WO2021105721A1

WO2021105721A1 - An article for use in a non-combustible aerosol provision system

Info

Publication number: WO2021105721A1
Application number: PCT/GB2020/053063
Authority: WO
Inventors: Barry DIMMICK; Steven Holford
Original assignee: Nicoventures Trading Limited
Priority date: 2019-11-29
Filing date: 2020-11-27
Publication date: 2021-06-03
Also published as: US20230011768A1; JP2023504077A; IL293313A; JP2024029206A; KR20220103966A; AU2020392905A1; CN114901090A; AU2020392905B2; CA3159854A1; EP4064882A1; MX2022006477A; GB201917513D0; BR112022010459A2; JP7455208B2

Abstract

An article for use in a non-combustible aerosol provision system. The article comprising a mouthpiece comprising a body of material. The body comprises amorphous solid material. Also disclosed is a system comprising such an article and a non-combustible aerosol provision device for heating the aerosol generating material of the article, and a method of manufacturing such an article.

Description

An article for use in a non-combustible aerosol provision system Technical Field

The present invention relates to an article for use in a non-combustible aerosol provision system and a non-combustible aerosol provision system including an article.

Background

Smoking articles such as cigarettes, cigars and the like burn tobacco during use to create tobacco smoke. Alternative smoking articles produce an inhalable aerosol or vapour by releasing compounds from a substrate material without burning. These articles may be referred to as non-combustible smoking articles or aerosol provision systems. Such articles commonly include a mouthpiece through which the aerosol passes to reach the users mouth. Summary

A first aspect of the invention provides an article for use in a non-combustible aerosol provision system, the article comprising a mouthpiece comprising a body of material, wherein the body comprises amorphous solid material. A second aspect of the invention provides an article for use in a non-combustible aerosol provision system, comprising a mouthpiece according to the first aspect of the invention connected to a source of aerosol generating material.

A third aspect of the invention provides a non-combustible aerosol provision system comprising an article according to the second aspect of the invention and a non combustible aerosol provision device.

A fourth aspect of the invention provides a method for forming an article according to the first aspect of the invention.

Brief Description of the Drawings

Embodiments of the invention will now be described, by way of example only, with reference to the accompanying drawings, in which:

Figure l is a side-on, cross sectional view of an article for use with a non-combustible aerosol provision device, the article including a mouthpiece;

Figure 2 is a side-on cross sectional view of a further article for use with a non- combustible aerosol provision device, in this example the mouthpiece including a hollow tubular element;

Figure 3 is a side-on cross sectional view of a further article for use with a non combustible aerosol provision device, in this example the mouthpiece including a second hollow tubular element;

Figure 4 is a side-on cross sectional view of a further article for use with a non combustible aerosol provision device, in this example mouthpiece comprising a body of fibrous material;

Figure 5a is a side-on cross sectional view of a further article for use with a non- combustible aerosol provision device, in this example the article including a capsule- containing mouthpiece;

Figure 5b is a cross sectional view of the capsule-containing mouthpiece shown in Figure 5a;

Figure 6 is a perspective illustration of a non-combustible aerosol provision device for generating aerosol from the aerosol generating material of the articles of Figures 1, 2a and 2b and 3;

Figure 7 illustrates the device of Figure 6 with the outer cover removed and without an article present;

Figure 8 is a side view of the device of Figure 6 in partial cross-section; Figure 9 is an exploded view of the device of Figure 6, with the outer cover omitted; Figure 10A is a cross sectional view of a portion of the device of Figure 6;

Figure 10B is a close-up illustration of a region of the device of Figure 10A; and Figure 11 is a flow diagram illustrating a method of manufacturing an article for use with a non-combustible aerosol provision device. Figure 12 is a side view of an apparatus for producing a rod of the body of material according to the invention.

Detailed Description

As used herein, the term “delivery system” is intended to encompass systems that deliver at least one substance to a user, and includes: combustible aerosol provision systems, such as cigarettes, cigarillos, cigars, and tobacco for pipes or for roll-your-own or for make-your-own cigarettes (whether based on tobacco, tobacco derivatives, expanded tobacco, reconstituted tobacco, tobacco substitutes or other smokable material); non-combustible aerosol provision systems that release compounds from an aerosol-generating material without combusting the aerosol-generating material, such as electronic cigarettes, tobacco heating products, and hybrid systems to generate aerosol using a combination of aerosol-generating materials; and aerosol-free delivery systems that deliver the at least one substance to a user orally, nasally, transdermally or in another way without forming an aerosol, including but not limited to, lozenges, gums, patches, articles comprising inhalable powders, and oral products such as oral tobacco which includes snus or moist snuff, wherein the at least one substance may or may not comprise nicotine.

According to the present disclosure, a “combustible” aerosol provision system is one where a constituent aerosolisable material of the aerosol provision system (or component thereof) is combusted or burned in order to facilitate delivery to a user.

According to the present disclosure, a “non-combustible” aerosol provision system is one where a constituent aerosol-generating material of the aerosol provision system (or component thereof) is not combusted or burned in order to facilitate delivery of at least one substance to a user.

In embodiments described herein, the delivery system is a non-combustible aerosol provision system, such as a powered non-combustible aerosol provision system.

In some embodiments, the non-combustible aerosol provision system is an electronic cigarette, also known as a vaping device or electronic nicotine delivery system (END), although it is noted that the presence of nicotine in the aerosol-generating material is not a requirement.

In some embodiments, the non-combustible aerosol provision system is an aerosol generating material heating system, also known as a heat-not-burn system. An example of such a system is a tobacco heating system. In some embodiments, the non-combustible aerosol provision system is a hybrid system to generate aerosol using a combination of aerosol-generating materials, one or a plurality of which may be heated. Each of the aerosol-generating materials may be, for example, in the form of a solid, liquid or gel and may or may not contain nicotine.

In some embodiments, the hybrid system comprises a liquid or gel aerosol-generating material and a solid aerosol-generating material. The solid aerosol-generating material may comprise, for example, tobacco or a non-tobacco product. Typically, the non-combustible aerosol provision system may comprise a non combustible aerosol provision device and a consumable for use with the non combustible aerosol provision device.

In some embodiments, the disclosure relates to consumables comprising aerosol generating material and configured to be used with non-combustible aerosol provision devices. These consumables are sometimes referred to as articles throughout the disclosure.

In some embodiments, the non-combustible aerosol provision system, such as a non combustible aerosol provision device thereof, may comprise a power source and a controller. The power source may, for example, be an electric power source or an exothermic power source. In some embodiments, the exothermic power source comprises a carbon substrate which may be energised so as to distribute power in the form of heat to an aerosol-generating material or to a heat transfer material in proximity to the exothermic power source.

In some embodiments, the non-combustible aerosol provision system may comprise an area for receiving the consumable, an aerosol generator, an aerosol generation area, a housing, a mouthpiece, a filter and/ or an aerosol-modifying agent.

In some embodiments, the consumable for use with the non-combustible aerosol provision device may comprise aerosol-generating material, an aerosol-generating material storage area, an aerosol-generating material transfer component, an aerosol generator, an aerosol generation area, a housing, a wrapper, a filter, a mouthpiece, and/ or an aerosol-modifying agent.

In some embodiments, the substance to be delivered may be an aerosol-generating material or a material that is not intended to be aerosolised. As appropriate, either material may comprise one or more active constituents, one or more flavours, one or more aerosol-former materials, and/or one or more other functional materials. In some embodiments, the substance to be delivered comprises an active substance.

The active substance as used herein may be a physiologically active material, which is a material intended to achieve or enhance a physiological response. The active substance may for example be selected from nutraceuticals, nootropics, psychoactives. The active substance may be naturally occurring or synthetically obtained. The active substance may comprise for example nicotine, caffeine, taurine, theine, vitamins such as B6 or Bi2 or C, melatonin, cannabinoids, or constituents, derivatives, or combinations thereof. The active substance may comprise one or more constituents, derivatives or extracts of tobacco, cannabis or another botanical.

In some embodiments, the active substance comprises nicotine. In some embodiments, the active substance comprises caffeine, melatonin or vitamin B12. As noted herein, the active substance may comprise or be derived from one or more botanicals or constituents, derivatives or extracts thereof. As used herein, the term "botanical" includes any material derived from plants including, but not limited to, extracts, leaves, bark, fibres, stems, roots, seeds, flowers, fruits, pollen, husk, shells or the like. Alternatively, the material may comprise an active compound naturally existing in a botanical, obtained synthetically. The material may be in the form of liquid, gas, solid, powder, dust, crushed particles, granules, pellets, shreds, strips, sheets, or the like. Example botanicals are tobacco, eucalyptus, star anise, hemp, cocoa, cannabis, fennel, lemongrass, peppermint, spearmint, rooibos, chamomile, flax, ginger, ginkgo biloba, hazel, hibiscus, laurel, licorice (liquorice), matcha, mate, orange skin, papaya, rose, sage, tea such as green tea or black tea, thyme, clove, cinnamon, coffee, aniseed (anise), basil, bay leaves, cardamom, coriander, cumin, nutmeg, oregano, paprika, rosemary, saffron, lavender, lemon peel, mint, juniper, elderflower, vanilla, wintergreen, beefsteak plant, curcuma, turmeric, sandalwood, cilantro, bergamot, orange blossom, myrtle, cassis, valerian, pimento, mace, damien, marjoram, olive, lemon balm, lemon basil, chive, carvi, verbena, tarragon, geranium, mulberry, ginseng, theanine, theacrine, maca, ashwagandha, damiana, guarana, chlorophyll, baobab or any combination thereof. The mint maybe chosen from the following mint varieties: Mentha Arventis, Mentha c.v., Mentha niliaca, Mentha piperita, Mentha piperita citrata c.v., Mentha piperita c.v, Mentha spicata crispa, Mentha cardifolia, Memtha longifolia, Mentha suaveolens variegata, Mentha pulegium, Mentha spicata c.v. and Mentha suaveolens

In some embodiments, the active substance comprises or is derived from one or more botanicals or constituents, derivatives or extracts thereof and the botanical is tobacco. In some embodiments, the active substance comprises or derived from one or more botanicals or constituents, derivatives or extracts thereof and the botanical is selected from eucalyptus, star anise, cocoa and hemp.

In some embodiments, the active substance comprises or derived from one or more botanicals or constituents, derivatives or extracts thereof and the botanical is selected from rooibos and fennel.

In some embodiments, the substance to be delivered comprises a flavour. As used herein, the terms "flavour" and "flavourant" refer to materials which, where local regulations permit, maybe used to create a desired taste, aroma or other somatosensorial sensation in a product for adult consumers. They may include naturally occurring flavour materials, botanicals, extracts of botanicals, synthetically obtained materials, or combinations thereof (e.g., tobacco, cannabis, licorice (liquorice), hydrangea, eugenol, Japanese white bark magnolia leaf, chamomile, fenugreek, clove, maple, matcha, menthol, Japanese mint, aniseed (anise), cinnamon, turmeric, Indian spices, Asian spices, herb, wintergreen, cherry, berry, red berry, cranberry, peach, apple, orange, mango, clementine, lemon, lime, tropical fruit, papaya, rhubarb, grape, durian, dragon fruit, cucumber, blueberry, mulberry, citrus fruits, Drambuie, bourbon, scotch, whiskey, gin, tequila, rum, spearmint, peppermint, lavender, aloe vera, cardamom, celery, cascarilla, nutmeg, sandalwood, bergamot, geranium, khat, naswar, betel, shisha, pine, honey essence, rose oil, vanilla, lemon oil, orange oil, orange blossom, cherry blossom, cassia, caraway, cognac, jasmine, ylang- ylang, sage, fennel, wasabi, piment, ginger, coriander, coffee, hemp, a mint oil from any species of the genus Mentha, eucalyptus, star anise, cocoa, lemongrass, rooibos, flax, ginkgo biloba, hazel, hibiscus, laurel, mate, orange skin, rose, tea such as green tea or black tea, thyme, juniper, elderflower, basil, bay leaves, cumin, oregano, paprika, rosemary, saffron, lemon peel, mint, beefsteak plant, curcuma, cilantro, myrtle, cassis, valerian, pimento, mace, damien, marjoram, olive, lemon balm, lemon basil, chive, carvi, verbena, tarragon, limonene, thymol, camphene), flavour enhancers, bitterness receptor site blockers, sensorial receptor site activators or stimulators, sugars and/or sugar substitutes (e.g., sucralose, acesulfame potassium, aspartame, saccharine, cyclamates, lactose, sucrose, glucose, fructose, sorbitol, or mannitol), and other additives such as charcoal, chlorophyll, minerals, botanicals, or breath freshening agents. They maybe imitation, synthetic or natural ingredients or blends thereof. They may be in any suitable form, for example, liquid such as an oil, solid such as a powder, or gas.

In some embodiments, the flavour comprises menthol, spearmint and/or peppermint. In some embodiments, the flavour comprises flavour components of cucumber, blueberry, citrus fruits and/or redberry. In some embodiments, the flavour comprises eugenol. In some embodiments, the flavour comprises flavour components extracted from tobacco. In some embodiments, the flavour comprises flavour components extracted from cannabis. In some embodiments, the flavour may comprise a sensate, which is intended to achieve a somatosensorial sensation which are usually chemically induced and perceived by the stimulation of the fifth cranial nerve (trigeminal nerve), in addition to or in place of aroma or taste nerves, and these may include agents providing heating, cooling, tingling, numbing effect. A suitable heat effect agent may be, but is not limited to, vanillyl ethyl ether and a suitable cooling agent may be, but not limited to eucolyptol, WS-3.

Aerosol-generating material is a material that is capable of generating aerosol, for example when heated, irradiated or energized in any other way. Aerosol-generating material may, for example, be in the form of a solid, liquid or gel which may or may not contain an active substance and/or flavourants. In some embodiments, the aerosol generating material may comprise an “amorphous solid”, which may alternatively be referred to as a “monolithic solid” (i.e. non-fibrous). In some embodiments, the amorphous solid may be a dried gel. The amorphous solid is a solid material that may retain some fluid, such as liquid, within it. In some embodiments, the aerosol- generating material may for example comprise from about 50wt%, 6owt% or 70wt% of amorphous solid, to about 90wt%, 95wt% or ioowt% of amorphous solid.

The aerosol-generating material may comprise one or more active substances and/or flavours, one or more aerosol-former materials, and optionally one or more other functional material.

The aerosol-former material may comprise one or more constituents capable of forming an aerosol. In some embodiments, the aerosol-former material may comprise one or more of glycerine, glycerol, propylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol, 1,3-butylene glycol, erythritol, meso-Erythritol, ethyl vanillate, ethyl laurate, a diethyl suberate, triethyl citrate, triacetin, a diacetin mixture, benzyl benzoate, benzyl phenyl acetate, tributyrin, lauryl acetate, lauric acid, myristic acid, and propylene carbonate. In other embodiments, the aerosol former comprises one or more polyhydric alcohols, such as 1 ,3-butanediol; esters of polyhydric alcohols, such as glycerol mono-, di- or triacetate; and/or aliphatic esters of mono-, di- or polycarboxylic acids, such as dimethyl dodecanedioate and dimethyl tetradecanedioate.

The one or more other functional materials may comprise one or more of pH regulators, colouring agents, preservatives, binders, fillers, stabilizers, and/or antioxidants.

The material may be present on or in a support, to form a substrate. The support may, for example, be or comprise paper, card, paperboard, cardboard, reconstituted material, a plastics material, a ceramic material, a composite material, glass, a metal, or a metal alloy. In some embodiments, the support comprises a susceptor. In some embodiments, the susceptor is embedded within the material. In some alternative embodiments, the susceptor is on one or either side of the material. A consumable is an article comprising or consisting of aerosol-generating material, part or all of which is intended to be consumed during use by a user. A consumable may comprise one or more other components, such as an aerosol-generating material storage area, an aerosol-generating material transfer component, an aerosol generation area, a housing, a wrapper, a mouthpiece, a filter and/ or an aerosol-modifying agent. A consumable may also comprise an aerosol generator, such as a heater, that emits heat to cause the aerosol-generating material to generate aerosol in use. The heater may, for example, comprise combustible material, a material heatable by electrical conduction, or a susceptor.

A susceptor is a material that is heatable by penetration with a varying magnetic field, such as an alternating magnetic field. The susceptor may be an electrically-conductive material, so that penetration thereof with a varying magnetic field causes induction heating of the heating material. The heating material may be magnetic material, so that penetration thereof with a varying magnetic field causes magnetic hysteresis heating of the heating material. The susceptor maybe both electrically-conductive and magnetic, so that the susceptor is heatable by both heating mechanisms. The device that is configured to generate the varying magnetic field is referred to as a magnetic field generator, herein.

An aerosol-modifying agent is a substance, typically located downstream of the aerosol generation area, that is configured to modify the aerosol generated, for example by changing the taste, flavour, acidity or another characteristic of the aerosol. The aerosol modifying agent may be provided in an aerosol-modifying agent release component, that is operable to selectively release the aerosol-modifying agent The aerosol-modifying agent may, for example, be an additive or a sorbent. The aerosol-modifying agent may, for example, comprise one or more of a flavourant, a colourant, water, and a carbon adsorbent. The aerosol-modifying agent may, for example, be a solid, a liquid, or a gel. The aerosol-modifying agent maybe in powder, thread or granule form. The aerosol-modifying agent may be free from filtration material.

An aerosol generator is an apparatus configured to cause aerosol to be generated from the aerosol-generating material. In some embodiments, the aerosol generator is a heater configured to subject the aerosol-generating material to heat energy, so as to release one or more volatiles from the aerosol-generating material to form an aerosol.

In some embodiments, the aerosol generator is configured to cause an aerosol to be generated from the aerosol-generating material without heating. For example, the aerosol generator maybe configured to subject the aerosol-generating material to one or more of vibration, increased pressure, or electrostatic energy. The aerosol generating material may comprise a carrier on which the amorphous solid is provided. The carrier functions as a support on which the amorphous solid layer forms, easing manufacture. The carrier may provide tensile strength to the amorphous solid layer, easing handling.

The mouthpiece of the article may comprise amorphous solid material, suitably in the form of a gathered sheet of amorphous solid material.

The present invention provides a mouthpiece comprising amorphous solid material. It has surprisingly been found that including amorphous solid material in the mouthpiece results in an improved aerosol, with desirable flavour properties and/or reduced temperature, which improves the sensation for the user.

In the present case, the amorphous solid material is a sheet, optionally in gathered, wound or coiled form. In some cases, the sheet may be incorporated into the mouthpiece in sheet form. In other cases, the sheet may be shredded and then incorporated into the mouthpiece.

The aerosol generating material comprising the amorphous solid may have any suitable area density, such as from 30 g/m² to 120 g/m². In some cases, the sheet may have a mass per unit area of 80-120 g/m², or from about 70 to 110 g/m², or particularly from about 90 to 110 g/m², or suitably about 100 g/m².

In some examples, the amorphous solid in sheet form may have a tensile strength of from around 200 N/m to around 900 N/m. In some examples, such as where the amorphous solid does not comprise a filler, the amorphous solid may have a tensile strength of from 200 N/m to 400 N/m, or 200 N/m to 300 N/m, or about 250 N/m.

In some examples, such as where the amorphous solid comprises a filler, the amorphous solid may have a tensile strength of from 600 N/m to 900 N/m, or from 700 N/m to 900 N/m, or around 800 N/m. Such tensile strengths maybe particularly suitable for embodiments wherein the amorphous solid material is included in an aerosol generating article/assembly as a rolled sheet, suitably in the form of a tube. In some cases, the carrier layer may be substantially or wholly impermeable to gas and/or aerosol. This prevents aerosol or gas passage through the carrier, thereby controlling the flow and ensuring good delivery to the user. The carrier may be any suitable material which can be used to support an amorphous solid. In some cases, the carrier may be formed from materials selected from metal foil, paper, carbon paper, greaseproof paper, ceramic, carbon allotropes such as graphite and graphene, plastic, cardboard, wood or combinations thereof. In some cases, the carrier may comprise or consist of a tobacco material, such as a sheet of reconstituted tobacco. In some cases, the carrier may be formed from materials selected from metal foil, paper, cardboard, wood or combinations thereof. In some cases, the carrier itself may be a laminate structure comprising layers of materials selected from the preceding lists. In some cases, the carrier may also function as a flavour carrier. For example, the carrier may be impregnated with a flavourant or with tobacco extract.

In some cases, the surface of the carrier that abuts the amorphous solid maybe porous. For example, in some cases, the carrier comprises paper. The inventors have found that a porous carrier such as paper is particularly suitable for the present invention; the porous (paper) layer abuts the amorphous solid layer and forms a strong bond. The amorphous solid is formed by drying a gel and, without being limited by theory, it is thought that the slurry from which the gel is formed partially impregnates the porous carrier (e.g. paper) so that when the gel sets and forms cross-links, the carrier is partially bound into the gel. This provides a strong binding between the gel and the carrier (and between the dried gel and the carrier).

Additionally, surface roughness may contribute to the strength of bond between the amorphous material and the carrier. The inventors have found that the paper roughness (for the surface abutting the carrier) may suitably be in the range of 50-1000 Bekk seconds, suitably 50-150 Bekk seconds, suitably 100 Bekk seconds (measured over an air pressure interval of 50.66-48.00 kPa). (A Bekk smoothness tester is an instrument used to determine the smoothness of a paper surface, in which air at a specified pressure is leaked between a smooth glass surface and a paper sample, and the time (in seconds) for a fixed volume of air to seep between these surfaces is the "Bekk smoothness”.) In another case, a paper and greaseproof paper laminate has also been found to be particularly useful for the present invention. The paper layer abuts the amorphous solid and the tacky amorphous solid does not stick readily to the greaseproof paper carrier backing.

In some cases, the carrier may have a thickness of between about o.oiomm and about 2.omm, suitably from about 0.015mm, 0.02mm, 0.05mm or 0.1mm to about 1.5mm, 1.0mm, or 0.5mm. In some cases, the amorphous solid layer may have a thickness of about 0.015mm to about 1.5mm, suitably about 0.05mm to about 1.5mm or 0.05mm to about 1.0mm. Suitably, the thickness maybe in the range of about 0.1mm or 0.15mm to about imm, 0.5mm or 0.3mm. The amorphous solid may comprise more than one layer, and the thickness described herein refers to the aggregate thickness of those layers.

The thickness stipulated herein is a mean thickness for the material. In some cases, the amorphous solid thickness may vary by no more than 25%, 20%, 15%, 10%, 5% or 1%.

In some cases, the amorphous solid may comprise i-6owt% of a gelling agent wherein these weights are calculated on a dry weight basis.

Suitably, the amorphous solid may comprise from about iwt%, 5wt%, iowt%, I5wt%, 20wt% or 25wt% to about 6owt%, 50wt%, 45wt%, 40wt%, 35wt%, 30wt% or 27wt% of a gelling agent (all calculated on a dry weight basis). For example, the amorphous solid may comprise i-50wt%, 5-40wt%, io-30wt% or i5-27wt% of a gelling agent.

The gelling agent may comprise one or more compounds selected from cellulosic gelling agents, non-cellulosic gelling agents, guar gum, acacia gum and mixtures thereof.

In some embodiments, the cellulosic gelling agent is selected from the group consisting of: hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, carboxymethylcellulose (CMC), hydroxypropyl methylcellulose (HPMC), methyl cellulose, ethyl cellulose, cellulose acetate (CA), cellulose acetate butyrate (CAB), cellulose acetate propionate (CAP) and combinations thereof. In some embodiments, the gelling agent comprises (or is) one or more of hydroxyethyl cellulose, hydroxypropyl cellulose, hydroxypropyl methylcellulose (HPMC), carboxymethylcellulose, guar gum, or acacia gum. In some embodiments, the gelling agent comprises (or is) one or more non-cellulosic gelling agents, including, but not limited to, agar, xanthan gum, gum Arabic, guar gum, locust bean gum, pectin, carrageenan, starch, alginate, and combinations thereof. In preferred embodiments, the non-cellulose based gelling agent is alginate or agar. In some embodiments, the gelling agent comprises a hydrocolloid. In some embodiments, the gelling agent comprises one or more compounds selected from the group comprising alginates, pectins, starches (and derivatives), celluloses (and derivatives), gums, silica or silicones compounds, clays, polyvinyl alcohol and combinations thereof. For example, in some embodiments, the gelling agent comprises one or more of alginates, pectins, hydroxyethyl cellulose, hydroxypropyl cellulose, carboxymethylcellulose, pullulan, xanthan gum, guar gum, carrageenan, agarose, acacia gum, fumed silica, PDMS, sodium silicate, kaolin and polyvinyl alcohol. In some cases, the gelling agent comprises alginate and/or pectin, and maybe combined with a setting agent (such as a calcium source) during formation of the amorphous solid. In some cases, the amorphous solid may comprise a calcium-crosslinked alginate and/ or a calcium-crosslinked pectin.

In some embodiments, the gelling agent comprises alginate, and the alginate is present in the amorphous solid in an amount of from io-30wt% of the amorphous solid (calculated on a dry weight basis). In some embodiments, alginate is the only gelling agent present in the amorphous solid. In other embodiments, the gelling agent comprises alginate and at least one further gelling agent, such as pectin.

In some embodiments the amorphous solid may include gelling agent comprising carrageenan.

Suitably, the amorphous solid may comprise from about o.iwt%, o.5wt%, iwt%, 3wt%, 5wt%, 7wt% or 10% to about 50wt%, 45wt%, 40wt%, 35wt%, 30wt% or 25wt% of an aerosol generating agent (all calculated on a dry weight basis). The aerosol generating agent may act as a plasticiser. For example, the amorphous solid may comprise 0.5- 40wt%, 3 35wt% or io-25wt% of an aerosol generating agent. In some cases, the aerosol generating agent comprises one or more compound selected from erythritol, propylene glycol, glycerol, triacetin, sorbitol and xylitol. In some cases, the aerosol generating agent comprises, consists essentially of or consists of glycerol. The inventors have established that if the content of the plasticiser is too high, the amorphous solid may absorb water resulting in a material that does not create an appropriate consumption experience in use. The inventors have established that if the plasticiser content is too low, the amorphous solid may be brittle and easily broken. The plasticiser content specified herein provides an amorphous solid flexibility which allows the amorphous solid sheet to be wound onto a bobbin, which is useful in manufacture of aerosol generating articles.

The amorphous solid may comprise a flavour. In some cases, the amorphous solid may comprise up to about 8owt%, 70wt%, 6owt%, 55wt%, 50wt% or 45wt% of a flavour.

In some cases, the amorphous solid may comprise at least about o.iwt%, iwt%, iowt%, 20wt%, 30wt%, 35wt% or 40wt% of a flavour (all calculated on a dry weight basis).

For example, the amorphous solid may comprise i-8owt%, io-8owt%, 20-70wt%, 30- 6owt%, 35 55wt% or 30-45wt% of a flavour. In some cases, the flavour comprises, consists essentially of or consists of menthol. The amorphous solid may comprise a colourant. The addition of a colourant may alter the visual appearance of the amorphous solid. The presence of colourant in the amorphous solid may enhance the visual appearance of the amorphous solid and the aerosol-generating material. By adding a colourant to the amorphous solid, the amorphous solid may be colour-matched to other components of the aerosol- generating material or to other components of an article comprising the amorphous solid.

A variety of colourants may be used depending on the desired colour of the amorphous solid. The colour of amorphous solid may be, for example, white, green, red, purple, blue, brown or black. Other colours are also envisaged. Natural or synthetic colourants, such as natural or synthetic dyes, food-grade colourants and pharmaceutical-grade colourants may be used. In certain embodiments, the colourant is caramel, which may confer the amorphous solid with a brown appearance. In such embodiments, the colour of the amorphous solid maybe similar to the colour of other components (such as tobacco material) in an aerosol-generating material comprising the amorphous solid. In some embodiments, the addition of a colourant to the amorphous solid renders it visually indistinguishable from other components in the aerosol-generating material.

The colourant maybe incorporated during the formation of the amorphous solid (e.g. when forming a slurry comprising the materials that form the amorphous solid) or it maybe applied to the amorphous solid after its formation (e.g. by spraying it onto the amorphous solid).

In some cases, the amorphous solid may additionally comprise an emulsifying agent, which emulsified molten flavour during manufacture. For example, the amorphous solid may comprise from about 5wt% to about I5wt% of an emulsifying agent (calculated on a dry weight basis), suitably about iowt%. The emulsifying agent may comprise acacia gum. In some embodiments, the amorphous solid is a hydrogel and comprises less than about 20 wt% of water calculated on a wet weight basis. In some cases, the hydrogel may comprise less than about i5wt%, 12 wt% or 10 wt% of water calculated on a wet weight basis. In some cases, the hydrogel may comprise at least about iwt%, 2wt% or at least about 5wt% of water (WWB).

The amorphous solid may comprise an acid. The acid may be an organic acid. In some of these embodiments, the acid may be at least one of a monop rotic acid, a diprotic acid and a triprotic acid. In some such embodiments, the acid may contain at least one carboxyl functional group. In some such embodiments, the acid maybe at least one of an alpha-hydroxy acid, carboxylic acid, dicarboxylic acid, tricarboxylic acid and keto acid. In some such embodiments, the acid maybe an alpha-keto acid.

In some such embodiments, the acid may be at least one of succinic acid, lactic acid, benzoic acid, citric acid, tartaric acid, fumaric acid, levulinic acid, acetic acid, malic acid, formic acid, sorbic acid, benzoic acid, propanoic and pyruvic acid.

Suitably the acid is lactic acid. In other embodiments, the acid is benzoic acid. In other embodiments the acid may be an inorganic acid. In some of these embodiments the acid may be a mineral acid. In some such embodiments, the acid may be at least one of sulphuric acid, hydrochloric acid, boric acid and phosphoric acid. In some embodiments, the acid is levulinic acid. In certain embodiments, the amorphous solid comprises a gelling agent comprising a cellulosic gelling agent and/or a non-cellulosic gelling agent, an active substance and an acid.

In some embodiments, the amorphous solid additionally comprises an active substance. For example, in some cases, the amorphous solid additionally comprises a tobacco material and/or nicotine. In some cases, the amorphous solid may comprise 5- 6owt% (calculated on a dry weight basis) of a tobacco material and/or nicotine. In some cases, the amorphous solid may comprise from about iwt%, 5wt%, iowt%, I5wt%, 20wt% or 25wt% to about 70wt%, 6owt%, 50wt%, 45wt%, 40wt%, 35wt%, or 30wt% (calculated on a dry weight basis) of an active substance. In some cases, the amorphous solid may comprise from about iwt%, 5wt%, iowt%, I5wt%, 20wt% or 25wt% to about 70wt%, 6owt%, 50wt%, 45wt%, 40wt%, 35wt%, or 30wt% (calculated on a dry weight basis) of a tobacco material. For example, the amorphous solid may comprise 10-

50wt%, i5-40wt% or 20-35wt% of a tobacco material. In some cases, the amorphous solid may comprise from about iwt%, 2wt%, 3wt% or 4wt% to about 20wt%, i8wt%, i5wt% or i2wt% (calculated on a dry weight basis) of nicotine. For example, the amorphous solid may comprise i-20wt%, 2-i8wt% or 3-i2wt% of nicotine.

In some cases, the amorphous solid comprises an active substance such as tobacco extract. In some cases, the amorphous solid may comprise 5-6owt% (calculated on a dry weight basis) of tobacco extract. In some cases, the amorphous solid may comprise from about 5wt%, iowt%, I5wt%, 20wt% or 25wt% to about 6owt%, 50wt%, 45wt% or 40wt%, 35wt% or 30wt% (calculated on a dry weight basis) tobacco extract. For example, the amorphous solid may comprise io-50wt%, i4-40wt% or 20-35wt% of tobacco extract. The tobacco extract may contain nicotine at a concentration such that the amorphous solid comprises iwt% i.5wt%, 2wt% or 2.5wt% to about 6wt%, 5wt%, 4-5wt% or 4wt% (calculated on a dry weight basis) of nicotine. In some cases, there may be no nicotine in the amorphous solid other than that which results from the tobacco extract.

In some embodiments the amorphous solid comprises no tobacco material but does comprise nicotine. In some such cases, the amorphous solid may comprise from about iwt%, 2wt%, 3wt% or 4wt% to about 20wt%, i8wt%, i5wt%, or i2wt% (calculated on a dry weight basis) of nicotine. For example, the amorphous solid may comprise l- 20wt%, 2-i8wt% or 3-i2wt% of nicotine.

In some cases, the total content of active substance and flavour may be at least about o.iwt%, iwt%, 5wt%, iowt%, 20wt%, 25wt% or 30wt%. In some cases, the total content of active substance and flavour may be less than about 90wt%, 8owt%, 70wt%, 6owt%, 50wt% or 40wt% (all calculated on a dry weight basis).

In some cases, the total content of tobacco material, nicotine and flavour may be at least about o.iwt%, iwt%, 5wt%, iowt%, 20wt%, 25wt% or 30wt%. In some cases, the total content of active substance and/or flavour maybe less than about 90wt%, 8owt%, 70wt%, 6owt%, 50wt% or 40wt% (all calculated on a dry weight basis).

The amorphous solid may be made from a gel, and this gel may additionally comprise a solvent, included at o.i-50wt%. However, the inventors have established that the inclusion of a solvent in which the flavour is soluble may reduce the gel stability and the flavour may crystallise out of the gel. As such, in some cases, the gel does not include a solvent in which the flavour is soluble. In some embodiments, the amorphous solid comprises less than 6owt% of a filler, such as from iwt% to 6owt%, or 5wt% to 50wt%, or 5wt% to 30wt%, or iowt% to 20wt%.

In other embodiments, the amorphous solid comprises less than 20wt%, suitably less than iowt% or less than 5wt% of a filler. In some cases, the amorphous solid comprises less than iwt% of a filler, and in some cases, comprises no filler.

The filler, if present, may comprise one or more inorganic filler materials, such as calcium carbonate, perlite, vermiculite, diatomaceous earth, colloidal silica, magnesium oxide, magnesium sulphate, magnesium carbonate, and suitable inorganic sorbents, such as molecular sieves. The filler may comprise one or more organic filler materials such as wood pulp, cellulose and cellulose derivatives. In some cases, the amorphous solid comprises less than iwt% of a filler, and in some cases, comprises no filler. In particular, in some cases, the amorphous solid comprises no calcium carbonate such as chalk. In particular embodiments which include filler, the filler is fibrous. For example, the filler may be a fibrous organic filler material such as wood pulp, hemp fibre, cellulose or cellulose derivatives. Without wishing to be bound by theory, it is believed that including fibrous filler in an amorphous solid may increase the tensile strength of the material. This may be particularly advantageous since the increased tensile strength can make it less likely that defects are introduced to the amorphous solid material during manufacture.

In some embodiments, the amorphous solid does not comprise tobacco fibres. In particular embodiments, the amorphous solid does not comprise fibrous material.

In some embodiments, the aerosol generating material does not comprise tobacco fibres. In particular embodiments, the aerosol generating material does not comprise fibrous material.

In some cases, the amorphous solid may consist essentially of, or consist of a gelling agent, an aerosol generating agent, water, and optionally a flavour and/ or a tobacco material and/or a nicotine source. In some cases, the amorphous solid may consist essentially of, or consist of a gelling agent, water, an aerosol generating agent, and optionally a flavour and/or an active substance.

Induction heating is a process in which an electrically-conductive object is heated by penetrating the object with a varying magnetic field. The process is described by Faraday's law of induction and Ohm's law. An induction heater may comprise an electromagnet and a device for passing a varying electrical current, such as an alternating current, through the electromagnet. When the electromagnet and the object to be heated are suitably relatively positioned so that the resultant varying magnetic field produced by the electromagnet penetrates the object, one or more eddy currents are generated inside the object. The object has a resistance to the flow of electrical currents. Therefore, when such eddy currents are generated in the object, their flow against the electrical resistance of the object causes the object to be heated. This process is called Joule, ohmic, or resistive heating. An object that is capable of being inductively heated is known as a susceptor. In one embodiment, the susceptor is in the form of a closed circuit. It has been found that, when the susceptor is in the form of a closed circuit, magnetic coupling between the susceptor and the electromagnet in use is enhanced, which results in greater or improved Joule heating.

Magnetic hysteresis heating is a process in which an object made of a magnetic material is heated by penetrating the object with a varying magnetic field. A magnetic material can be considered to comprise many atomic-scale magnets, or magnetic dipoles. When a magnetic field penetrates such material, the magnetic dipoles align with the magnetic field. Therefore, when a varying magnetic field, such as an alternating magnetic field, for example as produced by an electromagnet, penetrates the magnetic material, the orientation of the magnetic dipoles changes with the varying applied magnetic field. Such magnetic dipole reorientation causes heat to be generated in the magnetic material.

When an object is both electrically-conductive and magnetic, penetrating the object with a varying magnetic field can cause both Joule heating and magnetic hysteresis heating in the object. Moreover, the use of magnetic material can strengthen the magnetic field, which can intensify the Joule heating.

In each of the above processes, as heat is generated inside the object itself, rather than by an external heat source by heat conduction, a rapid temperature rise in the object and more uniform heat distribution can be achieved, particularly through selection of suitable object material and geometry, and suitable varying magnetic field magnitude and orientation relative to the object. Moreover, as induction heating and magnetic hysteresis heating do not require a physical connection to be provided between the source of the varying magnetic field and the object, design freedom and control over the heating profile may be greater, and cost may be lower. Articles, for instance those in the shape of rods, are often named according to the product length: “regular” (typically in the range 68 - 75 mm, e.g. from about 68 mm to about 72 mm), “short” or “mini” (68 mm or less), “king-size” (typically in the range 75 - 91 mm, e.g. from about 79 mm to about 88 mm), “long” or “super-king” (typically in the range 91 - 105 mm, e.g. from about 94 mm to about 101 mm) and “ultra-long” (typically in the range from about 110 mm to about 121 mm). They are also named according to the product circumference: “regular” (about 23 - 25 mm), “wide” (greater than 25 mm), “slim” (about 22 - 23 mm), “demi-slim” (about 19 - 22 mm), “super-slim” (about 16 - 19 mm), and “micro-slim” (less than about 16 mm). Accordingly, an article in a king-size, super-slim format will, for example, have a length of about 83 mm and a circumference of about 17 mm.

Each format may be produced with mouthpieces of different lengths. The mouthpiece length will be from about 30 mm to 50 mm. A tipping paper connects the mouthpiece to the aerosol generating material and will usually have a greater length than the mouthpiece, for example from 3 to 10 mm longer, such that the tipping paper covers the mouthpiece and overlaps the aerosol generating material, for instance in the form of a rod of substrate material, to connect the mouthpiece to the rod. Articles and their aerosol generating materials and mouthpieces described herein can be made in, but are not limited to, any of the above formats.

The terms ‘upstream’ and ‘downstream’ used herein are relative terms defined in relation to the direction of mainstream aerosol drawn though an article or device in use.

The filamentary tow material described herein can comprise cellulose acetate fibre tow. The filamentary tow can also be formed using other materials used to form fibres, such as polyvinyl alcohol (PVOH), polylactic acid (PLA), polycaprolactone (PCL), poly(i-4 butanediol succinate) (PBS), poly(butylene adipate-co-terephthalate)(PBAT), starch based materials, cotton, aliphatic polyester materials and polysaccharide polymers or a combination thereof. The filamentary tow may be plasticised with a suitable plasticiser for the tow, such as triacetin where the material is cellulose acetate tow, or the tow may be non-plasticised. The tow can have any suitable specification, such as fibres having a Ύ’ shaped or other cross section such as ‘X’ shaped, filamentary denier values between 2.5 and 15 denier per filament, for example between 8.0 and 11.0 denier per filament and total denier values of 5,000 to 50,000, for example between 10,000 and 40,000.

As used herein, the term “tobacco material” refers to any material comprising tobacco or derivatives or substitutes thereof. The term “tobacco material” may include one or more of tobacco, tobacco derivatives, expanded tobacco, reconstituted tobacco or tobacco substitutes. The tobacco material may comprise one or more of ground tobacco, tobacco fibre, cut tobacco, extruded tobacco, tobacco stem, tobacco lamina, reconstituted tobacco and/or tobacco extract. In the figures described herein, like reference numerals are used to illustrate equivalent features, articles or components.

Figure l is a side-on cross sectional view of an article l for use with a non-combustible aerosol provision device. As shown in Figure l, the article comprises a mouthpiece 2 having an upstream end 2a and a downstream end 2b. The mouthpiece 2 comprises a body 6, comprising a sheet of amorphous solid material. In the present example, the amorphous solid material is gathered and wrapped by a first plug wrap 7 to form a substantially cylindrical body 6. In the present example body 6 is formed from a single gathered sheet of amorphous solid sheet material. However in alternative embodiments, the sheet of amorphous solid material may be cut into strips prior to gathering to form body 6.

In the embodiment shown in Figure 1, the article comprises the mouthpiece 2, and further comprises a cylindrical rod of aerosol generating material 3, in the present case tobacco material, connected to the mouthpiece 2. The upstream end 2a of the mouthpiece is disposed adjacent to the rod of aerosol generating material 3 and the downstream end 2b of the mouthpiece 2 is disposed distal from the rod of aerosol generating material 3. The inventors have found that providing a body of amorphous solid material in the mouthpiece advantageously provides a cooling effect to the aerosol as it is drawn through the mouthpiece in use. Without wishing to be bound by theory, it is hypothesised that heat transferred to the amorphous solid material from the aerosol as it passes through the body 6, in use, aerosolises components of the amorphous solid material, resulting in cooling of the aerosol, and advantageously, the ability to simultaneously modify the flavour of the aerosol passing through the mouthpiece, if desired. This arrangement can reduce a known problem with smoking articles where an aerosol is too warm when it reaches a consumer’s lips, and also provide a means for adding additional flavour to an aerosol, without increasing manufacturing complexity.

In the present example, the length of the body 6 of amorphous solid material is 40 mm. The body may be formed using methods known to those skilled in the art for producing a paper filter for a smoking article. In the present example, the body of amorphous solid material 6 is formed from a single gathered sheet of amorphous solid material. In alternative embodiments, the body 6 may be formed from two or more sheets of amorphous solid material, or a single sheet of material cut into strips prior being gathered to form the body. In the present case the amorphous solid material comprises a single layer, and is not laminated on a carrier material. In other embodiments the amorphous solid material maybe laminated on a carrier material such as paper or foil, and the laminated amorphous solid material may be used to form the body in any of the ways described herein.

In the present case, the amorphous solid material has a thickness of 0.09 mm. In alternative embodiments the amorphous solid material may have any suitable thickness as described herein. Suitably, the amorphous solid material may have a thickness in the range 0.05 mm- 0.2 mm. Suitably, in any of the embodiments described herein, the amorphous solid layer has a thickness of from about 50 pm to about 200 pm, or about 50 pm to about too pm, or about 60 pm to about 90 pm, suitably about 77 pm. The density of the body 6 may be determined by dividing the total weight of the body 6 by the total volume of the body 6, wherein the total volume can be calculated using appropriate measurements of the body 6, for example, using callipers. Where necessary, the appropriate dimensions maybe measured using a microscope. In the present case, the body has a density of 0.51 x to^-3 g/mm³. In other embodiments the body may have a density between 0.1 x io^_3g/mm³to 1 x to^-3 g/mm³.

The body 6 is wrapped in a first plug wrap 7. Preferably, the first plug wrap 7 has a basis weight of less than 50 gsm, more preferably between about 20 gsm and 40 gsm. Preferably, the first plug wrap 7 has a thickness of between 30 pm and 60 pm, more preferably between 35 pm and 45 pm. Preferably, the first plug wrap 7 is a non-porous plug wrap, for instance having a permeability of less than too Coresta units, for instance less than 50 Coresta units. However, in other embodiments, the first plug wrap 7 can be a porous plug wrap, for instance having a permeability of greater than 200 Coresta Units. Figure 2 is a side-on cross sectional view of an article l’ comprising a mouthpiece 2’ for use with a non-combustible aerosol provision device. Article 1’ comprises a body 6 similar to that as described in relation to Figure 1, except in the present case body 6 has a length of 10 mm. In addition to body 6, the mouthpiece 2’ comprises a hollow tubular element 8, and a body of fibrous material 4. In the embodiment shown in Figure 2, the article 1’ further comprises a rod of aerosol generating material 3 connected to an upstream end 2’a of the mouthpiece 2’, opposite to a downstream end 2’b of the mouthpiece 2’. Preferably, the length of the body 6 is less than about 15 mm. More preferably, the length of the body 6 is less than about 10 mm. In addition, or as an alternative, the length of the body 6 is at least about 5 mm. Preferably, the length of the body 6 is at least about 6 mm. In some preferred embodiments, the length of the body 6 is from about 5 mm to about 15 mm, more preferably from about 6 mm to about 12 mm, even more preferably from about 6 mm to about 12 mm, most preferably about 6 mm, 7 mm, 8 mm, 9 mm or 10 mm. In the present example, body 6 has a length of 10 mm.

The pressure drop or difference (also referred to as resistance to draw) across the mouthpiece, for instance the part of the article 1 downstream of the aerosol generating material 3, is preferably less than about 40 mmH₂o. Such pressure drops have been found to allow sufficient aerosol, including desirable compounds such as flavour compounds, to pass through the mouthpiece 2 to the consumer. More preferably, the pressure drop across the mouthpiece 2 is less than about 32 mmH₂0. In some embodiments, particularly improved aerosol has been achieved using a mouthpiece 2 having a pressure drop of less than 31 mmH₂0, for instance about 29 mmH₂0, about 28 mmH₂0 or about 27.5 mmH₂0. Alternatively or additionally, the mouthpiece pressure drop can be at least 10 mmH₂o, preferably at least 15 mmH₂0 and more preferably at least 20 mmH₂0. In some embodiments, the mouthpiece pressure drop can be between about 15 mm H₂0 and 40 mmH₂0. These values enable the mouthpiece 2 to slow down the aerosol as it passes through the mouthpiece 2 such that the temperature of the aerosol has time to reduce before reaching the downstream end 2b of the mouthpiece 2.

The pressure drop or difference across the body is suitably between 0.01 mmH₂0 and too mmH₂0. In some embodiments, the pressure drop across the body is less than about 50 mmF O, less than about 45 mmF O, or less than about 30 mmF O. In the present example, body 6 is positioned downstream of, adjacent to and abutting hollow tubular element 8, also referred to as a cooling element. The hollow tubular element 8 is formed from a plurality of layers of paper which are parallel wound, with butted seams, to form the tubular element 8. In the present example, first and second paper layers are provided in a two-ply tube, although in other examples 3, 4 or more paper layers can be used forming 3, 4 or more ply tubes. Other constructions can be used, such as spirally wound layers of paper, cardboard tubes, tubes formed using a papier-mache type process, moulded or extruded plastic tubes or similar. The hollow tubular element 8 can also be formed using a stiff plug wrap and/ or tipping paper, for instance as the third plug wrap 11 and/or tipping paper 5 described in more detail below, meaning that a separate tubular element is not required. The stiff plug wrap and/or tipping paper is manufactured to have a rigidity that is sufficient to withstand the axial compressive forces and bending moments that might arise during manufacture and whilst the article 1’ is in use. For instance, the stiff plug wrap and/or tipping paper can have a basis weight between 70 gsm and 120 gsm, more preferably between 80 gsm and 110 gsm. Additionally or alternatively, the stiff plug wrap and/or tipping paper can have a thickness between 80 pm and 200 pm, more preferably between too pm and 160 pm, or from 120 pm to 150 pm. It can be desirable for both the third plug wrap 11 and tipping paper 5 to have values in these ranges, to achieve an acceptable overall level of rigidity for the hollow tubular element 8.

The hollow tubular element 8 preferably has a wall thickness, which can be measured, for example using a calliper, of at least about too pm and up to about 1.5mm, preferably between 100 pm and 1 mm and more preferably between 150 pm and 500 pm, or about 300 pm. In the present example, the hollow tubular element 8 has a wall thickness of about 290 pm.

Preferably, the length of the hollow tubular element 8 is less than about 50 mm. More preferably, the length of the hollow tubular element 8 is less than about 40 mm. Still more preferably, the length of the hollow tubular element 8 is less than about 30 mm. In addition, or as an alternative, the length of the hollow tubular element 8 is preferably at least about 10 mm. Preferably, the length of the hollow tubular element 8 is at least about 15 mm. In some preferred embodiments, the length of the hollow tubular element 8 is from about 20 mm to about 30 mm, more preferably from about 22 mm to about 28 mm, even more preferably from about 24 to about 26 mm, most preferably about 25 mm. In the present example, the length of the hollow tubular element 8 is 25 mm.

The hollow tubular element 8 is located around and defines an air gap within the mouthpiece 2 which acts as a cooling segment. The air gap provides a chamber through which heated volatilised components generated by the aerosol generating material 3 flow. The hollow tubular element 8 is hollow to provide a chamber for aerosol accumulation yet rigid enough to withstand axial compressive forces and bending moments that might arise during manufacture and whilst the article 1’ is in use. The hollow tubular element 8 provides a physical displacement between the aerosol generating material 3 and the body of material 6. The physical displacement provided by the hollow tubular element 8 will provide a thermal gradient across the length of the hollow tubular element 8. The hollow tubular element 8 can be configured to provide a temperature differential of at least 40 degrees Celsius between a heated volatilised component entering a first, upstream end of the hollow tubular element 8 and a heated volatilised component exiting a second, downstream end of the hollow tubular element 8. The hollow tubular element 8 is preferably configured to provide a temperature differential of at least 60, 80 or preferably too degrees Celsius between a heated volatilised component entering a first, upstream end of the hollow tubular element 8 and a heated volatilised component exiting a second, downstream end of the hollow tubular element 8. This temperature differential across the length of the hollow tubular element 8 protects the temperature sensitive body of material 6 from the high temperatures of the aerosol generating material 3 when it is heated.

In alternative articles, the hollow tubular element 8 can be replaced with an alternative cooling element, for instance an element formed from a body of material which allows aerosol to pass through it longitudinally, and which also performs the function of cooling the aerosol, for example, a body 6 of amorphous solid material.

In the present example, a body of fibrous material 4 is positioned at the downstream, mouth end 2’b of the mouthpiece 2’, immediately downstream of and in an abutting relationship with the body 6. Body of fibrous material 4 is wrapped by a second plug wrap 9, which in the present example is the same as first plug wrap 7. The body 6 and body of fibrous material 4 each define a substantially cylindrical overall outer shape and share a common longitudinal axis.

In the present example, hollow tubular element 8, body 6, and body of fibrous material 4 are combined using a third plug wrap 11, which is wrapped around all three sections.

Preferably, the third plug wrap 11 has a basis weight of less than 50 gsm, more preferably between about 20 gsm and 45 gsm. Preferably, the third plug wrap 11 has a thickness of between 30 pm and 60 pm, more preferably between 35 pm and 45 pm.

The third plug wrap 11 is preferably a non-porous plug wrap having a permeability of less than too Coresta Units, for instance less than 50 Coresta Units. However, in alternative embodiments, the third plug wrap 11 can be a porous plug wrap, for instance having a permeability of greater than 200 Coresta Units.

In the present example, the body of fibrous material 4 is formed from filamentary tow. In the present example, the tow used in the body of fibrous material 4 has a denier per filament (d.p.f.) of 8.4 and a total denier of 21,000. Alternatively, the tow can, for instance, have a denier per filament (d.p.f.) of 9.5 and a total denier of 12,000. Alternatively, the tow can, for instance, have a denier per filament (d.p.f.) of 8 and a total denier of 15,000. In the present example, the tow comprises plasticised cellulose acetate tow. The plasticiser used in the tow comprises about 7% by weight of the tow.

In the present example, the plasticiser is triacetin. In other examples, different materials can be used to form the body of fibrous material 4. For instance, rather than tow, the body of fibrous material 4 can be formed from paper, for instance in a similar way to paper filters known for use in cigarettes. Alternatively, the body of fibrous material 4 can be formed from tows other than cellulose acetate, for instance polylactic acid (PLA), other materials described herein for filamentary tow or similar materials. The tow is preferably formed from cellulose acetate. The tow, whether formed from cellulose acetate or other materials, preferably has a d.p.f. of at least 5, more preferably at least 6 and still more preferably at least 7. These values of denier per filament provide a tow which has relatively coarse, thick fibres with a lower surface area which result in a lower pressure drop across the mouthpiece 2’ than tows having lower d.p.f. values. Preferably, to achieve a sufficiently uniform body of fibrous material 4, the tow has a denier per filament of no more than 12 d.p.f., preferably no more than 11 d.p.f. and still more preferably no more than 10 d.p.f. The total denier of the tow forming the body of fibrous material 4 is preferably at most 30,000, more preferably at most 28,000 and still more preferably at most 25,000. These values of total denier provide a tow which takes up a reduced proportion of the cross sectional area of the mouthpiece 2’ which results in a lower pressure drop across the mouthpiece 2’ than tows having higher total denier values. For appropriate firmness of the body of fibrous material 4, the tow preferably has a total denier of at least 8,000 and more preferably at least 10,000. Preferably, the denier per filament is between 5 and 12 while the total denier is between 10,000 and 25,000. More preferably, the denier per filament is between 6 and 10 while the total denier is between 11,000 and 22,000. Preferably the cross-sectional shape of the filaments of tow are Ύ’ shaped, although in other embodiments other shapes such as ‘X’ shaped filaments can be used, with the same d.p.f. and total denier values as provided herein.

Preferably, the length of the body of fibrous material 4 is less than about 15 mm. More preferably, the length of the body of fibrous material 4 is less than about 10 mm. In addition, or as an alternative, the length of the body of fibrous material 4 is at least about 5 mm. Preferably, the length of the body of fibrous material 4 is at least about 6 mm. In some preferred embodiments, the length of the body of fibrous material 4 is from about 5 mm to about 15 mm, more preferably from about 6 mm to about 12 mm, even more preferably from about 6 mm to about 12 mm, most preferably about 6 mm, 7 mm, 8 mm, 9 mm or 10 mm. In the present example, the length of the body of fibrous material 4 is 10 mm.

In the present example, the aerosol generating material 3 is wrapped in a wrapper 10. The wrapper 10 can, for instance, be a paper or paper-backed foil wrapper. In the present example, the wrapper 10 is substantially impermeable to air. In alternative embodiments, the wrapper 10 preferably has a permeability of less than too Coresta Units, more preferably less than 60 Coresta Units. It has been found that low permeability wrappers, for instance having a permeability of less than too Coresta Units, more preferably less than 60 Coresta Units, result in an improvement in the aerosol formation in the aerosol generating material 3. Without wishing to be bound by theory, it is hypothesised that this is due to reduced loss of aerosol compounds through the wrapper 10. The permeability of the wrapper 10 can be measured in accordance with ISO 2965:2009 concerning the determination of air permeability for materials used as cigarette papers, filter plug wrap and filter joining paper. In the present embodiment, the wrapper 10 comprises aluminium foil. Aluminium foil has been found to be particularly effective at enhancing the formation of aerosol within the aerosol generating material 3. In the present example, the aluminium foil has a metal layer having a thickness of about 6 pm. In the present example, the aluminium foil has a paper backing. However, in alternative arrangements, the aluminium foil can be other thicknesses, for instance between 4 pm and 16 pm in thickness. The aluminium foil also need not have a paper backing, but could have a backing formed from other materials, for instance to help provide an appropriate tensile strength to the foil, or it could have no backing material. Metallic layers or foils other than aluminium can also be used. The total thickness of the wrapper is preferably between 20 pm and 60 pm, more preferably between 30 pm and 50 pm, which can provide a wrapper having appropriate structural integrity and heat transfer characteristics. The tensile force which can be applied to the wrapper before it breaks can be greater than 3,000 grams force, for instance between 3,000 and 10,000 grams force or between 3,000 and 4,500 grams force.

The article has a ventilation level of about 60% of the aerosol drawn through the article. In alternative embodiments, the article can have a ventilation level of between 50% and 80% of aerosol drawn through the article, for instance between 65% and 75%. Ventilation at these levels helps to slow down the flow of aerosol drawn through the mouthpiece 2’ and thereby enable the aerosol to cool sufficiently before it reaches the downstream end 2b of the mouthpiece 2’. The ventilation is provided directly into the mouthpiece 2’ of the article 1’. In the present example, the ventilation is provided into the hollow tubular element 8, which has been found to be particularly beneficial in assisting with the aerosol generation process. The ventilation is provided via first and second parallel rows of perforations 12, in the present case formed as laser perforations, at positions 17.925 mm and 18.625 mm respectively from the downstream, mouth-end 2’b of the mouthpiece 2’. These perforations pass though the tipping paper 5, third plug wrap 11 and hollow tubular element 8. In alternative embodiments, the ventilation can be provided into the mouthpiece at other locations, for instance into the fibrous section 4 or first tubular element 11.

The aerosol generating material comprises an aerosolisable material, also called an aerosol forming material. The aerosolisable material maybe present on a substrate. The substrate may, for example, be or comprise paper, card, paperboard, cardboard, reconstituted aerosolisable material, a plastics material, a ceramic material, a composite material, glass, a metal, or a metal alloy.

In the present example, the aerosol forming material added to the aerosol generating material 3 comprises 14% by weight of the aerosol generating material 3. Preferably, the aerosol forming material comprises at least 5% by weight of the aerosol generating material, more preferably at least 10%. Preferably, the aerosol forming material comprises less than 25% by weight of the aerosol generating material, more preferably less than 20%, for instance between 10% and 20%, between 12% and 18% or between 13% and 16%.

Preferably the aerosol generating material 3 is provided as a cylindrical rod of aerosol generating material. Irrespective of the form of the aerosol generating material, it preferably has a length of about 10 mm to too mm. In some embodiments, the length of the aerosol generating material is preferably in the range about 25 mm to 50 mm, more preferably in the range about 30 mm to 45 mm, and still more preferably about 30 mm to 40 mm.

The volume of aerosol generating material 3 provided can vary from about 200 mm3 to about 4300 mm3, preferably from about 500 mm3 to 1500 mm3, more preferably from about 1000 mm3 to about 1300 mm3. The provision of these volumes of aerosol generating material, for instance from about 1000 mm3 to about 1300 mm3, has been advantageously shown to achieve a superior aerosol, having a greater visibility and sensory performance compared to that achieved with volumes selected from the lower end of the range.

The mass of aerosol generating material 3 provided can be greater than 200 mg, for instance from about 200 mg to 400 mg, preferably from about 230 mg to 360 mg, more preferably from about 250 mg to 360 mg. It has been advantageously found that providing a higher mass of aerosol generating material results in improved sensory performance compared to aerosol generated from a lower mass of tobacco material.

Preferably the aerosol generating material 3 is formed from tobacco material as described herein, which includes a tobacco component. In the tobacco material described herein, the tobacco component preferably contains paper reconstituted tobacco. The tobacco component may also contain leaf tobacco, extruded tobacco, and/or bandcast tobacco. The aerosol generating material 3 can comprise reconstituted tobacco material having a density of less than about 700 milligrams per cubic centimetre (mg/cc). Such tobacco material has been found to be particularly effective at providing an aerosol generating material which can be heated quickly to release an aerosol, as compared to denser materials. For instance, the inventors tested the properties of various aerosol generating materials, such as bandcast reconstituted tobacco material and paper reconstituted tobacco material, when heated. It was found that, for each given aerosol generating material, there is a particular zero heat flow temperature below which net heat flow is endothermic, in other words more heat enters the material than leaves the material, and above which net heat flow is exothermic, in other words more heat leaves the material than enters the material, while heat is applied to the material. Materials having a density less than 700 mg/ cc had a lower zero heat flow temperature. Since a significant portion of the heat flow out of the material is via the formation of aerosol, having a lower zero heat flow temperature has a beneficial effect on the time it takes to first release aerosol from the aerosol generating material. For instance, aerosol generating materials having a density of less than 700 mg/ cc were found to have a zero heat flow temperature of less than I64°C, as compared to materials with a density over 700 mg/ cc, which had zero heat flow temperatures greater than I64°C.

The density of the aerosol generating material also has an impact on the speed at which heat conducts through the material, with lower densities, for instance those below 700 mg/ cc, conducting heat more slowly through the material, and therefore enabling a more sustained release of aerosol.

Preferably, the aerosol generating material 3 comprises reconstituted tobacco material having a density of less than about 700 mg/ cc, for instance paper reconstituted tobacco material. More preferably, the aerosol generating material 3 comprises reconstituted tobacco material having a density of less than about 600 mg/cc. Alternatively or in addition, the aerosol generating material 3 preferably comprises reconstituted tobacco material having a density of at least 350 mg/cc, which is considered to allow for a sufficient amount of heat conduction through the material. The tobacco material maybe provided in the form of cut rag tobacco. The cut rag tobacco can have a cut width of at least 15 cuts per inch (about 5.9 cuts per cm, equivalent to a cut width of about 1.7mm). Preferably, the cut rag tobacco has a cut width of at least 18 cuts per inch (about 7.1 cuts per cm, equivalent to a cut width of about 1.4mm), more preferably at least 20 cuts per inch (about 7.9 cuts per cm, equivalent to a cut width of about 1.27mm). In one example, the cut rag tobacco has a cut width of 22 cuts per inch (about 8.7 cuts per cm, equivalent to a cut width of about 1.15mm). Preferably, the cut rag tobacco has a cut width at or below 40 cuts per inch (about 15.7 cuts per cm, equivalent to a cut width of about 0.64mm). Cut widths between 0.5 mm and 2.0 mm, for instance between 0.6 mm and 1.5 mm, or between

0.6 mm and 1.7 mm have been found to result in tobacco material which is preferable in terms of surface area to volume ratio, particularly when heated, and the overall density and pressure drop of the material 3. The cut rag tobacco can be formed from a mixture of forms of tobacco material, for instance a mixture of one or more of paper reconstituted tobacco, leaf tobacco, extruded tobacco and bandcast tobacco. Preferably the tobacco material comprises paper reconstituted tobacco or a mixture of paper reconstituted tobacco and leaf tobacco.

In the tobacco material described herein, the tobacco material may contain a filler component. The filler component is generally a non-tobacco component, that is, a component that does not include ingredients originating from tobacco. The filler component may be a non-tobacco fibre such as wood fibre or pulp or wheat fibre. The filler component may also be an inorganic material such as chalk, perlite, vermiculite, diatomaceous earth, colloidal silica, magnesium oxide, magnesium sulphate, magnesium carbonate. The filler component may also be a non-tobacco cast material or a non-tobacco extruded material. The filler component maybe present in an amount of o to 20% by weight of the tobacco material, or in an amount of from 1 to 10% by weight of the composition. In some embodiments, the filler component is absent. In the tobacco material described herein, the tobacco material contains an aerosol forming material. In this context, an "aerosol forming material" is an agent that promotes the generation of an aerosol. An aerosol forming material may promote the generation of an aerosol by promoting an initial vaporisation and/or the condensation of a gas to an inhalable solid and/or liquid aerosol. In some embodiments, an aerosol forming material may improve the delivery of flavour from the aerosol generating material. In general, any suitable aerosol forming material or agents may be included in the aerosol generating material of the invention, including those described herein. Other suitable aerosol forming materials include, but are not limited to: a polyol such as sorbitol, glycerol, and glycols like propylene glycol or triethylene glycol; a non-polyol such as monohydric alcohols, high boiling point hydrocarbons, acids such as lactic acid, glycerol derivatives, esters such as diacetin, triacetin, triethylene glycol diacetate, triethyl citrate or myristates including ethyl myristate and isopropyl myristate and aliphatic carboxylic acid esters such as methyl stearate, dimethyl dodecanedioate and dimethyl tetradecanedioate. In some embodiments, the aerosol forming material may be glycerol, propylene glycol, or a mixture of glycerol and propylene glycol. Glycerol may be present in an amount of from to to 20 % by weight of the tobacco material, for example 13 to 16 % by weight of the composition, or about 14% or 15% by weight of the composition. Propylene glycol, if present, maybe present in an amount of from 0.1 to 0.3% by weight of the composition. The aerosol forming material may be included in any component, for example any tobacco component, of the tobacco material, and/ or in the filler component, if present. Alternatively or additionally the aerosol forming material may be added to the tobacco material separately. In either case, the total amount of the aerosol forming material in the tobacco material can be as defined herein.

The tobacco material can contain between 10% and 90% by weight tobacco leaf, wherein the aerosol forming material is provided in an amount of up to about 10% by weight of the leaf tobacco. To achieve an overall level of aerosol forming material between 10% and 20% by weight of the tobacco material, it has been advantageously found that this can be added in higher weight percentages to the another component of the tobacco material, such as reconstituted tobacco material.

The tobacco material described herein contains nicotine. The nicotine content is from 0.5 to 1.75% by weight of the tobacco material, and maybe, for example, from 0.8 to 1.5% by weight of the tobacco material. Additionally or alternatively, the tobacco material contains between 10% and 90% by weight tobacco leaf having a nicotine content of greater than 1.5% by weight of the tobacco leaf. It has been advantageously found that using a tobacco leaf with nicotine content higher than 1.5% in combination with a lower nicotine base material, such as paper reconstituted tobacco, provides a tobacco material with an appropriate nicotine level but better sensory performance than the use of paper reconstituted tobacco alone. The tobacco leaf, for instance cut rag tobacco, can, for instance, have a nicotine content of between 1.5% and 5% by weight of the tobacco leaf.

The tobacco material described herein can contain an aerosol modifying agent, such as any of the flavours described herein. In one embodiment, the tobacco material contains menthol, forming a mentholated article. The tobacco material can comprise from 3mg to 2omg of menthol, preferably between 5mg and i8mg and more preferably between 8mg and i6mg of menthol. In the present example, the tobacco material comprises i6mg of menthol. The tobacco material can contain between 2% and 8% by weight of menthol, preferably between 3% and 7% by weight of menthol and more preferably between 4% and 5.5% by weight of menthol. In one embodiment, the tobacco material includes 4.7% by weight of menthol. Such high levels of menthol loading can be achieved using a high percentage of reconstituted tobacco material, for instance greater than 50% of the tobacco material by weight. Alternatively or additionally, the use of a high volume of aerosol generating material, for instance tobacco material, can increase the level of menthol loading that can be achieved, for instance where greater than about 500 mm3₀r suitably more than about 1000 mm3₀f aerosol generating material, such as tobacco material, are used. In the compositions described herein, where amounts are given in % by weight, for the avoidance of doubt this refers to a dry weight basis, unless specifically indicated to the contrary. Thus, any water that maybe present in the tobacco material, or in any component thereof, is entirely disregarded for the purposes of the determination of the weight %. The water content of the tobacco material described herein may vary and may be, for example, from 5 to 15% by weight. The water content of the tobacco material described herein may vary according to, for example, the temperature, pressure and humidity conditions at which the compositions are maintained. The water content can be determined by Karl-Fisher analysis, as known to those skilled in the art. On the other hand, for the avoidance of doubt, even when the aerosol forming material is a component that is in liquid phase, such as glycerol or propylene glycol, any component other than water is included in the weight of the tobacco material. However, when the aerosol forming material is provided in the tobacco component of the tobacco material, or in the filler component (if present) of the tobacco material, instead of or in addition to being added separately to the tobacco material, the aerosol forming material is not included in the weight of the tobacco component or filler component, but is included in the weight of the "aerosol forming material" in the weight % as defined herein. All other ingredients present in the tobacco component are included in the weight of the tobacco component, even if of non-tobacco origin (for example non tobacco fibres in the case of paper reconstituted tobacco). In an embodiment, the tobacco material comprises the tobacco component as defined herein and the aerosol forming material as defined herein. In an embodiment, the tobacco material consists essentially of the tobacco component as defined herein and the aerosol forming material as defined herein. In an embodiment, the tobacco material consists of the tobacco component as defined herein and the aerosol forming material as defined herein.

Paper reconstituted tobacco is present in the tobacco component of the tobacco material described herein in an amount of from 10% to 100% by weight of the tobacco component. In embodiments, the paper reconstituted tobacco is present in an amount of from 10% to 80% by weight, or 20% to 70% by weight, of the tobacco component. In a further embodiment, the tobacco component consists essentially of, or consists of, paper reconstituted tobacco. In preferred embodiments, leaf tobacco is present in the tobacco component of the tobacco material in an amount of from at least 10% by weight of the tobacco component. For instance, leaf tobacco can be present in an amount of at least 10% by weight of the tobacco component, while the remainder of the tobacco component comprises paper reconstituted tobacco, bandcast reconstituted tobacco, or a combination of bandcast reconstituted tobacco and another form of tobacco such as tobacco granules. Paper reconstituted tobacco refers to tobacco material formed by a process in which tobacco feedstock is extracted with a solvent to afford an extract of solubles and a residue comprising fibrous material, and then the extract (usually after concentration, and optionally after further processing) is recombined with fibrous material from the residue (usually after refining of the fibrous material, and optionally with the addition of a portion of non-tobacco fibres) by deposition of the extract onto the fibrous material. The process of recombination resembles the process for making paper.

The paper reconstituted tobacco may be any type of paper reconstituted tobacco that is known in the art. In a particular embodiment, the paper reconstituted tobacco is made from a feedstock comprising one or more of tobacco strips, tobacco stems, and whole leaf tobacco. In a further embodiment, the paper reconstituted tobacco is made from a feedstock consisting of tobacco strips and/or whole leaf tobacco, and tobacco stems. However, in other embodiments, scraps, fines and winnowings can alternatively or additionally be employed in the feedstock. The paper reconstituted tobacco for use in the tobacco material described herein may be prepared by methods which are known to those skilled in the art for preparing paper reconstituted tobacco.

In the present example, the article T has an outer circumference of about 21 mm (i.e. the article is in the demi-slim format). In other examples, the article can be provided in any of the formats described herein, for instance having an outer circumference of between 15 mm and 25 mm. Since the article is to be heated to release an aerosol, improved heating efficiency can be achieved using articles having lower outer circumferences within this range, for instance circumferences of less than 23 mm. To achieve improved aerosol via heating, while maintaining a suitable product length, article circumferences of greater than 19 mm have also been found to be particularly effective. Articles having circumferences of between 19 mm and 23 mm, and more preferably between 20 mm and 22 mm, have been found to provide a good balance between providing effective aerosol delivery while allowing for efficient heating.

The outer circumference of the mouthpiece 2’ is substantially the same as the outer circumference of the rod of aerosol generating material 3, such that there is a smooth transition between these components. In the present example, the outer circumference of the mouthpiece 2’ is about 20.8mm. A tipping paper 5 is wrapped around the full length of the mouthpiece 2’ and over part of the rod of aerosol generating material 3 and has an adhesive on its inner surface to connect the mouthpiece 2’ and rod 3. In the present example, the tipping paper 5 extends 5 mm over the rod of aerosol generating material 3 but it can alternatively extend between 3 mm and 10 mm over the rod 3, or more preferably between 4 mm and 6 mm, to provide a secure attachment between the mouthpiece 2’ and rod 3. The tipping paper 5 can have a basis weight which is higher than the basis weight of plug wraps used in the article T, for instance a basis weight of 40 gsm to 80 gsm, more preferably between 50 gsm and 70 gsm, and in the present example 58 gsm. These ranges of basis weights have been found to result in tipping papers having acceptable tensile strength while being flexible enough to wrap around the article 1 and adhere to itself along a longitudinal lap seam on the paper. The outer circumference of the tipping paper 5, once wrapped around the mouthpiece 2’, is about 21mm.

Figure 3 is a side on, cross sectional view of a further article 1”. Article 1” is substantially the same as article 1’, except that mouthpiece 2” comprises a second hollow tubular element 13 at the mouth end 2”b, in place of the body of fibrous material

4·

Second hollow tubular element 13 is formed from filamentary tow. This has advantageously been found to significantly reduce the temperature of the outer surface of the mouthpiece 2” at the downstream end 2”b of the mouthpiece which comes into contact with a consumer’s mouth when the article 1” is in use. In addition, the use of the tubular element 13 has also been found to significantly reduce the temperature of the outer surface of the mouthpiece 2” even upstream of the tubular element 13. Without wishing to be bound by theory, it is hypothesised that this is due to the tubular element 13 channelling aerosol closer to the centre of the mouthpiece 2”, and therefore reducing the transfer of heat from the aerosol to the outer surface of the mouthpiece 2”.

The "wall thickness" of the second hollow tubular element 13 corresponds to the thickness of the wall of the tube 13 in a radial direction. This may be measured in the same way as for hollow tubular element 8. The wall thickness is advantageously greater than 0.9 mm, and more preferably 1.0 mm or greater. Preferably, the wall thickness is substantially constant around the entire wall of the second hollow tubular element 11. However, where the wall thickness is not substantially constant, the wall thickness is preferably greater than 0.9 mm at any point around the second hollow tubular element 11, more preferably 1.0 mm or greater.

Preferably, the length of the second hollow tubular element 13 is less than about 20 mm. More preferably, the length of the second hollow tubular element 13 is less than about 15 mm. Still more preferably, the length of the second hollow tubular element 13 is less than about 10 mm. In addition, or as an alternative, the length of the second hollow tubular element 13 is at least about 5 mm. Preferably, the length of the second hollow tubular element 13 is at least about 6 mm. In some preferred embodiments, the length of the second hollow tubular element 13 is from about 5 mm to about 20 mm, more preferably from about 6 mm to about 10 mm, even more preferably from about 6 mm to about 8 mm, most preferably about 6 mm, 7 mm or about 8 mm. In the present example, the length of the second hollow tubular element 13 is 6 mm.

Preferably, the density of the second hollow tubular element 13 is at least about 0.25 grams per cubic centimetre (g/cc), more preferably at least about 0.3 g/cc. Preferably, the density of the second hollow tubular element 13 is less than about 0.75 grams per cubic centimetre (g/cc), more preferably less than 0.6 g/cc. In some embodiments, the density of the second hollow tubular element i3is between 0.25 and 0.75 g/cc, more preferably between 0.3 and 0.6 g/cc, and more preferably between 0.4 g/cc and 0.6 g/cc or about 0.5 g/cc. These densities have been found to provide a good balance between improved firmness afforded by denser material and the lower heat transfer properties of lower density material. For the purposes of the present example, the "density" of the second hollow tubular element 13 refers to the density of the filamentary tow forming the element with any plasticiser incorporated. The density of the second hollow tubular element 13 may be determined in the same way as described for the body 6.

The filamentary tow forming the second hollow tubular element 13 preferably has a total denier of less than 45,000, more preferably less than 42,000. This total denier has been found to allow the formation of a tubular element 13 which is not too dense. Preferably, the total denier is at least 20,000, more preferably at least 25,000. In preferred embodiments, the filamentary tow forming the second hollow tubular element 13 has a total denier between 25,000 and 45,000, more preferably between 35,000 and 45,000. Preferably the cross-sectional shape of the filaments of tow are Ύ’ shaped, although in other embodiments other shapes such as ‘X’ shaped filaments can be used.

The filamentary tow forming the second hollow tubular element 13 preferably has a denier per filament of greater than 3. This denier per filament has been found to allow the formation of a tubular element 13 which is not too dense. Preferably, the denier per filament is at least 4, more preferably at least 5. In preferred embodiments, the filamentary tow forming the second hollow tubular element 13 has a denier per filament between 4 and 10, more preferably between 4 and 9. In one example, the filamentary tow forming the second hollow tubular element 13 has an 8Y40,000 tow formed from cellulose acetate and comprising 18% plasticiser, for instance triacetin. The second hollow tubular element 13 preferably has an internal diameter of greater than 3.0mm. Smaller diameters than this can result in increasing the velocity of aerosol passing though the mouthpiece 2 to the consumers’ mouth more than is desirable, such that the aerosol becomes too warm, for instance reaching temperatures greater than 40°C or greater than 45°C. More preferably, the second hollow tubular element 13 has an internal diameter of greater than 3.1mm, and still more preferably greater than 3.5 mm or 3.6 mm. In one embodiment, the internal diameter of the second hollow tubular element 13 is about 3.9 mm. The second hollow tubular element 13 preferably comprises from 15% to 22% by weight of plasticiser. For cellulose acetate tow, the plasticiser is preferably triacetin, although other plasticisers such as polyethelyne glycol (PEG) can be used. More preferably, the tubular element 13 comprises from 16% to 20% by weight of plasticiser, for instance about 17%, about 18% or about 19% plasticiser.

The combination of the aerosol cooling effect of hollow tubular element 8 and body 6, and of second hollow tubular element 13 providing a reduced temperature of the outer surface of the mouthpiece together result in a more comfortable user experience, since the aerosol temperature, and the temperature of the outer surface of the article at the mouth end are reduced.

Figure 4 is a side on, cross sectional view of a further article T”. Article T” and mouthpiece 2’” are substantially the same as Article 1’ and mouthpiece 2’, except that body 6 of amorphous solid material is provided at the distal end of the mouthpiece 2’”, adjacent to and in an abutting relationship with the aerosol generating material 3, and hollow tubular element 8 is provided downstream of the body 6, positioned in between body 6 at the distal end of the mouthpiece and fibrous section 4 at the mouth end of the mouthpiece. Providing body 6 of amorphous solid material adjacent to the aerosol generating material results in the body 6 being subject to greater heating compared to when body 6 is positioned downstream of the cooling element. The result of this arrangement can be improved release of flavour from the amorphous solid material, when said amorphous solid material contains a flavourant. Figure 5a is a side-on cross sectional view of a further article 1”” including a capsule- containing mouthpiece 2””. Figure 5b is a cross sectional view of the capsule- containing mouthpiece shown in Figure 5a. Article 1”” and mouthpiece 2”” are the same as article 1’ and mouthpiece 2’, except that in addition to hollow tubular element 8, body 6 of amorphous solid material, and body of fibrous material 4, mouthpiece 2”” includes a capsule containing section 14. Capsule containing section 14 comprises an aerosol modifying agent provided in the form of a capsule 15, and is surrounded by an oil resistant plug wrap 16. In other examples, the aerosol modifying agent can be provided in other forms, such as material injected into the body of fibrous material 4 or provided on a thread, for instance the thread carrying a flavourant or other aerosol modifying agent, which may also be disposed within the body of fibrous material 4. The amorphous solid material forming the body 6 may also comprise an aerosol modifying agent, such as a flavourant. Where the amorphous solid material comprises a flavourant, the aerosol modifying agent contained within capsule 15 maybe selected to be complementary to the flavourant contained in the amorphous solid material.

The capsule 15 can comprise a breakable capsule, for instance a capsule which has a solid, frangible shell surrounding a liquid payload. In the present example, a single capsule 15 is used. The capsule 15 is entirely embedded within a body of material, which is substantially the same as body of fibrous material 4. In other words, the capsule 15 is completely surrounded by the material forming the body 14. In other examples, a plurality of breakable capsules maybe disposed within the body of material 14, for instance 2, 3 or more breakable capsules. The length of the body of material 14 can be increased to accommodate the number of capsules required. In examples where a plurality of capsules is used, the individual capsules may be the same as each other, or may differ from one another in terms of size and/or capsule payload. In other examples, multiple bodies of material 14 may be provided, with each body containing one or more capsules.

The capsule 15 has a core-shell structure. In other words, the capsule 15 comprises a shell encapsulating a liquid agent, for instance a flavourant or other agent, which can be any one of the flavourants or aerosol modifying agents described herein. The shell of the capsule can be ruptured by a user to release the flavourant or other agent into the body of material 14. The oil resistant plug wrap 16 can comprise a barrier coating to make the material of the plug wrap substantially impermeable to the liquid payload of the capsule 15. Alternatively or in addition, the second plug wrap 9 and/or tipping paper 5 can comprise a barrier coating to make the material of that plug wrap and/ or tipping paper substantially impermeable to the liquid payload of the capsule 15.

In the present example, the capsule 15 is spherical and has a diameter of about 3 mm.

In other examples, other shapes and sizes of capsule can be used. The total weight of the capsule 15 may be in the range about 10 mg to about 50 mg. In the present example, the capsule 15 is located at a longitudinally central position within the body of material 14. That is, the capsule 15 is positioned so that its centre is 4 mm from each end of the body of material 14. In other examples, the capsule 15 can be located at a position other than a longitudinally central position in the body of material 14, i.e. closer to the downstream end of the body of material 14 than the upstream end, or closer to the upstream end of the body of material 14 than the downstream end. Preferably, the mouthpiece 2”” is configured so that the capsule 15 and the ventilation holes 12 are longitudinally offset from each other in the mouthpiece A cross section of the mouthpiece 2”” is shown in Figure 5b. Figure 5b shows the capsule 15, the body of material 14, the oil resistant plug wrap 16, the third plug wrap 11, and the tipping paper 5. In the present example, the capsule 15 is centred on the longitudinal axis (not shown) of the mouthpiece 2””. The oil resistant plug wrap 16, the third plug wrap 11, and the tipping paper 5 are arranged concentrically around the body of material 14.

The breakable capsule 15 has a core-shell structure. That is, the encapsulating material or barrier material creates a shell around a core that comprises the aerosol modifying agent. The shell structure hinders migration of the aerosol modifying agent during storage of the article 1”” but allows controlled release of the aerosol modifying agent, also referred to as an aerosol modifier, during use.

In some cases, the barrier material (also referred to herein as the encapsulating material) is frangible. The capsule is crushed or otherwise fractured or broken by the user to release the encapsulated aerosol modifier. Typically, the capsule is broken immediately prior to heating being initiated but the user can select when to release the aerosol modifier. The term "breakable capsule" refers to a capsule, wherein the shell can be broken by means of a pressure to release the core; more specifically the shell can be ruptured under the pressure imposed by the user's fingers when the user wants to release the core of the capsule.

In some cases, the barrier material is heat resistant. That is to say, in some cases, the barrier will not rupture, melt or otherwise fail at the temperature reached at the capsule site during operation of the aerosol provision device. Illustratively, a capsule located in a mouthpiece maybe exposed to temperatures in the range of 30°C to ioo°C for example, and the barrier material may continue to retain the liquid core up to at least about 50°C to 120°C.

In other cases, the capsule releases the core composition on heating, for example by melting of the barrier material or by capsule swelling leading to rupture of the barrier material.

The total weight of a capsule may be in the range of about 1 mg to about too mg, suitably about 5 mg to about 60 mg, about 8 mg to about 50 mg, about 10 mg to about 20 mg, or about 12 mg to about 18 mg.

The total weight of the core formulation may be in the range of about 2 mg to about 90 mg, suitably about 3 mg to about 70 mg, about 5 mg to about 25 mg, about 8 mg to about 20 mg, or about 10 mg to about 15 mg. The capsule according to the invention comprises a core as described above, and a shell. The capsules may present a crush strength from about 4.5 N to about 40 N, more preferably from about 5 N to about 30 N or to about 28 N (for instance about 9.8 N to about 24.5 N). The capsule burst strength can be measured when the capsule is removed from the body of material 14 and using a force gauge to measure the force at which the capsule bursts when pressed between two flat metal plates. A suitable measurement device is the Sauter FK 50 force gauge with a flat headed attachment, which can be used to crush the capsule against a flat, hard surface having a surface similar to the attachment. The capsules may be substantially spherical and have a diameter of at least about 0.4 mm, 0.6 mm, 0.8 mm, 1.0 mm, 2.0 mm, 2.5 mm, 2.8 mm or 3.0 mm. The diameter of the capsules maybe less than about 10.0 mm, 8.0 mm, 7.0 mm, 6.0 mm, 5.5 mm, 5.0 mm, 4.5 mm, 4.0 mm, 3.5 mm or 3.2 mm. Illustratively, the capsule diameter maybe in the range of about 0.4 mm to about 10.0 mm, about 0.8 mm to about 6.0 mm, about 2.5 mm to about 5.5 mm or about 2.8 mm to about 3.2 mm. In some cases, the capsule may have a diameter of about 3.0 mm. These sizes are particularly suitable for incorporation of the capsule into an article as described herein.

The cross-sectional area of the capsule 15 at its largest cross sectional area is in some embodiments less than 28% of the cross sectional area of the portion of the mouthpiece 2’ in which the capsule 15 is provided, more preferably less than 27% and still more preferably less than 25%. For instance, for the spherical capsule having a diameter of 3.0 mm, the largest cross sectional area of the capsule is 7.07 mm². For the mouthpiece 2”” having a circumference of 21 mm as described herein, the body of material 14 has an outer circumference of 20.8 mm, and the radius of this component will be 3.31 mm, corresponding to a cross sectional area of 34.43 mm². The capsule cross sectional area is, in this example, 20.5% of the cross-sectional area of the mouthpiece 2””. As another example, if the capsule had a diameter of 3.2mm, its largest cross sectional area would be 8.04 mm². In this case, the cross sectional area of the capsule would be 23.4% of the cross sectional area of the body of material 14. A capsule with a largest cross sectional area less than 28% of the cross sectional area of the portion of the mouthpiece 2”” in which the capsule 15 is provided has the advantage that the pressure drop across the mouthpiece 2”” is reduced as compared to capsules with larger cross sectional areas and adequate space remains around the capsule for aerosol to pass without the body of material 14 removing significant amounts of the aerosol mass as it passes through the mouthpiece 2””.

Preferably the pressure drop or difference (also referred to a resistance to draw) across the article, measured as the open pressure drop (i.e. with the ventilation openings open), reduces by less than 8 mmH₂0 when the capsule is broken. More preferably, the open pressure drop reduces by less than 6 mmH₂0 and more preferably less than 5 mmH₂0. These values are measured as the average achieved by at least 80 articles made to the same design. Such small changes in pressure drop mean that other aspects of the product design, such as setting the correct ventilation level for a given product pressure drop, can be achieved irrespective of whether or not the consumer chooses to break the capsule. In some embodiments, when the aerosol generating material 3 is heated to provide an aerosol, for instance within a non-combustible aerosol provision device as described herein, the part of the mouthpiece 2 in which the capsule is located reaches a temperature of between 58 and 70 degrees Centigrade during use of the system to generate an aerosol. As a result of this temperature, the capsule contents are warmed sufficiently to promote volatisation of the capsule contents, for instance an aerosol modifying agent, into the aerosol formed by the system as the aerosol passes through the mouthpiece 2””. Warming the content of the capsule 15 can take place, for instance, before the capsule 15 has been broken, such that when the capsule 15 is broken, its contents are more readily released into the aerosol passing through the mouthpiece 2””. Alternatively, the content of the capsule 15 can be warmed to this temperature after the capsule 15 has been broken, again resulting in the increased release of the content into the aerosol. Advantageously, mouthpiece temperatures in the range of 58 to 70 degrees Centigrade have been found to be high enough that the capsule content can be more readily released, but low enough that the outer surface of the portion of the mouthpiece 2”” in which the capsule is located does not reach an uncomfortable temperature for the consumer to touch in order to burst the capsule 15 by squeezing on the mouthpiece 2””. The capsule 15 is breakable by external force applied to the mouthpiece 2””, for instance by a consumer using their fingers or other mechanism to squeeze the mouthpiece 2””. As described above, the part of the mouthpiece in which the capsule is located is arrange to reach a temperature of greater than 58°C during use of the aerosol provision system to generate an aerosol. Preferably, the burst strength of the capsule 15 when located within the mouthpiece 2”” and prior to heating of the aerosol generating material 3 is between 1500 and 4000 grams force. Preferably, the burst strength of the capsule 15 when located within the mouthpiece 2”” and within 30 seconds of use of the aerosol provision system to generate an aerosol is between 1000 and 4000 grams force. Accordingly, despite being subjected to a temperature above 58 °C, for instance between 58°C to 70°C, the capsule 15 is able to maintain a burst strength within a range which has been found to enable the capsule 15 to be readily crushable by a consumer, while providing the consumer with sufficient tactile feedback that the capsule 15 has been broken. Maintaining such a burst strength is achieved by selecting an appropriate gelling agent for the capsule, as described herein, such as a polysaccharide including, for instance, gum Arabic, gellan gum, acacia gum, xanthan gums or carrageenans, alone or in combination with gelatine. In addition, a suitable wall thickness for the capsule shell should be selected.

Suitably, the burst strength of the capsule when located within the mouthpiece and prior to heating of the aerosol generating material is between 2000 and 3500 grams force, or between 2500 and 3500 grams force. Suitably, the burst strength of the capsule when located within the mouthpiece and within 30 s of use of the system to generate an aerosol is between 1500 and 4000 grams force, or between 1750 and 3000 grams force. In one example, the average burst strength of the capsule when located within the mouthpiece and prior to heating of the aerosol generating material is about 3175 grams force and the average burst strength of the capsule when located within the mouthpiece and within 30 s of use of the system to generate an aerosol is about 2345 grams force. The burst strength of the capsule can be tested using a force measuring instrument such as a Texture Analyser.

The barrier material may comprise one or more of a gelling agent, a bulking agent, a buffer, a colouring agent and a plasticiser.

Suitably, the gelling agent may be, for example, a polysaccharide or cellulosic gelling agent, a gelatin, a gum, a gel, a wax or a mixture thereof. Suitable polysaccharides include alginates, dextrans, maltodextrins, cyclodextrins and pectins. Suitable alginates include, for instance, a salt of alginic acid, an esterified alginate or glyceryl alginate. Salts of alginic acid include ammonium alginate, triethanolamine alginate, and group I or II metal ion alginates like sodium, potassium, calcium and magnesium alginate. Esterified alginates include propylene glycol alginate and glyceryl alginate. In an embodiment, the barrier material is sodium alginate and/ or calcium alginate. Suitable cellulosic materials include methyl cellulose, ethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, carboxymethyl cellulose, cellulose acetate and cellulose ethers. The gelling agent may comprise one or more modified starches. The gelling agent may comprise carrageenans. Suitable gums include agar, gellan gum, gum Arabic, pullulan gum, mannan gum, gum ghatti, gum tragacanth, Karaya, locust bean, acacia gum, guar, quince seed and xanthan gums. Suitable gels include agar, agarose, carrageenans, furoidan and furcellaran. Suitable waxes include carnauba wax. In some cases, the gelling agent may comprise carrageenans and/or gellan gum; these gelling agents are particularly suitable for inclusion as the gelling agent as the pressure required to break the resulting capsules is particularly suitable.

The barrier material may comprise one or more bulking agents, such as starches, modified starches (such as oxidised starches) and sugar alcohols such as maltitol.

The barrier material may comprise a colouring agent which renders easier the location of the capsule within the aerosol generating device during the manufacturing process of the aerosol generating device. The colouring agent is preferably chosen among colorants and pigments.

The barrier material may further comprise at least one buffer, such as a citrate or phosphate compound. The barrier material may further comprise at least one plasticiser, which may be glycerol, sorbitol, maltitol, triacetin, polyethylene glycol, propylene glycol or another polyalcohol with plasticising properties, and optionally one acid of the monoacid, diacid or triacid type, especially citric acid, fumaric acid, malic acid, and the like. The amount of plasticiser ranges from 1% to 30% by weight, preferably from 2% to 15% by weight, and even more preferably from 3 to 10% by weight of the total dry weight of the shell.

The barrier material may also comprise one or more filler materials. Suitable filler materials include comprising starch derivatives such as dextrin, maltodextrin, cyclodextrin (alpha, beta or gamma), or cellulose derivatives such as hydroxypropyl- methylcellulose (HPMC), hydroxypropylcellulose (HPC), methylcellulose (MC), carboxy-methylcellulose (CMC), polyvinyl alcohol, polyols or mixture thereof. Dextrin is a preferred filler. The amount of filler in the shell is at most 98.5%, preferably from 25 to 95% more preferably from 40 to 80% and even more preferably from 50 to 60 % by weight on the total dry weight of the shell.

The capsule shell may additionally comprise a hydrophobic outer layer which reduces the susceptibility of the capsule to moisture-induced degradation. The hydrophobic outer layer is suitably selected from the group comprising waxes, especially carnauba wax, candelilla wax or beeswax, carbowax, shellac (in alcoholic or aqueous solution), ethyl cellulose, hydroxypropyl methyl cellulose, hydroxyl- propylcellulose, latex composition, polyvinyl alcohol, or a combination thereof. More preferably, the at least one moisture barrier agent is ethyl cellulose or a mixture of ethyl cellulose and shellac.

The capsule core comprises the aerosol modifier. This aerosol modifier may be any volatile substance which modifies at least one property of the aerosol. For example, the aerosol substance may modify the pH, the sensorial properties, the water content, the delivery characteristics or the flavour. In some cases, the aerosol modifier may be selected from an acid, a base, water or a flavourant. In some embodiments, the aerosol modifier comprises one or more flavourants.

The flavourant may suitably be licorice, rose oil, vanilla, lemon oil, orange oil, a mint- flavour, suitably menthol and/or a mint oil from any species of the genus Mentha such as peppermint oil and/or spearmint oil, or lavender, fennel or anise. In some cases, the flavourant comprises menthol.

In some cases, the capsule may comprise at least about 25% w/w flavourant (based on the total weight of the capsule), suitably at least about 30% w/w flavourant, 35% w/w flavourant, 40% w/w flavourant, 45% w/w flavourant or 50% w/w flavourant.

In some cases, the core may comprise at least about 25% w/w flavourant (based on the total weight of the core), suitably at least about 30% w/w flavourant, 35% w/w flavourant, 40% w/w flavourant, 45% w/w flavourant or 50% w/w flavourant. In some cases, the core may comprise less than or equal to about 75% w/w flavourant (based on the total weight of the core), suitably less than or equal to about 65% w/w flavourant, 55% w/w flavourant, or 50% w/w flavourant. Illustratively, the capsule may include an amount of flavourant in the range of 25-75% w/w (based on the total weight of the core), about 35-60% w/w or about 40-55% w/w. The capsules may include at least about 2 mg, 3 mg or 4 mg of the aerosol modifier, suitably at least about 4.5 mg of the aerosol modifier, 5 mg of the aerosol modifier, 5.5 mg of the aerosol modifier or 6 mg of the aerosol modifier.

In some cases, the consumable comprises at least about 7 mg of the aerosol modifier, suitably at least about 8 mg of the aerosol modifier, 10 mg of the aerosol modifier, 12 mg of the aerosol modifier or 15 mg of the aerosol modifier. The core may also comprise a solvent which dissolves the aerosol modifier.

Any suitable solvent may be used.

Where the aerosol modifier comprises a flavourant, the solvent may suitably comprise short or medium chain fats and oils. For example, the solvent may comprise tri-esters of glycerol such as C2-C12 triglycerides, suitably C6-C10 triglycerides or Cs- C12 triglycerides. For example, the solvent may comprise medium chain triglycerides (MCT - C8-C12), which may be derived from palm oil and/ or coconut oil.

The esters maybe formed with caprylic acid and/or capric acid. For example, the solvent may comprise medium chain triglycerides which are caprylic triglycerides and/or capric tryglycerides. For example, the solvent may comprise compounds identified in the CAS registry by numbers 73398-61-5, 65381-09-1, 85409-09-2. Such medium chain triglycerides are odourless and tasteless.

The hydrophilic-lipophilic balance (HLB) of the solvent may be in the range of 9 to 13, suitably 10 to 12. Methods of making the capsules include co-extrusion, optionally followed by centrifugation and curing and/ or drying. The contents of WO 2007/ 010407 A2 is incorporated by reference, in its entirety.

Mouthpieces 2, 2’, 2”, 2’”, and 2”” can, in alternative embodiments, each be formed from any combination of the mouthpiece components described herein.

A non-combustible aerosol provision device is used to heat the aerosol generating material 3 of the articles 1, 1’, 1”, 1’”, 1”” described herein. The non-combustible aerosol provision device preferably comprises a coil, since this has been found to enable improved heat transfer to the article 1, 1’, 1”, 1’”, 1”” as compared to other arrangements.

In some examples, the coil is configured to, in use, cause heating of at least one electrically-conductive heating element, so that heat energy is conductible from the at least one electrically-conductive heating element to the aerosol generating material to thereby cause heating of the aerosol generating material. In some examples, the coil is configured to generate, in use, a varying magnetic field for penetrating at least one heating element, to thereby cause induction heating and/ or magnetic hysteresis heating of the at least one heating element. In such an arrangement, the or each heating element may be termed a “susceptor” as defined herein. A coil that is configured to generate, in use, a varying magnetic field for penetrating at least one electrically-conductive heating element, to thereby cause induction heating of the at least one electrically-conductive heating element, may be termed an “induction coil” or “inductor coil”. The device may include the heating element(s), for example electrically-conductive heating element(s), and the heating element(s) may be suitably located or locatable relative to the coil to enable such heating of the heating element(s). The heating element(s) may be in a fixed position relative to the coil. Alternatively, the at least one heating element, for example at least one electrically-conductive heating element, may be included in the article 1, 1’ for insertion into a heating zone of the device, wherein the article 1, 1’ also comprises the aerosol generating material 3 and is removable from the heating zone after use. Alternatively, both the device and such an article 1, 1’ may comprise at least one respective heating element, for example at least one electrically- conductive heating element, and the coil may be to cause heating of the heating element(s) of each of the device and the article when the article is in the heating zone.

In some examples, the coil is helical. In some examples, the coil encircles at least a part of a heating zone of the device that is configured to receive aerosol generating material. In some examples, the coil is a helical coil that encircles at least a part of the heating zone.

In some examples, the device comprises an electrically-conductive heating element that at least partially surrounds the heating zone, and the coil is a helical coil that encircles at least a part of the electrically-conductive heating element. In some examples, the electrically-conductive heating element is tubular. In some examples, the coil is an inductor coil.

In some examples, the use of a coil enables the non-combustible aerosol provision device to reach operational temperature more quickly than a non-coil aerosol provision device. For instance, the non-combustible aerosol provision device including a coil as described above can reach an operational temperature such that a first puff can be provided in less than 30 seconds from initiation of a device heating program, more preferably in less than 25 seconds. In some examples, the device can reach an operational temperature in about 20 seconds from the initiation of a device heating program. The use of a coil as described herein in the device to cause heating of the aerosol generating material has been found to enhance the aerosol which is produced. For instance, consumers have reported that the aerosol generated by a device including a coil such as that described herein is sensorially closer to that generated in factory made cigarette (FMC) products than the aerosol produced by other non-combustible aerosol provision systems. Without wishing to be bound by theory, it is hypothesised that this is the result of the reduced time to reach the required heating temperature when the coil is used, the higher heating temperatures achievable when the coil is used and/or the fact that the coil enables such systems to simultaneously heat a relatively large volume of aerosol generating material, resulting in aerosol temperatures resembling FMC aerosol temperatures. In FMC products, the burning coal generates a hot aerosol which heats tobacco in the tobacco rod behind the coal, as the aerosol is drawn through the rod. This hot aerosol is understood to release flavour compounds from tobacco in the rod behind the burning coal. A device including a coil as described herein is thought to also be capable of heating aerosol generating material, such as tobacco material described herein, to release flavour compounds, resulting in an aerosol which has been reported to more closely resemble an FMC aerosol.

Using an aerosol provision system including a coil as described herein, for instance an induction coil which heats at least some of the aerosol generating material to at least 200°C, more preferably at least 220°C, can enable the generation of an aerosol from an aerosol generating material that has particular characteristics which are thought to more closely resemble those of an FMC product. For example, when heating an aerosol generating material, including nicotine, using an induction heater, heated to at least 250°C, for a two-second period, under an airflow of at least i.50L/m during the period, one or more of the following characteristics has been observed: at least 10 pg of nicotine is aerosolised from the aerosol generating material; the weight ratio in the generated aerosol, of aerosol forming material to nicotine is at least about 2.5:1, suitably at least 8.5:1; at least 100 pg of the aerosol forming material can be aerosolised from the aerosol generating material; the mean particle or droplet size in the generated aerosol is less than about 1000 nm; and the aerosol density is at least o.i pg/cc. In some cases, at least 10 pg of nicotine, suitably at least 30 pg or 40 pg of nicotine, is aerosolised from the aerosol generating material under an airflow of at least i.50L/m during the period. In some cases, less than about 200 pg, suitably less than about 150 pg or less than about 125 pg, of nicotine is aerosolised from the aerosol generating material under an airflow of at least i.50L/m during the period.

In some cases, the aerosol contains at least 100 pg of the aerosol forming material, suitably at least 200 pg, 500 pg or 1 mg of aerosol forming material is aerosolised from the aerosol generating material under an airflow of at least i.50L/m during the period. Suitably, the aerosol forming material may comprise or consist of glycerol.

As defined herein, the term “mean particle or droplet size” refers to the mean size of the solid or liquid components of an aerosol (i.e. the components suspended in a gas). Where the aerosol contains suspended liquid droplets and suspended solid particles, the term refers to the mean size of all components together.

In some cases, the mean particle or droplet size in the generated aerosol may be less than about 900 nm, 800 nm, 700, nm 600 nm, 500nm, 450nm or 400 nm. In some cases, the mean particle or droplet size maybe more than about 25 nm, 50 nm or loonm.

In some cases, the aerosol density generated during the period is at least 0.1 pg/cc. In some cases, the aerosol density is at least 0.2 pg/cc, 0.3 pg/cc or 0.4 pg/cc. In some cases, the aerosol density is less than about 2.5 pg/cc, 2.0 pg/cc, 1.5 pg/cc or 1.0 pg/cc. The non-combustible aerosol provision device is preferably arranged to heat the aerosol generating material 3 of the article 1, 1’, 1”, to a maximum temperature of at least i6o°C. Preferably, the non-combustible aerosol provision device is arranged to heat the aerosol forming material 3 of the article 1, 1’, 1”, to a maximum temperature of at least about 200 °C, or at least about 220 °C, or at least about 240°C, more preferably at least about 270°C, at least once during the heating process followed by the non combustible aerosol provision device. Using an aerosol provision system including a coil as described herein, for instance an induction coil which heats at least some of the aerosol generating material to at least 200°C, more preferably at least 220°C, can enable the generation of an aerosol from an aerosol generating material in an article 1, T, 1”, T”, i”” as described herein that has a higher temperature as the aerosol leaves the mouth end of the mouthpiece 2, 2’, 2”, 2’”, 2”” than previous devices, contributing to the generation of an aerosol which is considered closer to an FMC product. For instance, the maximum aerosol temperature measured at the mouth-end of the article 1, 1’, 1”, 1’”, 1”” can preferably be greater than 50°C, more preferably greater than 55°C and still more preferably greater than 50°C or

57°C. Additionally or alternatively, the maximum aerosol temperature measured at the mouth-end of the article 1, 1’, 1”, 1’”, 1”” can be less than 62°C, more preferably less than 6o°C and more preferably less than 59°C. In some embodiments, the maximum aerosol temperature measured at the mouth-end of the article 1, 1’, 1”, 1’”, 1”” can preferably be between 50°C and 62°C, more preferably between 50°C and 6o°C.

Figure 6 shows an example of a non-combustible aerosol provision device too for generating aerosol from an aerosol generating medium/material such as the aerosol generating material 3 of the articles 1, 1’, 1”, 1’”, 1”” described herein. In broad outline, the device too may be used to heat a replaceable article 110 comprising the aerosol generating medium, for instance the articles 1, 1’, 1”, 1’”, 1”” described herein, to generate an aerosol or other inhalable medium which is inhaled by a user of the device too. The device too and replaceable article 110 together form a system. The device too comprises a housing 102 (in the form of an outer cover) which surrounds and houses various components of the device too. The device too has an opening 104 in one end, through which the article 110 maybe inserted for heating by a heating assembly. In use, the article 110 may be fully or partially inserted into the heating assembly where it may be heated by one or more components of the heater assembly.

The device too of this example comprises a first end member 106 which comprises a lid 108 which is moveable relative to the first end member 106 to close the opening 104 when no article 110 is in place. In Figure 6, the lid 108 is shown in an open configuration, however the lid 108 may move into a closed configuration. For example, a user may cause the lid 108 to slide in the direction of arrow “B”. The device 100 may also include a user-operable control element 112, such as a button or switch, which operates the device 100 when pressed. For example, a user may turn on the device 100 by operating the switch 112.

The device 100 may also comprise an electrical component, such as a socket/port 114, which can receive a cable to charge a battery of the device 100. For example, the socket 114 may be a charging port, such as a USB charging port. Figure 7 depicts the device 100 of Figure 6 with the outer cover 102 removed and without an article 110 present. The device 100 defines a longitudinal axis 134.

As shown in Figure 7, the first end member 106 is arranged at one end of the device 100 and a second end member 116 is arranged at an opposite end of the device 100. The first and second end members 106, 116 together at least partially define end surfaces of the device 100. For example, the bottom surface of the second end member 116 at least partially defines a bottom surface of the device 100. Edges of the outer cover 102 may also define a portion of the end surfaces. In this example, the lid 108 also defines a portion of a top surface of the device too. The end of the device closest to the opening 104 may be known as the proximal end (or mouth end) of the device too because, in use, it is closest to the mouth of the user. In use, a user inserts an article 110 into the opening 104, operates the user control 112 to begin heating the aerosol generating material and draws on the aerosol generated in the device. This causes the aerosol to flow through the device too along a flow path towards the proximal end of the device too.

The other end of the device furthest away from the opening 104 may be known as the distal end of the device too because, in use, it is the end furthest away from the mouth of the user. As a user draws on the aerosol generated in the device, the aerosol flows away from the distal end of the device too.

The device too further comprises a power source 118. The power source 118 maybe, for example, a battery, such as a rechargeable battery or a non-rechargeable battery. Examples of suitable batteries include, for example, a lithium battery (such as a lithium-ion battery), a nickel battery (such as a nickel-cadmium battery), and an alkaline battery. The battery is electrically coupled to the heating assembly to supply electrical power when required and under control of a controller (not shown) to heat the aerosol generating material. In this example, the battery is connected to a central support 120 which holds the battery 118 in place. The device further comprises at least one electronics module 122. The electronics module 122 may comprise, for example, a printed circuit board (PCB). The PCB 122 may support at least one controller, such as a processor, and memory. The PCB 122 may also comprise one or more electrical tracks to electrically connect together various electronic components of the device 100. For example, the battery terminals maybe electrically connected to the PCB 122 so that power can be distributed throughout the device 100. The socket 114 may also be electrically coupled to the battery via the electrical tracks.

In the example device too, the heating assembly is an inductive heating assembly and comprises various components to heat the aerosol generating material of the article 110 via an inductive heating process. Induction heating is a process of heating an electrically conducting object (such as a susceptor) by electromagnetic induction. An induction heating assembly may comprise an inductive element, for example, one or more inductor coils, and a device for passing a varying electric current, such as an alternating electric current, through the inductive element. The varying electric current in the inductive element produces a varying magnetic field. The varying magnetic field penetrates a susceptor suitably positioned with respect to the inductive element, and generates eddy currents inside the susceptor. The susceptor has electrical resistance to the eddy currents, and hence the flow of the eddy currents against this resistance causes the susceptor to be heated by Joule heating. In cases where the susceptor comprises ferromagnetic material such as iron, nickel or cobalt, heat may also be generated by magnetic hysteresis losses in the susceptor, i.e. by the varying orientation of magnetic dipoles in the magnetic material as a result of their alignment with the varying magnetic field. In inductive heating, as compared to heating by conduction for example, heat is generated inside the susceptor, allowing for rapid heating. Further, there need not be any physical contact between the inductive heater and the susceptor, allowing for enhanced freedom in construction and application.

The induction heating assembly of the example device too comprises a susceptor arrangement 132 (herein referred to as “a susceptor”), a first inductor coil 124 and a second inductor coil 126. The first and second inductor coils 124, 126 are made from an electrically conducting material. In this example, the first and second inductor coils 124, 126 are made from Litz wire/cable which is wound in a helical fashion to provide helical inductor coils 124, 126. Litz wire comprises a plurality of individual wires which are individually insulated and are twisted together to form a single wire. Litz wires are designed to reduce the skin effect losses in a conductor. In the example device 100, the first and second inductor coils 124, 126 are made from copper Litz wire which has a rectangular cross section. In other examples the Litz wire can have other shape cross sections, such as circular. The first inductor coil 124 is configured to generate a first varying magnetic field for heating a first section of the susceptor 132 and the second inductor coil 126 is configured to generate a second varying magnetic field for heating a second section of the susceptor 132. In this example, the first inductor coil 124 is adjacent to the second inductor coil 126 in a direction along the longitudinal axis 134 of the device too (that is, the first and second inductor coils 124, 126 to not overlap). The susceptor arrangement 132 may comprise a single susceptor, or two or more separate susceptors. Ends 130 of the first and second inductor coils 124, 126 can be connected to the PCB 122.

It will be appreciated that the first and second inductor coils 124, 126, in some examples, may have at least one characteristic different from each other. For example, the first inductor coil 124 may have at least one characteristic different from the second inductor coil 126. More specifically, in one example, the first inductor coil 124 may have a different value of inductance than the second inductor coil 126. In Figure 7, the first and second inductor coils 124, 126 are of different lengths such that the first inductor coil 124 is wound over a smaller section of the susceptor 132 than the second inductor coil 126. Thus, the first inductor coil 124 may comprise a different number of turns than the second inductor coil 126 (assuming that the spacing between individual turns is substantially the same). In yet another example, the first inductor coil 124 may be made from a different material to the second inductor coil 126. In some examples, the first and second inductor coils 124, 126 may be substantially identical.

In this example, the first inductor coil 124 and the second inductor coil 126 are wound in opposite directions. This can be useful when the inductor coils are active at different times. For example, initially, the first inductor coil 124 may be operating to heat a first section/portion of the article 110, and at a later time, the second inductor coil 126 may be operating to heat a second section/portion of the article 110. Winding the coils in opposite directions helps reduce the current induced in the inactive coil when used in conjunction with a particular type of control circuit. In Figure 7, the first inductor coil 124 is a right-hand helix and the second inductor coil 126 is a left-hand helix. However, in another embodiment, the inductor coils 124, 126 may be wound in the same direction, or the first inductor coil 124 may be a left-hand helix and the second inductor coil 126 may be a right-hand helix.

The susceptor 132 of this example is hollow and therefore defines a receptacle within which aerosol generating material is received. For example, the article 110 can be inserted into the susceptor 132. In this example the susceptor 120 is tubular, with a circular cross section.

The susceptor 132 maybe made from one or more materials. Preferably the susceptor 132 comprises carbon steel having a coating of Nickel or Cobalt.

In some examples, the susceptor 132 may comprise at least two materials capable of being heated at two different frequencies for selective aerosolization of the at least two materials. For example, a first section of the susceptor 132 (which is heated by the first inductor coil 124) may comprise a first material, and a second section of the susceptor 132 which is heated by the second inductor coil 126 may comprise a second, different material. In another example, the first section may comprise first and second materials, where the first and second materials can be heated differently based upon operation of the first inductor coil 124. The first and second materials maybe adjacent along an axis defined by the susceptor 132, or may form different layers within the susceptor 132. Similarly, the second section may comprise third and fourth materials, where the third and fourth materials can be heated differently based upon operation of the second inductor coil 126. The third and fourth materials maybe adjacent along an axis defined by the susceptor 132, or may form different layers within the susceptor 132. Third material may the same as the first material, and the fourth material may be the same as the second material, for example. Alternatively, each of the materials may be different. The susceptor may comprise carbon steel or aluminium for example.

The device too of Figure 7 further comprises an insulating member 128 which may be generally tubular and at least partially surround the susceptor 132. The insulating member 128 may be constructed from any insulating material, such as plastic for example. In this particular example, the insulating member is constructed from polyether ether ketone (PEEK). The insulating member 128 may help insulate the various components of the device 100 from the heat generated in the susceptor 132.

The insulating member 128 can also fully or partially support the first and second inductor coils 124, 126. For example, as shown in Figure 7, the first and second inductor coils 124, 126 are positioned around the insulating member 128 and are in contact with a radially outward surface of the insulating member 128. In some examples the insulating member 128 does not abut the first and second inductor coils 124, 126. For example, a small gap maybe present between the outer surface of the insulating member 128 and the inner surface of the first and second inductor coils 124, 126.

In a specific example, the susceptor 132, the insulating member 128, and the first and second inductor coils 124, 126 are coaxial around a central longitudinal axis of the susceptor 132.

Figure 8 shows a side view of device too in partial cross-section. The outer cover 102 is present in this example. The rectangular cross-sectional shape of the first and second inductor coils 124, 126 is more clearly visible. The device too further comprises a support 136 which engages one end of the susceptor 132 to hold the susceptor 132 in place. The support 136 is connected to the second end member 116.

The device may also comprise a second printed circuit board 138 associated within the control element 112.

The device too further comprises a second lid/cap 140 and a spring 142, arranged towards the distal end of the device too. The spring 142 allows the second lid 140 to be opened, to provide access to the susceptor 132. A user may open the second lid 140 to clean the susceptor 132 and/ or the support 136.

The device too further comprises an expansion chamber 144 which extends away from a proximal end of the susceptor 132 towards the opening 104 of the device. Located at least partially within the expansion chamber 144 is a retention clip 146 to abut and hold the article 110 when received within the device too. The expansion chamber 144 is connected to the end member 106. Figure 9 is an exploded view of the device 100 of Figure 8, with the outer cover 102 omitted. Figure 10A depicts a cross section of a portion of the device 100 of Figure 8. Figure 10B depicts a close-up of a region of Figure 10A. Figures 8A and 8B show the article 110 received within the susceptor 132, where the article 110 is dimensioned so that the outer surface of the article 110 abuts the inner surface of the susceptor 132. This ensures that the heating is most efficient. The article 110 of this example comprises aerosol generating material 110a. The aerosol generating material 110a is positioned within the susceptor 132. The article 110 may also comprise other components such as a filter, wrapping materials and/ or a cooling structure.

Figure 10B shows that the outer surface of the susceptor 132 is spaced apart from the inner surface of the inductor coils 124, 126 by a distance 150, measured in a direction perpendicular to a longitudinal axis 158 of the susceptor 132. In one particular example, the distance 150 is about 3 mm to 4mm, about 3-3.5mm, or about 3.25mm.

Figure 10B further shows that the outer surface of the insulating member 128 is spaced apart from the inner surface of the inductor coils 124, 126 by a distance 152, measured in a direction perpendicular to a longitudinal axis 158 of the susceptor 132. In one particular example, the distance 152 is about 0.05 mm. In another example, the distance 152 is substantially omm, such that the inductor coils 124, 126 abut and touch the insulating member 128.

In one example, the susceptor 132 has a wall thickness 154 of about 0.025mm to imm, or about 0.05 mm.

In one example, the susceptor 132 has a length of about 40mm to 60mm, about 40mm to 45 mm, or about 44.5 mm.

In one example, the insulating member 128 has a wall thickness 156 of about 0.25 mm to 2 mm, 0.25 mm to imm, or about 0.5 mm. In use, the articles 1, T, 1”, T”, 1”” described herein can be inserted into a non combustible aerosol provision device such as the device too described with reference to Figures 6 to 10. At least a portion of the mouthpiece 2, 2’, 2”, 2’”, 2”” of the article 1, 1’, 1”, 1’”, 1”” protrudes from the non-combustible aerosol provision device 100 and can be placed into a user’s mouth. An aerosol is produced by heating the aerosol generating material 3 using the device 100. The aerosol produced by the aerosol generating material 3 passes through the mouthpiece 2, 2’, 2”, 2’”, 2”” to the user’s mouth.

The articles 1, 1’, 1”, 1”’, 1”” described herein have particular advantages, for instance when used with non-combustible aerosol provision devices such as the device 100 described with reference to Figures 6 to 10. In particular, the body 6 of amorphous solid material has surprisingly been found to have a significant influence on the temperature of the aerosol delivered to the mouth end of the articles 1, 1’, 1”, 1”’, 1””, in use.

Testing was performed on two comparative smoking articles and an exemplary embodiment of the invention. Comparative examples A and B are the same as Article 1”, except that comparative examples A and B comprise a body of fibrous material 4 in place of body 6 of amorphous solid material. Comparative example A has a 60% level of ventilation, and comparative example B has a 75% level of ventilation. The exemplary article is the same as Article 1”, and is provided with 60% ventilation.

Testing was performed for the first 2 puffs on the article. Each sample was tested 9 times, and the temperatures provided are an average of these 9 tests. The known Health Canada Intense puffing regime was applied (55 ml puff volume applied for 2 seconds duration every 30 seconds) using standard testing equipment. The results of the testing are shown in Table 1.0, where the puff temperature represents the difference between room temperature and aerosol temperature.

As shown in Table 1.0 the aerosol temperature across a first and second puff from the exemplary article, comprising the body of amorphous solid material, is lower than the aerosol temperature across these puffs in either comparative example A or B. The aerosol temperature across puff 1 and puff 2 of the exemplary article at 60% ventilation is comparable to the aerosol temperature across puffs 1 and 2 of comparative example B, at 75% ventilation. Higher levels of ventilation have a cooling effect on aerosol temperature, so it is significant to achieve a comparable aerosol temperature in an article with a 15% lower ventilation level.

Table 1.0

Figure 11 illustrates a method of manufacturing an article for use in a non-combustible aerosol provision system. At step Sioi a source of amorphous solid material in sheet form is passed through an apparatus to form the sheet material into a rod of gathered amorphous solid material.

At step S102 the rod of gathered amorphous solid material is cut to length to form a body of amorphous solid material as defined herein.

Figure 12 is a side view showing an apparatus for producing a rod of the body of material according to the invention.

Figure 12 shows an apparatus 200 for producing a rod of the body of material according to the invention, and comprises a tongue 211, a guide nozzle 212 including a funnel portion. The tongue 211 is a tapered duct having a wide entrance opening 211b and a narrow exit opening 211a. The tongue 211 is generally circular in cross-section and is open at its underside in the form of an elongate slot (not shown) extending along its length in an axial direction thereof such that, in cross-section, the tongue 211 does not quite form a complete circle. The tongue 211 is located on a rod forming guide (not shown) which comprises a shaped track along which a continuous belt or ‘garniture’ 215 runs. The garniture 215 extends over a plurality of guide rollers 216 and is driven to be conveyed around the rollers 216 in the direction shown by arrows ‘A’. A wrapping paper ‘P’ is fed from a spool 217 onto the upper surface of the garniture 215 and is conveyed through the tongue 211 by the moving garniture 215. As the wrapping paper P travels through the tongue 211, the shaped track is configured to deform the garniture and wrapping paper P thereon such that, in cross-section, the wrapping paper P goes from being flat (as it is in the spool 217) when it enters the wide entrance opening 11b of the tongue 211, to a closed circle as it leaves the narrow exit opening 211a of the tongue 211, completely surrounding the formed rod. In use, a bobbin of amorphous solid material (not shown), is fed into the funnel of the guide nozzle 212 and is guided into the tongue 211 amorphous solid material is fed through the continually tapering tongue 211 to form the sheet of amorphous solid material into a rod by gathering the material as it emerges from the narrow distal end 211a.

As the amorphous solid material is fed into the tongue 211, it is gathered onto the wrapping material P being conveyed on the garniture 215 and is conveyed therewith through the tongue 211. As the amorphous solid material travels through the tongue 211, it is compressed as the tongue 211 inwardly tapers and the wrapping paper P is folded around the outside of the compressed cylinder of gathered amorphous solid material, such that when the amorphous solid material exits through the narrow exit opening 211a of the tongue 211, it is formed into a compressed cylindrical rod circumscribed by an outer wrapping paper P.

The rod formed by the process described herein can then be cut to length to form a multiple bodies 6 according to the present invention.

The various embodiments described herein are presented only to assist in understanding and teaching the claimed features. These embodiments are provided as a representative sample of embodiments only, and are not exhaustive and/or exclusive. It is to be understood that advantages, embodiments, examples, functions, features, structures, and/or other aspects described herein are not to be considered limitations on the scope of the invention as defined by the claims or limitations on equivalents to the claims, and that other embodiments may be utilised and modifications may be made without departing from the scope of the claimed invention. Various embodiments of the invention may suitably comprise, consist of, or consist essentially of, appropriate combinations of the disclosed elements, components, features, parts, steps, means, etc, other than those specifically described herein. In addition, this disclosure may include other inventions not presently claimed, but which may be claimed in future.

Claims

1. An article for use in a non-combustible aerosol provision system, the article comprising a mouthpiece comprising a body of material, wherein the body comprises amorphous solid material.

2. An article according to claim l, wherein the body comprises a gathered sheet of amorphous solid material.

3. An article according to claim l or 2, wherein the body comprises elongate strips of amorphous solid material.

4. An article according to claim 3, wherein the elongate strips are substantially aligned with the longitudinal axis of the article.

5. An article according to any one of claims 1 to 4, wherein the mouthpiece comprises a further section, wherein the further section is a body of fibrous material or a hollow tubular element, and wherein the mouthpiece comprises a mouth end and a distal end.

6. An article according to claim 5, wherein the further section is positioned at the mouth end of the mouthpiece.

7. An article according to claim 5 or 6, wherein the further section is a first further section, and the mouthpiece additionally comprises a second further section.

8. An article according to claim 7, wherein the second further section is a body of fibrous material or a hollow tubular element.

9. An article according to claim 7 or 8, wherein the both of the first further section and the second further section are hollow tubular elements.

10. An article according to claim 9, wherein each of the hollow tubular elements may be a paper tube or a hollow tubular element formed from filamentary tow.

11. An article according to any one of claims 7 to 10, wherein the second further section is positioned at the distal end of the mouthpiece.

12. An article according to any of claims 5 to 8, wherein the body is positioned at the distal end of the mouthpiece.

13. An article according to any one of claims 1 to 12, wherein the amorphous solid material has a thickness of between 0.015 mm and 0.5 mm, or between 0.1 mm and 0.3 mm, or between 0.15 mm and 0.25 mm.

14. An article according to any one of claims 1 to 13, wherein the amorphous solid material is laminated on a supporting material.

15. An article according to claim 14, wherein the supporting material is paper or foil.

16. An article according to any one of claims 1 to 15, wherein the amorphous solid material is crimped.

17. An article according to any one of claims 1 to 16, wherein the amorphous solid material comprises a flavourant, and optionally, wherein the flavourant is menthol.

18. An article according to claim 17, wherein the amorphous solid material comprises from 0.1% to 65% menthol by dry weight, or from 1% to 60% by dry weight, or from 10% to 55% by dry weight, preferably from 40% to 50% by dry weight.

19. An article according to any one of claims 1 to 18, wherein the amorphous solid material comprises a gelling agent, and wherein the gelling agent is one of pectin, gelatin, polysaccharide or carageenan.

20. An article according to any one of claims 1 to 19, wherein the article further comprises an aerosol generating material.

21. An article according to claim 20, wherein the aerosol generating material is connected to the distal end of the mouthpiece.

22. A system comprising an article according to claim 20 or 21, and a non combustible aerosol provision device for heating the aerosol generating material of the article.

23. A system according to claim 22, wherein the non-combustible aerosol provision device comprises a coil.

24. A system according to claim 22 or 23, wherein the non-combustible aerosol provision device is configured to heat the aerosol generating material of the article to a maximum temperature of at least 200°C.

25. A system according to claim 24, wherein the non-combustible aerosol provision device is configured to heat the aerosol generating material of the article to a maximum temperature of at least about 160 °C, or at least about 200°C, or at least about 220 °C, or at least about 240 °C, or at least about 270 °C .

26. A method for manufacturing an article for use in a non-combustible aerosol provision system, wherein the article comprises a mouthpiece comprising a body of material, the body comprising amorphous solid material, and wherein the method comprises providing a source of amorphous solid material, passing the amorphous solid material through an apparatus to form a rod of gathered amorphous solid material, and cutting the rod of amorphous solid material to form said body.

27. A method according to claim 26, wherein the amorphous solid material has a width of between 150 mm and 500 mm.

28. A method according to claim 26 or 27, wherein the amorphous solid material is cut into strips before passing through the apparatus.

29. A method according to claim 26, 27 or 28, wherein the amorphous solid material is crimped prior to passing through the apparatus.

30. A method according to claim 26, 27, 28, or 29, wherein the body of amorphous solid material is combined with a source of aerosol generating material to form an article for use in a non-combustible aerosol provision system.