WO2021198613A1 - Kit pour l'obtention d'une couche de sol de batiment - Google Patents
Kit pour l'obtention d'une couche de sol de batiment Download PDFInfo
- Publication number
- WO2021198613A1 WO2021198613A1 PCT/FR2021/050561 FR2021050561W WO2021198613A1 WO 2021198613 A1 WO2021198613 A1 WO 2021198613A1 FR 2021050561 W FR2021050561 W FR 2021050561W WO 2021198613 A1 WO2021198613 A1 WO 2021198613A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- component
- layer
- weight
- acrylate
- soil
- Prior art date
Links
- 239000002689 soil Substances 0.000 title claims abstract description 39
- 239000004014 plasticizer Substances 0.000 claims abstract description 26
- 229920000642 polymer Polymers 0.000 claims abstract description 26
- 239000006185 dispersion Substances 0.000 claims abstract description 23
- 239000000203 mixture Substances 0.000 claims abstract description 18
- 230000009477 glass transition Effects 0.000 claims abstract description 16
- 239000000843 powder Substances 0.000 claims abstract description 16
- 239000011230 binding agent Substances 0.000 claims abstract description 14
- 239000012071 phase Substances 0.000 claims abstract description 11
- 229920001971 elastomer Polymers 0.000 claims abstract description 9
- 239000005060 rubber Substances 0.000 claims abstract description 9
- 150000001252 acrylic acid derivatives Chemical class 0.000 claims abstract description 8
- 239000012074 organic phase Substances 0.000 claims abstract description 6
- FEIQOMCWGDNMHM-UHFFFAOYSA-N 5-phenylpenta-2,4-dienoic acid Chemical class OC(=O)C=CC=CC1=CC=CC=C1 FEIQOMCWGDNMHM-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000010410 layer Substances 0.000 claims description 57
- 239000004570 mortar (masonry) Substances 0.000 claims description 24
- 229920000058 polyacrylate Polymers 0.000 claims description 22
- NJVOHKFLBKQLIZ-UHFFFAOYSA-N (2-ethenylphenyl) prop-2-enoate Chemical compound C=CC(=O)OC1=CC=CC=C1C=C NJVOHKFLBKQLIZ-UHFFFAOYSA-N 0.000 claims description 17
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 14
- 238000013016 damping Methods 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 7
- 239000000758 substrate Substances 0.000 claims description 6
- 238000004078 waterproofing Methods 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 3
- 239000012790 adhesive layer Substances 0.000 claims description 2
- 230000005540 biological transmission Effects 0.000 claims description 2
- 239000004568 cement Substances 0.000 description 6
- 239000000853 adhesive Substances 0.000 description 5
- 230000001070 adhesive effect Effects 0.000 description 5
- 230000006872 improvement Effects 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 3
- 239000011398 Portland cement Substances 0.000 description 3
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- JEYLQCXBYFQJRO-UHFFFAOYSA-N 2-[2-[2-(2-ethylbutanoyloxy)ethoxy]ethoxy]ethyl 2-ethylbutanoate Chemical compound CCC(CC)C(=O)OCCOCCOCCOC(=O)C(CC)CC JEYLQCXBYFQJRO-UHFFFAOYSA-N 0.000 description 2
- 235000019738 Limestone Nutrition 0.000 description 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- 239000011324 bead Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000001747 exhibiting effect Effects 0.000 description 2
- 239000010881 fly ash Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 239000002893 slag Substances 0.000 description 2
- 229920003048 styrene butadiene rubber Polymers 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 150000003505 terpenes Chemical class 0.000 description 2
- 235000007586 terpenes Nutrition 0.000 description 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- JLBJTVDPSNHSKJ-UHFFFAOYSA-N 4-Methylstyrene Chemical compound CC1=CC=C(C=C)C=C1 JLBJTVDPSNHSKJ-UHFFFAOYSA-N 0.000 description 1
- 229920005789 ACRONAL® acrylic binder Polymers 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 description 1
- 239000001692 EU approved anti-caking agent Substances 0.000 description 1
- 229920000463 Poly(ethylene glycol)-block-poly(propylene glycol)-block-poly(ethylene glycol) Polymers 0.000 description 1
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 1
- 239000004141 Sodium laurylsulphate Substances 0.000 description 1
- FRQDZJMEHSJOPU-UHFFFAOYSA-N Triethylene glycol bis(2-ethylhexanoate) Chemical compound CCCCC(CC)C(=O)OCCOCCOCCOC(=O)C(CC)CCCC FRQDZJMEHSJOPU-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000004026 adhesive bonding Methods 0.000 description 1
- 239000004964 aerogel Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- 235000011116 calcium hydroxide Nutrition 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000000113 differential scanning calorimetry Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- VICYBMUVWHJEFT-UHFFFAOYSA-N dodecyltrimethylammonium ion Chemical compound CCCCCCCCCCCC[N+](C)(C)C VICYBMUVWHJEFT-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000004794 expanded polystyrene Substances 0.000 description 1
- -1 for example Chemical class 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000009499 grossing Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000006028 limestone Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000010451 perlite Substances 0.000 description 1
- 235000019362 perlite Nutrition 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000011505 plaster Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 229920001451 polypropylene glycol Polymers 0.000 description 1
- 238000010944 pre-mature reactiony Methods 0.000 description 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 229910021487 silica fume Inorganic materials 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000019333 sodium laurylsulphate Nutrition 0.000 description 1
- 238000004611 spectroscopical analysis Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 150000003440 styrenes Chemical class 0.000 description 1
- 125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 239000013008 thixotropic agent Substances 0.000 description 1
- 229920000428 triblock copolymer Polymers 0.000 description 1
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical class OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
- 239000010455 vermiculite Substances 0.000 description 1
- 235000019354 vermiculite Nutrition 0.000 description 1
- 229910052902 vermiculite Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/06—Aluminous cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
- C04B24/24—Macromolecular compounds
- C04B24/26—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C04B24/2641—Polyacrylates; Polymethacrylates
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/021—Ash cements, e.g. fly ash cements ; Cements based on incineration residues, e.g. alkali-activated slags from waste incineration ; Kiln dust cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/04—Portland cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/06—Aluminous cements
- C04B28/065—Calcium aluminosulfate cements, e.g. cements hydrating into ettringite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/08—Slag cements
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D125/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
- C09D125/02—Homopolymers or copolymers of hydrocarbons
- C09D125/04—Homopolymers or copolymers of styrene
- C09D125/08—Copolymers of styrene
- C09D125/14—Copolymers of styrene with unsaturated esters
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2103/00—Function or property of ingredients for mortars, concrete or artificial stone
- C04B2103/0045—Polymers chosen for their physico-chemical characteristics
- C04B2103/0065—Polymers characterised by their glass transition temperature (Tg)
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00482—Coating or impregnation materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00482—Coating or impregnation materials
- C04B2111/00491—Primers
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/2038—Resistance against physical degradation
- C04B2111/2046—Shock-absorbing materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/52—Sound-insulating materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/60—Flooring materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/91—Use of waste materials as fillers for mortars or concrete
Definitions
- Kit for obtaining a layer of building soil The invention relates to the field of building floors, in particular for residential, commercial, industrial or tertiary use.
- Floor layers in particular interior layers, are layers generally deposited on top of a floor substrate, such as a slab or screed, and under a finishing floor covering (for example a tile, a parquet, a carpet).
- Floor layers can have several alternative or cumulative functions: they can be used in particular to fill a thickness, to fix the finishing floor covering (for example gluing a tile), to ensure the waterproofing, or to dampen the noise of the floor. 'impact.
- the soil layers must also meet stringent requirements in terms of mechanical strength (particularly in terms of resistance to compression, bending, wear or impact), so as to withstand the stresses exerted by people, furniture etc ...
- Floor layers are frequently based on cementitious materials which, by their rigid and dense nature, are known to transmit impact noise, at least when they are applied to thicknesses admissible in the field of construction of buildings.
- An object of the invention is to provide a layer of soil based on mortar comprising a hydraulic binder. exhibiting by themselves, therefore without requiring the addition of an acoustic underlayer, acoustic properties, in particular in terms of impact sound insulation.
- the invention relates to a kit for obtaining a layer of building soil, comprising:
- component A which is a powder mixture comprising a hydraulic binder and aggregates, including rubber powder, and
- a component B which is an aqueous dispersion comprising a dispersed organic phase comprising a polymer chosen from acrylates and styrene-acrylates or a mixture of two or more of these polymers, and optionally tackifiers and / or plasticizers, the temperature of glass transition of the phase consisting of said polymer or mixture of polymers and any tackifiers and / or plasticizers being less than or equal to -5 ° C.
- Another object of the invention is a process for obtaining a layer of building floor, in which the components A and B of the kit are mixed to form a paste, then said paste is applied to an element of said floor, in particular on a slab, a screed or a floor surface to be restored.
- Another object of the invention is also a layer of hardened mortar building soil comprising at least one hydraulic binder and aggregates, said hardened mortar exhibiting, at a temperature of 20 ° C and for at least a frequency of between 100 and 1000 Hz, a dynamic shear modulus G 'of at most 70 MPa and a loss factor tand of at least 0.30.
- the soil layer is in particular obtained or capable of being obtained by the process of the invention.
- the hardened mortar preferably comprises at least one polymer, in particular chosen from acrylates and styrene-acrylates.
- the layer of hardened mortar soil is preferably obtained from the kit of the invention and / or by the process of the invention.
- the following details concerning the composition of the kit preferably also apply to the soil layer according to the invention, in the sense that the ingredients of one or other of the components of the kit will be found in the soil layer. .
- contents indicated are always contents by weight.
- a content of a component in a given component or product is expressed relative to the weight, respectively, of that component or product.
- Component A is a powder mixture, in particular of the ready-to-mix dry mortar type.
- the hydraulic binder of component A or of the soil layer is preferably chosen from Portland cements, aluminous cements, sulphoaluminous cements, hydrated lime, ground granulated blast furnace slags, fly ash and mixtures of two or more of these binders.
- Portland cements cover CEM I and CEM II type cements as defined by standard EN 197-1.
- a CEM I cement comprises at least 95% clinker while a CEM II cement comprises at least 65% of clinker and at most 35% of blast furnace slag, silica fume, pozzolan, fly ash, calcined shale and / or limestone.
- the aggregates of component A or of the soil layer are preferably chosen from siliceous and / or carbonate aggregates, in particular silica sands, limestones and crushed dolomites.
- the aggregates can also comprise light aggregates chosen from perlite, vermiculite, expanded glass beads, beads. expanded polystyrene, cenospheres, expanded silicates, aerogels and mixtures thereof.
- component A comprises rubber powder, in particular in a weight content of at least 5% by weight, in particular between 7 and 20%, relative to the weight of component A.
- This powder is part of the aggregate.
- the soil layer therefore preferably comprises rubber powder, in particular in a content of at least 1% by weight, in particular between 2 and 10% by weight, relative to the weight of the soil layer.
- the rubber powder preferably has a particle size distribution by volume such that the D50 is between 80 and 160 ⁇ m, in particular between 100 and 150 ⁇ m.
- the D90 is preferably less than 250 ⁇ m, in particular less than 180 ⁇ m.
- the total content of hydraulic binder in component A is preferably between 5 and 30% by weight.
- the total aggregate content in component A is preferably between 50 and 90% by weight. These contents are indicated relative to the weight of component A.
- the total hydraulic binder content in the hardened mortar of the soil layer is preferably between 2 and 20%, in particular between 3 and 15% by weight.
- the total aggregate content in the hardened mortar of the soil layer is preferably between 15 and 60%, in particular between 20 and 50% by weight. These contents are indicated in relation to the weight of the soil layer.
- acrylate polymer means in particular a polymer obtained from monomers chosen from acrylic acid, acrylate salts and / or acrylate esters.
- the acrylate esters are preferably esters of C1-C10 alcohols.
- styrene-acrylate polymer is understood to mean in particular a copolymer of styrene (or of styrene derivatives, such as, for example, methylstyrene) and of acrylate monomers as defined above.
- the hardened mortar of the soil layer therefore preferably comprises such a polymer.
- the total acrylate and styrene-acrylate polymer content in the hardened mortar of the soil layer is preferably between 9 and 50% by weight, in particular between 15 and 35% by weight.
- the acrylate or styrene-acrylate polymers in the aqueous dispersion are preferably in the form of particles, the size of which is preferably between 0.1 and 100 ⁇ m, in particular between 0.15 and 50 ⁇ m, or even between 0.2 and 2 ym.
- size is understood to mean the number-average equivalent diameter, for example determined by laser diffraction spectroscopy.
- the aqueous dispersion (component B) is preferably an emulsion in which the organic phase is stabilized by an emulsifying agent, in particular a surfactant.
- the surfactant can be nonionic (for example based on polyethylene oxide - PEO - or on polypropylene oxide - PPO, including their triblock copolymer derivatives of the PEO-PPO-PEO type), anionic (for example salts of sulphates or sulphonates such as sodium lauryl sulphate) or else cationic (for example quaternary ammonium salts such as dodecyltrimethylammonium or hexadecyltrimethylammonium bromide).
- the total acrylate and styrene-acrylate polymer content in component B is preferably between 25 and 75% by weight, in particular between 35 and 65% by weight, or even between 45 and 60% by weight. Too high a concentration leads to too viscous a dispersion, while high dilutions lead to a reduction in acoustic performance.
- acrylate or styrene-acrylate polymers can be used in the present invention. Mention may in particular be made of dispersions sold under the reference Acronal® by the company BASF, or under the reference Encor® by the company Arkema, or alternatively under the reference Revacryl® by the company Synthomer.
- Component B and / or component A, and therefore the hardened mortar preferably comprises tackifiers and / or plasticizers, in order to adjust the vibration damping as well as the position of the damping peak on the frequency of interest. .
- component B which constitutes a preferred embodiment. They can alternatively be in powder form, obtained for example by atomization, and in this case be added to component A.
- the or each tackifier is preferably chosen from natural tackifying resins (for example rosins, rosin derivatives, such as hydrogenated rosins, terpenes) and synthetic tackifying resins (for example aliphatic, aromatic and hydrogenated resins derived from petroleum. ).
- the tackifier used is a rosin and / or a terpene, in particular in the form of a dispersion and / or a powder. Mention may in particular be made of the products Dermulsene® (A7510, RE1513, TR602, etc.), Dertoline®, Staybelite®, Forai®,
- the plasticizer makes it possible to shift the glass transition temperature (Tg) of the material constituting the soil layer towards lower temperatures, in other words towards higher frequencies.
- Tg glass transition temperature
- the plasticizer used is a derivative of triethylene glycol. It may be, for example, triethylene glycol bis (2-ethylbutyrate) known under the trade name 3GH, or triethylene glycol bis (2-ethylhexanoate) known under the name 3G8.
- the total weight content of tackifier in component B is preferably between 0.5 and 40%, in particular between 2 and 20%, or even between 3 and 15%, relative to the weight of dry matter.
- the total weight content of tackifier in the hardened mortar of the soil layer is then preferably between 0.2 and 25%, in particular between 5 and 15%, or even between 8 and 10%.
- the total weight content of plasticizer in component B is preferably between 0.5 and 20%, in particular between 1 and 10%, or even between 2 and 8%, relative to the weight of dry matter.
- the total weight content of plasticizer in the hardened mortar of the soil layer is then preferably between 0.2 and 15%, in particular between 0.5 and 8%, or even between 1 and 6%.
- the phase whose glass transition temperature is measured is the phase, in component B, consisting of the acrylate or styrene-acrylate polymer or of the mixture of such polymers and, when such compounds are present in component B, tackifiers and / or plasticizers.
- component B is an aqueous dispersion of a single acrylate or styrene-acrylate polymer, with no added tackifier or plasticizer.
- the glass transition temperature to be considered corresponds to the glass transition temperature of said polymer.
- component B is an aqueous dispersion comprising at least two polymers selected from acrylates and styrene-acrylates, without the addition of tackifier or plasticizer. In this case, the glass transition temperature to be considered corresponds to the glass transition temperature of the mixture of these polymers.
- the glass transition temperature to be considered corresponds to the glass transition temperature of the mixture consisting of the acrylate or styrene-acrylate polymer (s) and the tackifiers and / or plasticizers.
- the glass transition temperature of the phase to be considered is preferably less than or equal to - 10 ° C, and even at -20 ° C, or even at -30 ° C or -40 ° C. It is preferably greater than or equal to -100 ° C.
- Such a glass transition temperature has proved to be advantageous for obtaining good absorption of impact noise by conferring a viscoelastic character on the hardened mortar.
- the glass transition temperature of the phase to be considered is determined by differential scanning calorimetry (DSC) between -100 ° C and 120 ° C with a heating rate of 20 ° C per minute. The determination is made from the curve obtained using the tangent method, taking the point of intersection with the curve of the bisector of the tangents to the curve. The measurement is carried out on the phase to be considered, obtained after drying the aqueous dispersion.
- DSC differential scanning calorimetry
- the respective mass proportions of component A and of component B preferably vary from 30:70 to 70:30, in particular from 40:60 to 60:40, or even from 45:55 to 55:45.
- Component A and / or component B can also comprise at least one additive chosen from setting retarders, setting accelerators, rheological agents (in particular thickening or thixotropic agents), dispersing agents, leveling agents, retention agents. water, anti-caking agents, plasticizers or superplasticizers.
- the hardened mortar has, at a temperature of 20 ° C and for at least one frequency between 100 and 1000 Hz, and advantageously for any frequency between 100 and 1000, at least one of the following characteristics: a module dynamic shear G 'of at most 70 MPa, in particular at most 60 MPa, and even at most 50 MPa, in particular at most 40 MPa, or even at most 30 MPa,
- tano loss factor of at least 0.30, in particular of at least 0.33, or even of at least 0.35.
- G ' corresponds to the real part of the complex shear modulus. It is also called “modulus of conservation in shear”.
- the tano loss factor (also called the damping factor) is equal to the ratio between G '' and G ', the quantity G' ', called “shear loss modulus”, corresponding to the imaginary part of the complex shear modulus .
- the kit according to the invention generally consists of component A and component B; it is then a two-component kit.
- the two components of the kit are normally physically separated in order to avoid any premature reaction between them.
- the kit can for example include two containers separate each containing one of the components A or B.
- the kit can also comprise a container comprising two separate compartments each containing one of the components A or B.
- the kit can for example be sold in the form of a bucket containing two plastic bags each containing one of the components. The two bags can then be emptied into the bucket for mixing in the latter.
- Component B usually contains the amount of water required for mixing, but it is of course possible to add water if necessary.
- components A and B generally takes place on site, for example manually or by means of a mixer in order to obtain a paste which will then be applied to the soil substrate to be coated, for example a screed.
- the application can be carried out in a known manner by means of a brush, a roller or a brush, a spatula, a Flemish plaster, a trowel, a smoothing machine or even by spraying .
- a subject of the invention is also a floor comprising a layer of soil according to the invention, in particular in the form of an adhesive layer and / or of a waterproofing layer and / or of an under-layer, said layer being interposed between a soil substrate. (such as for example a slab, a screed or a floor to be renovated) and a finishing floor covering.
- a layer of soil according to the invention in particular in the form of an adhesive layer and / or of a waterproofing layer and / or of an under-layer, said layer being interposed between a soil substrate. (such as for example a slab, a screed or a floor to be renovated) and a finishing floor covering.
- the floor finish covering is in particular of the tiling or parquet type, or even of PVC tiles, in particular rigid, that is to say hard coatings for which the damping of impact noise is particularly crucial.
- the thickness of the soil layer is preferably between 1 and 30 mm, in particular between 5 and 20 mm, or even between 8 and 15 mm.
- the floor comprises, between the floor substrate (in particular a screed) and the floor finishing coating, only the layer according to the invention. This layer therefore plays an adhesive role (for example of tile adhesive) in addition to ensuring the acoustic damping properties, and possibly other functions (sealing, leveling, flatness, etc.).
- the thickness of the layer is preferably between 5 and 15 mm.
- the floor comprises, from the substrate (in particular a screed), a layer according to the invention, a layer of adhesive (for example of tile adhesive or parquet adhesive), then the finishing coating of ground. The layer is then an underlayer with acoustic properties, and possibly a waterproofing layer.
- the thickness of the layer is preferably between 8 and 15 mm.
- a subject of the invention is the use of a layer of building soil as defined above for damping the transmission of impact noise.
- Layers of sol were obtained by mixing component A and component B, then depositing the paste obtained on a screed so as to form a layer 10 mm thick.
- the measurements on the hardened mortar were carried out after 28 days of hardening.
- component A was a dry mortar marketed by the Applicant under the reference weber.xerm 844.
- a dry mortar comprises as hydraulic binder Portland cement as well as aggregates, including rubber powder in a weight content of 10% relative to the weight of dry mortar.
- Component B was an aqueous dispersion comprising a dispersed organic phase.
- the organic phase consisted of a polymer, with in some cases the addition of plasticizer and tackifier.
- component B in the various examples was as follows:
- Example 1 dispersion comprising 65% by weight of an acrylate polymer having a glass transition temperature Tg of -55 ° C.
- Example 2 dispersion comprising 69% by weight of an acrylate polymer having a Tg of -40 ° C.
- Example 3 dispersion comprising 60% by weight of an acrylate polymer having a Tg of -38 ° C.
- Example 4 dispersion comprising 54% by weight of a styrene-acrylate polymer having a Tg of -30 ° C.
- Example 5 dispersion comprising 57% by weight of a styrene-acrylate polymer having a Tg of -8 ° C.
- Example 6 dispersion comprising 57% by weight of a styrene-acrylate polymer (having a Tg of -2 ° C.) with addition, for one part of polymer, of 0.1 part of plasticizer and of 0.3 part of tackifier.
- the Tg of the phase consisting of the polymer, the plasticizer and the tackifier was below -5 ° C.
- Example 7 dispersion of Example 5 with addition, for one part of polymer, of 0.1 part of plasticizer and 0.3 part of tackifier.
- Comparative Example C1 dispersion comprising 48% by weight of a styrene-butadiene elastomer having a Tg of - 16 ° C.
- Comparative example C2 dispersion comprising 57% by weight of a styrene-butadiene elastomer having a Tg of + 5 ° C.
- Comparative Example C3 dispersion of Example 6, but without tackifier or plasticizer.
- the plasticizer was triethylene glycol bis (2-ethylbutyrate).
- the tackifier was a rosin sold under the name Dermulsene® A7510 by the company DRT.
- Table 1 shows the results obtained by indicating the shear modulus G '(in MPa) and the loss factor tand, for the frequencies of 100 and 1000 Hz, as well as the improvement in noise at impact. AL W.
- the shear modulus and the loss factor were determined by temperature dynamic mechanical analysis (DMTA).
- DMTA temperature dynamic mechanical analysis
- the hardened mortar sample is subjected to a sinusoidal stress for frequencies ranging from 1 to 100 HZ in a temperature range from -40 ° C to 40 ° C with steps every 5 ° C.
- a master curve for the values of G 'and tand between 0.1 and 10,000 Hz can then be obtained by applying the theory of Williams-Landel-Ferry (WLF).
- the acoustic performances of the hardened mortar in this case the improvement in noise at impact AL W (expressed in dB) were determined by the method described in standard ISO 10140-3: 2010, but with samples of 2 , 5 m 2 .
- the tests were carried out on a system comprising, on a screed, a layer of soil 10 mm thick covered with a tiling.
- FIG. 1 shows the noise improvement curves on impact (denoted AL) as a function of the frequency (denoted f), in the range from 100 to 5000 Hz, for each of the examples.
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Combustion & Propulsion (AREA)
- Life Sciences & Earth Sciences (AREA)
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Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CH000961/2022A CH718816B1 (fr) | 2020-03-31 | 2021-03-30 | Kit pour l'obtention d'une couche de sol de bâtiment. |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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FR2003179A FR3108604B1 (fr) | 2020-03-31 | 2020-03-31 | Kit pour l’obtention d’une couche de sol de bâtiment |
FR2003179 | 2020-03-31 |
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WO2021198613A1 true WO2021198613A1 (fr) | 2021-10-07 |
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PCT/FR2021/050561 WO2021198613A1 (fr) | 2020-03-31 | 2021-03-30 | Kit pour l'obtention d'une couche de sol de batiment |
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CH (1) | CH718816B1 (forum.php) |
FR (1) | FR3108604B1 (forum.php) |
WO (1) | WO2021198613A1 (forum.php) |
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EP4385964A1 (en) * | 2022-12-15 | 2024-06-19 | Sika Technology AG | Cementitious hybrid primer composition |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2008035197A2 (en) * | 2006-09-22 | 2008-03-27 | Daniele Furin | A sound-proofing/heat insulating material and a process for production thereof |
FR3002772A1 (fr) * | 2013-03-01 | 2014-09-05 | Bostik Sa | Composition de colle bicomposante |
CN105753419A (zh) * | 2016-01-27 | 2016-07-13 | 佛山市佳密特防水材料有限公司 | 一种地面找平用快流平砂浆 |
FR3077828A1 (fr) * | 2018-02-14 | 2019-08-16 | Coformex | Composition pour surface sportive, notamment de sport equestre, et procede de fabrication d'une telle composition |
WO2020225300A1 (en) * | 2019-05-06 | 2020-11-12 | Sika Technology Ag | Mortar composition for acoustic damping and fire protection |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
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DE202005015351U1 (de) * | 2005-09-28 | 2005-12-08 | Maxit Deutschland Gmbh | Flexibles Baustoffsystem |
EP3233752B1 (en) * | 2014-12-19 | 2020-09-30 | Saint-Gobain Weber | Multicomponent adhesive system and its use as adhesive in building and construction |
-
2020
- 2020-03-31 FR FR2003179A patent/FR3108604B1/fr active Active
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2021
- 2021-03-30 CH CH000961/2022A patent/CH718816B1/fr not_active IP Right Cessation
- 2021-03-30 WO PCT/FR2021/050561 patent/WO2021198613A1/fr active Application Filing
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2008035197A2 (en) * | 2006-09-22 | 2008-03-27 | Daniele Furin | A sound-proofing/heat insulating material and a process for production thereof |
FR3002772A1 (fr) * | 2013-03-01 | 2014-09-05 | Bostik Sa | Composition de colle bicomposante |
CN105753419A (zh) * | 2016-01-27 | 2016-07-13 | 佛山市佳密特防水材料有限公司 | 一种地面找平用快流平砂浆 |
FR3077828A1 (fr) * | 2018-02-14 | 2019-08-16 | Coformex | Composition pour surface sportive, notamment de sport equestre, et procede de fabrication d'une telle composition |
WO2020225300A1 (en) * | 2019-05-06 | 2020-11-12 | Sika Technology Ag | Mortar composition for acoustic damping and fire protection |
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FR3108604B1 (fr) | 2022-07-22 |
CH718816B1 (fr) | 2024-02-15 |
CH718816A4 (forum.php) | 2022-12-01 |
FR3108604A1 (fr) | 2021-10-01 |
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