AT386611B - Hydrometallurgical process for separating out and enriching gold, platinum and palladium and obtaining selenium from the anode slurry from copper electrolysis and similar raw materials - Google Patents

Hydrometallurgical process for separating out and enriching gold, platinum and palladium and obtaining selenium from the anode slurry from copper electrolysis and similar raw materials

Info

Publication number
AT386611B
AT386611B AT290485A AT290485A AT386611B AT 386611 B AT386611 B AT 386611B AT 290485 A AT290485 A AT 290485A AT 290485 A AT290485 A AT 290485A AT 386611 B AT386611 B AT 386611B
Authority
AT
Austria
Prior art keywords
platinum
gold
precipitated
selenium
palladium
Prior art date
Application number
AT290485A
Other languages
German (de)
Other versions
ATA290485A (en
Inventor
Josef Ing Bertha
Joerg Dipl Ing Wallner
Helmut Dipl Ing Woerz
Original Assignee
Austria Metall
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Austria Metall filed Critical Austria Metall
Priority to AT290485A priority Critical patent/AT386611B/en
Publication of ATA290485A publication Critical patent/ATA290485A/en
Application granted granted Critical
Publication of AT386611B publication Critical patent/AT386611B/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B19/00Selenium; Tellurium; Compounds thereof
    • C01B19/02Elemental selenium or tellurium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B11/00Obtaining noble metals
    • C22B11/04Obtaining noble metals by wet processes
    • C22B11/042Recovery of noble metals from waste materials
    • C22B11/044Recovery of noble metals from waste materials from pyrometallurgical residues, e.g. from ashes, dross, flue dust, mud, skim, slag, sludge
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B11/00Obtaining noble metals
    • C22B11/06Chloridising
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B7/00Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
    • C22B7/006Wet processes
    • C22B7/007Wet processes by acid leaching
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

Hydrometallurgical process for separating out and enriching gold, platinum and palladium and obtaining selenium from the anode slurry of copper electrolyses and similar raw materials which, in addition to silver, may also contain lead, gold, platinum metals, Se, Te, Sb, As, Bi, Cu, Ni, Zn, Fe, sulphate, chloride, BaSO4, silica and the like, the filtrate which is obtained after the chlorination being mixed at room temperature with an excess of gaseous chlorine in order to completely convert the Se<IV> into Se<VI>, then the gold being precipitated at room temperature or low heat using suitable reducing agents, and, after a defined quantity of Se<IV> has been added, the platinum metals also being reductively precipitated out of this acidic solution, after which the precious metal cement which has been precipitated in this way is filtered out, while the selenium which is present in the cement filtrate as Se<VI> is converted into Se<IV> by heating in hydrochlorinic acid solution, is quantitatively precipitated as pure selenium by the addition of suitable reducing agents and is separated from the filtrate by filtration.
AT290485A 1985-10-08 1985-10-08 Hydrometallurgical process for separating out and enriching gold, platinum and palladium and obtaining selenium from the anode slurry from copper electrolysis and similar raw materials AT386611B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AT290485A AT386611B (en) 1985-10-08 1985-10-08 Hydrometallurgical process for separating out and enriching gold, platinum and palladium and obtaining selenium from the anode slurry from copper electrolysis and similar raw materials

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
AT290485A AT386611B (en) 1985-10-08 1985-10-08 Hydrometallurgical process for separating out and enriching gold, platinum and palladium and obtaining selenium from the anode slurry from copper electrolysis and similar raw materials

Publications (2)

Publication Number Publication Date
ATA290485A ATA290485A (en) 1988-02-15
AT386611B true AT386611B (en) 1988-09-26

Family

ID=3542163

Family Applications (1)

Application Number Title Priority Date Filing Date
AT290485A AT386611B (en) 1985-10-08 1985-10-08 Hydrometallurgical process for separating out and enriching gold, platinum and palladium and obtaining selenium from the anode slurry from copper electrolysis and similar raw materials

Country Status (1)

Country Link
AT (1) AT386611B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001083835A2 (en) * 2000-04-28 2001-11-08 Mintek Gold recovery process with hydrochloric acid lixiviant
CN107991207A (en) * 2017-11-29 2018-05-04 长春黄金研究院 Golden assay method in a kind of high impurity copper anode mud

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113092305A (en) * 2021-04-12 2021-07-09 北矿检测技术有限公司 Method for detecting gold content in coarse impure copper and application

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2558115B2 (en) * 1975-12-23 1977-10-20 Preussag Ag Metall, 3380 Goslar PROCESS FOR THE SIMULTANEOUS RECOVERY OF SELENIUM AND MERCURY

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2558115B2 (en) * 1975-12-23 1977-10-20 Preussag Ag Metall, 3380 Goslar PROCESS FOR THE SIMULTANEOUS RECOVERY OF SELENIUM AND MERCURY

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
GMELINS HANDBUCH DER ANORGANISCHEN CHEMIE, 8. AUFLAGE, SYSTEM NR.10 SELEN B, 1949, SEITEN 74 BIS 76 UND 96 BIS 103, INSBES.SEITE 75, ZEILEN 17-20 UND SEITE 97, ZEILEN 31-34 *
GMELINS HANDBUCH DER ANORGANISCHEN CHEMIE, 8. AUFLAGE, SYSTEM NR.10, SELEN TEIL A, 1953, SEITEN 76 UND 77, INSBES. SEITE 76, AB 4. ZEILE VON UNTEN. *
REMY, LEHRBUCH DER ANORGANISCHEN CHEMIE, 10. AUFLAGE, BND.1, 1960, AKADEM.VERLAGSGESELLSCHAFT, LEIPZIG, SEITE 880, INSBES.ZEILEN 27 BIS 34. *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001083835A2 (en) * 2000-04-28 2001-11-08 Mintek Gold recovery process with hydrochloric acid lixiviant
WO2001083835A3 (en) * 2000-04-28 2002-03-07 Mintek Gold recovery process with hydrochloric acid lixiviant
CN107991207A (en) * 2017-11-29 2018-05-04 长春黄金研究院 Golden assay method in a kind of high impurity copper anode mud

Also Published As

Publication number Publication date
ATA290485A (en) 1988-02-15

Similar Documents

Publication Publication Date Title
CN101434385B (en) Process for extracting tellurium from copper anode mud
CN101338368A (en) Method for preprocessing anode sludge and recovering dissipated metal
US4002544A (en) Hydrometallurgical process for the recovery of valuable components from the anode slime produced in the electrolytical refining of copper
CN103966456B (en) A kind of method from silver separating residue of copper anode slime comprehensively recovering valuable metal
CN103757421A (en) Method for extracting rare and precious metals from platinum-palladium mud
EP0263910B1 (en) Hydrometallurgical process for separating and concentrating gold, platinum and palladium, as well as recovering selenium from electrolytic copper refinery slimes and similar non-metallic materials
NO139096B (en) PROCEDURE FOR THE PREPARATION OF HIGH-RIGHT ELECTROLYTE COPPER BY REDUCTION ELECTROLYSIS
CN107779599A (en) A kind of preparation of new rare precious metal complex reducing agent and its application method
US4666514A (en) Hydrometallurgical process for recovering silver from copper-electrolysis anode sludge
US4366127A (en) Hydrometallurgical process for the recovery of lead, silver and gold, as well as zinc, from impure jarosite residues of an electrolytic zinc process
AT386611B (en) Hydrometallurgical process for separating out and enriching gold, platinum and palladium and obtaining selenium from the anode slurry from copper electrolysis and similar raw materials
US5939042A (en) Tellurium extraction from copper electrorefining slimes
Stanojević et al. Evaluation of cobalt from cobaltic waste products from the production of electrolytic zinc and cadmium
EP0266337B1 (en) Hydrometallurgical process for recovering silver from electrolytic copper refinery slimes and from similar raw materials
US2048563A (en) Recovery of selenium
CN110791667A (en) Process method for recycling bismuth from bismuth slag
JPH0781172B2 (en) Silver refining ore mud purification method
EP0089184A1 (en) Process for the recovery of silver from metallurgical intermediates
Lee et al. Recovery of silver and mercury from dental amalgam waste
US3615190A (en) Oxidation of lead blast furnance matte
WO2019154530A1 (en) Method for hydrometallurgical processing of a noble metal-tin alloy
RU2667927C1 (en) Method of producing of high purity copper
AU8190598A (en) Production of electrolytic copper from dilute solutions contaminated by other metals
IE50094B1 (en) Process for the treatment of solutions of lead chloride
RU2034063C1 (en) Method of silver purification

Legal Events

Date Code Title Description
ELJ Ceased due to non-payment of the annual fee