AR075595A1 - TECNICA DE SEPARACION DE CROMATOGRAFIA LIQUIDA DE ALTO RENDIMIENTO MULTIDIMENSIONAL (STAR7) PARA DETERMINACIONES CUANTITATIVAS DE 7 FRACCIONES EN CORRIENTES DE HIDROCARBUROS PESADOS QUE EBULLEN A MAS DE 550s F ( 288s C) - Google Patents

TECNICA DE SEPARACION DE CROMATOGRAFIA LIQUIDA DE ALTO RENDIMIENTO MULTIDIMENSIONAL (STAR7) PARA DETERMINACIONES CUANTITATIVAS DE 7 FRACCIONES EN CORRIENTES DE HIDROCARBUROS PESADOS QUE EBULLEN A MAS DE 550s F ( 288s C)

Info

Publication number
AR075595A1
AR075595A1 ARP100100533A ARP100100533A AR075595A1 AR 075595 A1 AR075595 A1 AR 075595A1 AR P100100533 A ARP100100533 A AR P100100533A AR P100100533 A ARP100100533 A AR P100100533A AR 075595 A1 AR075595 A1 AR 075595A1
Authority
AR
Argentina
Prior art keywords
present application
fractions
liquid chromatography
star7
blow
Prior art date
Application number
ARP100100533A
Other languages
English (en)
Original Assignee
Exxonmobil Res & Eng Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Exxonmobil Res & Eng Co filed Critical Exxonmobil Res & Eng Co
Publication of AR075595A1 publication Critical patent/AR075595A1/es

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/96—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation using ion-exchange
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G01N30/46—Flow patterns using more than one column
    • G01N30/461—Flow patterns using more than one column with serial coupling of separation columns
    • G01N30/462—Flow patterns using more than one column with serial coupling of separation columns with different eluents or with eluents in different states
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G01N30/46—Flow patterns using more than one column
    • G01N30/468—Flow patterns using more than one column involving switching between different column configurations
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26—Oils; Viscous liquids; Paints; Inks
    • G01N33/28—Oils, i.e. hydrocarbon liquids
    • G01N33/2823—Raw oil, drilling fluid or polyphasic mixtures
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/84—Preparation of the fraction to be distributed
    • G01N2030/8447—Nebulising, aerosol formation or ionisation
    • G01N2030/847—Nebulising, aerosol formation or ionisation by pneumatic means
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/62—Detectors specially adapted therefor
    • G01N30/74—Optical detectors
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/21—Hydrocarbon

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Pathology (AREA)
  • Immunology (AREA)
  • General Physics & Mathematics (AREA)
  • General Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Medicinal Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Food Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

La presente solicitud provee la cuantificacion de siete clases de compuestos (saturados, aromáticos de 1-4+ anillos, sulfuros y polares) presentes en corrientes de hidrocarburos que bullen a 550-1050s F (288-565sC). La operacion de la presente solicitud en el modo preparatorio nos permitirá la carga y recoleccion de cantidades de material en términos de multimiligramos. En la presente solicitud, las siete fracciones son producidas en una sola ejecucion, mientras que las separaciones de cromatografía líquida preparatoria más comunmente utilizadas requieren dos o más separaciones de gran escala para generar fracciones similares. La presente solicitud utiliza 100 veces menos solvente. El protocolo de la presente solicitud proporciona una alternativa más rápida y más economica para las separaciones de cromatografía líquida preparatoria más comunmente utilizadas, y es lo suficientemente flexible para dirigirse a muchos problemas relacionados con la refinería y la química.
ARP100100533A 2009-02-24 2010-02-24 TECNICA DE SEPARACION DE CROMATOGRAFIA LIQUIDA DE ALTO RENDIMIENTO MULTIDIMENSIONAL (STAR7) PARA DETERMINACIONES CUANTITATIVAS DE 7 FRACCIONES EN CORRIENTES DE HIDROCARBUROS PESADOS QUE EBULLEN A MAS DE 550s F ( 288s C) AR075595A1 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US20845709P 2009-02-24 2009-02-24
US12/658,566 US8114678B2 (en) 2009-02-24 2010-02-05 Multi-dimensional high performance liquid chromatographic separation technique (STAR7) for quantitative determinations of 7 fractions in heavy petroleum streams boiling above 550 degrees F

Publications (1)

Publication Number Publication Date
AR075595A1 true AR075595A1 (es) 2011-04-20

Family

ID=42666412

Family Applications (1)

Application Number Title Priority Date Filing Date
ARP100100533A AR075595A1 (es) 2009-02-24 2010-02-24 TECNICA DE SEPARACION DE CROMATOGRAFIA LIQUIDA DE ALTO RENDIMIENTO MULTIDIMENSIONAL (STAR7) PARA DETERMINACIONES CUANTITATIVAS DE 7 FRACCIONES EN CORRIENTES DE HIDROCARBUROS PESADOS QUE EBULLEN A MAS DE 550s F ( 288s C)

Country Status (9)

Country Link
US (1) US8114678B2 (es)
EP (1) EP2401247B1 (es)
CN (1) CN102428059B (es)
AR (1) AR075595A1 (es)
AU (1) AU2010232960B2 (es)
CA (1) CA2753358C (es)
MY (1) MY152083A (es)
SG (1) SG173660A1 (es)
WO (1) WO2010114587A1 (es)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008150763A1 (en) * 2007-05-29 2008-12-11 Waters Investments Limited Apparatus and methods for multidimensional analysis
US9487723B2 (en) 2010-06-29 2016-11-08 Exxonmobil Research And Engineering Company High viscosity high quality group II lube base stocks
US8992764B2 (en) 2010-06-29 2015-03-31 Exxonmobil Research And Engineering Company Integrated hydrocracking and dewaxing of hydrocarbons
CN102382484A (zh) * 2010-08-31 2012-03-21 中国石油大学(北京) 一种多核芳烃光敏材料和由其制备的染料敏化太阳能电池
US20150106029A1 (en) * 2011-06-28 2015-04-16 Omer Refa Koseoglu Method of characterizing crude oil by high pressure liquid chromatography
US10684239B2 (en) 2011-02-22 2020-06-16 Saudi Arabian Oil Company Characterization of crude oil by NMR spectroscopy
US11022588B2 (en) 2011-02-22 2021-06-01 Saudi Arabian Oil Company Characterization of crude oil by simulated distillation
US10677718B2 (en) 2011-02-22 2020-06-09 Saudi Arabian Oil Company Characterization of crude oil by near infrared spectroscopy
US10571452B2 (en) * 2011-06-28 2020-02-25 Saudi Arabian Oil Company Characterization of crude oil by high pressure liquid chromatography
US10725013B2 (en) 2011-06-29 2020-07-28 Saudi Arabian Oil Company Characterization of crude oil by Fourier transform ion cyclotron resonance mass spectrometry
US8887557B2 (en) * 2011-09-01 2014-11-18 Exxonmobil Research And Engineering Company Fractionation of de-asphalted oil of vacuum resid using preparative high performance liquid chromatographic separations
US20140131257A1 (en) * 2012-11-12 2014-05-15 Exxonmobil Research And Engineering Company Preparatory high performance liquid chromatographic (hplc) separation technique for quantitative fractionation of heavy petroleum streams
US20140166542A1 (en) 2012-12-18 2014-06-19 Exxonmobil Research And Engineering Company Preparatory high performance liquid chromatographic (hplc) separation system and technique for quantitative fractionation of total vacuum resid
WO2014151460A1 (en) * 2013-03-15 2014-09-25 Florida State University Research Foundation, Inc. Determination of the distribution of reactive and non-reactive sulfur in petroleum and its fractions
WO2016112002A1 (en) 2015-01-05 2016-07-14 Saudi Arabian Oil Company Characterizatin of crude oil by ultraviolet visible spectroscopy
WO2016111997A1 (en) 2015-01-05 2016-07-14 Saudi Arabian Oil Company Relative valuation method for naphtha streams
WO2016111958A1 (en) 2015-01-05 2016-07-14 Saudi Arabian Oil Company Characterization of crude oil and its fractions by thermogravimetric analysis
CN107250770B (zh) 2015-01-05 2020-08-21 沙特阿拉伯石油公司 通过近红外光谱法表征原油
SG11201707966PA (en) 2015-06-30 2018-01-30 Exxonmobil Res & Eng Co Fuel production from fcc products
US10457877B2 (en) 2016-03-31 2019-10-29 Exxonmobil Research And Engineering Company Lubricant basestock production with enhanced aromatic saturation
US20180080915A1 (en) * 2016-09-19 2018-03-22 Exxonmobil Research And Engineering Company Methods for quantifying olefins in hydrocarbons
US20180187092A1 (en) 2016-12-29 2018-07-05 Exxonmobil Research And Engineering Company Block processing for base stock production from deasphalted oil
EP3396372B1 (en) * 2017-04-26 2020-04-08 Watrex Praha, s.r.o. Apparatus and method for recirculation of fluids including two 4-port 2-way-valves
SG11201910263YA (en) 2017-06-27 2020-01-30 Exxonmobil Res & Eng Co Fuel components from hydroprocessed deasphalted oils
WO2019231898A1 (en) 2018-06-01 2019-12-05 Exxonmobil Research And Engineering Company Boiling free fractionation of hydrocarbon steams utilizing a membrane cascade
CN110870985B (zh) * 2018-08-31 2021-12-17 中国石油化工股份有限公司 重油芳烃组分的分离、表征方法和二维液相色谱及装置
US11377605B2 (en) 2019-04-12 2022-07-05 ExxonMobil Technology and Engineering Company Molecular separations process
US11873451B2 (en) 2021-05-14 2024-01-16 ExxonMobil Technology and Engineering Company Products from FCC processing of high saturates and low heteroatom feeds
US11913332B2 (en) 2022-02-28 2024-02-27 Saudi Arabian Oil Company Method to prepare virtual assay using fourier transform infrared spectroscopy
US11781988B2 (en) 2022-02-28 2023-10-10 Saudi Arabian Oil Company Method to prepare virtual assay using fluorescence spectroscopy

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4430205A (en) * 1983-06-13 1984-02-07 Exxon Research And Engineering Company Method for the improvement of the oxidation resistance of hydrocarbon oil, especially transformer oils by the selective removal of pro-oxidant nitrogen and sulfur compounds therefrom
US4826603A (en) * 1986-09-09 1989-05-02 United States Of America As Represented By The Secretary Of The Air Force Hydrocarbon group-type analyzer system
US4851355A (en) * 1987-06-05 1989-07-25 Hayes Jr Paul C Hydrocarbon group-type analyzer system
CN2195758Y (zh) * 1994-03-22 1995-04-26 中国石油化工总公司石油化工科学研究院 高效液相色谱移动丝检测器双向进样装置
US6175409B1 (en) * 1999-04-02 2001-01-16 Symyx Technologies, Inc. Flow-injection analysis and variable-flow light-scattering methods and apparatus for characterizing polymers
DE60012934T2 (de) * 1999-02-26 2005-08-25 Martek Biosciences Corp. Verfahren zum Abtrennen von einem Docosahexaensäure enthaltenden Triglycerid aus einem Triglyceridgemisch
US6339182B1 (en) * 2000-06-20 2002-01-15 Chevron U.S.A. Inc. Separation of olefins from paraffins using ionic liquid solutions
US6849774B2 (en) * 2001-12-31 2005-02-01 Chevron U.S.A. Inc. Separation of dienes from olefins using ionic liquids
EP1938097A4 (en) * 2005-09-09 2009-12-09 Eksigent Technologies Llc SYSTEM WITH CHANGING FLOW SPEED FOR COLUMN CHROMATOGRAPHY
US7598487B2 (en) 2005-11-22 2009-10-06 Exxonmobil Research And Engineering Company Micro-hydrocarbon analysis

Also Published As

Publication number Publication date
CN102428059A (zh) 2012-04-25
US8114678B2 (en) 2012-02-14
AU2010232960B2 (en) 2016-01-07
CA2753358A1 (en) 2010-10-07
US20100218585A1 (en) 2010-09-02
EP2401247A4 (en) 2012-12-19
SG173660A1 (en) 2011-09-29
WO2010114587A1 (en) 2010-10-07
MY152083A (en) 2014-08-15
CN102428059B (zh) 2014-05-14
EP2401247A1 (en) 2012-01-04
AU2010232960A1 (en) 2011-09-15
CA2753358C (en) 2015-09-29
EP2401247B1 (en) 2018-04-25

Similar Documents

Publication Publication Date Title
AR075595A1 (es) TECNICA DE SEPARACION DE CROMATOGRAFIA LIQUIDA DE ALTO RENDIMIENTO MULTIDIMENSIONAL (STAR7) PARA DETERMINACIONES CUANTITATIVAS DE 7 FRACCIONES EN CORRIENTES DE HIDROCARBUROS PESADOS QUE EBULLEN A MAS DE 550s F ( 288s C)
Chen et al. Contamination by perfluoroalkyl substances and microbial community structure in Pearl River Delta sediments
Ma et al. Extraction of carbamate pesticides in fruit samples by graphene reinforced hollow fibre liquid microextraction followed by high performance liquid chromatographic detection
Xia et al. A novel method for profiling and quantifying short-and medium-chain chlorinated paraffins in environmental samples using comprehensive two-dimensional gas chromatography–electron capture negative ionization high-resolution time-of-flight mass spectrometry
BR0312830B1 (pt) processo contínuo para a separação de uma fração c4 por destilação extrativa com um solvente seletivo em uma coluna de destilação extrativa
Ilyas et al. Characterization of polychlorinated biphenyls and brominated flame retardants in surface soils from Surabaya, Indonesia
Focant et al. Measurement of PCDDs, PCDFs, and non-ortho-PCBs by comprehensive two-dimensional gas chromatography-isotope dilution time-of-flight mass spectrometry (GC× GC-IDTOFMS)
Springer et al. A simple and fast method for chlorsulfuron and metsulfuron methyl determination in water samples using multiwalled carbon nanotubes (MWCNTs) and capillary electrophoresis
BR9807521A (es)
Martínez et al. Development of a matrix solid-phase dispersion method for the screening of polybrominated diphenyl ethers and polychlorinated biphenyls in biota samples using gas chromatography with electron-capture detection
BRPI0700974A (pt) aparelho e método para separar um material misturado nos materiais constituintes e, sistema
Dong et al. Determination of type A trichothecenes in coix seed by magnetic solid-phase extraction based on magnetic multi-walled carbon nanotubes coupled with ultra-high performance liquid chromatography-tandem mass spectrometry
Rosati et al. Strain-dependent exciton diffusion in transition metal dichalcogenides
Antunes et al. Optimization of pressurized liquid extraction (PLE) of dioxin-furans and dioxin-like PCBs from environmental samples
Alharbi et al. Comparison of the effects of extraction techniques on mass spectrometry profiles of dissolved organic compounds in oil sand process-affected water
WO2006135426A3 (en) APPLICATION OF STATIC LIGHT TO A FLUID FLOW OF CNTs FOR PURPOSES OF SORTING THE CNTs
Regan et al. Development of comparative methods using gas chromatography–mass spectrometry and capillary electrophoresis for determination of endocrine disrupting chemicals in bio-solids
Poster et al. Three new mussel tissue standard reference materials (SRMs) for the determination of organic contaminants
Kishida et al. Effect of extraction temperature on pressurized liquid extraction of polychlorinated dibenzo-p-dioxins, polychlorinated dibenzofurans, and dioxin-like polychlorinated biphenyls from a sediment sample using polar and non-polar solvents
Parette et al. Response to the comment on ‘Halogenated indigo dyes: A likely source of 1, 3, 6, 8-tetrabromocarbazole and some other halogenated carbazoles in the environment’
WO2003107453A3 (de) Material für eine funktionsschicht eines organischen elektronikbauteils herstellungsverfahren und verwendung dazu
Hanai Analysis of the mechanism of retention on graphitic carbon by a computational chemical method
BAI et al. Seismic performance evaluation of reinforced concrete frame structures using the endurance time method
Dehghan Abkenar et al. Determination of organochlorine pesticides in river waters by GC-ECD after solid phase extraction, Mazandaran
Zhou et al. Separation and sensitive analysis of chlorophenols by MEEKC

Legal Events

Date Code Title Description
FA Abandonment or withdrawal