WO2023093351A1 - Film-forming device - Google Patents

Film-forming device Download PDF

Info

Publication number
WO2023093351A1
WO2023093351A1 PCT/CN2022/125287 CN2022125287W WO2023093351A1 WO 2023093351 A1 WO2023093351 A1 WO 2023093351A1 CN 2022125287 W CN2022125287 W CN 2022125287W WO 2023093351 A1 WO2023093351 A1 WO 2023093351A1
Authority
WO
WIPO (PCT)
Prior art keywords
top plate
gap
area
forming device
annular
Prior art date
Application number
PCT/CN2022/125287
Other languages
French (fr)
Chinese (zh)
Inventor
张俊杰
Original Assignee
无锡先为科技有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 无锡先为科技有限公司 filed Critical 无锡先为科技有限公司
Publication of WO2023093351A1 publication Critical patent/WO2023093351A1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/46Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for heating the substrate

Abstract

The present application relates to the related technical field of MOCVD apparatuses. Disclosed is a film-forming device, which is used for solving the problem of a poor temperature control effect caused by uneven temperature distribution on a top plate. The film-forming device provided in the present application is provided with a reaction cavity, and comprises a base, a cover assembly and a heating device, wherein the base is positioned at the bottom of the reaction cavity and is used for bearing a substrate; the cover assembly is positioned at the top of the reaction cavity and is arranged opposite the base; the heating device is used for heating the base; and the cover assembly comprises a top plate facing the reaction cavity, and a cooling plate assembly arranged adjacent to the top plate, wherein the top plate is provided with a heated surface facing the reaction cavity and a radiating surface facing the cooling plate assembly, and a circulation gap is formed between the radiating surface of the top plate and the cooling plate assembly, with the circulation gap having a plurality of different heights along the center of the top plate toward the edge of same, and the heights being gap distances between the radiating surface and the cooling plate assembly. The present application is used for improving the temperature uniformity of the top plate.

Description

成膜装置Film forming device 技术领域technical field
本申请涉及MOCVD设备相关技术领域,具体涉及一种成膜装置。The present application relates to the technical field related to MOCVD equipment, in particular to a film forming device.
背景技术Background technique
金属有机物化学气相沉淀(Metal Organic Chemical Vapor Deposition,简称MOCVD)是以Ⅲ族、Ⅱ族元素的有机化合物和V、Ⅵ族元素的氢化物等作为晶体生长源材料,以热分解反应方式在衬底上进行气相外延,生长各种Ⅲ-V族、Ⅱ-Ⅵ族化合物半导体以及它们的多元固溶体的薄层单晶材料。通常MOCVD系统中的晶体生长都是在常压或低压(10-100Torr)下在成膜装置内进行。Metal Organic Chemical Vapor Deposition (MOCVD for short) uses organic compounds of group III and group II elements and hydrides of group V and group VI elements as crystal growth source materials. Vapor phase epitaxy is carried out on the surface to grow thin-layer single crystal materials of various III-V, II-VI compound semiconductors and their multiple solid solutions. Usually, the crystal growth in the MOCVD system is carried out in the film forming device under normal pressure or low pressure (10-100 Torr).
其中,成膜装置是由石英管和石墨基座组成。为了生长组分均匀、超薄层、异质结构的化合物半导体材料,各生产厂家和研究者在成膜装置结构的设计上下了很大功夫,设计出了不同结构的成膜装置。成膜装置中的石墨基座是由高纯石墨制成并包裹SIC层。Among them, the film forming device is composed of a quartz tube and a graphite base. In order to grow compound semiconductor materials with uniform components, ultra-thin layers, and heterogeneous structures, various manufacturers and researchers have put a lot of effort into the design of the film-forming device structure, and have designed film-forming devices with different structures. The graphite base in the film forming device is made of high-purity graphite and wraps the SIC layer.
成膜装置的底部由基座形成,成膜装置的顶部由顶板形成,基座的下方设置有加热装置,该加热装置能够加热基座以及成膜装置内的气体,使得位于成膜装置顶部的顶板的温度升高,为了避免顶板在高温下发生变形,需要控制顶板的温度,由此,通常会在顶板的上方设有冷却板组件,用于给顶板进行降温。The bottom of the film-forming device is formed by a base, the top of the film-forming device is formed by a top plate, and a heating device is arranged below the base, and the heating device can heat the gas in the base and the film-forming device, so that the gas at the top of the film-forming device The temperature of the top plate rises. In order to avoid deformation of the top plate under high temperature, it is necessary to control the temperature of the top plate. Therefore, a cooling plate assembly is usually provided above the top plate for cooling the top plate.
然而,现有技术中顶板上与加热装置对应的区域温度最高,其余区域的温度相对较低,即顶板上沿着所述顶板的中心向所述顶板的边缘方向存在温差,由此导致顶板上的温度分布不均匀,顶板的温度控制效果差。However, in the prior art, the area on the top plate corresponding to the heating device has the highest temperature, and the temperature in the remaining areas is relatively low, that is, there is a temperature difference on the top plate along the center of the top plate to the edge of the top plate, thus causing The temperature distribution of the roof is uneven, and the temperature control effect of the roof is poor.
技术解决方案technical solution
本申请提供一种成膜装置,以解决顶板上的温度分布不均匀、温度控制效果差的问题。The present application provides a film forming device to solve the problems of uneven temperature distribution and poor temperature control effect on the top plate.
为达上述目的,一方面,本申请提供的成膜装置具有至少一个用于在基片表面成膜的反应腔,所述成膜装置包括基座、盖组件和加热装置,基座位于所述反应腔的底部、用于承载至少一基片;盖组件位于所述反应腔的顶部且与所述基座相对而设;加热装置用来加热所述基座;所述盖组件包括面向所述反应腔的顶板及与所述顶板相邻设置的冷却板组件,所述顶板具有一朝向所述反应腔的受热表面和一朝向所述冷却板组件的散热表面;所述顶板的所述散热表面与所述冷却板组件之间形成有流通间隙,所述流通间隙沿着所述顶板的中心向所述顶板的边缘方向具有多个不同的高度,所述高度为所述散热表面和所述冷却板组件之间的间隙距离;至少包括一个围绕所述顶板的中心的第一圆周,在所述第一圆周上的所述流通间隙具有不同高度。In order to achieve the above purpose, on the one hand, the film forming device provided by the present application has at least one reaction chamber for forming a film on the surface of the substrate, the film forming device includes a base, a cover assembly and a heating device, and the base is located on the The bottom of the reaction chamber is used to carry at least one substrate; the cover assembly is located on the top of the reaction chamber and is opposite to the base; the heating device is used to heat the base; the cover assembly includes a The top plate of the reaction chamber and the cooling plate assembly arranged adjacent to the top plate, the top plate has a heated surface facing the reaction chamber and a heat dissipation surface facing the cooling plate assembly; the heat dissipation surface of the top plate A flow gap is formed between the cooling plate assembly, and the flow gap has a plurality of different heights along the center of the top plate to the edge of the top plate, and the height is the heat dissipation surface and the cooling plate. Gap distance between plate assemblies; comprising at least a first circumference around the center of said top plate, said flow gaps on said first circumference having different heights.
在本申请的一些实施例中,所述冷却板组件具有一朝向所述散热表面的冷却表面,所述冷却表面为一平面;所述顶板的所述散热表面为一不平整的表面,所述盖组件至少包括一面向所述散热表面的进气口,以向所述流通间隙内填充导热气体。In some embodiments of the present application, the cooling plate assembly has a cooling surface facing the heat dissipation surface, the cooling surface is a plane; the heat dissipation surface of the top plate is an uneven surface, the The cover assembly at least includes an air inlet facing the heat dissipation surface for filling heat transfer gas into the circulation gap.
在本申请的一些实施例中,在所述散热表面上形成有靠近所述顶板的中心的第一环形区域,所述顶板在所述第一环形区域与所述冷却表面之间形成所述流通间隙的第一间隙;在所述第一环形区域内设置有多个整流块,多个所述整流块环绕所述中心且间隔设置。In some embodiments of the present application, a first annular area close to the center of the top plate is formed on the heat dissipation surface, and the top plate forms the communication between the first annular area and the cooling surface. The first gap of the gap; a plurality of rectifying blocks are arranged in the first annular area, and the plurality of rectifying blocks surround the center and are arranged at intervals.
在本申请的一些实施例中,所述第一环形区域包括沿着所述顶板的中心向所述顶板的边缘方向依次分布的内环形区、中间环形区和外环形区;所述整流块呈辐射状设置于所述中间环形区内;在水平投影面内,所述进气口位于所述内环形区。In some embodiments of the present application, the first annular area includes an inner annular area, a middle annular area and an outer annular area distributed sequentially along the center of the top plate toward the edge of the top plate; the rectifying block is Radially arranged in the middle annular area; in the horizontal projection plane, the air inlet is located in the inner annular area.
在本申请的一些实施例中,相邻两个所述整流块之间形成有气流通道,所述第一圆周位于所述中间环形区内,在所述第一圆周上具有不同高度的所述流通间隙包括所述整流块处的流通间隙和所述气流通道处的流通间隙。In some embodiments of the present application, an air flow passage is formed between two adjacent rectifying blocks, the first circumference is located in the middle annular region, and the first circumference has different heights of the The flow gap includes the flow gap at the rectifying block and the flow gap at the airflow channel.
在本申请的一些实施例中,相邻两个所述整流块之间形成有气流通道,所述气流通道靠近所述进气口处的分布密度小于所述气流通道远离所述进气口处的分布密度。In some embodiments of the present application, airflow passages are formed between two adjacent rectifying blocks, and the distribution density of the airflow passages near the air inlet is smaller than that of the airflow passages away from the air inlet. distribution density.
在本申请的一些实施例中,相邻两个所述整流块之间形成有气流通道,所述气流通道在所述第一环形区域的周向上的宽度相等,多个所述整流块的高度均小于所述第一间隙的高度,所述整流块与所述冷却表面之间的距离小于相邻两个所述整流块之间的气流通道的宽度,所述第一间隙的高度的取值范围为:3mm~6mm。In some embodiments of the present application, an airflow channel is formed between two adjacent rectifying blocks, and the width of the airflow channel in the circumferential direction of the first annular region is equal, and the height of a plurality of rectifying blocks is are less than the height of the first gap, the distance between the rectifying block and the cooling surface is smaller than the width of the airflow channel between two adjacent rectifying blocks, and the value of the height of the first gap is The range is: 3mm~6mm.
在本申请的一些实施例中,所述散热表面还包括依次位于所述第一环形区域的径向外侧的第二环形区域、第三环形区域和第四环形区域;所述第二环形区域与所述冷却表面之间形成所述流通间隙的第二间隙;所述第三环形区域与所述冷却表面之间形成所述流通间隙的第三间隙;所述第四环形区域与所述冷却表面之间形成所述流通间隙的第四间隙;其中,所述第二间隙的高度小于所述第一间隙的高度、所述第三间隙的高度和所述第四间隙的高度;所述基座上设有凹槽,所述凹槽用于容置所述基片,所述加热装置的直接加热区域至少部分覆盖所述凹槽;在水平投影面内,所述第二环形区域的至少一部分与所述凹槽重合。In some embodiments of the present application, the heat dissipation surface further includes a second annular area, a third annular area and a fourth annular area sequentially located radially outside the first annular area; the second annular area and A second gap forming the flow gap between the cooling surfaces; a third gap forming the flow gap between the third annular region and the cooling surface; a third gap forming the flow gap between the fourth annular region and the cooling surface A fourth gap forming the flow gap between them; wherein, the height of the second gap is less than the height of the first gap, the height of the third gap and the height of the fourth gap; the base There is a groove on the top, the groove is used to accommodate the substrate, and the direct heating area of the heating device at least partially covers the groove; in the horizontal projection plane, at least a part of the second annular region coincides with the groove.
在本申请的一些实施例中,在所述流通间隙的高度方向上,所述凹槽的中心和所述第二环形区域在径向方向上的中间位置共线;所述第二间隙的高度的取值范围为:0.1mm~0.5mm。In some embodiments of the present application, in the height direction of the flow gap, the center of the groove and the middle position of the second annular region in the radial direction are collinear; the height of the second gap The value range is: 0.1mm~0.5mm.
在本申请的一些实施例中,在水平投影面内,所述基座包括被所述加热装置的直接加热区域覆盖的第一区域和位于第一加热区域之外的第二区域,所述第三环形区域与所述第二区域至少部分重合,所述第三间隙的高度的取值范围为:1.5mm~3mm。In some embodiments of the present application, in the horizontal projection plane, the base includes a first area covered by the direct heating area of the heating device and a second area located outside the first heating area, the first The three-ring area overlaps with the second area at least partially, and the height of the third gap ranges from 1.5 mm to 3 mm.
在本申请的一些实施例中,所述第四间隙的高度的取值范围为:2mm~5mm。In some embodiments of the present application, the height of the fourth gap ranges from 2 mm to 5 mm.
相较于现有技术,本申请中的成膜装置通过将所述流通间隙从靠近所述顶板的中心至远离所述顶板的中心的方向设置成具有不同间隙高度的结构,使得冷却板组件对顶板的冷却效果得到调节,从而通过不同的间隙高度对顶板上不同的区域的温度能够分别进行控制,使得顶板上的温度场分布较为均匀,进而提高了冷却板组件对顶板的温度控制效果。Compared with the prior art, the film forming device in the present application sets the flow gap from the direction close to the center of the top plate to the direction away from the center of the top plate to have a structure with different gap heights, so that the cooling plate assembly The cooling effect of the top plate is adjusted, so that the temperature of different regions on the top plate can be controlled separately through different gap heights, so that the temperature field distribution on the top plate is relatively uniform, thereby improving the temperature control effect of the cooling plate assembly on the top plate.
第二方面,本申请还提供了一种MOCVD设备,MOCVD设备包括上述成膜装置。In a second aspect, the present application also provides an MOCVD equipment, which includes the above-mentioned film forming device.
此外,由于本申请提供的MOCVD设备中的成膜装置和上述成膜装置具有相同的结构,由此本申请提供的MOCVD设备能够达到和上述成膜装置相同的技术效果。In addition, since the film-forming device in the MOCVD equipment provided by the present application has the same structure as the above-mentioned film-forming device, the MOCVD equipment provided in the present application can achieve the same technical effect as the above-mentioned film-forming device.
第三方面,本申请还提供了一种顶板,应用于一成膜装置中,所述顶板具有相对设置的一受热表面和一散热表面;所述散热表面设置有多个高度不同的环形区域,所述多个高度不同的环形区域沿着所述顶板的中心向所述顶板的边缘分布。In a third aspect, the present application also provides a top plate used in a film forming device, the top plate has a heat receiving surface and a heat dissipation surface oppositely arranged; the heat dissipation surface is provided with a plurality of annular regions with different heights, The plurality of annular regions with different heights are distributed along the center of the top plate to the edge of the top plate.
在本申请的一些实施例中,在所述散热表面上形成有沿着所述顶板的中心向所述顶板的边缘方向依次排布的第一环形区域、第二环形区域、第三环形区域和第四环形区域;所述第二环形区域的高度大于所述第一环形区域的高度、所述第三环形区域的高度和所述第四环形区域的高度;所述第一环形区域包括沿着所述顶板的中心向所述顶板的边缘方向依次分布的内环形区、中间环形区和外环形区,在所述中间环形区设置有多个整流块,多个所述整流块呈辐射状环绕所述顶板的中心间隔设置;所述整流块的高度小于所述第二环形区域的高度。以通过该等整流块打散流通的导热气体,使得位于所述整流块下游的导热气体流通经上述一个或多个环形区域时,其在该等环形区域的周向上能均匀分布,以增强顶板的温度的均匀性的改善效果。In some embodiments of the present application, a first annular area, a second annular area, a third annular area and The fourth annular area; the height of the second annular area is greater than the height of the first annular area, the height of the third annular area and the height of the fourth annular area; the first annular area includes along The inner annular area, the middle annular area and the outer annular area are distributed sequentially from the center of the top plate to the edge of the top plate, and a plurality of rectifying blocks are arranged in the middle annular area, and the plurality of rectifying blocks surround radially The center of the top plate is arranged at intervals; the height of the rectifying block is smaller than the height of the second annular area. The heat-conducting gas that passes through the rectifying blocks is broken up so that when the heat-conducting gas downstream of the rectifying block flows through the above-mentioned one or more annular regions, it can be evenly distributed in the circumferential direction of the annular regions, so as to strengthen the top plate The improvement effect of the temperature uniformity.
本申请中所述顶板的所述散热表面设置有多个高度不同的环形区域,所述多个高度不同的环形区域沿着所述顶板的中心向所述顶板的边缘分布,将上述顶板应用于成膜装置时,能够使得顶板和成膜装置中的冷却板组件之间具有不同间隙高度的结构,从而使得冷却板组件对顶板的冷却效果得到调节,使得顶板上的温度场分布较为均匀。The heat dissipation surface of the top plate in the present application is provided with a plurality of annular regions with different heights, and the plurality of annular regions with different heights are distributed along the center of the top plate to the edge of the top plate, and the above-mentioned top plate is applied to In the film forming device, it is possible to have a structure with different gap heights between the top plate and the cooling plate assembly in the film forming device, so that the cooling effect of the cooling plate assembly on the top plate can be adjusted, so that the temperature field distribution on the top plate is relatively uniform.
附图说明Description of drawings
为了更清楚地说明本申请实施例中的技术方案,下面将对实施例描述中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本申请的一些实施例,对于本领域技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其他的附图。In order to more clearly illustrate the technical solutions in the embodiments of the present application, the drawings that need to be used in the description of the embodiments will be briefly introduced below. Obviously, the drawings in the following description are only some embodiments of the present application. For those skilled in the art, other drawings can also be obtained based on these drawings without any creative effort.
图1是本申请实施中成膜装置的纵截面的结构示意图。FIG. 1 is a structural schematic diagram of a longitudinal section of a film-forming device in the practice of the present application.
图2是图1中的A部放大图。Fig. 2 is an enlarged view of part A in Fig. 1 .
图3是本申请实施例中成膜装置中的顶板的立体结构示意图。FIG. 3 is a schematic perspective view of the top plate in the film forming device in the embodiment of the present application.
图4是本申请实施例中基座的温度曲线图。Fig. 4 is a temperature curve diagram of the susceptor in the embodiment of the present application.
图5是本申请实施例中顶板上未设置环形分区的温度曲线图和本申请实施例中顶板上设置环形分区结构后的温度曲线图。Fig. 5 is a temperature curve diagram of the embodiment of the present application without an annular partition on the top plate and a temperature curve diagram of the embodiment of the present application after the annular partition structure is arranged on the top plate.
本申请说明书附图中的主要附图标记说明如下:1-基座;100-基片;2-顶板;20-通孔;21-第一环形区域;211-整流块;212-内环形区;213-中间环形区;214-外环形区;22-第二环形区域;23-第三环形区域;24-第四环形区域;3-加热装置;4-冷却板组件;40-进气口;5-上盖;6-进气装置;7-旋转轴。The main reference signs in the drawings of this application specification are explained as follows: 1-base; 100-substrate; 2-top plate; 20-through hole; 21-first annular area; 213-middle annular area; 214-outer annular area; 22-second annular area; 23-third annular area; 24-fourth annular area; 3-heating device; 4-cooling plate assembly; 40-air inlet ; 5-top cover; 6-air intake device; 7-rotary shaft.
本发明的实施方式Embodiments of the present invention
下面将结合本申请实施例中的附图,对本申请实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本申请一部分实施例,而不是全部的实施例。基于本申请中的实施例,本领域技术人员在没有作出创造性劳动前提下所获得的所有其它实施例,都属于本申请保护的范围。The following will clearly and completely describe the technical solutions in the embodiments of the application with reference to the drawings in the embodiments of the application. Apparently, the described embodiments are only some of the embodiments of the application, not all of them. Based on the embodiments in this application, all other embodiments obtained by those skilled in the art without making creative efforts belong to the scope of protection of this application.
在本申请的描述中,需要理解的是,术语“中心”、“上”、“下”、“前”、“后”、“左”、“右”、“竖直”、“水平”、“顶”、“底”、“内”、“外”等指示的方位或位置关系为基于附图所示的方位或位置关系,仅是为了便于描述本申请和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本申请的限制。In the description of this application, it is to be understood that the terms "center", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", The orientations or positional relationships indicated by "top", "bottom", "inner", "outer", etc. are based on the orientations or positional relationships shown in the drawings, and are only for the convenience of describing the application and simplifying the description, rather than indicating or implying References to devices or elements must have a particular orientation, be constructed, and operate in a particular orientation and therefore should not be construed as limiting the application.
术语“第一”、“第二”仅用于描述目的,而不能理解为指示或暗示相对重要性或者隐含指明所指示的技术特征的数量。由此,限定有“第一”、“第二”的特征可以明示或者隐含地包括一个或者更多个该特征。在本申请的描述中,除非另有说明,“多个”的含义是两个或两个以上。The terms "first" and "second" are used for descriptive purposes only, and cannot be interpreted as indicating or implying relative importance or implicitly specifying the quantity of indicated technical features. Thus, a feature defined as "first" and "second" may explicitly or implicitly include one or more of these features. In the description of the present application, unless otherwise specified, "plurality" means two or more.
在本申请的描述中,需要说明的是,除非另有明确的规定和限定,术语“安装”、“相连”、“连接”应做广义理解,例如,可以是固定连接,也可以是可拆卸连接,或一体地连接;可以是机械连接,可以是直接相连,也可以通过中间媒介间接相连,可以是两个元件内部的连通。对于本领域的普通技术人员而言,可以具体情况理解上述术语在本申请中的具体含义。In the description of this application, it should be noted that unless otherwise specified and limited, the terms "installation", "connection", and "connection" should be understood in a broad sense, for example, it can be a fixed connection or a detachable connection. Connected, or integrally connected; can be mechanically connected, can be directly connected, can also be indirectly connected through an intermediary, and can be an internal communication between two elements. Those of ordinary skill in the art can understand the specific meanings of the above terms in this application in specific situations.
本申请提供一种成膜装置,以下将对上述装置分别进行详细说明。需要说明的是,以下实施例的描述顺序不作为对本申请实施例优选顺序的限定。且在以下实施例中,对各个实施例的描述都各有侧重,某个实施例中没有详述的部分,可以参见其它实施例的相关描述。The present application provides a film forming device, and the above devices will be described in detail below. It should be noted that the description order of the following embodiments is not intended to limit the preferred order of the embodiments of the present application. And in the following embodiments, the description of each embodiment has its own focus, and for the part not described in detail in a certain embodiment, you can refer to the relevant descriptions of other embodiments.
参照图1~图3,本申请提供的成膜装置具有至少一个用于在基片100表面成膜的反应腔,所述成膜装置包括基座1、盖组件和加热装置3,所述基座1位于所述反应腔的底部、用于承载至少一基片100;所述盖组件位于所述反应腔的顶部且与所述基座1相对而设,加热装置3能够加热所述基座1;所述盖组件包括面向所述反应腔的顶板2及与所述顶板2相邻设置的冷却板组件4,所述顶板2具有一朝向所述反应腔的受热表面和一朝向所述冷却板组件4的散热表面;所述顶板2的所述散热表面与所述冷却板组件4之间形成有流通间隙,所述流通间隙沿着所述顶板2的中心向所述顶板2的边缘方向具有多个不同的高度,所述高度为所述散热表面和所述冷却板组件4之间的间隙距离。在其中一实施例中,所述基片100可以是晶片。Referring to FIGS. 1 to 3 , the film forming device provided by the present application has at least one reaction chamber for forming a film on the surface of a substrate 100. The film forming device includes a base 1, a cover assembly and a heating device 3. The base The base 1 is located at the bottom of the reaction chamber and is used to carry at least one substrate 100; the cover assembly is located on the top of the reaction chamber and is opposite to the base 1, and the heating device 3 can heat the base 1; the cover assembly includes a top plate 2 facing the reaction chamber and a cooling plate assembly 4 adjacent to the top plate 2, the top plate 2 has a heated surface facing the reaction chamber and a cooling surface facing the reaction chamber. The heat dissipation surface of the plate assembly 4; a flow gap is formed between the heat dissipation surface of the top plate 2 and the cooling plate assembly 4, and the flow gap is along the direction from the center of the top plate 2 to the edge of the top plate 2 There are several different heights, the height being the gap distance between the heat dissipation surface and the cooling plate assembly 4 . In one embodiment, the substrate 100 may be a wafer.
相较于现有技术,本申请提供的成膜装置通过将所述流通间隙从靠近所述顶板2的中心至远离所述顶板2的中心的方向设置成具有不同间隙高度的结构,使得冷却板组件4对顶板2的冷却效果得到调节,从而通过不同的间隙高度对顶板2上不同的区域的温度能够分别进行控制,使得顶板2上的温度场分布较为均匀,进而提高了冷却板组件4对顶板2的温度控制效果。Compared with the prior art, the film forming device provided by the present application has a structure with different gap heights by setting the flow gap from the direction close to the center of the top plate 2 to the direction away from the center of the top plate 2, so that the cooling plate The cooling effect of the component 4 on the top plate 2 is adjusted, so that the temperature of different regions on the top plate 2 can be controlled separately through different gap heights, so that the temperature field distribution on the top plate 2 is relatively uniform, thereby improving the cooling effect of the cooling plate component 4. The temperature control effect of the top plate 2.
通常,上述成膜装置具有圆柱形的中空结构的反应腔,与之对应的,所述顶板2和所述基座1均为圆形板状结构。在所述基座1的中间位置处连接有一旋转轴7,旋转轴7用于带动基座1绕着其轴线旋转,即,该旋转轴7的轴线也就是成膜装置的轴线、顶板2的中心。Usually, the above-mentioned film forming device has a cylindrical hollow reaction chamber, and correspondingly, the top plate 2 and the base 1 are circular plate-shaped structures. A rotating shaft 7 is connected to the middle position of the base 1, and the rotating shaft 7 is used to drive the base 1 to rotate around its axis, that is, the axis of the rotating shaft 7 is also the axis of the film forming device, the axis of the top plate 2 center.
可以理解的是,上述基座1、顶板2、冷却板组件4均关于旋转轴7的轴线呈对称设置。其中,所述顶板2由石墨材料制成。It can be understood that the base 1 , the top plate 2 , and the cooling plate assembly 4 are arranged symmetrically with respect to the axis of the rotating shaft 7 . Wherein, the top plate 2 is made of graphite material.
以下,对顶板2和冷却板组件4之间的流通间隙、以及顶板2的结构进行更为详细的说明。The flow gap between the top plate 2 and the cooling plate assembly 4 and the structure of the top plate 2 will be described in more detail below.
在本申请的一些实施例中,所述冷却板组件4具有一朝向所述散热表面的冷却表面,所述冷却表面为一平面;所述顶板2的所述散热表面为一不平整的表面,所述盖组件至少包括一面向所述散热表面的进气口40;即本申请是通过调节顶板2的散热表面的结构来调节顶板2和冷却板组件4之间的流通间隙,以保证流通间隙的调节方式易于实现。In some embodiments of the present application, the cooling plate assembly 4 has a cooling surface facing the heat dissipation surface, the cooling surface is a plane; the heat dissipation surface of the top plate 2 is an uneven surface, The cover assembly at least includes an air inlet 40 facing the heat dissipation surface; that is, the application adjusts the flow gap between the top plate 2 and the cooling plate assembly 4 by adjusting the structure of the heat dissipation surface of the top plate 2 to ensure the flow gap The adjustment method is easy to realize.
基于上述实施例,在所述散热表面上形成有靠近所述顶板2的中心的第一环形区域21,所述顶板2在所述第一环形区域21与所述冷却表面之间形成所述流通间隙的第一间隙;在所述第一环形区域21内设置有多个整流块211,多个所述整流块211环绕所述中心且间隔设置,通过整流块211使得第一环形区域21内载气流动较为均匀。Based on the above embodiment, a first annular area 21 close to the center of the top plate 2 is formed on the heat dissipation surface, and the top plate 2 forms the circulation between the first annular area 21 and the cooling surface. The first gap of the gap; a plurality of rectifying blocks 211 are arranged in the first annular area 21, and a plurality of rectifying blocks 211 are arranged at intervals around the center, and the first annular area 21 is loaded by the rectifying blocks 211 The air flow is relatively uniform.
基于上述实施例,所述第一环形区域21包括沿着所述顶板2的中心向所述顶板的边缘方向依次分布的内环形区212、中间环形区213和外环形区214;多个整流块211呈辐射状设置于所述中间环形区213内,在水平投影面内,所述进气口40位于所述内环形区212,如图2所示。Based on the above embodiment, the first annular area 21 includes an inner annular area 212, a middle annular area 213 and an outer annular area 214 distributed sequentially along the center of the top plate 2 toward the edge of the top plate; a plurality of rectifying blocks 211 is arranged radially in the middle annular area 213 , and in the horizontal projection plane, the air inlet 40 is located in the inner annular area 212 , as shown in FIG. 2 .
可以理解的是,上述盖组件的进气口40用于排出经冷却板组件4冷却后温度较低的载气,且上述进气口40通常为两个孔状结构,即载气在进入上述流通间隙后,靠近进气口40处的载气的气流速度较大,远离进气口40处的载气的气流速度较小,由此本申请通过将进气口40设置在内环形区212内,使得第一环形区域21在内环形区212形成一内环形空腔,即载气通过进气口40先进入到内环形空腔时,会发生气体弥散,随后载气会流经上述相邻两个整流块211之间的间隔处,即通过整流块211对上述载气起到分流、整流的效果,流经整流块211的载气在第一环形区域21的外环形区214形成的外环形空腔内再次发生气体弥散,以提高第一环形区域21内载气的匀一性。It can be understood that the air inlet 40 of the cover assembly is used to discharge the lower-temperature carrier gas cooled by the cooling plate assembly 4, and the air inlet 40 is generally two hole-shaped structures, that is, the carrier gas enters the above-mentioned After passing through the gap, the airflow velocity of the carrier gas near the air inlet 40 is relatively high, and the airflow velocity of the carrier gas far away from the air inlet 40 is relatively small. Therefore, the present application sets the air inlet 40 in the inner annular region 212 inside, so that the first annular region 21 forms an inner annular cavity in the inner annular region 212, that is, when the carrier gas first enters the inner annular cavity through the gas inlet 40, gas dispersion will occur, and then the carrier gas will flow through the above phase Adjacent to the space between the two rectifying blocks 211, that is, through the rectifying block 211, the above-mentioned carrier gas has the effect of splitting and rectifying. Gas dispersion occurs again in the outer annular cavity to improve the uniformity of the carrier gas in the first annular region 21 .
同时,由于靠近进气口40处的载气的气流速度较大,远离进气口40处的载气的气流速度较小,因此,本申请实施例中相邻两个所述整流块211之间形成有气流通道,所述气流通道靠近所述进气口40处的分布密度小于所述气流通道远离所述进气口40处的分布密度,如图3所示,即靠近进气口40处的气流通道的数量较少,同理,远离进气口40处的气流通道的数量较多,进而使得经进气口40排出的气体更好的流动至远离进气口40的区域,以进一步提高载气流动的匀一性。At the same time, since the airflow velocity of the carrier gas near the air inlet 40 is relatively high, and the airflow velocity of the carrier gas far away from the air inlet 40 is relatively small, therefore, in the embodiment of the present application, between two adjacent rectifying blocks 211 Airflow passages are formed between them, and the distribution density of the airflow passages near the air inlet 40 is smaller than the distribution density of the airflow passages away from the air inlet 40, as shown in Figure 3, that is, near the air inlet 40 The number of airflow passages at the location is less, and similarly, the number of airflow passages away from the air inlet 40 is larger, so that the gas discharged through the air inlet 40 can better flow to the area away from the air inlet 40, so as to Further improve the uniformity of carrier gas flow.
可以理解的是,上述整流块211的分布密度可以根据整流块211的在圆周方向上的尺寸得到控制,即,靠近进气口40处的整流块在圆周方向上的尺寸稍大一些,远离进气口40处的整流块在圆周方向上的尺寸稍小一些。It can be understood that the distribution density of the above-mentioned rectifying blocks 211 can be controlled according to the size of the rectifying blocks 211 in the circumferential direction, that is, the rectifying blocks near the air inlet 40 have a slightly larger size in the circumferential direction, The size of the rectifying block at the air port 40 in the circumferential direction is slightly smaller.
基于上述实施例,相邻两个所述整流块211之间形成有气流通道,所述气流通道在所述第一环形区域21的周向上的宽度相等,以使的气流通道的分布密度易于控制,且气流通道的加工方式较为简单方便。Based on the above embodiment, an airflow channel is formed between two adjacent rectifying blocks 211, and the width of the airflow channel in the circumferential direction of the first annular region 21 is equal, so that the distribution density of the airflow channels is easy to control , and the processing method of the airflow channel is relatively simple and convenient.
此外,每相邻两个所述整流块211之间的气流通道的宽度在径向上处处相等,即上述整流块211可以由车刀在凸出于所述第一环形区域21的凸环切割一径向方向的通槽形成,气流通道的宽度与车刀的切割宽度相等,从而使得相邻整流块211之间的气流通道的加工过程更加易于实现。In addition, the width of the airflow channel between every two adjacent rectifying blocks 211 is equal everywhere in the radial direction, that is, the rectifying block 211 can be cut by a turning tool on the protruding ring protruding from the first annular region 21. The through grooves in the radial direction are formed, and the width of the air flow channel is equal to the cutting width of the turning tool, so that the machining process of the air flow channel between adjacent rectifying blocks 211 is easier to realize.
继续参照图2和图3,多个所述整流块211的高度均小于所述第一环形区域21的第一间隙的高度,所述整流块211与所述冷却板组件4的冷却表面之间的距离小于相邻两个所述整流块211之间的气流通道的宽度,即整流块211与冷却板组件4的冷却表面之间存在一间隙,且该间隙的距离小于气流通道的宽度,通过该间隙和气流通道能够使得载气流动的匀一性得到进一步提高。Continuing to refer to FIG. 2 and FIG. 3 , the heights of the plurality of rectifying blocks 211 are all smaller than the height of the first gap in the first annular region 21 , and between the rectifying blocks 211 and the cooling surface of the cooling plate assembly 4 The distance is less than the width of the airflow passage between two adjacent rectification blocks 211, that is, there is a gap between the rectification block 211 and the cooling surface of the cooling plate assembly 4, and the distance of the gap is less than the width of the airflow passage, through The gap and the gas flow channel can further improve the uniformity of the flow of the carrier gas.
其中,所述第一间隙的高度的取值范围为:3mm~6mm,由此在保证第一环形区域21的导热率的基础上,还能够保证整流板对载气的匀一性。Wherein, the value range of the height of the first gap is: 3mm~6mm, so that on the basis of ensuring the thermal conductivity of the first annular region 21, the uniformity of the rectifying plate to the carrier gas can also be ensured.
可以理解的是,上述顶板2由四个环状部件嵌套构成的,该四个环状部件的轴线互相重合,每一环状部件的在径向方向上的尺寸并不相同,且每一环状构件与冷却板组件4之间形成的间隙也不相同。It can be understood that the above-mentioned top plate 2 is formed by nesting four ring-shaped parts, the axes of the four ring-shaped parts coincide with each other, and the size of each ring-shaped part in the radial direction is not the same, and each The gap formed between the ring member and the cooling plate assembly 4 is also different.
以下,对顶板2的其他环形区域的结构进行详细说明。Hereinafter, the structure of other annular regions of the top plate 2 will be described in detail.
在本申请的一些实施例中,基座1上凹槽所在的区域的温度通常最高,由此顶板2上与该凹槽相对的区域(第二环形区域22)的温度最高,为了保证顶板2各个区域的温度分布更加均匀,即载气经过此区域时需要带走的热量最多,由此,本申请中的所述散热表面还包括依次位于第一环形区域21的径向外侧的第二环形区域22、第三环形区域23和第四环形区域24,所述第二环形区域22与所述冷却表面之间形成所述流通间隙的第二间隙;所述第三环形区域23与所述冷却表面之间形成所述流通间隙的第三间隙;所述第四环形区域24与所述冷却表面之间形成所述流通间隙的第四间隙;其中,所述第二间隙的高度小于所述第一间隙的高度、所述第三间隙的高度和所述第四间隙的高度,所述基座1上设有凹槽,所述凹槽用于容置所述基片100,所述加热装置3的直接加热区域至少部分覆盖所述凹槽,在水平投影面内,所述第二环形区域22的至少一部分与所述凹槽重合。In some embodiments of the present application, the temperature of the region where the groove is located on the base 1 is usually the highest, thus the temperature of the region (second annular region 22 ) opposite to the groove on the top plate 2 is the highest, in order to ensure that the top plate 2 The temperature distribution in each area is more uniform, that is, when the carrier gas passes through this area, the heat that needs to be taken away is the most. Therefore, the heat dissipation surface in this application also includes a second annular ring that is sequentially located on the radially outer side of the first annular area 21. Area 22, the third annular area 23 and the fourth annular area 24, the second gap of the flow gap is formed between the second annular area 22 and the cooling surface; the third annular area 23 and the cooling surface A third gap of the flow gap is formed between the surfaces; a fourth gap of the flow gap is formed between the fourth annular region 24 and the cooling surface; wherein, the height of the second gap is smaller than that of the first gap. The height of the first gap, the height of the third gap and the height of the fourth gap, the base 1 is provided with a groove, the groove is used to accommodate the substrate 100, the heating device The direct heating area of 3 at least partly covers the groove, and in the horizontal projection plane, at least a part of the second annular region 22 coincides with the groove.
由于所述顶板2在第二环形区域22与所述冷却板组件4之间的第二间隙高度最小,进而增加了载气的流动速度以及第二环形区域22的导热率,使得载气经过第二环形区域22时带走较多的热量,顶板2在第二环形区域22的散热效率较高。Since the second gap height of the top plate 2 between the second annular region 22 and the cooling plate assembly 4 is the smallest, the flow velocity of the carrier gas and the thermal conductivity of the second annular region 22 are increased, so that the carrier gas passes through the first More heat is taken away in the second annular region 22 , and the heat dissipation efficiency of the top plate 2 in the second annular region 22 is higher.
基于上述实施例,为了进一步提高顶板2上温度分布的均匀性、以及顶板2在第二环形区域22的散热效率,所述基座1上设有凹槽,所述凹槽用于容置所述基片100,所述加热装置3的直接加热区域至少部分覆盖所述凹槽;在水平投影面内,所述第二环形区域的至少一部分与所述凹槽重合。Based on the above-mentioned embodiment, in order to further improve the uniformity of the temperature distribution on the top plate 2 and the heat dissipation efficiency of the top plate 2 in the second annular area 22, the base 1 is provided with grooves for accommodating the For the substrate 100, the direct heating area of the heating device 3 at least partially covers the groove; in the horizontal projection plane, at least a part of the second annular area coincides with the groove.
其中,在所述流通间隙的高度方向上,所述凹槽的中心和所述第二环形区域22在径向方向上的中间位置共线,所述第二间隙的高度的取值范围为:0.1mm~0.5mm,以更好的保证顶板2在第二环形区域22的散热效率。Wherein, in the height direction of the flow gap, the center of the groove and the middle position of the second annular region 22 in the radial direction are collinear, and the value range of the height of the second gap is: 0.1mm~0.5mm, to better ensure the heat dissipation efficiency of the top plate 2 in the second annular region 22 .
基于上述实施例,在水平投影面内,所述基座1包括被所述加热装置3的直接加热区域覆盖的第一区域和位于第一加热区域之外的第二区域,所述第三环形区域23与所述第二区域至少部分重合,所述第三间隙的高度的取值范围为:1.5mm~3mm。Based on the above-mentioned embodiment, in the horizontal projection plane, the base 1 includes a first area covered by the direct heating area of the heating device 3 and a second area located outside the first heating area, the third annular The region 23 at least partially overlaps with the second region, and the height of the third gap ranges from 1.5 mm to 3 mm.
通过实验表明,顶板2的第二环形区域22(即顶板2上与基座1下方的加热装置3对应的区域)的温度最高,顶板2在第二环形区域22的径向外侧的温度与第二环形区域22的温度会存在较大的波动,由此,本申请在第二环形区域22的径向外侧设置了第三环形区域23,由此使得顶板2和冷却板组件4之间的热传导率更加符合顶板2的使用工况。Experiments have shown that the second annular region 22 of the top plate 2 (that is, the region on the top plate 2 corresponding to the heating device 3 below the base 1) has the highest temperature, and the temperature of the top plate 2 on the radially outer side of the second annular region 22 is the same as that of the second annular region 22. The temperature of the second annular area 22 will have large fluctuations, therefore, the present application sets the third annular area 23 on the radially outer side of the second annular area 22, thereby enabling the heat conduction between the top plate 2 and the cooling plate assembly 4 The rate is more in line with the working conditions of the top plate 2.
在本申请的一些实施例中,由于第三环形区域23临近第二环形区域22,其位于基座1上加热区域的径向外侧,即顶板2在第三环形区域23的温度略低于顶板2在第二环形区域22的温度,载气在流经第三环形区域23时不需要较高的热传导率,由此,使得第三间隙的高度的取值范围为1.5mm~3mm,进而保证顶板2在第三环形区域23和顶板2在第二环形区域22的温度更加接近。In some embodiments of the present application, since the third annular area 23 is adjacent to the second annular area 22, it is located on the radially outer side of the heating area on the base 1, that is, the temperature of the top plate 2 in the third annular area 23 is slightly lower than that of the top plate 2. At the temperature of the second annular region 22, the carrier gas does not need a high thermal conductivity when flowing through the third annular region 23, so that the range of the height of the third gap is 1.5mm~3mm, thereby ensuring The temperature of the top plate 2 in the third annular region 23 and the temperature of the top plate 2 in the second annular region 22 are closer.
同理,所述第四间隙的高度的取值范围为:2mm~5mm。Similarly, the range of the height of the fourth gap is: 2mm~5mm.
即,顶板2在第一环形区域21中的第一间隙的高度最高,其一,由于在其在进入第一环形区域21时的温度最低;其二;由于第一环形区域21并未和基座1下方的加热装置3相对设置,因此使得第一间隙的高度最高,以保证顶板2中第一环形区域21的热传导率较为合适。That is, the height of the first gap of the top plate 2 in the first annular region 21 is the highest, one, due to the lowest temperature when it enters the first annular region 21; The heating device 3 under the seat 1 is arranged oppositely, so the height of the first gap is the highest, so as to ensure that the thermal conductivity of the first annular region 21 in the top plate 2 is relatively suitable.
参照图4和图5,图4为本申请实施例中基座1上不同区域对应的温度曲线图,图5为本申请实施例中顶板2上不同区域对应的温度曲线图,其中,B曲线为顶板2上未设置环形分区结构时,顶板2上的温度曲线图,B'曲线为顶板2上设置上述环形分区结构后,顶板2上不同环形区域的温度曲线图。Referring to Fig. 4 and Fig. 5, Fig. 4 is the temperature graph corresponding to different regions on the base 1 in the embodiment of the present application, and Fig. 5 is the temperature graph corresponding to different regions on the top plate 2 in the embodiment of the present application, wherein, the B curve It is the temperature graph on the top plate 2 when the annular partition structure is not set on the top plate 2, and the B' curve is the temperature graph of different annular regions on the top plate 2 after the above-mentioned annular partition structure is set on the top plate 2.
其中,R1表示的是第一环形区域21的半径范围,R2表示的是第二环形区域22的半径范围,R3表示的是第三环形区域23的半径范围,R4表示的是第四环形区域24的半径范围。Wherein, R1 represents the radius range of the first annular area 21, R2 represents the radius range of the second annular area 22, R3 represents the radius range of the third annular area 23, and R4 represents the fourth annular area 24 radius range.
由此可以知道,通过加热装置3加热基座1的话,基座1上靠近加热装置3和远离加热装置3的温度不同,基座1上会形成径向不均匀的温度场,即顶板2上会对应基座1上不均匀的温度场也形成径向不均匀的温度场,通过使用本申请上述结构的顶板2后,即顶板2靠近冷却板组件4的一侧表面为台阶面结构,即通过控制顶板2与冷却板组件4之间的间隙使得顶板2上不同区域的温度分别得到控制,进而使得顶板2上的温度分布的较为均匀。It can be known from this that if the base 1 is heated by the heating device 3, the temperature on the base 1 close to the heating device 3 and the temperature away from the heating device 3 are different, and a radially uneven temperature field will be formed on the base 1, that is, on the top plate 2 Corresponding to the uneven temperature field on the base 1, a radially uneven temperature field will also be formed. After using the top plate 2 with the above-mentioned structure of the application, that is, the side surface of the top plate 2 close to the cooling plate assembly 4 has a stepped surface structure, that is By controlling the gap between the top plate 2 and the cooling plate assembly 4, the temperatures of different regions on the top plate 2 are controlled respectively, so that the temperature distribution on the top plate 2 is relatively uniform.
需要说明的是,在所述顶板2的第一环形区域21的径向内侧还形成有一通孔20,冷却板组件4上形成有与该通孔20的对应的另一通孔,在上述通孔处安装有进气装置6,以供气体进入到反应腔内,来激发或促进用于供给热量、等离子、光等能量的化学反应,从而合成薄膜并吸附及沉积在基片100上。It should be noted that a through hole 20 is also formed on the radial inner side of the first annular region 21 of the top plate 2, and another through hole corresponding to the through hole 20 is formed on the cooling plate assembly 4. An air inlet device 6 is installed at the place for gas to enter the reaction chamber to stimulate or promote chemical reactions for supplying energy such as heat, plasma, light, etc., so as to synthesize a thin film and adsorb and deposit it on the substrate 100 .
其中,上述成膜装置还包括有上盖5,其中,顶板2和冷却板组件4均固定安装在上盖5上。Wherein, the above-mentioned film forming device further includes an upper cover 5 , wherein the top plate 2 and the cooling plate assembly 4 are both fixedly installed on the upper cover 5 .
再者,本申请还提供了一种MOCVD设备,MOCVD设备包括上述的成膜装置。Furthermore, the present application also provides an MOCVD equipment, which includes the above-mentioned film forming device.
由于本申请提供的MOCVD设备中的成膜装置和上述成膜装置具有相同的结构,由此本申请提供的MOCVD设备能够达到和上述成膜装置相同的技术效果。Since the film-forming device in the MOCVD equipment provided by the present application has the same structure as the above-mentioned film-forming device, the MOCVD equipment provided in the present application can achieve the same technical effect as the above-mentioned film-forming device.
此外,本申请还提供了一种顶板2,应用于上述成膜装置中,所述顶板2具有相对设置的一受热表面和一散热表面;所述散热表面设置有多个高度不同的环形区域,所述多个高度不同的环形区域沿着所述顶板2的中心向所述顶板2的边缘分布。In addition, the present application also provides a top plate 2, which is applied in the above-mentioned film forming device, the top plate 2 has a heat receiving surface and a heat dissipation surface oppositely arranged; the heat dissipation surface is provided with a plurality of annular regions with different heights, The plurality of annular regions with different heights are distributed along the center of the top board 2 to the edge of the top board 2 .
其中,在所述散热表面上形成有沿着所述顶板2的中心向所述顶板2的边缘方向依次排布的第一环形区域21、第二环形区域22、第三环形区域23和第四环形区域24;所述第二环形区域22的高度大于所述第一环形区域21的高度、所述第三环形区域23的高度和所述第四环形区域24的高度;所述第一环形区域21包括沿着所述顶板2的中心向所述顶板2的边缘方向依次分布的内环形区212、中间环形区213和外环形区214,在所述中间环形区213设置有多个整流块211,多个所述整流块211呈辐射状环绕所述顶板2的中心间隔设置;所述整流块211的高度小于所述第二环形区域22的高度。Wherein, a first annular area 21 , a second annular area 22 , a third annular area 23 and a fourth annular area 23 are arranged in sequence along the center of the top plate 2 toward the edge of the top plate 2 on the heat dissipation surface. Annular area 24; the height of the second annular area 22 is greater than the height of the first annular area 21, the height of the third annular area 23 and the height of the fourth annular area 24; the first annular area 21 includes an inner annular area 212, a middle annular area 213 and an outer annular area 214 distributed sequentially along the center of the top plate 2 toward the edge of the top plate 2, and a plurality of rectifying blocks 211 are arranged in the middle annular area 213 A plurality of rectifying blocks 211 are arranged radially around the center of the top plate 2 at intervals; the height of the rectifying blocks 211 is smaller than the height of the second annular region 22 .
需要说明的是,多个整流块211并不是均匀分布的,由此在具体安装时,可以将整流块211的分布密度较小的位置靠近成膜装置中盖组件的进气口40设置,将整流块211的分布密度较大的位置远离成膜装置中盖组件的进气口40设置即可。It should be noted that the plurality of rectifying blocks 211 are not uniformly distributed, thus during specific installation, the position where the distribution density of the rectifying blocks 211 is small can be set close to the air inlet 40 of the cover assembly in the film forming device, and the The position where the distribution density of the rectifying blocks 211 is relatively high may be set away from the air inlet 40 of the cover assembly in the film forming device.
在本说明书的描述中,具体特征、结构、材料或者特点可以在任何的一个或多个实施例或示例中以合适的方式结合。In the description of this specification, specific features, structures, materials or characteristics may be combined in any one or more embodiments or examples in an appropriate manner.
以上所述,仅为本申请的具体实施方式,但本申请的保护范围并不局限于此,任何熟悉本技术领域的技术人员在本申请揭露的技术范围内,可轻易想到变化或替换,都应涵盖在本申请的保护范围之内。因此,本申请的保护范围应以所述权利要求的保护范围为准。此外,说明书中应用了具体个例对本申请的原理及实施方式进行了阐述,以上实施例的说明只是用于帮助理解本申请的方法及其核心思想,本说明书内容不应理解为对本申请的限制。The above is only a specific implementation of the application, but the scope of protection of the application is not limited thereto. Anyone familiar with the technical field can easily think of changes or substitutions within the technical scope disclosed in the application. Should be covered within the protection scope of this application. Therefore, the protection scope of the present application should be determined by the protection scope of the claims. In addition, specific examples are used in the description to illustrate the principles and implementation methods of the present application. The descriptions of the above examples are only used to help understand the method and core idea of the present application, and the contents of this description should not be construed as limiting the application .

Claims (11)

  1. 一种成膜装置,具有至少一个用于在基片表面成膜的反应腔,其特征在于,所述成膜装置包括:A film-forming device having at least one reaction chamber for film-forming on a substrate surface, characterized in that the film-forming device comprises:
    基座,位于所述反应腔的底部、用于承载至少一基片;a base, located at the bottom of the reaction chamber, for carrying at least one substrate;
    盖组件,位于所述反应腔的顶部且与所述基座相对而设;a cover assembly, located on the top of the reaction chamber and opposite to the base;
    加热装置,用来加热所述基座;a heating device for heating the base;
    所述盖组件包括面向所述反应腔的顶板及与所述顶板相邻设置的冷却板组件,所述顶板具有一朝向所述反应腔的受热表面和一朝向所述冷却板组件的散热表面;所述顶板的所述散热表面与所述冷却板组件之间形成有流通间隙,所述流通间隙沿着所述顶板的中心向所述顶板的边缘方向具有多个不同的高度,所述高度为所述散热表面和所述冷却板组件之间的间隙距离;The cover assembly includes a top plate facing the reaction chamber and a cooling plate assembly adjacent to the top plate, the top plate has a heated surface facing the reaction chamber and a heat dissipation surface facing the cooling plate assembly; A flow gap is formed between the heat dissipation surface of the top plate and the cooling plate assembly, and the flow gap has a plurality of different heights along the center of the top plate to the edge of the top plate, and the heights are a gap distance between the heat dissipation surface and the cooling plate assembly;
    至少包括一个围绕所述顶板的中心的第一圆周,在所述第一圆周上的所述流通间隙具有不同高度。At least one first circumference around the center of the top plate is included, the flow gaps on the first circumference have different heights.
  2. 根据权利要求1所述的成膜装置,其特征在于,所述冷却板组件具有一朝向所述散热表面的冷却表面,所述冷却表面为一平面;The film forming device according to claim 1, wherein the cooling plate assembly has a cooling surface facing the heat dissipation surface, and the cooling surface is a plane;
    所述顶板的所述散热表面为一不平整的表面,所述盖组件至少包括一面向所述散热表面的进气口,以向所述流通间隙内填充导热气体。The heat dissipation surface of the top plate is an uneven surface, and the cover assembly at least includes an air inlet facing the heat dissipation surface, so as to fill the flow gap with heat conducting gas.
  3. 根据权利要求2所述的成膜装置,其特征在于,在所述散热表面上形成有靠近所述顶板的中心的第一环形区域,所述顶板在所述第一环形区域与所述冷却表面之间形成所述流通间隙的第一间隙;The film forming device according to claim 2, wherein a first annular area close to the center of the top plate is formed on the heat dissipation surface, and the top plate is between the first annular area and the cooling surface. forming a first gap between said flow gaps;
    在所述第一环形区域内设置有多个整流块,多个所述整流块环绕所述中心且间隔设置。A plurality of rectifying blocks are arranged in the first annular area, and the plurality of rectifying blocks surround the center and are arranged at intervals.
  4. 根据权利要求3所述的成膜装置,其特征在于,所述第一环形区域包括沿着所述顶板的中心向所述顶板的边缘方向依次分布的内环形区、中间环形区和外环形区;The film forming device according to claim 3, wherein the first annular area includes an inner annular area, a middle annular area and an outer annular area distributed sequentially along the center of the top plate toward the edge of the top plate ;
    所述整流块呈辐射状设置于所述中间环形区内;The rectifying blocks are arranged radially in the middle annular area;
    在水平投影面内,所述进气口位于所述内环形区。In the horizontal projection plane, the air inlet is located in the inner annular area.
  5. 根据权利要求4所述的成膜装置,其特征在于,相邻两个所述整流块之间形成有气流通道,所述第一圆周位于所述中间环形区内,在所述第一圆周上具有不同高度的所述流通间隙包括所述整流块处的流通间隙和所述气流通道处的流通间隙。The film-forming device according to claim 4, wherein an air flow channel is formed between two adjacent rectifying blocks, the first circumference is located in the middle annular region, and on the first circumference The flow gaps having different heights include a flow gap at the rectifying block and a flow gap at the airflow channel.
  6. 根据权利要求4所述的成膜装置,其特征在于,相邻两个所述整流块之间形成有气流通道,所述气流通道靠近所述进气口处的分布密度小于所述气流通道远离所述进气口处的分布密度。The film forming device according to claim 4, wherein an air flow channel is formed between two adjacent rectifying blocks, and the distribution density of the air flow channel near the air inlet is smaller than that of the air flow channel far away from the air inlet. The distribution density at the inlet.
  7. 根据权利要求3所述的成膜装置,其特征在于,相邻两个所述整流块之间形成有气流通道,所述气流通道在所述第一环形区域的周向上的宽度相等,多个所述整流块的高度均小于所述第一间隙的高度,所述整流块与所述冷却表面之间的距离小于相邻两个所述整流块之间的气流通道的宽度,所述第一间隙的高度的取值范围为:3mm~6mm。The film forming device according to claim 3, characterized in that, an airflow channel is formed between two adjacent rectifying blocks, and the width of the airflow channel in the circumferential direction of the first annular region is equal, and a plurality of The heights of the rectifying blocks are all smaller than the height of the first gap, the distance between the rectifying blocks and the cooling surface is smaller than the width of the airflow channel between two adjacent rectifying blocks, and the first The value range of the height of the gap is: 3mm~6mm.
  8. 根据权利要求3~7中任一项所述的成膜装置,其特征在于,所述散热表面还包括依次位于所述第一环形区域的径向外侧的第二环形区域、第三环形区域和第四环形区域;The film forming device according to any one of claims 3 to 7, wherein the heat dissipation surface further comprises a second annular area, a third annular area and a The fourth ring area;
    所述第二环形区域与所述冷却表面之间形成所述流通间隙的第二间隙;a second gap forming the flow gap between the second annular region and the cooling surface;
    所述第三环形区域与所述冷却表面之间形成所述流通间隙的第三间隙;a third gap forming the flow gap between the third annular region and the cooling surface;
    所述第四环形区域与所述冷却表面之间形成所述流通间隙的第四间隙;a fourth gap forming the flow gap between the fourth annular region and the cooling surface;
    其中,所述第二间隙的高度小于所述第一间隙的高度、所述第三间隙的高度和所述第四间隙的高度;Wherein, the height of the second gap is smaller than the height of the first gap, the height of the third gap and the height of the fourth gap;
    所述基座上设有凹槽,所述凹槽用于容置所述基片,所述加热装置的直接加热区域至少部分覆盖所述凹槽;A groove is provided on the base, the groove is used to accommodate the substrate, and the direct heating area of the heating device at least partially covers the groove;
    在水平投影面内,所述第二环形区域的至少一部分与所述凹槽重合。In a horizontal projection plane, at least a part of the second annular area coincides with the groove.
  9. 根据权利要求8所述的成膜装置,其特征在于,在所述流通间隙的高度方向上,所述凹槽的中心和所述第二环形区域在径向方向上的中间位置共线,所述第二间隙的高度的取值范围为:0.1mm~0.5mm。The film forming device according to claim 8, characterized in that, in the height direction of the flow gap, the center of the groove and the middle position of the second annular region in the radial direction are collinear, so The value range of the height of the second gap is: 0.1mm~0.5mm.
  10. 根据权利要求8所述的成膜装置,其特征在于,在水平投影面内,所述基座包括被所述加热装置的直接加热区域覆盖的第一区域和位于第一加热区域之外的第二区域,所述第三环形区域与所述第二区域至少部分重合,所述第三间隙的高度的取值范围为:1.5mm~3mm。The film forming device according to claim 8, wherein, in the horizontal projection plane, the base includes a first area covered by the direct heating area of the heating device and a second area outside the first heating area. In the second area, the third annular area at least partially overlaps with the second area, and the range of the height of the third gap is: 1.5mm~3mm.
  11. 根据权利要求9所述的成膜装置,其特征在于,所述第四间隙的高度的取值范围为:2mm~5mm。The film forming device according to claim 9, wherein the value range of the height of the fourth gap is: 2mm~5mm.
PCT/CN2022/125287 2021-11-24 2022-10-14 Film-forming device WO2023093351A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN202111404102.6 2021-11-24
CN202111404102.6A CN115838917A (en) 2021-11-24 2021-11-24 Film forming apparatus

Publications (1)

Publication Number Publication Date
WO2023093351A1 true WO2023093351A1 (en) 2023-06-01

Family

ID=85574599

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/CN2022/125287 WO2023093351A1 (en) 2021-11-24 2022-10-14 Film-forming device

Country Status (2)

Country Link
CN (1) CN115838917A (en)
WO (1) WO2023093351A1 (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11180796A (en) * 1997-12-22 1999-07-06 Japan Energy Corp Vapor growth method and vapor growth device for applying the same
CN101631901A (en) * 2007-02-24 2010-01-20 艾克斯特朗股份公司 Device and method for selectively depositing crystalline layers using MOCVD or HVPE
CN102428216A (en) * 2009-03-16 2012-04-25 艾克斯特朗欧洲公司 MOCVD reactor having a ceiling panel coupled locally differently to a heat dissipation member
TW202000964A (en) * 2018-06-21 2020-01-01 漢民科技股份有限公司 Reaction chamber for vapor deposition apparatus
CN112969815A (en) * 2018-09-07 2021-06-15 艾克斯特朗欧洲公司 Method for regulating the top temperature of a CVD reactor

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH11180796A (en) * 1997-12-22 1999-07-06 Japan Energy Corp Vapor growth method and vapor growth device for applying the same
CN101631901A (en) * 2007-02-24 2010-01-20 艾克斯特朗股份公司 Device and method for selectively depositing crystalline layers using MOCVD or HVPE
CN102428216A (en) * 2009-03-16 2012-04-25 艾克斯特朗欧洲公司 MOCVD reactor having a ceiling panel coupled locally differently to a heat dissipation member
TW202000964A (en) * 2018-06-21 2020-01-01 漢民科技股份有限公司 Reaction chamber for vapor deposition apparatus
CN112969815A (en) * 2018-09-07 2021-06-15 艾克斯特朗欧洲公司 Method for regulating the top temperature of a CVD reactor

Also Published As

Publication number Publication date
CN115838917A (en) 2023-03-24

Similar Documents

Publication Publication Date Title
KR101645262B1 (en) Gas dispersion apparatus
US11441236B2 (en) Chamber components for epitaxial growth apparatus
TWI612171B (en) Chemical vapor deposition device and deposition method thereof
JP2011500961A (en) Chemical vapor deposition reactor
WO2021238955A1 (en) Heating apparatus and semiconductor processing device
KR20140050682A (en) Methods and apparatus for the deposition of materials on a substrate
US20120108081A1 (en) Apparatus having improved substrate temperature uniformity using direct heating methods
US20160068959A1 (en) Atmospheric epitaxial deposition chamber
WO2021175089A1 (en) Reaction chamber
WO2016036868A1 (en) Atmospheric epitaxial deposition chamber
WO2020232602A1 (en) Carrier plate, growth device and growth method for growing thin film on substrate
TWI754765B (en) Inject assembly for epitaxial deposition processes
JP4855029B2 (en) Semiconductor crystal growth equipment
WO2023093351A1 (en) Film-forming device
US9267205B1 (en) Fastener system for supporting a liner plate in a gas showerhead reactor
JP3665672B2 (en) Film forming apparatus and film forming method
CN114540947B (en) Process chamber and semiconductor processing equipment
US20220093362A1 (en) Showerhead assembly with recursive gas channels
JP2023533400A (en) epitaxial growth equipment
CN117604494B (en) Chemical vapor deposition equipment
WO2020258676A1 (en) Graphite carrier and mocvd reaction apparatus having same
CN117604494A (en) Chemical vapor deposition equipment
CN117684262B (en) Gas injection device and gas phase reaction equipment
WO2022252709A1 (en) Epitaxial growth device
JP7417722B2 (en) Heating element for epitaxial growth equipment

Legal Events

Date Code Title Description
121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 22897434

Country of ref document: EP

Kind code of ref document: A1