AT52843B - Process for the preparation of solid molecular compounds of hexamethylenetetramine with guaiacol. - Google Patents
Process for the preparation of solid molecular compounds of hexamethylenetetramine with guaiacol.Info
- Publication number
- AT52843B AT52843B AT52843DA AT52843B AT 52843 B AT52843 B AT 52843B AT 52843D A AT52843D A AT 52843DA AT 52843 B AT52843 B AT 52843B
- Authority
- AT
- Austria
- Prior art keywords
- guaiacol
- hexamethylenetetramine
- preparation
- molecular compounds
- solid molecular
- Prior art date
Links
- LHGVFZTZFXWLCP-UHFFFAOYSA-N guaiacol Chemical compound COC1=CC=CC=C1O LHGVFZTZFXWLCP-UHFFFAOYSA-N 0.000 title claims description 18
- VKYKSIONXSXAKP-UHFFFAOYSA-N hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 title claims description 14
- 229960001867 guaiacol Drugs 0.000 title claims description 9
- 235000010299 hexamethylene tetramine Nutrition 0.000 title claims description 7
- 239000004312 hexamethylene tetramine Substances 0.000 title claims description 7
- 150000001875 compounds Chemical class 0.000 title description 3
- 238000000034 method Methods 0.000 title description 2
- 238000002360 preparation method Methods 0.000 title description 2
- 239000007787 solid Substances 0.000 title description 2
- 239000002904 solvent Substances 0.000 claims 1
- AGGKEGLBGGJEBZ-UHFFFAOYSA-N tetramethylenedisulfotetramine Chemical compound C1N(S2(=O)=O)CN3S(=O)(=O)N1CN2C3 AGGKEGLBGGJEBZ-UHFFFAOYSA-N 0.000 claims 1
- 239000000203 mixture Substances 0.000 description 2
- -1 hexamethylene tetrazine Chemical compound 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Processes Of Treating Macromolecular Substances (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Aiming, Guidance, Guns With A Light Source, Armor, Camouflage, And Targets (AREA)
Description
<Desc/Clms Page number 1>
Verfahren zur Darstellung von festen Molekularverbindungen von Hexamethylentetramin mit Guajakol.
EMI1.1
gelingt überraschender Weise auch durch Zusammenmischen von trockenem Hexamethylentetramin mit trockenem Guajakol. Dass hiebei eine chemische Verbindung vor sich geht, ist daraus ersichtlich, dass zunächst eine Verflüssigung und erst nach einiger Zeit wieder Erstarrung zu der nun gebildeten Molekularverbindung eintritt.
Verreibt man z. B. in einer Reibschale 124 g Guajakol mit 70 g Hexamethylentetramin, so wird das Gemenge zunächst breiig, dann dickflüssig. Rührt man nun weiter oder
EMI1.2
nisse von Hexamethylentetramin und Guajakol natürlich ändera und bekommt dann die in dem Zusatzpatente erwähnten Gemische der drei möglichen Molekularverbindungen von Hexamethylentetramin und Guajakol. Erst wenn man mit einem Molekül Hexamethylen- tetrazin mehr als drei Moleküle Guajakol zusammen verreibt, erhält man eine Paste, die nicht mehr vollständig erstarrt.
**WARNUNG** Ende DESC Feld kannt Anfang CLMS uberlappen**.
<Desc / Clms Page number 1>
Process for the preparation of solid molecular compounds of hexamethylenetetramine with guaiacol.
EMI1.1
surprisingly also succeeds by mixing dry hexamethylenetetramine with dry guaiacol. That a chemical connection is taking place can be seen from the fact that initially liquefaction and only after some time re-solidification to the molecular connection that has now formed occurs.
If you rub z. B. in a mortar 124 g of guaiacol with 70 g of hexamethylenetetramine, the mixture is first mushy, then viscous. Keep stirring or
EMI1.2
Nisse of hexamethylenetetramine and guaiacol, of course, changes and then gets the mixtures of the three possible molecular compounds of hexamethylenetetramine and guaiacol mentioned in the additional patent. Only when more than three molecules of guaiacol is rubbed together with one molecule of hexamethylene tetrazine will you get a paste that no longer solidifies completely.
** WARNING ** End of DESC field may overlap beginning of CLMS **.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE45443X | 1908-10-05 | ||
| DE52843X | 1909-08-05 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AT52843B true AT52843B (en) | 1912-03-26 |
Family
ID=25749015
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT52843D AT52843B (en) | 1908-10-05 | 1910-04-29 | Process for the preparation of solid molecular compounds of hexamethylenetetramine with guaiacol. |
Country Status (1)
| Country | Link |
|---|---|
| AT (1) | AT52843B (en) |
-
1910
- 1910-04-29 AT AT52843D patent/AT52843B/en active
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