ATE149152T1 - Hydrierung von meta-tolvendiamin - Google Patents
Hydrierung von meta-tolvendiaminInfo
- Publication number
- ATE149152T1 ATE149152T1 AT94114878T AT94114878T ATE149152T1 AT E149152 T1 ATE149152 T1 AT E149152T1 AT 94114878 T AT94114878 T AT 94114878T AT 94114878 T AT94114878 T AT 94114878T AT E149152 T1 ATE149152 T1 AT E149152T1
- Authority
- AT
- Austria
- Prior art keywords
- hydrogenation
- meta
- catalyst
- tolvenediamine
- support
- Prior art date
Links
- 238000005984 hydrogenation reaction Methods 0.000 title abstract 4
- 239000003054 catalyst Substances 0.000 abstract 4
- 229910052703 rhodium Inorganic materials 0.000 abstract 2
- 239000010948 rhodium Substances 0.000 abstract 2
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 abstract 2
- 150000003333 secondary alcohols Chemical class 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- PZKPUGIOJKNRQZ-UHFFFAOYSA-N 1-methylcyclohexa-3,5-diene-1,3-diamine Chemical compound CC1(N)CC(N)=CC=C1 PZKPUGIOJKNRQZ-UHFFFAOYSA-N 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- UAEPNZWRGJTJPN-UHFFFAOYSA-N Methylcyclohexane Natural products CC1CCCCC1 UAEPNZWRGJTJPN-UHFFFAOYSA-N 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- GYNNXHKOJHMOHS-UHFFFAOYSA-N methyl-cycloheptane Natural products CC1CCCCCC1 GYNNXHKOJHMOHS-UHFFFAOYSA-N 0.000 abstract 1
- -1 methylcyclohexane diamine Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
- C07C209/70—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton by reduction of unsaturated amines
- C07C209/72—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton by reduction of unsaturated amines by reduction of six-membered aromatic rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/127,659 US5973207A (en) | 1993-09-27 | 1993-09-27 | Hydrogenation of meta-toluenediamine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE149152T1 true ATE149152T1 (de) | 1997-03-15 |
Family
ID=22431232
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT94114878T ATE149152T1 (de) | 1993-09-27 | 1994-09-21 | Hydrierung von meta-tolvendiamin |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US5973207A (de) |
| EP (1) | EP0645367B1 (de) |
| AT (1) | ATE149152T1 (de) |
| DE (1) | DE69401798T2 (de) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6429338B1 (en) * | 2002-01-17 | 2002-08-06 | Air Products And Chemicals, Inc. | Hydrogenation of single ring aromatic diamines |
| DE102004061608A1 (de) * | 2004-12-17 | 2006-07-06 | Basf Ag | Verfahren zur Herstellung von 1,2-Diamino-3-methylcyclohexan und/oder 1,2-Diamino-4-methylcyclohexan |
| CN104177262B (zh) * | 2014-07-15 | 2016-08-24 | 景县本源精化有限公司 | 脂环胺固化剂的制备方法 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA839281A (en) * | 1970-04-14 | E.I. Du Pont De Nemours And Company | Catalytic hydrogenation process utilizing ruthenium supported on calcium carbonate or a rare earth oxide | |
| CA892636A (en) * | 1972-02-08 | V. Norton Richard | Reduction of aromatic amines | |
| US2606928A (en) * | 1947-11-18 | 1952-08-12 | Du Pont | Preparation of amino alicyclic compounds |
| US2511028A (en) * | 1947-12-04 | 1950-06-13 | Du Pont | 4-[(para-aminophenyl) alkyl] cyclo-hexylamine |
| US2606924A (en) * | 1949-06-09 | 1952-08-12 | Du Pont | Bis (4-aminocyclohexyl)-methane |
| US2606925A (en) * | 1949-12-15 | 1952-08-12 | Du Pont | Ruthenium catalyzed hydrogenation process for obtaining aminocyclohexyl compounds |
| US3347917A (en) * | 1961-12-29 | 1967-10-17 | Du Pont | Process for the preparation of di (paraaminocyclohexyl) methane |
| US3155724A (en) * | 1961-12-29 | 1964-11-03 | Du Pont | Process for bringing stereoisomeric mixture of bis-(4-aminocyclohexane) methane close to the equilibrium concentration |
| US3450759A (en) * | 1965-09-07 | 1969-06-17 | Mobay Chemical Corp | Preparation of cycloaliphatic diamines free of 0-diamines |
| US3636108A (en) * | 1965-12-23 | 1972-01-18 | Du Pont | Catalytic hydrogenation of aromatic nitrogen containing compounds over alkali moderated ruthenium |
| US3445516A (en) * | 1966-01-28 | 1969-05-20 | Mobay Chemical Corp | Reduction of tolylene diamines |
| US3766272A (en) * | 1972-08-25 | 1973-10-16 | Du Pont | 4,4'-methylenedi(cyclohexylamine)isomerization over a supported catalyst |
| US3856862A (en) * | 1973-06-25 | 1974-12-24 | Upjohn Co | Process for hydrogenation of di(4-aminophenyl)methane with a rhodium catalyst |
| US3914307A (en) * | 1973-12-27 | 1975-10-21 | Universal Oil Prod Co | Hydrogenation of aromatic amines |
| US3959374A (en) * | 1974-05-30 | 1976-05-25 | Jefferson Chemical Company, Inc. | Process for the preparation of mixed isomeric methylene-bridged polycyclohexylpolyamines |
| CA1204785A (en) * | 1981-06-01 | 1986-05-20 | Gary F. Allen | Process for the catalytic hydrogenation of di (4- aminophenyl) methane |
| US4754070A (en) * | 1986-01-23 | 1988-06-28 | Air Products And Chemicals, Inc. | Hydrogenation of methylenedianiline to produce bis(para-aminocyclohexyl)methane |
| US4960941A (en) * | 1988-03-30 | 1990-10-02 | Air Products And Chemicals, Inc. | Hydrogenation of aromatic amines to produce their ring hydrogenated counterparts |
| US5026914A (en) * | 1989-04-11 | 1991-06-25 | Air Products And Chemicals, Inc. | Hydrogenation of aromatic amines using rhodium on titania or zirconia support |
| US5214212A (en) * | 1992-02-27 | 1993-05-25 | Olin Corporation | Promoters for hydrogenation of aromatic amines |
-
1993
- 1993-09-27 US US08/127,659 patent/US5973207A/en not_active Expired - Fee Related
-
1994
- 1994-09-21 DE DE69401798T patent/DE69401798T2/de not_active Expired - Fee Related
- 1994-09-21 EP EP94114878A patent/EP0645367B1/de not_active Expired - Lifetime
- 1994-09-21 AT AT94114878T patent/ATE149152T1/de not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| EP0645367B1 (de) | 1997-02-26 |
| US5973207A (en) | 1999-10-26 |
| EP0645367A1 (de) | 1995-03-29 |
| DE69401798T2 (de) | 1997-06-05 |
| DE69401798D1 (de) | 1997-04-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| UEP | Publication of translation of european patent specification | ||
| REN | Ceased due to non-payment of the annual fee |