ATE102446T1 - PROCESSES FOR REMOVAL OF BASIC MATERIALS FROM PLANT PRODUCTS. - Google Patents
PROCESSES FOR REMOVAL OF BASIC MATERIALS FROM PLANT PRODUCTS.Info
- Publication number
- ATE102446T1 ATE102446T1 AT87311430T AT87311430T ATE102446T1 AT E102446 T1 ATE102446 T1 AT E102446T1 AT 87311430 T AT87311430 T AT 87311430T AT 87311430 T AT87311430 T AT 87311430T AT E102446 T1 ATE102446 T1 AT E102446T1
- Authority
- AT
- Austria
- Prior art keywords
- tobacco
- nicotine
- solvent
- components
- plant products
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
Abstract
A process is provided for the selective removal of basic materials from plant products, in particular, for removing nicotine from tobacco without materially affecting the content of the other components of the tobacco. Tobacco is traversed with a solvent in the supercritical state or in the liquid state wherein nicotine and the other components dissolve in the solvent. The solvent is then passed through an acid-containing trap where the solvent is essentially freed of nicotine. The solvent, depleted of nicotine and enriched in the other components, is then recycled to the tobacco to reextract nicotine. In addition, the tobacco may be pretreated with a chemical base which does not substantially react withe the tobacco components under ambient conditions but rather is activated under the conditions of the extraction process. Pretreatment of the tobacco with a chemical base neutralizes nicotine salts and permits the extraction process to be carried out under milder conditions.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US94710286A | 1986-12-29 | 1986-12-29 | |
EP87311430A EP0280817B1 (en) | 1986-12-29 | 1987-12-24 | Process for the removal of basic materials from plant products |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE102446T1 true ATE102446T1 (en) | 1994-03-15 |
Family
ID=25485521
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT87311430T ATE102446T1 (en) | 1986-12-29 | 1987-12-24 | PROCESSES FOR REMOVAL OF BASIC MATERIALS FROM PLANT PRODUCTS. |
Country Status (9)
Country | Link |
---|---|
EP (1) | EP0280817B1 (en) |
JP (1) | JP2694253B2 (en) |
AT (1) | ATE102446T1 (en) |
AU (1) | AU612128B2 (en) |
BR (1) | BR8707110A (en) |
CA (1) | CA1317961C (en) |
DE (1) | DE3789300D1 (en) |
FI (1) | FI88453C (en) |
ZA (1) | ZA879384B (en) |
Families Citing this family (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5497792A (en) * | 1987-11-19 | 1996-03-12 | Philip Morris Incorporated | Process and apparatus for the semicontinuous extraction of nicotine from tobacco |
US5435325A (en) * | 1988-04-21 | 1995-07-25 | R. J. Reynolds Tobacco Company | Process for providing tobacco extracts using a solvent in a supercritical state |
US4967771A (en) * | 1988-12-07 | 1990-11-06 | R. J. Reynolds Tobacco Company | Process for extracting tobacco |
US5031644A (en) * | 1989-12-29 | 1991-07-16 | R. J. Reynolds Tobacco Company | Tobacco expansion process and product |
US5076293A (en) * | 1989-06-19 | 1991-12-31 | R. J. Reynolds Tobacco Company | Process and apparatus for the treatment of tobacco material |
US5025812A (en) * | 1989-08-10 | 1991-06-25 | R. J. Reynolds Tobacco Company | Tobacco processing |
DE4002784C1 (en) * | 1990-01-31 | 1991-04-18 | B.A.T. Cigarettenfabriken Gmbh, 2000 Hamburg, De | |
US5131414A (en) * | 1990-02-23 | 1992-07-21 | R. J. Reynolds Tobacco Company | Tobacco processing |
US5065775A (en) * | 1990-02-23 | 1991-11-19 | R. J. Reynolds Tobacco Company | Tobacco processing |
US5234008A (en) * | 1990-02-23 | 1993-08-10 | R. J. Reynolds Tobacco Company | Tobacco processing |
US5095923A (en) * | 1991-04-11 | 1992-03-17 | R. J. Reynolds Tobacco Company | Tobacco expansion process using 1,1,1,2-tetrafluoroethane |
DE19654945C2 (en) * | 1996-07-29 | 1998-05-20 | Mueller Extract Co Gmbh | Essentially nicotine-free tobacco flavor oil and process for its production |
DE19630619C2 (en) * | 1996-07-29 | 1998-07-09 | Mueller Extract Co Gmbh | Essentially nicotine-free tobacco flavor oil and process for its production |
AU2003261187B2 (en) * | 2002-07-18 | 2009-10-22 | Phasex Corporation | Reduction of constituents in tobacco |
CN100540104C (en) * | 2004-10-28 | 2009-09-16 | 日本烟草产业株式会社 | The device that from processed material, uses in the method for extracting composition and this method |
GB201003887D0 (en) | 2010-03-09 | 2010-05-12 | British American Tobacco Co | Methods for extracting and isolating constituents of cellulosic material |
US10405571B2 (en) | 2015-06-26 | 2019-09-10 | Altria Client Services Llc | Compositions and methods for producing tobacco plants and products having altered alkaloid levels |
GB201707761D0 (en) * | 2017-05-15 | 2017-06-28 | British American Tobacco Investments Ltd | Method of making a tobacco extract |
GB201707758D0 (en) | 2017-05-15 | 2017-06-28 | British American Tobacco Investments Ltd | Ground tobacco composition |
WO2019229704A1 (en) * | 2018-05-31 | 2019-12-05 | Radient Technologies Inc. | Process for reducing nicotine in tobacco biomass and tobacco composition |
CN113115976B (en) * | 2021-03-11 | 2022-07-19 | 浙江中烟工业有限责任公司 | Batch preparation method of nicotine salt and application of nicotine salt in electronic cigarette |
CN114868763A (en) * | 2022-05-13 | 2022-08-09 | 湖南省烟草公司郴州市公司 | Tobacco alkali-reducing agent and preparation method and application thereof |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR397021A (en) * | 1907-12-11 | 1909-04-27 | Tabacs Desintoxiques En Failli | Method and installation for the denicotinization of tobacco |
US2227863A (en) * | 1938-02-14 | 1941-01-07 | Kinetic Chemicals Inc | Extraction of tobacco with fluorochlorohydrocarbons |
DE1517273B2 (en) * | 1965-04-15 | 1976-06-24 | Eresta Warenhandelsgesellschaft mbH, 6052 Mühlheim | PROCESS FOR CONTINUOUS EXTRACTION OF NICOTINE FROM TOBACCO AND FOR THE OBTAINING PRE-CONCENTRATED NICOTINE SALT SOLUTIONS |
US4153063A (en) * | 1970-09-02 | 1979-05-08 | Studiengesellschaft Kohle Mbh | Process for the extraction of nicotine from tobacco |
US4215706A (en) * | 1978-10-13 | 1980-08-05 | Loew's Theatres, Inc. | Nicotine transfer process |
US5497792A (en) * | 1987-11-19 | 1996-03-12 | Philip Morris Incorporated | Process and apparatus for the semicontinuous extraction of nicotine from tobacco |
-
1987
- 1987-12-14 ZA ZA879384A patent/ZA879384B/en unknown
- 1987-12-22 FI FI875673A patent/FI88453C/en not_active IP Right Cessation
- 1987-12-23 CA CA000555304A patent/CA1317961C/en not_active Expired - Fee Related
- 1987-12-24 EP EP87311430A patent/EP0280817B1/en not_active Revoked
- 1987-12-24 AT AT87311430T patent/ATE102446T1/en not_active IP Right Cessation
- 1987-12-24 DE DE87311430T patent/DE3789300D1/en not_active Expired - Lifetime
- 1987-12-28 JP JP62336696A patent/JP2694253B2/en not_active Expired - Fee Related
- 1987-12-29 AU AU83109/87A patent/AU612128B2/en not_active Ceased
- 1987-12-29 BR BR8707110A patent/BR8707110A/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
CA1317961C (en) | 1993-05-18 |
FI88453B (en) | 1993-02-15 |
BR8707110A (en) | 1988-08-02 |
FI875673A (en) | 1988-06-30 |
EP0280817B1 (en) | 1994-03-09 |
DE3789300D1 (en) | 1994-04-14 |
EP0280817A2 (en) | 1988-09-07 |
JP2694253B2 (en) | 1997-12-24 |
JPS63229102A (en) | 1988-09-26 |
EP0280817A3 (en) | 1990-05-16 |
FI875673A0 (en) | 1987-12-22 |
ZA879384B (en) | 1988-09-28 |
FI88453C (en) | 1993-05-25 |
AU8310987A (en) | 1988-06-30 |
AU612128B2 (en) | 1991-07-04 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |