CN102688166A - Preparation method of cosmetics-used petals - Google Patents
Preparation method of cosmetics-used petals Download PDFInfo
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- CN102688166A CN102688166A CN2012101724054A CN201210172405A CN102688166A CN 102688166 A CN102688166 A CN 102688166A CN 2012101724054 A CN2012101724054 A CN 2012101724054A CN 201210172405 A CN201210172405 A CN 201210172405A CN 102688166 A CN102688166 A CN 102688166A
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Abstract
The invention discloses a preparation method of cosmetics-used petals. The method comprises the following steps: firstly, selecting the petals one by one; removing receptacles, stalks, pistils/ stamens and calyces of the petals; stirring and washing the petals with deionized water repeatedly to remove dusts and part of worm eggs on the surfaces of the petals; getting the petals out, and adding the petals into deionized water and then heating to 90 - 100 degrees; keeping the temperature for 25 to 35 minutes so as to sterilize and disinfect the petals and eliminate the residue worn eggs; and then, placing the petals into aqueous solution of potassium hydroxide with percent concentration ranging from 0.1% to 0.3%, and stirring the solution for 3 to 5 minutes for decoloration; adding 0.3% - 0.5% aqueous solution of citric acid into the aqueous solution of potassium hydroxide, and stirring for 3 to 5 minutes; adjusting the pH value within 5 to 7; and finally, placing the obtained solution into 0.1% - 0.3% aqueous solution of preservative substance for preservation, so as to obtain the cosmetics-used petals. The method disclosed by the invention is simple and convenient, and is easy to operate and low in cost. As the petals prepared through the method are added into cosmetic products, the stability of the cosmetics can be improved, the shelf period of the products is prolonged, and moreover, the petals selves are not deformed, so that the active ingredients in the petals can be brought into the skin directly, and the environment-friendly and natural effects as well as the plant beauty care can be achieved actually.
Description
Technical field
The invention belongs to the Cosmetic Manufacture technical field, particularly a kind of manufacture method of used for cosmetic petal, prepared petal can large batch ofly be applied in the cosmetics, and the nutrient in the petal can directly be brought skin into, accomplishes environmental protection, and is natural, the plant skin care.
Background technology
In recent years, the natural cosmetics that has defying age, a Bearberry Extract is more and more received the trust of consumer.Active component in the natural cosmetics is mainly derived from plant, animal and microorganism, and wherein the application of active components of plants is the most extensive.It has been successfully applied to skin protection, whiten, the anti-ageing field of waiting for a long time.Compare with traditional cosmetics, active components of plants is a natural materials, and molecule is littler, more easily by skin absorbs, and can not produce deposition in vivo, and life-time service has no side effect.
From plant, extract natural active component and need pass through complicated leaching process; And in leaching process; A lot of active component run off easily or change, and especially the effective active composition in the plant petals has only fraction to remain after extracting through existing method for distilling; Cause the wasting of resources on the one hand, increased the manufacturing cost of cosmetics on the other hand.
One Chinese patent application 200710029662.1 discloses a kind of natural petals face-mask and preparation method thereof, directly with being added in the cosmetic mask after the crushing of dry flower petal.Dry petal directly adds the stability that can influence mask product without pre-treatments such as sterilizing decolourings, and the existence of microorganisms such as antibacterial wherein also causes anaphylaxis easily, has certain potential safety hazard.
One Chinese patent application 200810215274.7 discloses a kind of chemical article that contains petal composition and preparation method thereof, and wherein the processing method to petal is the dry flower petal to be invaded bubble with ethanol after with ultraviolet radiation, be added in the cosmetic product in 1-2 days.This method consumed time is long, and power consumption is big, and the petal of handling still can not satisfy stability and each item index of cosmetic product.
Summary of the invention
In view of the above-mentioned defective that exists in the prior art, the invention provides a kind of manufacture method of used for cosmetic petal, method is simple, and the time is short; Cost is low, and the petal that is prepared from through this method adds in the toiletries product, can improve the stability of cosmetics; Prolong the product shelf cycle, and petal itself is indeformable, the active component in the petal can directly be brought skin into; Really accomplish environmental protection, natural, the plant skin care.
The manufacture method of used for cosmetic petal is characterized in that may further comprise the steps:
1) the dry flower petal with water content 5-15% is a raw material, removes holder, anthocaulus, pistil, calyx;
2) added deionized water stirring and washing 3-5 minute repeatedly, remove surface dirt, pull petal out with filter screen;
3) petal that cleans up is put into container, add deionized water, be heated to the 90-100 degree, kept 25-35 minute, pull petal out with filter screen;
4) potassium hydroxide aqueous solution of putting into 0.1-0.3% stirs decolouring in 3-5 minute, pulls petal out with filter screen, and filter is done;
5) aqueous citric acid solution of putting into 0.3-05% stirred 3-5 minute, and the adjusting pH value is 5-7;
6) putting into mass percent concentration at last is that the aqueous preservative solution of 0.1-0.3% is preserved, and promptly makes the used for cosmetic petal.
Further, in the step 2, the weight ratio of petal and deionized water is 40:60.
In the step 3, the weight ratio of petal and deionized water is 40:60.
In the step 4, the weight ratio of petal and potassium hydroxide aqueous solution is 40:60.
In the step 5, the weight ratio of petal and aqueous citric acid solution is 40:60.
The said antiseptic of step 6 is preferably Methylisothiazolinone; The weight ratio of petal and aqueous preservative solution is 40:60.
The present invention is raw materials used should to be selected open and petal is all also stayed epiclinal dry flower petal, and first-selection is selected one by one, removes holder; Anthocaulus, pistil, calyx; With deionized water repeatedly stirring and washing remove the dust and the part worm's ovum of petal surface; Pull petal out and add deionized water and be heated to the 90-100 degree, constant temperature 25-35 minute sterilizing is also killed residual worm's ovum, and then petal being put into mass percent concentration is that the potassium hydroxide aqueous solution of 0.1-0.3% stirs and decoloured in 3-5 minute; Decolouring can increase the stability of petal, can not decolour or variable color for a long time after handling so again; If do not decolour processing, the time has been grown the petal color can be slowly thin out, and the petal color can be dissolved in the color of polluted product in the product itself.The aqueous citric acid solution of putting into 0.3-05% again stirred 3-5 minute, and the adjusting pH value is 5-7, and purpose is to make things convenient for petal in Cosmetic Manufacture, directly to add on the one hand to use; Cosmetics itself require a suitable pH value, and after handling like this, petal can directly add in the cosmetics; Be to help the antiseptic requirement of subsequent step on the other hand, in this pH value scope, antiseptic effect is best.Put into mass percent concentration at last and be the aqueous preservative solution of 0.1-0.3% and preserve, promptly make the used for cosmetic petal.Of the present invention method is simple, and the processing time is short, and the entire process process is about 50 minutes, and cost is low, and efficient is high.
Through selecting, petal after cleaning, disinfection, decolouring, pH regulator and the preservative treatment, can large batch ofly be applied in the cosmetics.Effective active component in the petal is farthest kept, and can directly bring skin into and be absorbed, and its looks improving and the skin nourishing effect is remarkable, has promoted product quality greatly; Simultaneously, because through handling, the petal that is added into impacts can for the stability of cosmetic product, prolonged the product shelf cycle, and petal itself is indeformable, has kept the original attitude of petal, stays good visual impression to consumer.
Method of the present invention is applicable to the petal of various kinds, can increase the selectivity of toiletries product plant petals additive greatly.
Cosmetics of the present invention are meant to smear, to spray or other similar approach; Intersperse among any position of human body surface; Like skin, hair, refer to toenail, lips and teeth etc.; To reach cleaning, maintenance, beauty treatment, modify and to change outward appearance, perhaps revise human scent, maintaining a good state is the chemical industrial product or the fine chemical product of purpose.
The specific embodiment
The manufacture method of embodiment 1 used for cosmetic Damascus Flos Rosae Rugosae petal
1) selecting whole openings, water content for use is the Damascus Flos Rosae Rugosae dry flower petal of 5-15%, removes holder, anthocaulus, pistil, calyx.
2) added deionized water stirring and washing 3-5 minute repeatedly, the weight ratio of petal and deionized water is 40:60, removes surface dirt, pulls petal out with filter screen.
3) petal that cleans up is put into container, add deionized water, the weight ratio of petal and deionized water is 40:60, is heated to the 90-100 degree, keeps 25 minutes, pulls petal out with filter screen.
4) potassium hydroxide aqueous solution of putting into 0.1% (mass percent) stirs decolouring in 3-5 minute, and the weight ratio of petal and potassium hydroxide aqueous solution is 40:60, pulls petal out with filter screen, and filter is done.
5) aqueous citric acid solution of putting into 0.4% (mass percent) stirred 3-5 minute, and regulating pH value is 6.
6) putting into mass percent concentration at last is that 0.1 antiseptic Methylisothiazolinone aqueous solution is preserved, and promptly makes the used for cosmetic petal.
Embodiment 2: the manufacture method of used for cosmetic Calendula officinalis petal
1) selecting whole openings, water content for use is the Calendula officinalis dry flower petal of 5-15%, removes holder, anthocaulus, pistil, calyx.
2) added deionized water stirring and washing 3-5 minute repeatedly, the weight ratio of petal and deionized water is 40:60, removes surface dirt, pulls petal out with filter screen.
3) petal that cleans up is put into container, add deionized water, the weight ratio of petal and deionized water is 40:60, is heated to the 90-100 degree, keeps 35 minutes, pulls petal out with filter screen.
4) potassium hydroxide aqueous solution of putting into 0.2% (mass percent) stirs decolouring in 3-5 minute, and the weight ratio of petal and potassium hydroxide aqueous solution is 40:60, pulls petal out with filter screen, and filter is done.
5) aqueous citric acid solution of putting into 0.3% (mass percent) stirred 3-5 minute, and regulating pH value is 5.9.
6) putting into mass percent concentration at last is that 0.2 antiseptic Methylisothiazolinone aqueous solution is preserved, and promptly makes the used for cosmetic petal.
Embodiment 3: the manufacture method of used for cosmetic Chimonanthus praecox (L.) Link. petal
1) selecting whole openings, water content for use is the Chimonanthus praecox (L.) Link. dry flower petal of 5-15%, removes holder, anthocaulus, pistil, calyx.
2) added deionized water stirring and washing 3-5 minute repeatedly, the weight ratio of petal and deionized water is 40:60, removes surface dirt, pulls petal out with filter screen.
3) petal that cleans up is put into container, add deionized water, the weight ratio of petal and deionized water is 40:60, is heated to the 90-100 degree, keeps 30 minutes, pulls petal out with filter screen.
4) potassium hydroxide aqueous solution of putting into 0.3% (mass percent) stirs decolouring in 3-5 minute, and the weight ratio of petal and potassium hydroxide aqueous solution is 40:60, pulls petal out with filter screen, and filter is done.
5) aqueous citric acid solution of putting into 0.5% (mass percent) stirred 3-5 minute, and regulating pH value is 6.0.
6) putting into mass percent concentration at last is that 0.3 antiseptic Methylisothiazolinone aqueous solution is preserved, and promptly makes the used for cosmetic petal.
Embodiment 4: the manufacture method of used for cosmetic Dianthus carryophyllus petal
1) selecting whole openings, water content for use is the Dianthus carryophyllus dry flower petal of 5-15%, removes holder, anthocaulus, pistil, calyx.
2) added deionized water stirring and washing 3-5 minute repeatedly, the weight ratio of petal and deionized water is 40:60, removes surface dirt, pulls petal out with filter screen.
3) petal that cleans up is put into container, add deionized water, the weight ratio of petal and deionized water is 40:60, is heated to the 90-100 degree, keeps 25 minutes, pulls petal out with filter screen.
4) potassium hydroxide aqueous solution of putting into 0.1% (mass percent) stirs decolouring in 3-5 minute, and the weight ratio of petal and potassium hydroxide aqueous solution is 40:60, pulls petal out with filter screen, and filter is done.
5) aqueous citric acid solution of putting into 0.5% (mass percent) stirred 3-5 minute, and regulating pH value is 6.2.
6) putting into mass percent concentration at last is that 0.2 antiseptic Methylisothiazolinone aqueous solution is preserved, and promptly makes the used for cosmetic petal.
Embodiment 5: the manufacture method of used for cosmetic Flos Moutan dry petal
1) selecting whole openings, water content for use is the Flos Moutan dry flower petal of 5-15%, removes holder, anthocaulus, pistil, calyx.
2) added deionized water stirring and washing 3-5 minute repeatedly, the weight ratio of petal and deionized water is 40:60, removes surface dirt, pulls petal out with filter screen.
3) petal that cleans up is put into container, add deionized water, the weight ratio of petal and deionized water is 40:60, is heated to the 90-100 degree, keeps 30 minutes, pulls petal out with filter screen.
4) potassium hydroxide aqueous solution of putting into 0.2% (mass percent) stirs decolouring in 3-5 minute, and the weight ratio of petal and potassium hydroxide aqueous solution is 40:60, pulls petal out with filter screen, and filter is done.
5) aqueous citric acid solution of putting into 0.4% (mass percent) stirred 3-5 minute, and regulating pH value is 5.9.
6) putting into mass percent concentration at last is that 0.3 antiseptic Methylisothiazolinone aqueous solution is preserved, and promptly makes the used for cosmetic petal.
All kinds of petal products of making through above-mentioned process for making can directly be applied in interpolation use in the cosmetic product.
Claims (7)
1. the manufacture method of used for cosmetic petal is characterized in that may further comprise the steps:
1) the dry flower petal with water content 5-15% is a raw material, removes holder, anthocaulus, pistil, calyx;
2) added deionized water stirring and washing 3-5 minute repeatedly, remove surface dirt, pull petal out with filter screen;
3) petal that cleans up is put into container, add deionized water, be heated to the 90-100 degree, kept 25-35 minute, pull petal out with filter screen;
4) potassium hydroxide aqueous solution of putting into 0.1-0.3% stirs decolouring in 3-5 minute, pulls petal out with filter screen, and filter is done;
5) aqueous citric acid solution of putting into 0.3-05% stirred 3-5 minute, and the adjusting pH value is 5-7; Pull petal out with filter screen;
6) putting into mass percent concentration at last is that the aqueous preservative solution of 0.1-0.3% is preserved, and promptly makes the used for cosmetic petal.
2. the manufacture method of used for cosmetic petal according to claim 1 is characterized in that in the step 2, the weight ratio of petal and deionized water is 40:60.
3. the manufacture method of used for cosmetic petal according to claim 1 is characterized in that in the step 3, the weight ratio of petal and deionized water is 40:60.
4. the manufacture method of used for cosmetic petal according to claim 1 is characterized in that in the step 4, the weight ratio of petal and potassium hydroxide aqueous solution is 40:60.
5. the manufacture method of used for cosmetic petal according to claim 1 is characterized in that in the step 5, the weight ratio of petal and aqueous citric acid solution is 40:60.
6. the manufacture method of used for cosmetic petal according to claim 1 is characterized in that the said antiseptic of step 6 is a Methylisothiazolinone.
7. like the manufacture method of the said used for cosmetic petal of claim 6, it is characterized in that in the step 6, the weight ratio of petal and aqueous preservative solution is 40:60.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101724054A CN102688166B (en) | 2012-05-30 | 2012-05-30 | Preparation method of cosmetics-used petals |
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| CN2012101724054A CN102688166B (en) | 2012-05-30 | 2012-05-30 | Preparation method of cosmetics-used petals |
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| CN102688166A true CN102688166A (en) | 2012-09-26 |
| CN102688166B CN102688166B (en) | 2013-06-12 |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102885030A (en) * | 2012-10-29 | 2013-01-23 | 广州栋方日化有限公司 | Method for maintaining stability of rose petals in faintly-acid or neutral cosmetic system |
| CN108498411A (en) * | 2018-06-28 | 2018-09-07 | 厦门柔丝丽生物科技有限公司 | A kind of petal shower cream and preparation method thereof |
| CN109820783A (en) * | 2019-03-22 | 2019-05-31 | 云南省农业科学院花卉研究所 | A kind of discoloration method of plant petals |
| CN110582267A (en) * | 2017-11-30 | 2019-12-17 | 拉菲克化妆品株式会社 | Method for preparing cosmetic composition containing natural plant and cosmetic composition prepared by the same |
| CN111053710A (en) * | 2020-02-14 | 2020-04-24 | 广州巴宝莉化妆品有限公司 | Film forming agent and application of petals protected by film forming agent in cosmetics |
| CN111904905A (en) * | 2020-08-04 | 2020-11-10 | 广东鑫美鑫化妆品有限公司 | A cosmetic lotion containing marigold petal and multiple plant extracts |
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| KR20070002718A (en) * | 2005-06-30 | 2007-01-05 | (주)아모레퍼시픽 | Cosmetic composition containing a softened natural petal |
| CN101336869A (en) * | 2007-08-09 | 2009-01-07 | 吴志刚 | Natural petals face-mask and preparation method thereof |
| CN101411679A (en) * | 2007-09-20 | 2009-04-22 | 吴志刚 | Chemical article containing petal composition and preparation method thereof |
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2012
- 2012-05-30 CN CN2012101724054A patent/CN102688166B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1660050A (en) * | 2004-12-20 | 2005-08-31 | 史敬辉 | Bathing by using peony and preparation method |
| KR20070002718A (en) * | 2005-06-30 | 2007-01-05 | (주)아모레퍼시픽 | Cosmetic composition containing a softened natural petal |
| CN101336869A (en) * | 2007-08-09 | 2009-01-07 | 吴志刚 | Natural petals face-mask and preparation method thereof |
| CN101411679A (en) * | 2007-09-20 | 2009-04-22 | 吴志刚 | Chemical article containing petal composition and preparation method thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102885030A (en) * | 2012-10-29 | 2013-01-23 | 广州栋方日化有限公司 | Method for maintaining stability of rose petals in faintly-acid or neutral cosmetic system |
| CN110582267A (en) * | 2017-11-30 | 2019-12-17 | 拉菲克化妆品株式会社 | Method for preparing cosmetic composition containing natural plant and cosmetic composition prepared by the same |
| CN108498411A (en) * | 2018-06-28 | 2018-09-07 | 厦门柔丝丽生物科技有限公司 | A kind of petal shower cream and preparation method thereof |
| CN109820783A (en) * | 2019-03-22 | 2019-05-31 | 云南省农业科学院花卉研究所 | A kind of discoloration method of plant petals |
| CN111053710A (en) * | 2020-02-14 | 2020-04-24 | 广州巴宝莉化妆品有限公司 | Film forming agent and application of petals protected by film forming agent in cosmetics |
| CN111904905A (en) * | 2020-08-04 | 2020-11-10 | 广东鑫美鑫化妆品有限公司 | A cosmetic lotion containing marigold petal and multiple plant extracts |
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| CN102688166B (en) | 2013-06-12 |
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Address after: Hangzhou City, Zhejiang province 310012 Xihu District World Trade Center Building 1, and Richland city (area D) room 1605 Applicant after: PROYA COSMETICS Co.,Ltd. Address before: 313023 No. 16, National Road, Huzhou Industrial Park, Zhejiang Province Applicant before: Proya (Huzhou) cosmetics Limited by Share Ltd. Address after: 313023 No. 16, National Road, Huzhou Industrial Park, Zhejiang Province Applicant after: Proya (Huzhou) cosmetics Limited by Share Ltd. Address before: 313023 No. 16, National Road, Huzhou Industrial Park, Zhejiang Province Applicant before: Proya (Huzhou) Cosmetic Co.,Ltd. |
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Free format text: CORRECT: APPLICANT; FROM: PROYA (HUZHOU) COSMETIC CO., LTD. TO: PROYA (HUZHOU) COSMETICS CO., LTD. Free format text: CORRECT: APPLICANT; FROM: PROYA (HUZHOU) COSMETICS CO., LTD. TO: PROYA COSMETICS CO., LTD. |
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