CN111058824B - Temporary plugging and shunting acidification method for strong heterogeneous sandstone reservoir through sieve tube - Google Patents

Temporary plugging and shunting acidification method for strong heterogeneous sandstone reservoir through sieve tube Download PDF

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CN111058824B
CN111058824B CN201911337544.6A CN201911337544A CN111058824B CN 111058824 B CN111058824 B CN 111058824B CN 201911337544 A CN201911337544 A CN 201911337544A CN 111058824 B CN111058824 B CN 111058824B
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acidizing
fluid
temporary plugging
well
sandstone reservoir
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CN111058824A (en
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刘平礼
刘义刚
杨寨
刘长龙
孟祥海
杜娟
邹剑
赵立强
陈祥
罗志锋
兰夕堂
李年银
高尚
张璐
张丽平
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China National Offshore Oil Corp CNOOC
CNOOC China Ltd Tianjin Branch
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China National Offshore Oil Corp CNOOC
CNOOC China Ltd Tianjin Branch
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    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B43/00Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
    • E21B43/25Methods for stimulating production
    • E21B43/26Methods for stimulating production by forming crevices or fractures
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/50Compositions for plastering borehole walls, i.e. compositions for temporary consolidation of borehole walls
    • C09K8/504Compositions based on water or polar solvents
    • C09K8/506Compositions based on water or polar solvents containing organic compounds
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/52Compositions for preventing, limiting or eliminating depositions, e.g. for cleaning
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/60Compositions for stimulating production by acting on the underground formation
    • C09K8/62Compositions for forming crevices or fractures
    • C09K8/72Eroding chemicals, e.g. acids
    • C09K8/74Eroding chemicals, e.g. acids combined with additives added for specific purposes
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B33/00Sealing or packing boreholes or wells
    • E21B33/10Sealing or packing boreholes or wells in the borehole
    • E21B33/13Methods or devices for cementing, for plugging holes, crevices or the like
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B43/00Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
    • E21B43/02Subsoil filtering
    • E21B43/08Screens or liners
    • E21B43/086Screens with preformed openings, e.g. slotted liners

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Abstract

The invention discloses a temporary plugging and shunting acidizing method for a strong heterogeneous sandstone reservoir through a sieve tube, which mainly comprises the steps of sequentially injecting an acidizing spacer fluid A, an acidizing fluid B, a temporary plugging agent C, an acidizing fluid B, a post fluid D and a displacement fluid E into a shaft, closing the shaft for a period of time, determining whether to perform flowback according to the type of the shaft, and then opening the shaft for production. Wherein, the acidification spacer fluid A consists of the following components: HCl, corrosion inhibitor, iron ion stabilizer, anti-swelling agent, demulsifier and the balance of water; the acidizing fluid B consists of the following components: HCl, HF or HBF 4 Corrosion inhibitor, iron ion stabilizer, anti-swelling agent, demulsifier, cleanup additive and the balance of water; the temporary plugging agent C consists of the following components: d-glucosamine, glacial acetic acid, pyridine-borane complex, acetone, methanol, HCl and the balance of water. The method has the advantages of simple construction process, low cost and high temporary plugging strength, and can achieve ideal temporary plugging and shunting effects in high-permeability extremely-poor and high-heterogeneity sandstone reservoirs.

Description

Temporary plugging and shunting acidification method for strong heterogeneous sandstone reservoir through sieve tube
Technical Field
The invention relates to the technical field of acidification production increase of oil exploitation reservoirs, in particular to a temporary plugging and shunting acidification method for a strong heterogeneous sandstone reservoir through a sieve tube.
Background
Sandstone oil and gas reservoirs are an important component of oil and gas resources in the world and account for about 57 percent of the conventional oil and gas resources in the world. During the well construction process, the filtration loss of drilling completion fluid causes certain pollution to a production well and an injection well, and the skin coefficient is positive, so that the production or injection is usually carried out after acidification in an oil field. In addition, most sandstone reservoirs are strong heterogeneity, the permeability of each well section is very poor, if acid liquor is directly injected, most acid liquor directly flows into a high permeable layer based on the principle of minimum flow resistance, and a low permeable layer is not effectively acidized and modified, so that the whole well section can be uniformly acidized by using a temporary plugging agent. For a sandstone reservoir with loose cementation, a sand control completion process is often adopted, the most common sand control process is screen pipe completion, for sand control, the diameter of holes on the wall of a screen pipe is dozens of micrometers to hundreds of micrometers, and if a conventional solid temporary plugging agent such as particles, fibers and the like is adopted, the solid temporary plugging agent is difficult to reach the reservoir through the screen pipe and acid liquor shunting cannot be realized, so the temporary plugging agent is required to be liquid firstly, and becomes jelly or solid in the reservoir after passing through the screen pipe, and the acid liquor shunting is realized temporarily. Aiming at the special temporary plugging agent, a special construction process is required, so that a sandstone reservoir screen pipe passing temporary plugging diversion acidification method is very necessary.
At present, documents related to reservoir screening pipe diversion acidification are few, and a self-steering diversion acidification method for a sandstone reservoir disclosed in patent CN201610513187.4 realizes temporary blocking diversion by means of the change of self viscosity of diversion acid, wherein the viscosity of the self-steering diversion acidification method is from dozens of millipascal seconds to hundreds of millipascal seconds, the temporary blocking strength is very limited, and the self-steering diversion acidification method is suitable for reservoirs with extremely low permeability differences. For strong heterogeneous reservoirs, because the permeability of the reservoir is very poor, if diverting acid is still used, the diverting effect is very unsatisfactory according to the field application condition, and the expected design target is difficult to achieve. Patent CN201910701577.8 discloses a diversion flow-splitting acidification method for a long well section of a hypertonic sandstone reservoir, which provides a profile control agent B and a phase-change plugging agent C, wherein jelly is formed by relying on the profile control agent B, and then a solid-phase particle plugging agent is formed by relying on the phase-change plugging agent C.
Based on the situation, the invention provides the temporary plugging and shunting acidification method for the strong heterogeneous sandstone reservoir through the sieve tube, and the method has the advantages of simple construction process and low cost.
Disclosure of Invention
The invention aims to provide a temporary plugging and shunting acidification method for a strong heterogeneous sandstone reservoir through a sieve tube, aiming at the defects of a reservoir sieve tube shunting acidification technology in the prior art.
The invention provides a temporary plugging and shunting acidification method for a strong heterogeneous sandstone reservoir through a sieve tube, which comprises the following specific steps of:
s1, injecting an acidizing spacer fluid A into the shaft, wherein the acidizing spacer fluid A comprises the following components in percentage by weight: 3-15% of HCl, 0.1-0.6% of corrosion inhibitor, 1-2% of iron ion stabilizer, 1-2% of anti-swelling agent, 0.1-0.6% of demulsifier and the balance of water. The acidizing isolation fluid A mainly has the functions of reacting with carbonate minerals in the sandstone reservoir and isolating formation fluid from the acidizing fluid B, so that secondary precipitation generated by the acidizing fluid B during formation treatment is reduced.
S2, injecting an acidizing fluid B into the well bore, wherein the acidizing fluid B comprises the following components in percentage by weight: 6-15% HCl, 1-3% HF or 4-8% HBF 4 0.5-1.2% of corrosion inhibitor, 1-2% of iron ion stabilizer, 1-2% of anti-swelling agent, 0.1-0.6% of demulsifier, 0.1-0.6% of cleanup additive and the balance of water. The acidizing fluid B mainly has the effects of reacting with a sandstone reservoir matrix and hydrochloric acid insoluble plugs and improving the permeability of the reservoir.
S3, injecting a temporary plugging agent C into the shaft, wherein the temporary plugging agent C comprises the following components in percentage by weight: 2.1% D-glucosamine, 0.7% glacial acetic acid, 1.7% pyridine-borane complex, 2.3% acetone, 8.2% methanol, 0.9% HCl, the balance water; wherein the D-glucosamine is D-glucosamine with randomly distributed N-acetyl on beta-1 to 4 chains. The temporary plugging agent C is liquid at first, can smoothly pass through a sieve tube with any size, and has good injectability. The temporary plugging agent C mainly has the effect that the temporary plugging agent C smoothly passes through the sieve tube firstly, flows into the area treated by the acid liquor in the previous step based on the principle of minimum flow resistance, and is changed from liquid sol into solid gel under the stimulation of pH and temperature to form a temporary plugging layer with higher plugging strength. And (3) injecting an acidizing fluid B next step, wherein the acidizing fluid B flows to a low-permeability area which is not treated before on the basis of the principle of minimum flow resistance due to the blocking of the temporary plugging agent C, so that acid liquor shunting is realized.
S4, injecting acidizing fluid B into the well bore again;
s5, injecting a post fluid D into the well bore, wherein the post fluid D comprises the following components in percentage by weight: 5-12% of HCl, 2-3% of a gel breaker, 0.1-0.6% of a corrosion inhibitor, 1-2% of an iron ion stabilizer, 1-2% of an anti-swelling agent, 1-2% of a cleanup additive and the balance of water. The post-fluid D is mainly used for driving the acidizing fluid B near the shaft into the deep part of a reservoir, so that secondary precipitation possibly generated in residual acid is prevented from depositing near the shaft, and in addition, the most important is to inject the gel breaker into the reservoir, so that the solid gel formed in the early stage is broken, and the gel is conveniently drained back.
And S6, injecting the displacement fluid E into the well bore. The displacement fluid E primarily functions to displace the post fluid D in the wellbore into the reservoir.
And S7, closing the well for a period of time, determining whether to flow back or not according to the well type within the range of 60-100min, and then opening the well for production. If the well is an injection well, flowback is not needed, and the well can be directly opened for water injection; if the well is a production well, the well needs to be drained again and then the well is opened for production.
Preferably, in the above method, the amount of the acidified isolation solution A is 0.5m 3 /m~1.2m 3 The dosage of the acidizing fluid B is 1.6m 3 /m~2.8m 3 The dosage of the temporary plugging agent C is 1-2 times of the pore volume of the designed plugging removal radius, and the dosage of the postposition liquid D is 0.6m 3 /m~1.2m 3 And m, the using amount of the displacement liquid E is 1.1-2.5 times of the volume of the oil pipe.
Preferably, during specific construction, if the amount of the acidizing fluid B is designed to be large, the amount is generally more than 60m 3 Repeating the steps S3-S4, wherein the amount of the temporary plugging agent C and the acidizing fluid B injected in a single time is 0.2-0.4 times of the volume of the designed dosage, and repeatedly and alternately injecting the temporary plugging agent C and the acidizing fluid B until the designed acidizing fluid B is injected. The alternate injection can improve the acidification effect to a certain extent, but if the designed amount of the acidification liquid B is small, the construction procedure is complicated if the alternate injection is carried out, and the acidification effect is not obviously improved. In addition, in order to simplify the construction process, steps S3 and S4 may not be repeated, which is not obvious, although it has an effect.
Preferably, the displacement fluid E is an aqueous solution of ammonium chloride or potassium chloride, and the mass percentage concentration of the ammonium chloride or the potassium chloride is 2%.
Preferably, the corrosion inhibitor is one of 4-methylpyridine, propiolic alcohol, butynol, cinnamaldehyde and alpha-alkenylbenzophenone. The iron ion stabilizer is one of nitrilotriacetic acid and sodium ethylene diamine tetracetate. The anti-swelling agent is one of cationic polyacrylamide and polyquaternium. The demulsifier is one of alkyl sodium sulfonate, polyoxyethylene polyoxypropylene octadecanol ether and polyoxyethylene polyoxypropylene polyether. The cleanup additive is one of alkyl aryl sulfonate and ethyl alkyl aldehyde oxide. The gel breaker is at least one of ammonium persulfate, sodium persulfate, potassium persulfate, sodium periodate and potassium periodate.
Compared with the prior art, the invention has the advantages that:
(1) compared with diverting acid, the temporary plugging agent has high temporary plugging strength and can achieve ideal temporary plugging and shunting effects in high-permeability extremely poor and high-heterogeneity sandstone reservoirs. The method has simple construction process and low cost.
(2) The temporary plugging agent with temperature and pH stimulation response provided by the invention can realize temporary plugging only by one construction procedure, and has the advantages of simple construction process and low cost.
(3) The temporary plugging agent provided by the invention is liquid at first, can smoothly pass through sieve pipes of any size, and has good injectivity.
Additional advantages, objects, and features of the invention will be set forth in part in the description which follows and in part will become apparent to those having ordinary skill in the art upon examination of the following or may be learned from practice of the invention.
Drawings
Fig. 1 is a flow chart of the temporary plugging and shunt acidizing method of the strong heterogeneous sandstone reservoir by using the sieve tube.
Detailed Description
The preferred embodiments of the present invention will be described in conjunction with the accompanying drawings, and it should be understood that they are presented herein only to illustrate and explain the present invention and not to limit the present invention.
The process flow of the temporary plugging and shunting acidizing method for the strong heterogeneous sandstone reservoir through the sieve tube is shown in figure 1.
Example 1
The X production well of a certain oil field of the Bohai sea is used as an acidification modification object, the modification scheme design is carried out by using the temporary plugging and shunting acidification method of the strong heterogeneous sandstone reservoir through the sieve tube, the target well section is 2438-2527 m, the porosity is 21%, the sand production of the reservoir is realized, the well completion is carried out by using the sieve tube, and the reservoir is completed by using the sieve tubeStrong heterogeneity, great permeability difference, and uneven liquid production section, the designed blockage removal radius is 1.5m, the casing size is 157mm, and the blockage removal radius pore volume is 83.1m 3 The inner diameter of the oil pipe is 62mm, and the volume of the oil pipe is 7.6m 3
Preparing an acidizing isolation fluid A, an acidizing fluid B, a temporary plugging agent C, a post fluid D and a displacement fluid E in advance before construction.
The dosage of the acidification isolation liquid A is 0.8m 3 A specific value of 71.2m 3 . The dosage of the acidizing fluid B is 2.1m 3 A value of/m, in particular 174.5m 3 . The dosage of the temporary plugging agent C is 1 time of the pore volume of the designed plugging removal radius, specifically 83.1m 3 . The dosage of the postposition liquid D is 0.9m 3 A specific value of 80.1m 3 . The dosage of the displacing liquid E is 1.5 times of the volume of the oil pipe, and is specifically 11.4m 3
Acidifying the spacer fluid A: 15% of HCl, 0.6% of corrosion inhibitor, 2% of iron ion stabilizer, 2% of anti-swelling agent, 0.6% of demulsifier and the balance of water. The corrosion inhibitor is 4-methylpyridine. The iron ion stabilizer is sodium ethylene diamine tetracetate. The anti-swelling agent is cationic polyacrylamide. The demulsifier is polyoxyethylene polyoxypropylene octadecanol ether.
Acidifying liquid B: 15% of HCl, 3% of HF, 1.2% of corrosion inhibitor, 2% of iron ion stabilizer, 2% of anti-swelling agent, 0.6% of demulsifier, 0.6% of cleanup additive and the balance of water. The corrosion inhibitor is 4-methylpyridine. The iron ion stabilizer is sodium ethylene diamine tetracetate. The anti-swelling agent is cationic polyacrylamide. The demulsifier is polyoxyethylene polyoxypropylene octadecanol ether. The cleanup additive is an ethyl alkyl aldehyde oxide.
Temporary plugging agent C: 2.1% D-glucosamine with randomly distributed N-acetyl groups on the beta-1 to 4 chains, 0.7% glacial acetic acid, 1.7% pyridine-borane complex, 2.3% acetone, 8.2% methanol, 0.9% HCl, the remainder being water.
Postliquid D: 8% of HCl, 3% of gel breaker, 0.4% of corrosion inhibitor, 1.8% of iron ion stabilizer, 1.8% of anti-swelling agent, 2% of cleanup additive and the balance of water. The gel breaker consists of 2 percent of ammonium persulfate and 1 percent of sodium persulfate. The corrosion inhibitor is 4-methylpyridine. The iron ion stabilizer is sodium ethylene diamine tetracetate. The anti-swelling agent is cationic polyacrylamide. The cleanup additive is an ethyl alkyl aldehyde oxide.
Displacing liquid E: 2% NH 4 Cl and the balance of water.
The percentage contents of the components are all mass percentages.
The specific construction method comprises the following steps:
step S1: injection 71.2m into the wellbore 3 Acidifying spacer fluid A.
Step S2: injecting 34.9m into the well bore 3 The acidified liquid B of (1).
Step S3: injecting 20.8m into the well bore 3 The temporary plugging agent C.
Step S4: injecting 34.9m into the well bore 3 The acidizing fluid B; and then alternately repeating the steps S3 and S4 until the designed acidizing fluid B is filled, repeating the step S3 for 4 times in total, and repeating the step S4 for 4 times in total.
Step S5: injecting 80.1m into the well bore 3 And (3) postliquid D.
Step S6: injecting 11.4m into the well bore 3 Displacing fluid E from the wellbore into the reservoir.
Step S7: and (4) closing the well for 80 minutes, performing flowback, and after flowback is finished, starting normal production of the X well.
Although the present invention has been described with reference to a preferred embodiment, it should be understood that various changes, substitutions and alterations can be made herein without departing from the spirit and scope of the invention as defined by the appended claims.

Claims (9)

1. A temporary plugging and shunting acidizing method for a strong heterogeneous sandstone reservoir through a sieve tube is characterized by comprising the following steps of:
s1, injecting an acidizing spacer fluid A into the shaft, wherein the acidizing spacer fluid A comprises the following components in percentage by weight: 3-15% of HCl, 0.1-0.6% of corrosion inhibitor, 1-2% of iron ion stabilizer, 1-2% of anti-swelling agent, 0.1-0.6% of demulsifier and the balance of water;
s2, injecting an acidizing fluid B into the well bore, wherein the acidizing fluid B comprises the following components in percentage by weight: 6-15% HCl, 1-3% HF or 4-8% HBF 4 0.5-1.2% of corrosion inhibitor, 1-2% of iron ion stabilizer, 1-2% of anti-swelling agent, 0.1-0.6% of demulsifier, 0.1-0.6% of cleanup additive and the balance of water;
s3, injecting a temporary plugging agent C into the shaft, wherein the temporary plugging agent C comprises the following components in percentage by weight: 2.1% D-glucosamine, 0.7% glacial acetic acid, 1.7% pyridine-borane complex, 2.3% acetone, 8.2% methanol, 0.9% HCl, the balance water; wherein D-glucosamine is D-glucosamine with randomly distributed N-acetyl groups on the beta-1 to 4 chains;
s4, injecting acidizing fluid B into the well bore again;
s5, injecting a post fluid D into the shaft, wherein the post fluid D comprises the following components in percentage by weight: 5-12% of HCl, 2-3% of a gel breaker, 0.1-0.6% of a corrosion inhibitor, 1-2% of an iron ion stabilizer, 1-2% of an anti-swelling agent, 1-2% of a cleanup additive and the balance of water;
s6, injecting displacement fluid E into the well bore;
and S7, closing the well for a period of time, determining whether to flow back according to the well type, and then opening the well for production.
2. The screen-passing temporary plugging and shunt acidizing method for the strong heterogeneous sandstone reservoir of claim 1, wherein in the step S7, the well closing time is 60-100min, and if the well is an injection well, the well can be directly opened for water injection without flowback; if the well is a production well, the well needs to be drained again and then the well is opened for production.
3. The temporary plugging and shunting acidizing method for the sieve tube of the strongly heterogeneous sandstone reservoir as claimed in claim 1, wherein the dosage of the acidizing spacer fluid A is 0.5-1.2 m 3 M, the dosage of the acidizing fluid B is 1.6-2.8 m 3 The dosage of the temporary plugging agent C is 1-2 times of the pore volume of the designed plugging removal radius, and the dosage of the postposition liquid D is0.6~1.2m 3 And m, the using amount of the displacement liquid E is 1.1-2.5 times of the volume of the oil pipe.
4. The method for temporary plugging and shunting acidizing of strongly heterogeneous sandstone reservoir through a sieve tube according to claim 3, wherein the amount of the acidizing fluid B is designed to be larger and larger than 60m 3 If the acidizing fluid B is injected into the shaft again in the step S4, the temporary plugging agent C and the acidizing fluid B are repeatedly and alternately injected by repeating the steps S3-S4 until the designed acidizing fluid B is completely injected.
5. The method for screen pipe plugging and shunt acidizing of a strongly heterogeneous sandstone reservoir of claim 1, wherein the displacement fluid E is an aqueous solution of ammonium chloride or potassium chloride, and the mass percent concentration of the ammonium chloride or potassium chloride is 2%.
6. The method for screen pipe plugging and flow acidizing of a strongly heterogeneous sandstone reservoir of claim 1, wherein the corrosion inhibitor is one of 4-methylpyridine, propiolic alcohol, butynol, cinnamaldehyde and alpha-alkenylbenzophenone.
7. The method for screen pipe plugging and shunt acidizing of a strongly heterogeneous sandstone reservoir of claim 1, wherein the iron ion stabilizer is one of nitrilotriacetic acid and sodium ethylene diamine tetracetate.
8. The method for screen-through temporary plugging and shunt acidizing of a strongly heterogeneous sandstone reservoir of claim 1, wherein the swelling prevention agent is one of cationic polyacrylamide and polyquaternium.
9. The screen-through temporary plugging and shunt acidizing method for the strongly heterogeneous sandstone reservoir of claim 1, wherein the demulsifier is one of sodium alkylsulfonate, polyoxyethylene polyoxypropylene stearyl ether and polyoxyethylene polyoxypropylene polyether.
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