032031 2000-07-05
PCT/EP2001/007660 WO2002002514A1 (en) 2000-07-05 2001-07-04 Method for the production of trioxime derivatives

Publications (1)

Publication Number Publication Date
AU2001269120A1 true AU2001269120A1 (en) 2002-01-14

Family

ID=7647437

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2001269120A Abandoned AU2001269120A1 (en) 2000-07-05 2001-07-04 Method for the production of trioxime derivatives

Country Status (14)

Country Link
US (1) US6906223B2 (en)
EP (1) EP1296939B1 (en)
JP (1) JP4508526B2 (en)
KR (1) KR20030029608A (en)
CN (1) CN1215050C (en)
AT (1) ATE309203T1 (en)
AU (1) AU2001269120A1 (en)
BR (1) BR0112167B1 (en)
DE (1) DE50108012D1 (en)
DK (1) DK1296939T3 (en)
ES (1) ES2252250T3 (en)
HU (1) HUP0301141A3 (en)
IL (1) IL153414A0 (en)
WO (1) WO2002002514A1 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BRPI0617947A2 (en) * 2005-10-31 2011-08-09 Janssen Pharmaceutica Nv processes for the preparation of piperazinyl and diazapanyl benzamide derivatives
BRPI0618076A2 (en) * 2005-10-31 2011-08-16 Janssen Pharmaceutica Nv processes for the preparation of cyclopropyl amide derivatives
CN106137873A (en) * 2016-08-24 2016-11-23 祝家程 A kind of Fructus Fragariae Ananssae fragrance type hand sterilizer

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4435421A (en) * 1978-11-03 1984-03-06 Union Carbide Corporation Biocidal sulfur-containing bis-imino carbamate compounds
US4499097A (en) * 1983-03-10 1985-02-12 American Cyanamid Company 2-(Pyridyl)imidazolyl ketones
DE19539324A1 (en) * 1995-10-23 1997-04-24 Basf Ag Phenylacetic acid derivatives, processes and intermediates for their preparation and compositions containing them
WO1998016499A1 (en) * 1996-10-15 1998-04-23 Shionogi & Co., Ltd. Oxime derivatives, hydrazone derivatives, and use thereof
PL197555B1 (en) 1998-09-30 2008-04-30 Basf Ag Method for preparing trion-bis(oxime ether) derivatives andrion-mono and trion-bis(oxime ether) derivatives obtained therewith

Also Published As

Publication number Publication date
DE50108012D1 (en) 2005-12-15
BR0112167A (en) 2003-05-06
EP1296939B1 (en) 2005-11-09
US20030163002A1 (en) 2003-08-28
DK1296939T3 (en) 2006-01-30
CN1440384A (en) 2003-09-03
JP2004502671A (en) 2004-01-29
IL153414A0 (en) 2003-07-06
US6906223B2 (en) 2005-06-14
HUP0301141A3 (en) 2005-01-28
HUP0301141A2 (en) 2003-08-28
BR0112167B1 (en) 2012-03-20
KR20030029608A (en) 2003-04-14
JP4508526B2 (en) 2010-07-21
ES2252250T3 (en) 2006-05-16
ATE309203T1 (en) 2005-11-15
WO2002002514A1 (en) 2002-01-10
EP1296939A1 (en) 2003-04-02
CN1215050C (en) 2005-08-17

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