AT70646B - Process for the preparation of alizarin. - Google Patents
Process for the preparation of alizarin.Info
- Publication number
- AT70646B AT70646B AT70646DA AT70646B AT 70646 B AT70646 B AT 70646B AT 70646D A AT70646D A AT 70646DA AT 70646 B AT70646 B AT 70646B
- Authority
- AT
- Austria
- Prior art keywords
- alizarin
- preparation
- parts
- desc
- nitroanthrone
- Prior art date
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
<Desc/Clms Page number 1>
Verfahren zur Darstellung von Alizarin.
EMI1.1
technischen Anthrazen aus über ein einfach darzustellendes Zwischenprodukt Alizarin herzustellen.
Die umständliche Darstellung und Reinigung von Anthrachinon und Anthrachinonsulfosäuren fällt fort. Es lassen sich natürlich mit Vorteil auch Gemische der ms-Nitrierungsprodukte verwenden. So ist z. B. das Gemisch von Dihydrodinitroanthrazen und Nitroanthron, das nach Meisenheimer (Annalen der Chemie 330. Seite 163) durch Einwirkung von überschüssiger Salpeter- säure auf in Eisessig suspendiertes Anthrazen erhalten wird. hervorragend zur Darstellung von
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Beispiel 11.
40 Teile Nitroanthron, 134 Teile kaustische Soda, 16#5 Teile Chilisalpeter, 32 Teile Kalk. G4 Teile Natriumbisulfitlauge, neutralisiert mit 28 Teilen Natronla@ge 35 Bé und 581 Teile Wasser
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**WARNUNG** Ende DESC Feld kannt Anfang CLMS uberlappen**.
<Desc / Clms Page number 1>
Process for the preparation of alizarin.
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to produce technical anthracene from alizarin, an intermediate that is easy to prepare.
The laborious preparation and purification of anthraquinone and anthraquinone sulfonic acids is no longer necessary. Mixtures of the ms nitration products can of course also be used with advantage. So is z. B. the mixture of dihydrodinitroanthracene and nitroanthrone, which according to Meisenheimer (Annalen der Chemie 330. page 163) is obtained by the action of excess nitric acid on anthracene suspended in glacial acetic acid. excellent for displaying
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Example 11.
40 parts nitroanthrone, 134 parts caustic soda, 16 # 5 parts chilli nitrate, 32 parts lime. G4 parts of sodium bisulfite liquor, neutralized with 28 parts of sodium hydroxide 35 Bé and 581 parts of water
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** WARNING ** End of DESC field may overlap beginning of CLMS **.
Claims (1)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE70646X | 1913-11-22 |
Publications (1)
Publication Number | Publication Date |
---|---|
AT70646B true AT70646B (en) | 1915-12-10 |
Family
ID=5635513
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT70646D AT70646B (en) | 1913-11-22 | 1914-10-08 | Process for the preparation of alizarin. |
Country Status (1)
Country | Link |
---|---|
AT (1) | AT70646B (en) |
-
1914
- 1914-10-08 AT AT70646D patent/AT70646B/en active
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