ATE64410T1 - METHOD OF PURIFICATION OF TETRAACETYLETHYLENE DIAMINE. - Google Patents
METHOD OF PURIFICATION OF TETRAACETYLETHYLENE DIAMINE.Info
- Publication number
- ATE64410T1 ATE64410T1 AT87103737T AT87103737T ATE64410T1 AT E64410 T1 ATE64410 T1 AT E64410T1 AT 87103737 T AT87103737 T AT 87103737T AT 87103737 T AT87103737 T AT 87103737T AT E64410 T1 ATE64410 T1 AT E64410T1
- Authority
- AT
- Austria
- Prior art keywords
- purification
- tetraacetylethylene diamine
- odourless
- tetraacetylethylenediamine
- taed
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/32—Amides; Substituted amides
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Crude tetraacetylethylenediamine (TAED), such as obtained in crystalline form during synthesis, is converted by successive washing with acetic acid and water and subsequent drying into a colourless and odourless form, such as is required for use in detergents and bleaching agents.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19863609735 DE3609735A1 (en) | 1986-03-22 | 1986-03-22 | METHOD FOR PURIFYING TETRAACETYLETHYLENE DIAMINE |
EP87103737A EP0238958B1 (en) | 1986-03-22 | 1987-03-14 | Method for the purification of tetraacetylethylenediamine |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE64410T1 true ATE64410T1 (en) | 1991-06-15 |
Family
ID=6297039
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT87103737T ATE64410T1 (en) | 1986-03-22 | 1987-03-14 | METHOD OF PURIFICATION OF TETRAACETYLETHYLENE DIAMINE. |
Country Status (5)
Country | Link |
---|---|
EP (1) | EP0238958B1 (en) |
AT (1) | ATE64410T1 (en) |
DE (2) | DE3609735A1 (en) |
ES (1) | ES2022182B3 (en) |
IE (1) | IE59879B1 (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT1245724B (en) * | 1990-11-09 | 1994-10-14 | Caffaro Spa Ind Chim | TAED PURIFICATION PROCEDURE |
CN103121960B (en) * | 2013-02-22 | 2015-04-01 | 浙江金科日化原料有限公司 | Efficient recrystallization method of tetraacetylethylenediamine |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3824286A (en) * | 1970-07-07 | 1974-07-16 | Lever Brothers Ltd | Preparation of polyacetylalkylene diamines |
DE2118281A1 (en) | 1971-04-15 | 1972-11-02 | Badische Anilin- & Soda-Fabrik Ag, 6700 Ludwigshafen | Process for the continuous production of N, N, N, N-tetraacetylethylenediamine |
DE2906606A1 (en) * | 1979-02-21 | 1980-09-04 | Hoechst Ag | Colourless tetra:acetyl-ethylene di:amine prepn. - by di:acetyl ethylene di:amine acetylation with acetic anhydride opt. with ketene addn. |
ES479375A1 (en) | 1978-04-14 | 1979-07-16 | Hoechst Ag | Process for preparing N,N,N',N'-tetra-acetylethylene diamine. |
DE2832021A1 (en) | 1978-07-21 | 1980-01-31 | Basf Ag | METHOD FOR PRODUCING TETRAACETYLAETHYLENEDIAMIN |
DE3011998C2 (en) | 1980-03-28 | 1982-06-16 | Henkel KGaA, 4000 Düsseldorf | Process for the production of a storage-stable, easily soluble granulate with a content of bleach activators |
DE3024694A1 (en) | 1980-06-30 | 1982-01-28 | Warwick Chemicals Ltd., Leeds | Tetra:acetyl ethylene di:amine prodn. from ethylene di:amine - by reaction with acetic acid and anhydride in several cycles, useful in detergent as perborate activator |
DE3042148A1 (en) * | 1980-11-08 | 1982-06-24 | Basf Ag, 6700 Ludwigshafen | METHOD FOR PRODUCING N, N, N ', N'-TETRAACETYLETHYLENE DIAMINE |
GB2096133B (en) | 1981-04-03 | 1985-04-24 | Croda Chemicals Ltd | Production of tetraacetylethylene diamine |
DE3127435A1 (en) * | 1981-07-11 | 1983-02-03 | Bayer Ag, 5090 Leverkusen | METHOD FOR PRODUCING PURIFIED TETRAACETYLETHYLENE DIAMINE (TAED) |
EP0079671A3 (en) | 1981-09-28 | 1984-03-21 | Albright & Wilson Limited | Process for preparing tetraacetyl alkylene diamines |
-
1986
- 1986-03-22 DE DE19863609735 patent/DE3609735A1/en not_active Withdrawn
-
1987
- 1987-03-14 DE DE8787103737T patent/DE3770666D1/en not_active Revoked
- 1987-03-14 AT AT87103737T patent/ATE64410T1/en not_active IP Right Cessation
- 1987-03-14 ES ES87103737T patent/ES2022182B3/en not_active Expired - Lifetime
- 1987-03-14 EP EP87103737A patent/EP0238958B1/en not_active Revoked
- 1987-03-20 IE IE73487A patent/IE59879B1/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
IE870734L (en) | 1987-09-22 |
DE3770666D1 (en) | 1991-07-18 |
DE3609735A1 (en) | 1987-09-24 |
EP0238958A3 (en) | 1988-08-17 |
EP0238958B1 (en) | 1991-06-12 |
IE59879B1 (en) | 1994-04-20 |
EP0238958A2 (en) | 1987-09-30 |
ES2022182B3 (en) | 1991-12-01 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
REN | Ceased due to non-payment of the annual fee | ||
RZN | Patent revoked |