WO2022250797A3 - Nanocomposite aerogel - Google Patents

Nanocomposite aerogel Download PDF

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Publication number
WO2022250797A3
WO2022250797A3 PCT/US2022/024363 US2022024363W WO2022250797A3 WO 2022250797 A3 WO2022250797 A3 WO 2022250797A3 US 2022024363 W US2022024363 W US 2022024363W WO 2022250797 A3 WO2022250797 A3 WO 2022250797A3
Authority
WO
WIPO (PCT)
Prior art keywords
nanocomposite aerogel
aerogel
nanocomposite
sensors
conductive
Prior art date
Application number
PCT/US2022/024363
Other languages
French (fr)
Other versions
WO2022250797A2 (en
Inventor
Nasrullah SHAH
Dong Lin
Halil TETIK
Original Assignee
Kansas State University Research Foundation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kansas State University Research Foundation filed Critical Kansas State University Research Foundation
Publication of WO2022250797A2 publication Critical patent/WO2022250797A2/en
Publication of WO2022250797A3 publication Critical patent/WO2022250797A3/en

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/20Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
    • B01J20/205Carbon nanostructures, e.g. nanotubes, nanohorns, nanocones, nanoballs
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/24Naturally occurring macromolecular compounds, e.g. humic acids or their derivatives
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004Sorbent size or size distribution, e.g. particle size
    • B01J20/28007Sorbent size or size distribution, e.g. particle size with size in the range 1-100 nanometers, e.g. nanosized particles, nanofibers, nanotubes, nanowires or the like
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28011Other properties, e.g. density, crush strength
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28026Particles within, immobilised, dispersed, entrapped in or on a matrix, e.g. a resin
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28047Gels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28088Pore-size distribution
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/282Porous sorbents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/3085Chemical treatments not covered by groups B01J20/3007 - B01J20/3078

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)

Abstract

A biocompatible nanocomposite aerogel is provided that is relatively non- conductive in its dry form, but rendered conductive when wetted or moistened, making it suitable for use in a variety of sensors, including vapor sensors. The high porosity of the nanocomposite aerogel also renders it a good adsorbent for purposes such as environmental remediation of pollutants.
PCT/US2022/024363 2021-04-13 2022-04-12 Nanocomposite aerogel WO2022250797A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US202163174147P 2021-04-13 2021-04-13
US63/174,147 2021-04-13

Publications (2)

Publication Number Publication Date
WO2022250797A2 WO2022250797A2 (en) 2022-12-01
WO2022250797A3 true WO2022250797A3 (en) 2023-03-09

Family

ID=84230375

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2022/024363 WO2022250797A2 (en) 2021-04-13 2022-04-12 Nanocomposite aerogel

Country Status (1)

Country Link
WO (1) WO2022250797A2 (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050029191A1 (en) * 2001-10-12 2005-02-10 Bo Mattiasson Separation medium, its preparation and its use
KR101670181B1 (en) * 2015-08-03 2016-10-27 인천대학교 산학협력단 Preparation method of dopaminemelanin films for humidity sensor
CN107365427A (en) * 2017-03-21 2017-11-21 李阳阳 A kind of method that Frozen-thawed cycled method prepares aeroge
CN110339787A (en) * 2018-04-08 2019-10-18 中国科学院苏州纳米技术与纳米仿生研究所 A kind of gas-solid-liquid three-phase gel, preparation method and application

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050029191A1 (en) * 2001-10-12 2005-02-10 Bo Mattiasson Separation medium, its preparation and its use
KR101670181B1 (en) * 2015-08-03 2016-10-27 인천대학교 산학협력단 Preparation method of dopaminemelanin films for humidity sensor
CN107365427A (en) * 2017-03-21 2017-11-21 李阳阳 A kind of method that Frozen-thawed cycled method prepares aeroge
CN110339787A (en) * 2018-04-08 2019-10-18 中国科学院苏州纳米技术与纳米仿生研究所 A kind of gas-solid-liquid three-phase gel, preparation method and application

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
ALAM MD NUR, ISLAM MD. SHAHIDUL, CHRISTOPHER LEW P.: "Sustainable Production of Cellulose-Based Hydrogels with Superb Absorbing Potential in Physiological Saline", ACS OMEGA, ACS PUBLICATIONS, US, vol. 4, no. 5, 31 May 2019 (2019-05-31), US , pages 9419 - 9426, XP093043600, ISSN: 2470-1343, DOI: 10.1021/acsomega.9b00651 *
IEAMVITEEVANICH PIMCHANOK, PALAPORN DULYAWICH, CHANLEK NARONG, POO-ARPORN YINGYOT, MONGKOLTHANARUK WIYADA, EICHHORN STEPHEN J., PI: "Carbon Nanofiber Aerogel/Magnetic Core–Shell Nanoparticle Composites as Recyclable Oil Sorbents", ACS APPLIED NANO MATERIALS, vol. 3, no. 4, 24 April 2020 (2020-04-24), pages 3939 - 3950, XP093043602, ISSN: 2574-0970, DOI: 10.1021/acsanm.0c00818 *
YANG YUTONG, SU GUOTING, LI QILIN, ZHU ZIPIAO, LIU SHAORAN, ZHUO BING, LI XINPU, TI PU, YUAN QUANPING: "Performance of the highly sensitive humidity sensor constructed with nanofibrillated cellulose/graphene oxide/polydimethylsiloxane aerogel via freeze drying", RSC ADVANCES, vol. 11, no. 3, 5 January 2021 (2021-01-05), pages 1543 - 1552, XP093043603, DOI: 10.1039/D0RA08193K *
YEHONG CHENG, SHANBAO ZHOU, PING HU, GUANGDONG ZHAO, YONGXIA LI, XINGHONG ZHANG, WENBO HAN: "Enhanced mechanical, thermal, and electric properties of graphene aerogels via supercritical ethanol drying and high-temperature thermal reduction", SCIENTIFIC REPORTS, vol. 7, no. 1, 1 December 2017 (2017-12-01), XP055636084, DOI: 10.1038/s41598-017-01601-x *

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Publication number Publication date
WO2022250797A2 (en) 2022-12-01

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