ZA975388B - Process for the preparation of crystalline microporous and mesoporous metal silicates, products obtainable by said process and their use. - Google Patents

Process for the preparation of crystalline microporous and mesoporous metal silicates, products obtainable by said process and their use.

Info

Publication number
ZA975388B
ZA975388B ZA9705388A ZA975388A ZA975388B ZA 975388 B ZA975388 B ZA 975388B ZA 9705388 A ZA9705388 A ZA 9705388A ZA 975388 A ZA975388 A ZA 975388A ZA 975388 B ZA975388 B ZA 975388B
Authority
ZA
South Africa
Prior art keywords
preparation
metal silicates
crystalline microporous
products obtainable
mesoporous metal
Prior art date
Application number
ZA9705388A
Inventor
Steffen Hasenzahl
Eckehart Roland
Georg Thiele
Helmut Mangold
Mario Scholz
Original Assignee
Degussa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Degussa filed Critical Degussa
Publication of ZA975388B publication Critical patent/ZA975388B/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00Catalysts comprising molecular sieves
    • B01J29/04Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/20Silicates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00Compounds having molecular sieve properties but not having base-exchange properties
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/005Silicates, i.e. so-called metallosilicalites or metallozeosilites
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/065Galloaluminosilicates; Group IVB- metalloaluminosilicates; Ferroaluminosilicates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/12Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the replacing atoms being at least boron atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D301/00Preparation of oxiranes
    • C07D301/02Synthesis of the oxirane ring
    • C07D301/03Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Catalysts (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Epoxy Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
ZA9705388A 1996-06-19 1997-06-18 Process for the preparation of crystalline microporous and mesoporous metal silicates, products obtainable by said process and their use. ZA975388B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19624340A DE19624340A1 (en) 1996-06-19 1996-06-19 Process for the preparation of crystalline micro- and mesoporous metal silicates, process-available products and their use

Publications (1)

Publication Number Publication Date
ZA975388B true ZA975388B (en) 1998-01-05

Family

ID=7797298

Family Applications (1)

Application Number Title Priority Date Filing Date
ZA9705388A ZA975388B (en) 1996-06-19 1997-06-18 Process for the preparation of crystalline microporous and mesoporous metal silicates, products obtainable by said process and their use.

Country Status (14)

Country Link
EP (1) EP0814058B1 (en)
JP (1) JP3166904B2 (en)
KR (1) KR100460363B1 (en)
CN (1) CN1094899C (en)
AR (1) AR013582A1 (en)
BR (1) BR9703631A (en)
DE (2) DE19624340A1 (en)
ES (1) ES2132984T3 (en)
ID (1) ID17360A (en)
IN (1) IN191885B (en)
MY (1) MY115092A (en)
SG (1) SG52988A1 (en)
TW (1) TW416866B (en)
ZA (1) ZA975388B (en)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0987220A1 (en) * 1998-09-17 2000-03-22 Technische Universiteit Delft Mesoporous amorphous silicate materials and process for the preparation thereof
DE19731627A1 (en) 1997-07-23 1999-01-28 Degussa Granules containing titanium silicalite-l
US6906208B2 (en) 1999-09-07 2005-06-14 Abb Lummus Global Inc. Mesoporous material and use thereof for the selective oxidation of organic compounds
US7608747B2 (en) 1999-09-07 2009-10-27 Lummus Technology Inc. Aromatics hydrogenolysis using novel mesoporous catalyst system
IT1314001B1 (en) * 1999-11-19 2002-12-03 Enichem Spa METHOD FOR REMOVING THE TEMPLANT FROM SYNTHETIC ZEOLITES
WO2004020335A1 (en) * 2002-08-28 2004-03-11 Albemarle Netherlands B.V. Process for the preparation of doped pentasil-type zeolites using a doped reactant
US6969692B2 (en) 2002-08-28 2005-11-29 Albemarle Netherlands B.V. Process for the preparation of doped pentasil-type zeolites using a doped reactant
DE102006017701A1 (en) 2006-04-15 2007-10-25 Degussa Gmbh Silicon-titanium mixed oxide powder, dispersion thereof and titanium-containing zeolite produced therefrom
DE102006017700A1 (en) 2006-04-15 2007-10-25 Degussa Gmbh Silicon-titanium mixed oxide containing dispersion for the production of titanium-containing zeolites
DE102007049742A1 (en) * 2007-10-16 2009-04-23 Evonik Degussa Gmbh Process for the preparation of a dispersion containing titanium-silicon mixed oxide
DE102007049743A1 (en) * 2007-10-16 2009-04-23 Evonik Degussa Gmbh Silicon-titanium mixed oxide powder, dispersion thereof and titanium-containing zeolite produced therefrom
CN101659417B (en) * 2008-08-28 2011-06-22 中国科学院合肥物质科学研究院 Porous silicate nanometer hollow granule and preparation method thereof
CZ304248B6 (en) * 2009-07-28 2014-01-29 Výzkumný ústav anorganické chemie, a. s. Process for preparing titanium silicate Ti-ZSM-5 with MFI structure
CZ302444B6 (en) * 2010-04-01 2011-05-18 Výzkumný ústav anorganické chemie, a.s. Process for preparing titanium silicate Ti-ZSM-5 from half-finished product
US9475041B2 (en) 2012-04-24 2016-10-25 Basf Se Zeolitic materials and methods for their preparation using alkenyltrialkylammonium compounds
KR20150008884A (en) * 2012-04-24 2015-01-23 바스프 에스이 Catalytically active body for the synthesis of dimethyl ether from synthesis gas
CN104379504B (en) * 2012-04-24 2016-10-12 巴斯夫欧洲公司 Zeolitic material and utilize the preparation method of thiazolinyl trialkylammonium compounds
CN106795126B (en) 2014-07-29 2018-10-26 赢创德固赛有限公司 The epoxidizing method of alkene
EP3056501A1 (en) 2015-02-13 2016-08-17 Evonik Degussa GmbH Titanium-containing aqueous solution and dispersion
US10125108B2 (en) 2015-04-28 2018-11-13 Evonik Degussa Gmbh Process for the epoxidation of propene
UA124030C2 (en) 2017-01-09 2021-07-07 Евонік Оперейшнс Гмбх Method for producing metal oxides by means of spray pyrolysis
EP3438101A1 (en) 2017-08-01 2019-02-06 Evonik Degussa GmbH Process for the epoxidation of propene
EP3495321A1 (en) 2017-12-07 2019-06-12 Evonik Degussa GmbH Preparation of powdery, porous crystalline metal silicates by means of flame spray pyrolysis
EP3628642A1 (en) 2018-09-25 2020-04-01 Evonik Operations GmbH Process for the manufacture of pulverulent, porous crystalline metal silicates employing flame spray pyrolysis

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3021580A1 (en) * 1980-06-07 1981-12-24 Basf Ag, 6700 Ludwigshafen METHOD FOR PRODUCING ZEOLITHES AND USE THEREOF AS CATALYSTS
DE3031557C2 (en) * 1980-08-21 1986-05-22 Basf Ag, 6700 Ludwigshafen Crystalline borosilicate zeolite ZBM-30 and process for its preparation
FR2582639B1 (en) * 1985-05-28 1987-08-28 Centre Nat Rech Scient NOVEL PROCESS FOR THE SYNTHESIS OF BOROSILICATE-TYPE ZEOLITES, PRODUCTS THUS OBTAINED AND THEIR USE
DE3880369T2 (en) * 1987-05-22 1993-08-05 Rhone Poulenc Chimie ZEOLITE WITH MFI STRUCTURE BASED ON SILICONE AND TITANIUM OXIDE AND METHOD FOR THE SYNTHESIS THEREOF.
IT1222022B (en) * 1987-07-14 1990-08-31 Montedipe Spa METHOD FOR THE PREPARATION OF A CATALYST FOR THE AMMOSSIMATION OF CARBONYL COMPOUNDS
IT1222868B (en) * 1987-10-12 1990-09-12 Montedipe Spa METHOD FOR THE PREPARATION OF TITANIUM SILICALITES
DE4138155A1 (en) * 1991-11-21 1993-05-27 Basf Ag METHOD FOR PRODUCING ESSENTIALLY ALKALIFIED TITANICILICATE CRYSTALS WITH ZEOLITE STRUCTURE
DE4419195A1 (en) * 1993-07-12 1995-01-19 Degussa Structured catalyst consisting of microporous oxides of silicon, aluminum and titanium
US5646314A (en) * 1994-11-16 1997-07-08 Arco Chemical Technology, L.P. Process for titanium silicalite-catalyzed epoxidation
US5599955A (en) * 1996-02-22 1997-02-04 Uop Process for producing propylene oxide

Also Published As

Publication number Publication date
ES2132984T3 (en) 1999-08-16
DE59700056D1 (en) 1999-02-04
TW416866B (en) 2001-01-01
JP3166904B2 (en) 2001-05-14
KR980001826A (en) 1998-03-30
MY115092A (en) 2003-03-31
EP0814058A1 (en) 1997-12-29
AR013582A1 (en) 2001-01-10
EP0814058B1 (en) 1998-12-23
KR100460363B1 (en) 2005-02-03
CN1168860A (en) 1997-12-31
CN1094899C (en) 2002-11-27
ID17360A (en) 1997-12-24
DE19624340A1 (en) 1998-01-08
BR9703631A (en) 1998-11-10
SG52988A1 (en) 1998-09-28
JPH1095610A (en) 1998-04-14
IN191885B (en) 2004-01-10

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