ZA924594B - Process for making 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane - Google Patents

Process for making 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane

Info

Publication number
ZA924594B
ZA924594B ZA924594A ZA924594A ZA924594B ZA 924594 B ZA924594 B ZA 924594B ZA 924594 A ZA924594 A ZA 924594A ZA 924594 A ZA924594 A ZA 924594A ZA 924594 B ZA924594 B ZA 924594B
Authority
ZA
South Africa
Prior art keywords
tetraazacyclooctane
tetranitro
making
Prior art date
Application number
ZA924594A
Inventor
William Lukasavage
Steven M Nicolich
Jack Akster
Original Assignee
Us Health
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Us Health filed Critical Us Health
Publication of ZA924594B publication Critical patent/ZA924594B/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D257/00—Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms
    • C07D257/02—Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms not condensed with other rings
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
ZA924594A 1991-10-15 1992-06-23 Process for making 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane ZA924594B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/775,402 US5124493A (en) 1991-10-15 1991-10-15 Process of producing XMX in 100% yield and purity

Publications (1)

Publication Number Publication Date
ZA924594B true ZA924594B (en) 1993-12-23

Family

ID=25104296

Family Applications (1)

Application Number Title Priority Date Filing Date
ZA924594A ZA924594B (en) 1991-10-15 1992-06-23 Process for making 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane

Country Status (6)

Country Link
US (1) US5124493A (en)
EP (1) EP0547735A1 (en)
JP (1) JPH0741466A (en)
AU (1) AU651468B2 (en)
IL (1) IL102220A0 (en)
ZA (1) ZA924594B (en)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7129348B1 (en) * 1988-12-21 2006-10-31 Alliant Techsystems Inc. Polycyclic, polyamides as precursors for energetic polycyclic polynitramine oxidizers
US5120887A (en) * 1991-10-15 1992-06-09 The United States Of America As Represented By The Secretary Of The Army Process of making pure SOLEX
US5739325A (en) * 1995-12-07 1998-04-14 Thiokol Corporation Hydrogenolysis of 2,4,6,8,10,12-Hexabenzyl-2,4,6,8,10,12-Hexaazatetracyclo 5.5.0.05,9.03,11 !dodecane
DE69737685T2 (en) * 1996-08-07 2008-01-10 Asahi Kasei Kabushiki Kaisha PROCESS FOR THE PREPARATION OF HEXANITROHEXAAZAWURTZITANEES
CA2275317A1 (en) * 1996-12-17 1998-06-25 H. Eugene Johnston Salting-out process of crystallizing 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo¬5.5.0.05,903,11|-dodecane
US6214988B1 (en) 1999-01-03 2001-04-10 Schlumberger Technology Corporation Process for making an HMX product
JP2002538160A (en) 1999-02-16 2002-11-12 アライアント・テクシステムズ・インコーポレーテッド Method for producing 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexazaazatetracyclo [5.5.0.05,9.03,11] -dodecane
US6201117B1 (en) 1999-05-26 2001-03-13 Schlumberger Technology Corporation Process for making a 1,3,5,7-tetraalkanoyl-1,3,5,7-tetraazacyclooctane
US6194571B1 (en) 1999-05-26 2001-02-27 Schlumberger Technology Corporation HMX compositions and processes for their preparation
US6265573B1 (en) 1999-05-26 2001-07-24 Schlumberger Technology Corporation Purification process
US6428724B1 (en) 1999-05-26 2002-08-06 Schlumberger Technology Corporation Granulation process
CN101863849B (en) * 2010-06-28 2012-06-27 北京理工大学 Method for simultaneously preparing octogen and hexogen
CN102826938B (en) * 2012-08-28 2014-12-10 西安近代化学研究所 Continuous aftertreatment technology for single-compound explosive HMX
CN106977469A (en) * 2017-04-13 2017-07-25 西南科技大学 A kind of synthetic method of deuterated HMX
GB2616849A (en) * 2022-03-21 2023-09-27 Bae Systems Plc Improved synthesis

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3415868A (en) * 1967-06-09 1968-12-10 Texaco Inc Nitration of hydrocarbon in the presence of trifluoroacetic acid
US3939148A (en) * 1974-02-25 1976-02-17 The United States Of America As Represented By The Secretary Of The Army Process for preparing 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane
US4432902A (en) * 1982-07-20 1984-02-21 The United States Of America As Represented By The Department Of Energy Method for synthesizing HMX
US4534895A (en) * 1983-09-22 1985-08-13 Rockwell International Corporation 1-Azidomethyl-3,5,7-trinitro-1,3,5,7-tetrazacyclooctane and synthesis thereof via azidation with acetyl azide
US4614800A (en) * 1985-02-15 1986-09-30 The United States Of America As Represented By The Secretary Of The Navy Synthesis of cyclic dinitramines useful as explosive and propellant ingredients, gas generants and in other ordnance applications
US4920859A (en) * 1986-08-01 1990-05-01 Eaton Corporaton Radial piston pump and motor
US5120887A (en) * 1991-10-15 1992-06-09 The United States Of America As Represented By The Secretary Of The Army Process of making pure SOLEX

Also Published As

Publication number Publication date
AU1931692A (en) 1993-04-22
AU651468B2 (en) 1994-07-21
JPH0741466A (en) 1995-02-10
IL102220A0 (en) 1993-05-13
EP0547735A1 (en) 1993-06-23
US5124493A (en) 1992-06-23

Similar Documents

Publication Publication Date Title
YU106789A (en) Process for obtaining 1,3-diole from epoxyde
ZA924594B (en) Process for making 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane
KR960004869B1 (en) Process for preparing 1,1,12-tetrafluoro-ethane
EP0445589A3 (en) Process for the preparation of 1,4-alkylenediamines
HU9200354D0 (en) Process for the production of 2-ethyl-4-/2'/-1h-1,2,3,4-tetrazole-5-yl/-biphenyl-4-yl/-metoxi/-kinoline-hydrocloride
AU1077992A (en) Process for preparing 1,3-dioxols
ZA938576B (en) Process for preparing 1,3-difluorobenzene
EP0481950A3 (en) 1,4-dideoxy-4-fluoronojirimycin
EP0482206A4 (en) 4,6-o-hydroxyphosphorylglucosamine derivative
GB9022413D0 (en) Process for preparing 1,1,1-trichloroethane
HUT64032A (en) New process for producing 9-amino-1,2,3,4-tetrahydroacrydine
PH31154A (en) Process for preparing 1-alkylryl-2-alkyl-5-formyl-imidazole.
YU46689A (en) Process for making 1,4-dihydro-pyridinic derivatives
EP0480465A3 (en) Process for preparing 5-aroyl-2,3-dihydro-1h-pyrrolizine-1,1,-dicarboxylates
EP0475272A3 (en) Process for the preparation of 2,3,5-trimethyl-p-benzoquinone
IL104477A0 (en) Process for preparing 4,6-dialkoxy-pyrimidines
EP0649408A4 (en) Process for making phenylthiomethylpyridinylalkenoates.
EP0538686A3 (en) Process for the preparation of 2,2,-bis-hydroxymethyl-butanediol-(1,4)
EP0500083A3 (en) Process for the preparation of 2,4-dichloro-5-fluorobenzonitrile
RO105801B1 (en) Ppreparation process for alhylcyclohexanols
HU206496B (en) Process for producing 2,3-dichloro-6-nitro-benzonitril
HU911706D0 (en) Process for producing 2,3-dichlorine-6-amino-benzol derivatives
CS259690A3 (en) Process for preparing 1,1,3-trimethyl-3-phenylindane
CS688090A3 (en) Process for preparing 1,2,3,-trichloro-4-nitrobenzene
HU208016B (en) Process for producing 15,20-anhydrovinblastin-borane-complex