YU792A - PROCESS FOR PURIFICATION OF CARBOXYLIC ACIDS - Google Patents
PROCESS FOR PURIFICATION OF CARBOXYLIC ACIDSInfo
- Publication number
- YU792A YU792A YU792A YU792A YU792A YU 792 A YU792 A YU 792A YU 792 A YU792 A YU 792A YU 792 A YU792 A YU 792A YU 792 A YU792 A YU 792A
- Authority
- YU
- Yugoslavia
- Prior art keywords
- carboxylic acids
- purification
- purified
- hydrogen peroxide
- acid
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
- C07C67/303—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by hydrogenation of unsaturated carbon-to-carbon bonds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
POSTUPAK ZA PREČIŠĆAVANJE KARBOKSILNIH KISELINA. Karboksilne kiseline koje su proizvedene karbonilovanjem i koje imaju jodidne i oksidujuće nečistoće prečišćavaju se kontaktiranjem sa vodonik-peroksidom i regenerisanjem prečišćene kiseline destilacijom ili isparavanjem. Poželjno se kao katalizator koristi neka takva jaka kiselina kao što je sumporna kiselina. Kontaminacija proizvoda sa sumporom iz sumporne kiseline i sa viškom vodonik-peroksida može se smanjiti korišćenjem metalnih soli u fazi regenerisanja.PROCESS FOR PURIFICATION OF CARBOXYLIC ACIDS. Carboxylic acids produced by carbonylation and having iodide and oxidizing impurities are purified by contacting with hydrogen peroxide and regeneration of the purified acid by distillation or evaporation. Preferably, a strong acid such as sulfuric acid is used as the catalyst. Contamination of products with sulfuric acid sulfur and excess hydrogen peroxide can be reduced by using metal salts in the regeneration phase.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB919100216A GB9100216D0 (en) | 1991-01-05 | 1991-01-05 | Process |
Publications (1)
Publication Number | Publication Date |
---|---|
YU792A true YU792A (en) | 1994-06-10 |
Family
ID=10688016
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
YU792A YU792A (en) | 1991-01-05 | 1992-01-06 | PROCESS FOR PURIFICATION OF CARBOXYLIC ACIDS |
Country Status (20)
Country | Link |
---|---|
US (1) | US5387713A (en) |
EP (1) | EP0494527B2 (en) |
JP (1) | JPH04308548A (en) |
KR (1) | KR100189787B1 (en) |
CN (1) | CN1031507C (en) |
AR (1) | AR247378A1 (en) |
AT (1) | ATE125247T1 (en) |
AU (1) | AU646536B2 (en) |
BR (1) | BR9200013A (en) |
CA (1) | CA2057638A1 (en) |
DE (2) | DE69111410D1 (en) |
FI (1) | FI920033A (en) |
GB (1) | GB9100216D0 (en) |
HU (1) | HU9200026D0 (en) |
MX (1) | MX9200024A (en) |
NO (1) | NO920010L (en) |
NZ (1) | NZ241123A (en) |
PL (1) | PL293063A1 (en) |
YU (1) | YU792A (en) |
ZA (1) | ZA919854B (en) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP3377555B2 (en) * | 1993-05-31 | 2003-02-17 | ダイセル化学工業株式会社 | Method for removing iodine compound contained in carbonylation reaction product |
US5777157A (en) * | 1996-01-11 | 1998-07-07 | Industrias Monfel S.A. De C.V. | Process for production and purification of triacetin |
EP0968993B1 (en) * | 1998-06-30 | 2002-06-05 | DHW Deutsche Hydrierwerke GmbH Rodleben | Process for the treatment of natural fatty acids |
US6667418B2 (en) * | 2002-04-16 | 2003-12-23 | Celanese International Corporation | Oxidation treatment of a recycle stream in production of acetic acid by methanol carbonylation |
US7524988B2 (en) * | 2006-08-01 | 2009-04-28 | Lyondell Chemical Technology, L.P. | Preparation of acetic acid |
US7208625B1 (en) * | 2006-08-04 | 2007-04-24 | Lyondell Chemical Technology, L.P. | Removing permanganate-reducing impurities from acetic acid |
US7485749B2 (en) * | 2006-08-22 | 2009-02-03 | Lyondell Chemical Technology, L.P. | Preparation of acetic acid |
US10758838B2 (en) | 2015-02-25 | 2020-09-01 | Sabic Global Technologies B.V. | Process for removing impurities from acetic acid |
GB2546002B (en) | 2015-12-30 | 2019-10-30 | Lg Display Co Ltd | Organic light emitting diode display device |
WO2018116143A1 (en) * | 2016-12-19 | 2018-06-28 | Sabic Global Technologies B.V. | Method of purifying acetic acid |
CN113999109A (en) * | 2021-11-15 | 2022-02-01 | 聊城鲁西甲酸化工有限公司 | System and method for removing floccules in concentrated formic acid product |
Family Cites Families (33)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2286995A (en) * | 1942-06-16 | Purification of acetic acid | ||
US2504195A (en) * | 1950-04-18 | Heatcd | ||
GB372434A (en) * | 1931-02-17 | 1932-05-12 | Boehringer & Soehne Gmbh | Process for separation of acetic anhydride and acetic acid |
US2273459A (en) * | 1938-11-25 | 1942-02-17 | Dow Chemical Co | Purification of acetic acid |
US2352253A (en) * | 1941-03-21 | 1944-06-27 | Du Pont | Purification of aliphatic acids and anhydrides |
GB749098A (en) * | 1953-12-23 | 1956-05-16 | Courtaulds Ltd | Improvements in and relating to the purification of acetic anhydride |
DE1568341A1 (en) * | 1966-10-12 | 1970-03-19 | Huels Chemische Werke Ag | Process for the purification of technical terephthalic acid |
US3450754A (en) * | 1966-12-12 | 1969-06-17 | Us Rubber Co | Purification of formic acid |
SE364255B (en) * | 1967-04-05 | 1974-02-18 | Monsanto Co | |
US3551300A (en) * | 1968-12-13 | 1970-12-29 | Witco Chemical Corp | By-water dissolution,steam distillation,activated carbon and cation exchange treatment and crystallization |
US3709795A (en) * | 1970-02-02 | 1973-01-09 | Monsanto Co | Purification of carboxylic acids by chemical treatment and distillation |
JPS4830615A (en) * | 1971-08-24 | 1973-04-23 | ||
BE791577A (en) * | 1971-11-19 | 1973-05-17 | Monsanto Co | Purification of carboxylic acid streams |
US3928434A (en) * | 1973-04-02 | 1975-12-23 | Union Carbide Corp | Oxidative removal of impurities from acetic acid |
US4149013A (en) * | 1978-05-19 | 1979-04-10 | E. I. Du Pont De Nemours And Company | Process for purifying 1,12-dodecanedioic acid |
US4246195A (en) * | 1978-10-06 | 1981-01-20 | Halcon Research And Development Corporation | Purification of carbonylation products |
US4252741A (en) * | 1978-10-06 | 1981-02-24 | Halcon Research & Development Corp. | Carbonylation with Group VIII noble metal catalysts |
DE2901359A1 (en) * | 1979-01-15 | 1980-07-24 | Basf Ag | METHOD FOR REMOVING IODINE FROM ORGANIC COMPOUNDS |
FR2464947A1 (en) * | 1979-09-07 | 1981-03-20 | Ugine Kuhlmann | PROCESS FOR PRODUCING PERCARBOXYLIC ACIDS |
DE3016225A1 (en) * | 1980-04-26 | 1981-10-29 | Ruhrchemie Ag, 4200 Oberhausen | METHOD FOR PURIFYING POLYCARBONIC ACIDS |
JPS58116436A (en) * | 1981-12-28 | 1983-07-11 | Mitsubishi Gas Chem Co Inc | Purification of acetic anhydride |
FR2519634B1 (en) * | 1982-01-13 | 1986-09-12 | Ugine Kuhlmann | IMPROVEMENT IN PROCESSES FOR THE SYNTHESIS OF PERCABOXYLIC ACIDS |
NZ203226A (en) * | 1982-02-13 | 1985-08-30 | Bp Chemical Ltd | Production of acetic anhydride from methanol and carbon monoxide |
IT1169697B (en) * | 1983-12-16 | 1987-06-03 | Montedison Spa | PROCESS FOR THE OXIDATION OF ALDEHYDES TO CARBOXYLIC ACIDS |
JPS60139641A (en) * | 1983-12-27 | 1985-07-24 | Daicel Chem Ind Ltd | Purification of monochloroacetic acid |
JPH0635418B2 (en) * | 1984-08-27 | 1994-05-11 | ダイセル化学工業株式会社 | Purification method of acetic acid |
DE3612504A1 (en) * | 1985-09-30 | 1987-04-09 | Hoechst Ag | METHOD FOR SEPARATING IODINE AND ITS COMPOUNDS FROM CARBONYLATING PRODUCTS CONTAINING CARBBONYLATION OF DIMETHYL ETHER, METHYL ACETATE OR METHANOL |
SU1437363A1 (en) * | 1986-10-09 | 1988-11-15 | Предприятие П/Я А-7372 | Method of purifying acetic acid in its regeneration in production of cellulose acetates and acetic anhydride |
CA1313676C (en) * | 1987-12-23 | 1993-02-16 | Mark Owen Scates | Purification of acetic acid with ozone |
GB8822661D0 (en) * | 1988-09-27 | 1988-11-02 | Bp Chem Int Ltd | Removal of iodine/iodide impurities |
JPH07107013B2 (en) * | 1988-11-14 | 1995-11-15 | ダイセル化学工業株式会社 | Decolorization method of dilute acetic acid |
US5144067A (en) * | 1989-09-29 | 1992-09-01 | Eastman Kodak Company | Process for the coproduction of alkyl iodides and alpha-iodocarboxylic acids and/or anhydrides thereof |
JP3066978B2 (en) * | 1990-08-15 | 2000-07-17 | イーストマン ケミカル カンパニー | Acetic anhydride and acetic acid purification method |
-
1991
- 1991-01-05 GB GB919100216A patent/GB9100216D0/en active Pending
- 1991-12-11 US US07/805,373 patent/US5387713A/en not_active Expired - Fee Related
- 1991-12-13 CA CA002057638A patent/CA2057638A1/en not_active Abandoned
- 1991-12-13 ZA ZA919854A patent/ZA919854B/en unknown
- 1991-12-18 DE DE69111410A patent/DE69111410D1/en not_active Expired - Fee Related
- 1991-12-18 EP EP91311766A patent/EP0494527B2/en not_active Expired - Lifetime
- 1991-12-18 DE DE69111410T patent/DE69111410T3/en not_active Expired - Lifetime
- 1991-12-18 AT AT91311766T patent/ATE125247T1/en not_active IP Right Cessation
- 1991-12-20 NZ NZ241123A patent/NZ241123A/en unknown
- 1991-12-26 JP JP3344754A patent/JPH04308548A/en active Pending
-
1992
- 1992-01-02 NO NO92920010A patent/NO920010L/en unknown
- 1992-01-02 AU AU10017/92A patent/AU646536B2/en not_active Ceased
- 1992-01-03 AR AR92321590A patent/AR247378A1/en active
- 1992-01-03 BR BR929200013A patent/BR9200013A/en not_active Application Discontinuation
- 1992-01-03 FI FI920033A patent/FI920033A/en unknown
- 1992-01-03 PL PL29306392A patent/PL293063A1/en unknown
- 1992-01-03 MX MX9200024A patent/MX9200024A/en not_active IP Right Cessation
- 1992-01-03 KR KR1019920000004A patent/KR100189787B1/en not_active IP Right Cessation
- 1992-01-03 HU HU9200026A patent/HU9200026D0/en unknown
- 1992-01-04 CN CN92100037A patent/CN1031507C/en not_active Expired - Fee Related
- 1992-01-06 YU YU792A patent/YU792A/en unknown
Also Published As
Publication number | Publication date |
---|---|
GB9100216D0 (en) | 1991-02-20 |
NO920010L (en) | 1992-07-06 |
EP0494527A1 (en) | 1992-07-15 |
US5387713A (en) | 1995-02-07 |
JPH04308548A (en) | 1992-10-30 |
ATE125247T1 (en) | 1995-08-15 |
KR920014759A (en) | 1992-08-25 |
PL293063A1 (en) | 1992-08-24 |
HU9200026D0 (en) | 1992-03-30 |
ZA919854B (en) | 1993-06-14 |
CA2057638A1 (en) | 1992-07-06 |
EP0494527B2 (en) | 1998-12-16 |
EP0494527B1 (en) | 1995-07-19 |
NZ241123A (en) | 1993-02-25 |
NO920010D0 (en) | 1992-01-02 |
FI920033A (en) | 1992-07-06 |
DE69111410T2 (en) | 1996-01-04 |
KR100189787B1 (en) | 1999-06-01 |
BR9200013A (en) | 1992-09-08 |
FI920033A0 (en) | 1992-01-03 |
AU646536B2 (en) | 1994-02-24 |
AU1001792A (en) | 1992-07-09 |
AR247378A1 (en) | 1994-12-29 |
MX9200024A (en) | 1992-07-01 |
DE69111410D1 (en) | 1995-08-24 |
CN1063097A (en) | 1992-07-29 |
DE69111410T3 (en) | 1999-09-23 |
DE69111410T4 (en) | 1999-02-04 |
CN1031507C (en) | 1996-04-10 |
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