AR127007A1 - Una forma cristalina de metoxifenozida, un proceso para su preparación y uso de esta - Google Patents
Una forma cristalina de metoxifenozida, un proceso para su preparación y uso de estaInfo
- Publication number
- AR127007A1 AR127007A1 ARP220102430A ARP220102430A AR127007A1 AR 127007 A1 AR127007 A1 AR 127007A1 AR P220102430 A ARP220102430 A AR P220102430A AR P220102430 A ARP220102430 A AR P220102430A AR 127007 A1 AR127007 A1 AR 127007A1
- Authority
- AR
- Argentina
- Prior art keywords
- methoxyfenozide
- crystalline modification
- worm
- modification
- moth
- Prior art date
Links
- 239000005917 Methoxyfenozide Substances 0.000 title abstract 7
- QCAWEPFNJXQPAN-UHFFFAOYSA-N methoxyfenozide Chemical compound COC1=CC=CC(C(=O)NN(C(=O)C=2C=C(C)C=C(C)C=2)C(C)(C)C)=C1C QCAWEPFNJXQPAN-UHFFFAOYSA-N 0.000 title abstract 7
- 238000000034 method Methods 0.000 title abstract 2
- 230000004048 modification Effects 0.000 abstract 6
- 238000012986 modification Methods 0.000 abstract 6
- 241000607479 Yersinia pestis Species 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- 235000009434 Actinidia chinensis Nutrition 0.000 abstract 1
- 244000298697 Actinidia deliciosa Species 0.000 abstract 1
- 235000009436 Actinidia deliciosa Nutrition 0.000 abstract 1
- 244000144725 Amygdalus communis Species 0.000 abstract 1
- 235000011437 Amygdalus communis Nutrition 0.000 abstract 1
- 244000021317 Annona cherimola Species 0.000 abstract 1
- 235000002566 Capsicum Nutrition 0.000 abstract 1
- 241001414720 Cicadellidae Species 0.000 abstract 1
- 241001000394 Diaphania hyalinata Species 0.000 abstract 1
- 241000832202 Diaphania indica Species 0.000 abstract 1
- 241001012951 Diaphania nitidalis Species 0.000 abstract 1
- 240000001008 Dimocarpus longan Species 0.000 abstract 1
- 241001517923 Douglasiidae Species 0.000 abstract 1
- 235000000235 Euphoria longan Nutrition 0.000 abstract 1
- 235000007688 Lycopersicon esculentum Nutrition 0.000 abstract 1
- 241000208467 Macadamia Species 0.000 abstract 1
- 235000011430 Malus pumila Nutrition 0.000 abstract 1
- 244000070406 Malus silvestris Species 0.000 abstract 1
- 235000015103 Malus silvestris Nutrition 0.000 abstract 1
- 240000001307 Myosotis scorpioides Species 0.000 abstract 1
- 241001477931 Mythimna unipuncta Species 0.000 abstract 1
- 244000183278 Nephelium litchi Species 0.000 abstract 1
- 235000015742 Nephelium litchi Nutrition 0.000 abstract 1
- 241000346285 Ostrinia furnacalis Species 0.000 abstract 1
- 239000006002 Pepper Substances 0.000 abstract 1
- 244000025272 Persea americana Species 0.000 abstract 1
- 235000008673 Persea americana Nutrition 0.000 abstract 1
- 241000255969 Pieris brassicae Species 0.000 abstract 1
- 235000016761 Piper aduncum Nutrition 0.000 abstract 1
- 240000003889 Piper guineense Species 0.000 abstract 1
- 235000017804 Piper guineense Nutrition 0.000 abstract 1
- 235000008184 Piper nigrum Nutrition 0.000 abstract 1
- 235000014443 Pyrus communis Nutrition 0.000 abstract 1
- 240000001987 Pyrus communis Species 0.000 abstract 1
- 240000003768 Solanum lycopersicum Species 0.000 abstract 1
- 241000256011 Sphingidae Species 0.000 abstract 1
- 241000256247 Spodoptera exigua Species 0.000 abstract 1
- 241000256251 Spodoptera frugiperda Species 0.000 abstract 1
- 241000255901 Tortricidae Species 0.000 abstract 1
- 235000003095 Vaccinium corymbosum Nutrition 0.000 abstract 1
- 240000000851 Vaccinium corymbosum Species 0.000 abstract 1
- 235000017537 Vaccinium myrtillus Nutrition 0.000 abstract 1
- 235000020224 almond Nutrition 0.000 abstract 1
- 235000021014 blueberries Nutrition 0.000 abstract 1
- 235000012547 cherimoya Nutrition 0.000 abstract 1
- 235000020971 citrus fruits Nutrition 0.000 abstract 1
- 235000016213 coffee Nutrition 0.000 abstract 1
- 235000013353 coffee beverage Nutrition 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- 230000001376 precipitating effect Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C243/00—Compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
- C07C243/24—Hydrazines having nitrogen atoms of hydrazine groups acylated by carboxylic acids
- C07C243/38—Hydrazines having nitrogen atoms of hydrazine groups acylated by carboxylic acids with acylating carboxyl groups bound to carbon atoms of six-membered aromatic rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
- A01N37/38—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system
- A01N37/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system having at least one carboxylic group or a thio analogue, or a derivative thereof, and one oxygen or sulfur atom attached to the same aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01P—BIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
- A01P7/00—Arthropodicides
- A01P7/04—Insecticides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C241/00—Preparation of compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
- C07C241/04—Preparation of hydrazides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B2200/00—Indexing scheme relating to specific properties of organic compounds
- C07B2200/13—Crystalline forms, e.g. polymorphs
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Zoology (AREA)
- Engineering & Computer Science (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Insects & Arthropods (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Reivindicación 1: Modificación cristalina I de la N-tert-butil-N-(3,5-dimetilbenzoil)-3-metoxi-2-metilbenzohidrazida (metoxifenozida), que presenta al menos tres de las siguientes reflexiones, en cualquier combinación, como 2q ± 0.20 grados en un difractograma de rayos X en polvo (X-RPD) registrado usando radiación Cu-Ka a 25ºC: 2q = 9.47 ± 0.20 (1) 2q = 9.81 ± 0.20 (2) 2q = 12.63 ± 0.20 (3) 2q = 14.26 ± 0.20 (4) 2q = 16.49 ± 0.20 (5) 2q = 16.70 ± 0.20 (6) 2q = 18.01 ± 0.20 (7) 2q = 18.49 ± 0.20 (8) 2q = 19.65 ± 0.20 (9) 2q = 20.47 ± 0.20 (10) 2q = 21.44 ± 0.20 (11) 2q = 22.43 ± 0.20 (12) 2q = 23.55 ± 0.20 (13) 2q = 23.93 ± 0.20 (14) 2q = 25.41 ± 0.20 (15) 2q = 26.63 ± 0.20 (16). Reivindicación 7: Un proceso para la preparación de una modificación cristalina I de la metoxifenozida de acuerdo con una cualquiera de las reivindicaciones anteriores, que comprende las etapas de i) disolver la metoxifenozida en un sistema de disolvente que comprende uno o más disolventes; ii) precipitar el compuesto disuelto para obtener la modificación cristalina I de la metoxifenozida; y iii) aislar la modificación cristalina I precipitada. Reivindicación 21: El uso de la modificación cristalina I de la metoxifenozida de acuerdo con la reivindicación 20, donde la plaga se selecciona entre oruga militar, barreno, gusano cogollero, oruga de la col, oruga, barrenador del maíz, gusano gris, gusano de la mazorca, gusano bellotero, gusano cornudo, saltahojas, minador de la hoja, enrollador de la hoja, gusano medidor, gusano del melón, polilla, gusano del pepino y palomilla. Reivindicación 22: El uso de la modificación cristalina I de la metoxifenozida de acuerdo con cualquiera de las reivindicaciones 20 o 21, para el control de plagas en almendra, manzana, aguacate, arándanos, cítricos, café, chirimoya, vides, kiwi, longan, lichi, macadamia, pera, pimiento y tomate.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB2113267.5A GB2612942A (en) | 2021-09-16 | 2021-09-16 | A crystalline form of methoxyfenozide, a process for its preparation and use of the same |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR127007A1 true AR127007A1 (es) | 2023-12-06 |
Family
ID=85601885
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP220102430A AR127007A1 (es) | 2021-09-16 | 2022-09-08 | Una forma cristalina de metoxifenozida, un proceso para su preparación y uso de esta |
Country Status (4)
| Country | Link |
|---|---|
| AR (1) | AR127007A1 (es) |
| GB (1) | GB2612942A (es) |
| TW (1) | TW202328056A (es) |
| WO (1) | WO2023040759A1 (es) |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5530028A (en) * | 1992-11-23 | 1996-06-25 | Rohm And Haas Company | Insecticidal N'-substituted-N,N'-diacylhydrazines |
| DE69406227T2 (de) * | 1993-08-19 | 1998-04-30 | Rohm & Haas | Die Herstellung von 1,2-Diacyl-2-(t-alkyl)-Hydrazinen |
| WO2012121120A1 (ja) * | 2011-03-09 | 2012-09-13 | 住友化学株式会社 | 有害生物防除組成物及び有害生物の防除方法 |
| CN104803879A (zh) * | 2015-03-27 | 2015-07-29 | 江苏长青农化南通有限公司 | 甲氧虫酰肼的制备工艺 |
| CN106699596A (zh) * | 2016-12-30 | 2017-05-24 | 江苏永安化工有限公司 | 一种甲氧虫酰肼的制备工艺 |
| CN113248351B (zh) * | 2021-05-26 | 2022-10-11 | 绍兴上虞新银邦生化有限公司 | 6-氯-2-甲氧基甲苯的制备方法及甲氧虫酰肼的合成工艺 |
-
2021
- 2021-09-16 GB GB2113267.5A patent/GB2612942A/en active Pending
-
2022
- 2022-09-08 AR ARP220102430A patent/AR127007A1/es unknown
- 2022-09-09 WO PCT/CN2022/118027 patent/WO2023040759A1/en active Application Filing
- 2022-09-13 TW TW111134445A patent/TW202328056A/zh unknown
Also Published As
| Publication number | Publication date |
|---|---|
| WO2023040759A1 (en) | 2023-03-23 |
| GB2612942A (en) | 2023-05-24 |
| TW202328056A (zh) | 2023-07-16 |
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