WO2020209678A1 - Organic compound and organic electroluminescent device comprising same - Google Patents

Organic compound and organic electroluminescent device comprising same Download PDF

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WO2020209678A1
WO2020209678A1 PCT/KR2020/004924 KR2020004924W WO2020209678A1 WO 2020209678 A1 WO2020209678 A1 WO 2020209678A1 KR 2020004924 W KR2020004924 W KR 2020004924W WO 2020209678 A1 WO2020209678 A1 WO 2020209678A1
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김충한
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두산솔루스 주식회사
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    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K85/00Organic materials used in the body or electrodes of devices covered by this subclass
    • H10K85/60Organic compounds having low molecular weight
    • H10K85/649Aromatic compounds comprising a hetero atom
    • H10K85/657Polycyclic condensed heteroaromatic hydrocarbons
    • H10K85/6572Polycyclic condensed heteroaromatic hydrocarbons comprising only nitrogen in the heteroaromatic polycondensed ring system, e.g. phenanthroline or carbazole
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D401/00Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/02Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
    • C07D401/04Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings directly linked by a ring-member-to-ring-member bond
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D401/00Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/14Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing three or more hetero rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D405/00Heterocyclic compounds containing both one or more hetero rings having oxygen atoms as the only ring hetero atoms, and one or more rings having nitrogen as the only ring hetero atom
    • C07D405/14Heterocyclic compounds containing both one or more hetero rings having oxygen atoms as the only ring hetero atoms, and one or more rings having nitrogen as the only ring hetero atom containing three or more hetero rings
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    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K50/00Organic light-emitting devices
    • H10K50/10OLEDs or polymer light-emitting diodes [PLED]
    • H10K50/14Carrier transporting layers
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10KORGANIC ELECTRIC SOLID-STATE DEVICES
    • H10K50/00Organic light-emitting devices
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    • H10K50/17Carrier injection layers
    • H10K50/171Electron injection layers

Abstract

The present invention relates to a novel compound and an organic electroluminescent device comprising same. As the compound according to the present invention is used in an organic material layer, preferably an electron transport layer, an electron transport auxiliary layer, or a light-emitting layer of the organic electroluminescent device, it is possible to improve luminous efficiency, driving voltage, lifespan, etc. of the organic electroluminescent device.

Description

유기 화합물 및 이를 포함하는 유기 전계 발광 소자Organic compound and organic electroluminescent device comprising the same
본 발명은 신규한 유기 발광 화합물 및 이를 이용한 유기 전계 발광 소자에 관한 것으로, 보다 상세하게는 전자 주입 및 수송능 등이 우수한 신규한 피리미딘 유도체 화합물 및 이를 하나 이상의 유기물층에 포함함으로써 발광효율, 구동 전압, 수명 등의 특성이 향상된 유기 전계 발광 소자에 관한 것이다.The present invention relates to a novel organic light-emitting compound and an organic electroluminescent device using the same, and more particularly, a novel pyrimidine derivative compound having excellent electron injection and transport capabilities, and the luminous efficiency and driving voltage by including the same in one or more organic material layers. , It relates to an organic electroluminescent device having improved characteristics such as lifetime.
유기 전계 발광(electroluminescent, EL) 소자는, 전계를 인가함으로써 양극으로부터 주입된 정공과 음극으로부터 주입된 전자의 재결합 에너지에 의해 형광성 물질이 발광하는 원리를 이용한 자발광 소자이다.An organic electroluminescent (EL) device is a self-luminous device using the principle that a fluorescent material emits light by recombination energy of holes injected from an anode and electrons injected from a cathode by applying an electric field.
1950년대 베르나소스(Bernanose)의 유기 박막 발광 관측을 시점으로 하여, 1965년 안트라센 단결정을 이용한 청색 전기발광으로 이어진 유기 전계 발광(electroluminescent, EL) 소자에 대한 연구가 이어져 오다가, 1987년 탕(Tang)에 의하여 정공층과 발광층의 기능층으로 나눈 적층 구조의 유기 전계 발광 소자가 제시되었다. 이후, 고효율, 고수명의 유기 전계 발광 소자를 만들기 위하여, 소자 내 각각의 특징적인 유기물층을 도입하는 형태로 발전하여 왔으며, 이에 사용되는 특화된 물질의 개발로 이어졌다.With the observation of the light emission of organic thin films by Bernanose in the 1950s as the starting point, research on an organic electroluminescent (EL) device followed by blue electroluminescence using an anthracene single crystal in 1965 was continued. ), an organic electroluminescent device having a stacked structure divided into a hole layer and a functional layer of a light emitting layer was presented. Since then, in order to make a high-efficiency, high-life organic electroluminescent device, it has developed in the form of introducing each characteristic organic material layer in the device, leading to the development of specialized materials used therein.
유기 전계 발광 소자는 두 전극 사이에 전압을 걸어주면 양극에서는 정공이 유기물층으로 주입되고, 음극에서는 전자가 유기물층으로 주입된다. 주입된 정공과 전자가 만났을 때 엑시톤(exciton)이 형성되며, 이 엑시톤이 바닥상태로 떨어질 때 빛이 나게 된다. 이때, 유기물층으로 사용되는 물질은 그 기능에 따라, 발광 물질, 정공 주입 물질, 정공 수송 물질, 전자 수송 물질, 전자 주입 물질 등으로 분류될 수 있다.In an organic electroluminescent device, when a voltage is applied between two electrodes, holes are injected into the organic material layer from the anode and electrons are injected into the organic material layer from the cathode. When injected holes and electrons meet, excitons are formed, and when these excitons fall to the ground state, light is emitted. In this case, the material used as the organic material layer may be classified into a light emitting material, a hole injection material, a hole transport material, an electron transport material, an electron injection material, and the like according to their function.
유기 EL 소자의 발광층 형성재료는 발광색에 따라 청색, 녹색, 적색 발광 물질과, 보다 나은 천연색을 구현하기 위한 노란색 및 주황색 발광 물질로 구분될 수 있다. 또한, 색순도의 증가와 에너지 전이를 통한 발광 효율을 증가시키기 위하여, 발광 물질로서 호스트/도펀트 계를 사용할 수 있다.The material for forming the light-emitting layer of the organic EL device may be classified into blue, green, and red light-emitting materials and yellow and orange light-emitting materials for realizing better natural colors according to light emission colors. In addition, in order to increase color purity and increase luminous efficiency through energy transfer, a host/dopant system may be used as a light emitting material.
도펀트 물질은 유기 물질을 사용하는 형광 도펀트와 Ir, Pt 등의 중원자(heavy atoms)가 포함된 금속 착체 화합물을 사용하는 인광 도펀트로 나눌 수 있다. 이때, 인광 재료의 개발은 이론적으로 형광에 비해 4배까지 발광 효율을 향상시킬 수 있기 때문에, 인광 도펀트 뿐만 아니라 인광 호스트 재료들에 대한 연구도 많이 진행되고 있다.The dopant material can be classified into a fluorescent dopant using an organic material and a phosphorescent dopant using a metal complex compound containing heavy atoms such as Ir and Pt. At this time, since the development of a phosphorescent material can theoretically improve luminous efficiency up to four times as compared to fluorescence, a lot of research on phosphorescent host materials as well as phosphorescent dopants is being conducted.
현재까지 정공 주입층, 정공 수송층, 전자 수송 보조층, 전자 수송층 재료로는 NPB, BCP, Alq3 등이 널리 알려져 있으며, 발광층 재료로는 안트라센 유도체들이 보고되고 있다. 특히, 발광층 재료 중 효율 향상 측면에서 장점을 가지고 있는 인광 재료로서는 Firpic, Ir(ppy)3, (acac)Ir(btp)2 등과 같은 Ir을 포함하는 금속 착체 화합물이 청색(blue), 녹색(green), 적색(red)의 인광 도판트 재료로 사용되고 있으며, 4,4-디카바졸리비페닐(4,4-dicarbazolybiphenyl, CBP)은 인광 호스트 재료로 사용되고 있다.Until now, as a material for a hole injection layer, a hole transport layer, an electron transport auxiliary layer, and an electron transport layer, NPB, BCP, Alq3, etc. are widely known, and anthracene derivatives have been reported as the light emitting layer material. In particular, among the light emitting layer materials, metal complex compounds containing Ir such as Firpic, Ir(ppy)3, (acac)Ir(btp)2, etc., as phosphorescent materials that have an advantage in terms of efficiency improvement, are blue and green. ), is used as a red phosphorescent dopant material, and 4,4-dicarbazolybiphenyl (CBP) is used as a phosphorescent host material.
[규칙 제91조에 의한 정정 07.05.2020] 
Figure WO-DOC-FIGURE-cm1
[Correction 07.05.2020 pursuant to Rule 91]
Figure WO-DOC-FIGURE-cm1
그러나 종래의 유기물층 재료들은 발광 특성 측면에서는 유리한 면이 있으나, 유리전이온도가 낮아 열적 안정성이 매우 좋지 않기 때문에, 유기 전계 발광 소자의 수명 측면에서 만족할 만한 수준이 되지 못하고 있다. 따라서, 성능이 뛰어난 유기물층 재료의 개발이 요구되고 있다.However, conventional organic material layer materials have an advantage in terms of light emission characteristics, but their thermal stability is not very good due to a low glass transition temperature, and thus, they are not at a satisfactory level in terms of the lifespan of an organic electroluminescent device. Therefore, there is a demand for the development of an organic material layer material having excellent performance.
본 발명은 유기 전계 발광 소자에 적용할 수 있으며, 특별히 전자 주입 및 수송능이 모두 우수한 신규 유기 화합물을 제공하는 것을 목적으로 한다.The present invention can be applied to an organic electroluminescent device, and particularly has an object to provide a novel organic compound excellent in both electron injection and transport capabilities.
또한 본 발명은 상기 신규 유기 화합물을 포함하여 낮은 구동전압과 높은 발광효율을 나타내며 수명이 향상되는 유기 전계 발광 소자를 제공하는 것을 또 다른 목적으로 한다.Another object of the present invention is to provide an organic electroluminescent device including the novel organic compound, exhibiting a low driving voltage and high luminous efficiency, and improving lifespan.
상기한 목적을 달성하기 위해, 본 발명은 하기 화학식 1로 표시되는 화합물을 제공한다.In order to achieve the above object, the present invention provides a compound represented by the following formula (1).
[화학식 1][Formula 1]
Figure PCTKR2020004924-appb-I000002
Figure PCTKR2020004924-appb-I000002
상기 화학식 1에서,In Formula 1,
X1 내지 X3은 각각 독립적으로 N 또는 C(R1)이나, 이들 중 적어도 둘 이상은 N이고, R1은 수소이거나 치환 또는 비치환된 C1~C60의 알킬이고,X 1 to X 3 are each independently N or C (R 1 ), but at least two or more of them are N, and R 1 is hydrogen or a substituted or unsubstituted C 1 to C 60 alkyl,
L1 내지 L4는 각각 독립적으로 직접결합, 또는 C6~C18의 아릴렌기 및 핵원자수 5 내지 18개의 헤테로아릴렌기로 이루어진 군에서 선택되며,L 1 to L 4 are each independently a direct bond, or selected from the group consisting of an arylene group of C 6 to C 18 and a heteroarylene group having 5 to 18 nuclear atoms,
A와 B는 각각 독립적으로 치환 또는 비치환된 C6~C60의 아릴기 또는 핵원자수 5 내지 60개의 헤테로아릴기이며, 적어도 하나 이상은 함질소복소환을 포함하는 헤테로아릴기이며,A and B are each independently a substituted or unsubstituted C 6 to C 60 aryl group or a heteroaryl group having 5 to 60 nuclear atoms, and at least one is a heteroaryl group including a nitrogen-containing heterocycle,
Ar1 과 Ar2는 C6~C60의 아릴기 또는 핵원자수 5 내지 60개의 헤테로아릴기이며, , 적어도 하나 이상은 함질소복소환을 포함하는 헤테로아릴기이며,Ar 1 and Ar 2 is a C 6 ~ C 60 aryl group or a heteroaryl group having 5 to 60 nuclear atoms, at least one is a heteroaryl group containing a nitrogen-containing heterocycle,
상기 L1 내지 L4의 아릴렌기 및 헤테로아릴렌기와, 상기 A, B, Ar1 및 Ar2의 아릴기 및 헤테로아릴기는 각각 독립적으로 중수소, 할로겐, 시아노기, 니트로기, C1~C40의 알킬기, C2~C40의 알케닐기, C2~C40의 알키닐기, C6~C60의 아릴기, 핵원자수 5 내지 60개의 헤테로아릴기, C6~C60의 아릴옥시기, C1~C40의 알킬옥시기, C6~C60의 아릴아민기, C3~C40의 시클로알킬기, 핵원자수 3 내지 40개의 헤테로시클로알킬기, C1~C40의 알킬실릴기, C1~C40의 알킬보론기, C6~C60의 아릴보론기, C6~C60의 아릴포스핀기, C6~C60의 모노 또는 디아릴포스피닐기 및 C6~C60의 아릴실릴기로 이루어진 군에서 선택된 1종 이상의 치환기로 치환되거나 비치환되고, 복수 개의 치환기로 치환되는 경우, 이들은 서로 동일하거나 상이할 수 있다.The arylene group and heteroarylene group of L 1 to L 4, the aryl group and heteroaryl group of A, B, Ar 1 and Ar 2 are each independently deuterium, halogen, cyano group, nitro group, C 1 to C 40 Alkyl group, C 2 ~ C 40 alkenyl group, C 2 ~ C 40 alkynyl group, C 6 ~ C 60 aryl group, 5 to 60 nuclear atoms heteroaryl group, C 6 ~ C 60 aryloxy group , C 1 ~ C 40 alkyloxy group, C 6 ~ C 60 arylamine group, C 3 ~ C 40 cycloalkyl group, 3 to 40 nuclear atoms heterocycloalkyl group, C 1 ~ C 40 alkylsilyl group , C 1 ~ C 40 alkyl boron group, C 6 ~ C 60 aryl boron group, C 6 ~ C 60 arylphosphine group, C 6 ~ C 60 mono or diarylphosphine group and C 6 ~ C 60 When substituted or unsubstituted with one or more substituents selected from the group consisting of an arylsilyl group of, and when substituted with a plurality of substituents, they may be the same or different from each other.
본 발명에의 "알킬"은 탄소수 1 내지 40개의 직쇄 또는 측쇄의 포화 탄화수소에서 유래되는 1가의 치환기이며, 이의 예로는 메틸, 에틸, 프로필, 이소부틸, sec-부틸, 펜틸, iso-아밀, 헥실 등이 있는데, 이에 한정되지 않는다."Alkyl" in the present invention is a monovalent substituent derived from a linear or branched saturated hydrocarbon having 1 to 40 carbon atoms, examples of which include methyl, ethyl, propyl, isobutyl, sec-butyl, pentyl, iso-amyl, hexyl And the like, but are not limited thereto.
본 발명에서의 "알케닐(alkenyl)"은 탄소-탄소 이중 결합을 1개 이상 가진, 탄소수 2 내지 40개의 직쇄 또는 측쇄의 불포화 탄화수소에서 유래되는 1가의 치환기이며, 이의 예로는 비닐(vinyl), 알릴(allyl), 이소프로펜일(isopropenyl), 2-부텐일(2-butenyl) 등이 있는데, 이에 한정되지 않는다.In the present invention, "alkenyl" is a monovalent substituent derived from a straight or branched unsaturated hydrocarbon having 2 to 40 carbon atoms and having one or more carbon-carbon double bonds, examples of which are vinyl (vinyl), There are allyl (allyl), isopropenyl (isopropenyl), 2-butenyl (2-butenyl), and the like, but is not limited thereto.
본 발명에서의 "알키닐(alkynyl)"은 탄소-탄소 삼중 결합을 1개 이상 가진, 탄소수 2 내지 40개의 직쇄 또는 측쇄의 불포화 탄화수소에서 유래되는 1가의 치환기이며, 이의 예로는 에티닐(ethynyl), 2-프로파닐(2-propynyl) 등이 있는데, 이에 한정되지 않는다.In the present invention, "alkynyl" is a monovalent substituent derived from a straight or branched unsaturated hydrocarbon having 2 to 40 carbon atoms having at least one carbon-carbon triple bond, and examples thereof are ethynyl , 2-propynyl, and the like, but are not limited thereto.
본 발명에서의 "아릴"은 단독 고리 또는 2 이상의 고리가 조합된, 탄소수 6 내지 60개의 방향족 탄화수소로부터 유래된 1가의 치환기를 의미한다. 또한, 2 이상의 고리가 서로 축합되어 있고, 고리 형성 원자로서 탄소만을 포함(예를 들어, 탄소수는 8 내지 60개일 수 있음)하고, 분자 전체가 비-방향족성(non-aromacity)를 갖는 1가 치환기도 포함될 수 있다. 이러한 아릴의 예로는 페닐, 나프틸, 페난트릴, 안트릴, 플루오레닐 등이 있는데, 이에 한정되지 않는다.In the present invention, "aryl" refers to a monovalent substituent derived from an aromatic hydrocarbon having 6 to 60 carbon atoms in which a single ring or two or more rings are combined. In addition, two or more rings are condensed with each other, contain only carbon as a ring-forming atom (for example, the number of carbon atoms may be 8 to 60), and the entire molecule is a monovalent having non-aromacity Substituents may also be included. Examples of such aryl include phenyl, naphthyl, phenanthryl, anthryl, and fluorenyl, but are not limited thereto.
본 발명에서의 "헤테로아릴"은 핵원자수 5 내지 60개의 모노헤테로사이클릭 또는 폴리헤테로사이클릭 방향족 탄화수소로부터 유래된 1가의 치환기를 의미한다. 이때, 고리 중 하나 이상의 탄소, 바람직하게는 1 내지 3개의 탄소가 N, O, P, S 및 Se 중에서 선택된 헤테로원자로 치환될 수 있다. 또한, 2 이상의 고리가 서로 단순 부착(pendant)되거나 축합되어 있고, 고리 형성 원자로서 탄소 외에 N, O, P, S 및 Se 중에서 선택된 헤테로 원자를 포함하고, 분자 전체가 비-방향족성(non-aromacity)를 갖는 1가 그룹도 포함하는 것으로 해석된다. 이러한 헤테로아릴의 예로는 피리딜, 피라지닐, 피리미디닐, 피리다지닐, 트리아지닐과 같은 6-원 모노사이클릭 고리; 페녹사티에닐(phenoxathienyl), 인돌리지닐(indolizinyl), 인돌릴(indolyl), 퓨리닐(purinyl), 퀴놀릴(quinolyl), 벤조티아졸(벤조thiazole), 카바졸릴(carbazolyl)과 같은 폴리사이클릭 고리; 2-퓨라닐, N-이미다졸릴, 2-이속사졸릴, 2-피리디닐, 2-피리미디닐 등이 있는데, 이에 한정되지 않는다.In the present invention, "heteroaryl" means a monovalent substituent derived from a monoheterocyclic or polyheterocyclic aromatic hydrocarbon having 5 to 60 nuclear atoms. At this time, one or more carbons, preferably 1 to 3 carbons in the ring may be substituted with a heteroatom selected from N, O, P, S and Se. In addition, two or more rings are simply attached or condensed with each other, and a hetero atom selected from N, O, P, S and Se in addition to carbon as a ring forming atom is included, and the entire molecule is non-aromatic (non-aromatic) aromacity) is interpreted to include monovalent groups. Examples of such heteroaryl include 6-membered monocyclic rings such as pyridyl, pyrazinyl, pyrimidinyl, pyridazinyl, and triazinyl; Polycylates such as phenoxathienyl, indolizinyl, indolyl, purinyl, quinolyl, benzothiazole, and carbazolyl Click ring; 2-furanyl, N-imidazolyl, 2-isoxazolyl, 2-pyridinyl, 2-pyrimidinyl, and the like, but are not limited thereto.
본 발명에서의 "아릴옥시"는 RO-로 표시되는 1가의 치환기로, 상기 R은 탄소수 5 내지 60개의 아릴을 의미한다. 이러한 아릴옥시의 예로는 페닐옥시, 나프틸옥시, 디페닐옥시 등이 있는데, 이에 한정되지 않는다.In the present invention, "aryloxy" is a monovalent substituent represented by RO-, and R means an aryl having 5 to 60 carbon atoms. Examples of such aryloxy include, but are not limited to, phenyloxy, naphthyloxy, and diphenyloxy.
본 발명에서의 "알킬옥시"는 R'O-로 표시되는 1가의 치환기로, 상기 R'는 1 내지 40개의 알킬을 의미하며, 직쇄(linear), 측쇄(branched) 또는 사이클릭(cyclic) 구조를 포함하는 것으로 해석한다. 이러한 알킬옥시의 예로는 메톡시, 에톡시, n-프로폭시, 1-프로폭시, t-부톡시, n-부톡시, 펜톡시 등이 있는데, 이에 한정되지 않는다."Alkyloxy" in the present invention is a monovalent substituent represented by R'O-, wherein R'means 1 to 40 alkyl, and has a linear, branched, or cyclic structure It is interpreted as including. Examples of such alkyloxy include, but are not limited to, methoxy, ethoxy, n-propoxy, 1-propoxy, t-butoxy, n-butoxy, pentoxy, and the like.
본 발명에서의 "아릴아민"은 탄소수 6 내지 60개의 아릴로 치환된 아민을 의미한다."Arylamine" in the present invention means an amine substituted with an aryl having 6 to 60 carbon atoms.
본 발명에서의 "시클로알킬"은 탄소수 3 내지 40개의 모노사이클릭 또는 폴리사이클릭 비-방향족 탄화수소로부터 유래된 1가의 치환기를 의미한다. 이러한 사이클로알킬의 예로는 사이클로프로필, 사이클로펜틸, 사이클로헥실, 놀보닐(norbornyl), 아다만틴(adamantine) 등이 있는데, 이에 한정되지 않는다."Cycloalkyl" in the present invention means a monovalent substituent derived from a monocyclic or polycyclic non-aromatic hydrocarbon having 3 to 40 carbon atoms. Examples of such cycloalkyl include, but are not limited to, cyclopropyl, cyclopentyl, cyclohexyl, norbornyl, and adamantine.
본 발명에서의 "헤테로시클로알킬"은 핵원자수 3 내지 40개의 비-방향족 탄화수소로부터 유래된 1가의 치환기를 의미하며, 고리 중 하나 이상의 탄소, 바람직하게는 1 내지 3개의 탄소가 N, O, S 또는 Se와 같은 헤테로 원자로 치환된다. 이러한 헤테로시클로알킬의 예로는 모르폴린, 피페라진 등이 있는데, 이에 한정되지 않는다."Heterocycloalkyl" in the present invention means a monovalent substituent derived from a non-aromatic hydrocarbon having 3 to 40 nuclear atoms, and at least one carbon in the ring, preferably 1 to 3 carbons, is N, O, Substituted by a hetero atom such as S or Se. Examples of such heterocycloalkyl include morpholine and piperazine, but are not limited thereto.
본 발명에서의 "알킬실릴"은 탄소수 1 내지 40개의 알킬로 치환된 실릴이고, "아릴실릴"은 탄소수 5 내지 60개의 아릴로 치환된 실릴을 의미한다.In the present invention, "alkylsilyl" refers to silyl substituted with an alkyl having 1 to 40 carbon atoms, and "arylsilyl" refers to silyl substituted with an aryl having 5 to 60 carbon atoms.
본 발명에서의 "축합 고리"는 축합 지방족 고리, 축합 방향족 고리, 축합 헤테로지방족 고리, 축합 헤테로방향족 고리 또는 이들의 조합된 형태를 의미한다.."Condensed ring" in the present invention means a condensed aliphatic ring, a condensed aromatic ring, a condensed heteroaliphatic ring, a condensed heteroaromatic ring, or a combination thereof.
본 발명의 화합물은 열적 안정성 및 발광 특성이 우수하기 때문에 유기 전계 발광 소자의 유기물층의 재료로 사용될 수 있다. 특히, 본 발명의 화학식 1로 표시되는 화합물을 전자 수송 재료 또는 발광 호스트 재료로 사용할 경우, 종래의 재료에 비해 우수한 발광 성능, 낮은 구동전압, 높은 효율 및 장수명을 갖는 유기 전계 발광 소자를 제조할 수 있고, 나아가 성능 및 수명이 향상된 풀 칼라 디스플레이 패널도 제조할 수 있다.Since the compound of the present invention has excellent thermal stability and light emission properties, it can be used as a material for an organic material layer of an organic electroluminescent device. In particular, when the compound represented by Formula 1 of the present invention is used as an electron transport material or a light emitting host material, an organic electroluminescent device having excellent light emitting performance, low driving voltage, high efficiency, and long lifespan can be manufactured compared to conventional materials. Furthermore, it is possible to manufacture a full-color display panel with improved performance and lifespan.
도 1은 본 발명의 일 실시예에 따른 유기 전계 발광 소자의 단면도를 나타낸 것이다.1 is a cross-sectional view of an organic electroluminescent device according to an embodiment of the present invention.
도 2는 본 발명의 일 실시예에 따른 유기 전계 발광 소자의 단면도를 나타낸 것이다.2 is a cross-sectional view of an organic electroluminescent device according to an embodiment of the present invention.
이하, 본 발명을 상세히 설명한다.Hereinafter, the present invention will be described in detail.
1. 신규 유기 화합물1. New organic compounds
본 발명은 피리미딘계/트리아진계의 유기발광 화합물로, 기존 전자 주입 및 수송 재료에 비해 발광 효율이 좋고 재료의 수명특성이 뛰어나 소자의 구동 수명이 매우 우수할 뿐만 아니라 전력 효율의 상승을 유도하여 소비전력이 개선된 OLED소자를 제조할 수 있는 장점이 있다.The present invention is a pyrimidine-based/triazine-based organic light-emitting compound, which has excellent luminous efficiency compared to the existing electron injection and transport materials, and has excellent lifespan characteristics of the material, so that the driving life of the device is very excellent, as well as inducing an increase in power efficiency. There is an advantage of being able to manufacture OLED devices with improved power consumption.
피리미딘계/트리아진계 화합물에 페난트렌이나 카바졸 등이 도입된 유도체로 삼중항 에너지가 높고 안정한 구조를 기본으로 하는 Core를 가지며, 특히 페난트렌 또는 카바졸 등의 작용기가 치환되었을 때 전자 수송 능력이 향상되어 전력 효율의 상승을 유도하는 구조로 이루어져 있어서 효율 특성을 극대화할 수 있는 전자 주입 또는 수송 재료로써의 장점이 있다. 특히 화학식 1에서 A, B, Ar1 및 Ar2에 방향족 고리 및 헤테로 방향족 고리가 각각 독립적으로 치환되었을 때 평면구조를 개선하여 열적 안정도를 높일 뿐만아니라 전자 이동을 좋게 하여 전자수송층 재료로 적합하다.A derivative of phenanthrene or carbazole introduced into pyrimidine/triazine compounds. It has a core based on a stable structure with high triplet energy.Especially, electron transport ability when functional groups such as phenanthrene or carbazole are substituted. Since the structure is improved to induce an increase in power efficiency, there is an advantage as an electron injection or transport material that can maximize efficiency characteristics. In particular, when the aromatic ring and the heteroaromatic ring are independently substituted for A, B, Ar 1 and Ar 2 in Chemical Formula 1, the planar structure is improved to increase thermal stability and improve electron transfer, making it suitable as an electron transport layer material.
상기 본 발명에 따른 화합물은 하기 화학식 1로 표시된다.The compound according to the present invention is represented by the following formula (1).
[화학식 1][Formula 1]
Figure PCTKR2020004924-appb-I000003
Figure PCTKR2020004924-appb-I000003
상기 화학식 1에서,In Formula 1,
X1 내지 X3은 각각 독립적으로 N 또는 C(R1)이나, 이들 중 적어도 둘 이상은 N이고, R1은 수소이거나 치환 또는 비치환된 C1~C60의 알킬이고,X 1 to X 3 are each independently N or C (R 1 ), but at least two or more of them are N, and R 1 is hydrogen or a substituted or unsubstituted C 1 to C 60 alkyl,
L1 내지 L4는 각각 독립적으로 직접결합, 또는 C6~C18의 아릴렌기 및 핵원자수 5 내지 18개의 헤테로아릴렌기로 이루어진 군에서 선택되며,L 1 to L 4 are each independently a direct bond, or selected from the group consisting of an arylene group of C 6 to C 18 and a heteroarylene group having 5 to 18 nuclear atoms,
A와 B는 각각 독립적으로 치환 또는 비치환된 C6~C60의 아릴기 또는 핵원자수 5 내지 60개의 헤테로아릴기이며, 적어도 하나 이상은 함질소복소환을 포함하는 헤테로아릴기이며,A and B are each independently a substituted or unsubstituted C 6 to C 60 aryl group or a heteroaryl group having 5 to 60 nuclear atoms, and at least one is a heteroaryl group including a nitrogen-containing heterocycle,
Ar1 과 Ar2는 C6~C60의 아릴기 또는 핵원자수 5 내지 60개의 헤테로아릴기이며, , 적어도 하나 이상은 함질소복소환을 포함하는 헤테로아릴기이며,Ar 1 and Ar 2 is a C 6 ~ C 60 aryl group or a heteroaryl group having 5 to 60 nuclear atoms, at least one is a heteroaryl group containing a nitrogen-containing heterocycle,
상기 L1 내지 L4의 아릴렌기 및 헤테로아릴렌기와, 상기 A, B, Ar1 및 Ar2의 아릴기 및 헤테로아릴기는 각각 독립적으로 중수소, 할로겐, 시아노기, 니트로기, C1~C40의 알킬기, C2~C40의 알케닐기, C2~C40의 알키닐기, C6~C60의 아릴기, 핵원자수 5 내지 60개의 헤테로아릴기, C6~C60의 아릴옥시기, C1~C40의 알킬옥시기, C6~C60의 아릴아민기, C3~C40의 시클로알킬기, 핵원자수 3 내지 40개의 헤테로시클로알킬기, C1~C40의 알킬실릴기, C1~C40의 알킬보론기, C6~C60의 아릴보론기, C6~C60의 아릴포스핀기, C6~C60의 모노 또는 디아릴포스피닐기 및 C6~C60의 아릴실릴기로 이루어진 군에서 선택된 1종 이상의 치환기로 치환되거나 비치환되고, 복수 개의 치환기로 치환되는 경우, 이들은 서로 동일하거나 상이할 수 있다.The arylene group and heteroarylene group of L 1 to L 4, the aryl group and heteroaryl group of A, B, Ar 1 and Ar 2 are each independently deuterium, halogen, cyano group, nitro group, C 1 to C 40 Alkyl group, C 2 ~ C 40 alkenyl group, C 2 ~ C 40 alkynyl group, C 6 ~ C 60 aryl group, 5 to 60 nuclear atoms heteroaryl group, C 6 ~ C 60 aryloxy group , C 1 ~ C 40 alkyloxy group, C 6 ~ C 60 arylamine group, C 3 ~ C 40 cycloalkyl group, 3 to 40 nuclear atoms heterocycloalkyl group, C 1 ~ C 40 alkylsilyl group , C 1 ~ C 40 alkyl boron group, C 6 ~ C 60 aryl boron group, C 6 ~ C 60 arylphosphine group, C 6 ~ C 60 mono or diarylphosphine group and C 6 ~ C 60 When substituted or unsubstituted with one or more substituents selected from the group consisting of an arylsilyl group of, and when substituted with a plurality of substituents, they may be the same or different from each other.
상기 화학식 1로 표시되는 화합물은 하기 화합식 1-1 또는 1-2로 표시되는 것일 수 있다.The compound represented by Formula 1 may be represented by Formula 1-1 or 1-2 below.
[화학식 1-1][Formula 1-1]
Figure PCTKR2020004924-appb-I000004
Figure PCTKR2020004924-appb-I000004
[화학식 1-2][Formula 1-2]
Figure PCTKR2020004924-appb-I000005
Figure PCTKR2020004924-appb-I000005
상기 화학식 1-1 및 화학식 1-2에서, A, B, L1 내지 L4, Ar1 및 Ar2는 앞서 정의한 바와 같다.In Formulas 1-1 and 1-2, A, B, L 1 to L 4 , Ar 1 and Ar 2 are as previously defined.
또한, 상기 A 및 B는 각각 독립적으로 하기 치환기 군으로부터 어느 하나 선택되며, 적어도 하나 이상은 함질소복소환을 포함하는 치환기일 수 있다.In addition, each of A and B is independently selected from the following substituent groups, and at least one or more may be a substituent including a nitrogen-containing heterocycle.
Figure PCTKR2020004924-appb-I000006
Figure PCTKR2020004924-appb-I000006
또한, 상기 Ar1 및 Ar2는 각각 독립적으로 하기 치환기 군으로부터 어느 하나 선택되며, 적어도 하나 이상은 함질소복소환을 포함하는 치환기일 수 있다.In addition, Ar 1 and Ar 2 are each independently selected from the following substituent groups, and at least one may be a substituent including a nitrogen-containing heterocycle.
Figure PCTKR2020004924-appb-I000007
Figure PCTKR2020004924-appb-I000007
참고로, 상기 치환기 군에서 *는 결합이 이루어지는 부분이다.For reference, in the substituent group, * is a moiety in which a bond is formed.
또한, 화학식 1에서의 A, B, Ar1 및 Ar2는 서로 상이한 것일 수 있다. 이를 통해 각 치환기마다 Band gap 차이를 주어 전하의 흐름을 원활히 할 수 있고, 주변 재료와의 평면성을 보다 강화할 수 있는 moiety 도입으로 재료의 성능 및 안정성을 높일 수 있다.In addition, A, B, Ar 1 and Ar 2 in Formula 1 may be different from each other. Through this, it is possible to smooth the flow of charge by giving a band gap difference for each substituent, and the performance and stability of the material can be improved by introducing a moiety that can further enhance the planarity with the surrounding material.
또한, 상기 L1 내지 L4는 각각 독립적으로 직접결합 또는 아릴렌일 수 있다.In addition, the L 1 to L 4 may each independently be a direct bond or an arylene.
본 발명의 바람직한 한 구현 예에 따르면, 상기 화합물은 아래의 화합물로 이루어진 군에서 선택될 수 있다.According to a preferred embodiment of the present invention, the compound may be selected from the group consisting of the following compounds.
또한, 상기 L1 내지 L4는 각각 독립적으로 직접결합 또는 아릴렌일 수 있다.In addition, the L 1 to L 4 may each independently be a direct bond or an arylene.
본 발명의 바람직한 한 구현 예에 따르면, 상기 화합물은 아래의 화합물로 이루어진 군에서 선택될 수 있다.According to a preferred embodiment of the present invention, the compound may be selected from the group consisting of the following compounds.
Figure PCTKR2020004924-appb-I000008
Figure PCTKR2020004924-appb-I000008
Figure PCTKR2020004924-appb-I000009
Figure PCTKR2020004924-appb-I000009
Figure PCTKR2020004924-appb-I000010
Figure PCTKR2020004924-appb-I000010
Figure PCTKR2020004924-appb-I000011
Figure PCTKR2020004924-appb-I000011
Figure PCTKR2020004924-appb-I000012
Figure PCTKR2020004924-appb-I000012
Figure PCTKR2020004924-appb-I000013
Figure PCTKR2020004924-appb-I000013
Figure PCTKR2020004924-appb-I000014
Figure PCTKR2020004924-appb-I000014
Figure PCTKR2020004924-appb-I000015
Figure PCTKR2020004924-appb-I000015
Figure PCTKR2020004924-appb-I000016
Figure PCTKR2020004924-appb-I000016
Figure PCTKR2020004924-appb-I000017
Figure PCTKR2020004924-appb-I000017
Figure PCTKR2020004924-appb-I000018
Figure PCTKR2020004924-appb-I000018
Figure PCTKR2020004924-appb-I000019
Figure PCTKR2020004924-appb-I000019
Figure PCTKR2020004924-appb-I000020
Figure PCTKR2020004924-appb-I000020
Figure PCTKR2020004924-appb-I000021
Figure PCTKR2020004924-appb-I000021
Figure PCTKR2020004924-appb-I000022
Figure PCTKR2020004924-appb-I000022
Figure PCTKR2020004924-appb-I000023
Figure PCTKR2020004924-appb-I000023
Figure PCTKR2020004924-appb-I000024
Figure PCTKR2020004924-appb-I000024
Figure PCTKR2020004924-appb-I000025
Figure PCTKR2020004924-appb-I000025
화학식 1로 대표되는 본 발명의 화합물은 일반적인 합성방법에 따라 합성될 수 있다(Chem. Rev., 60:313 (1960); J. Chem. SOC. 4482 (1955); Chem. Rev. 95: 2457 (1995) 등 참조). 본 발명의 화합물에 대한 상세한 합성 과정은 후술하는 합성예에서 구체적으로 기술하도록 한다.The compound of the present invention represented by Formula 1 can be synthesized according to a general synthesis method ( Chem. Rev. , 60 :313 (1960); J. Chem. SOC . 4482 (1955); Chem. Rev. 95: 2457) (1995) et al.). Detailed synthesis procedures for the compounds of the present invention will be described in detail in the synthesis examples described later.
2. 유기 전계 발광 소자2. Organic EL device
한편, 본 발명의 다른 측면은 상기한 본 발명에 따른 화학식 1로 대표되는 화합물을 포함하는 유기 전계 발광 소자(유기 EL 소자)에 관한 것이다.On the other hand, another aspect of the present invention relates to an organic electroluminescent device (organic EL device) including the compound represented by Formula 1 according to the present invention.
구체적으로, 본 발명은 양극(anode), 음극(cathode), 및 상기 양극과 음극 사이에 개재(介在)된 1층 이상의 유기물층을 포함하는 유기 전계 발광 소자로서, 상기 1층 이상의 유기물층 중 적어도 하나는 상기 화학식 1로 표시되는 화합물을 포함한다. 이때, 상기 화합물은 단독 또는 2 이상 혼합되어 사용될 수 있다.Specifically, the present invention is an organic electroluminescent device comprising an anode, a cathode, and one or more organic material layers interposed between the anode and the cathode, wherein at least one of the one or more organic material layers It includes a compound represented by Formula 1. In this case, the compound may be used alone or in combination of two or more.
상기 1층 이상의 유기물층은 정공 주입층, 정공 수송층, 발광층, 전자 수송층, 전자 수송 보조층 및 전자 주입층 중 어느 하나 이상일 수 있고, 이 중에서 적어도 하나의 유기물층이 상기 화학식 1로 표시되는 화합물을 포함할 수 있으며, 보다 바람직하게는 상기 유기물층에서 전자 수송층, 전자 수송 보조층 또는 발광층이 상기 화학식 1로 표시되는 화합물을 포함할 수 있다.The one or more organic material layers may be any one or more of a hole injection layer, a hole transport layer, a light emitting layer, an electron transport layer, an electron transport auxiliary layer, and an electron injection layer, of which at least one organic material layer contains the compound represented by Formula 1 above. In the organic material layer, more preferably, the electron transport layer, the electron transport auxiliary layer, or the light-emitting layer may include the compound represented by Formula 1 above.
전술한 본 발명에 따른 유기 전계 발광 소자의 구조는 특별히 한정되지 않으나, 일 예시로 도 1을 참고하면, 예컨대 서로 마주하는 양극(10)과 음극(20), 그리고 상기 양극(10)과 음극(20) 사이에 위치하는 유기층(30)을 포함한다. 여기서, 상기 유기층(30)은 정공 수송층(31), 발광층(32) 및 전자 수송층(34)을 포함할 수 있다. 또한, 상기 정공 수송층(31)과 발광층(32) 사이에는 정공 수송 보조층(33)을 포함할 수 있으며, 상기 전자 수송층(34)과 발광층(32) 사이에는 전자 수송 보조층(35)을 포함할 수 있다.The structure of the organic electroluminescent device according to the present invention is not particularly limited, but referring to FIG. 1 as an example, for example, an anode 10 and a cathode 20 facing each other, and the anode 10 and the cathode ( 20) includes an organic layer 30 positioned between. Here, the organic layer 30 may include a hole transport layer 31, an emission layer 32 and an electron transport layer 34. In addition, a hole transport auxiliary layer 33 may be included between the hole transport layer 31 and the light emitting layer 32, and an electron transport auxiliary layer 35 may be included between the electron transport layer 34 and the light emitting layer 32. can do.
본 발명의 다른 예시로 도 2를 참고하면, 상기 유기층(30)은 정공 수송층(31)과 양극(10)사이에 정공 주입층(37)을 더 포함할 수 있으며, 전자 수송층(34)과 음극(20)사이에는 전자 주입층(36)을 추가로 더 포함할 수 있다.Referring to FIG. 2 as another example of the present invention, the organic layer 30 may further include a hole injection layer 37 between the hole transport layer 31 and the anode 10, and the electron transport layer 34 and the cathode An electron injection layer 36 may be further included between the 20.
본 발명에서 상기 정공 수송층(31)과 양극(10) 사이에 적층되는 정공 주입층(37)은 양극으로 사용되는 ITO와, 정공 수송층(31)으로 사용되는 유기물질 사이의 계면 특성을 개선할 뿐만 아니라 그 표면이 평탄하지 않은 ITO의 상부에 도포되어 ITO의 표면을 부드럽게 만들어주는 기능을 하는 층으로, 당 기술분야에서 통상적으로 사용되는 것이면 특별한 제한없이 사용할 수 있으며, 예컨대, 아민 화합물을 사용할 수 있으나 이에 한정되는 것은 아니다.In the present invention, the hole injection layer 37 stacked between the hole transport layer 31 and the anode 10 not only improves the interfacial characteristics between the ITO used as the anode and the organic material used as the hole transport layer 31. In addition, it is a layer that has a function of smoothing the surface of ITO by being applied on the top of the ITO, which is not flat, and can be used without particular limitation, as long as it is commonly used in the art. For example, an amine compound can be used. It is not limited thereto.
또한, 상기 전자 주입층(36)은 전자 수송층의 상부에 적층되어 음극으로부터의 전자 주입을 용이하게 해주어 궁극적으로 전력효율을 개선시키는 기능을 수행하는 층으로, 당 기술분야에서 통상적으로 사용되는 것이면 특별한 제한없이 사용할 수 있으며, 예컨대, LiF, Liq, NaCl, CsF, Li2O, BaO 등의 물질을 이용할 수 있다.In addition, the electron injection layer 36 is a layer that is stacked on top of the electron transport layer to facilitate electron injection from the cathode and ultimately improves power efficiency, and is a special layer that is commonly used in the art. It can be used without limitation, and materials such as LiF, Liq, NaCl, CsF, Li 2 O, and BaO may be used.
또한, 상기 전자 수송층 (34)과 발광층(32) 사이에 전자 수송 보조층(35)을 더 포함할 수 있다. 상기 발광층(32)으로 유기 발광 소자 내에서 이온화 포텐셜 레벨을 타고 이동하는 정공이 전자 수송 보조층(35)의 의 높은 에너지 장벽에 막혀 전자 수송층으로 확산, 또는 이동하지 못해, 결과적으로 정공을 발광층에 제한시키는 기능을 한다. 이렇게 정공을 발광층에 제한시키는 기능은 환원에 의해 전자를 이동시키는 전자 수송층으로 정공이 확산되는 것을 막아, 산화에 의한 비가역적 분해반응을 통한 수명저하 현상을 억제하여, 유기 발광 소자의 수명 개선에 기여할 수 있다.In addition, an electron transport auxiliary layer 35 may be further included between the electron transport layer 34 and the emission layer 32. Holes moving along the ionization potential level in the organic light-emitting device to the emission layer 32 are blocked by the high energy barrier of the electron transport auxiliary layer 35 and cannot diffuse or move to the electron transport layer, and as a result, holes are transferred to the emission layer. It serves as a limiting function. This function of restricting holes to the emission layer prevents the diffusion of holes to the electron transport layer that moves electrons by reduction, suppressing the reduction in lifespan through irreversible decomposition reactions caused by oxidation, and contributing to the improvement of the lifespan of the organic light emitting device. I can.
본 발명에서 상기 화학식 1로 대표되는 화합물은 전기화학적으로 안정하고, 전자 이동성이 우수할 뿐만 아니라 높은 유리 전이온도 및 열적 안정이 우수하며, 전자수송층에 더욱 적합한 물리화학적 성질을 가진다.In the present invention, the compound represented by Formula 1 is electrochemically stable, has excellent electron mobility, high glass transition temperature and thermal stability, and has a physicochemical property more suitable for an electron transport layer.
따라서, 본 발명의 화학식 1 구조의 화합물들은 유기 전계 발광 소자에 사용할 경우, 우수한 열적 안정성 및 캐리어 수송능(특히, 전자 수송능 및 발광능)을 기대할 수 있을 뿐만 아니라 소자의 구동전압, 효율, 수명 등이 향상될 수 있다.Therefore, when the compounds of the structure of Formula 1 of the present invention are used in an organic electroluminescent device, excellent thermal stability and carrier transport capability (especially, electron transport capability and luminescence capability) can be expected, as well as driving voltage, efficiency, and lifetime of the device. The back can be improved.
본 발명의 화학식 1로 대표되는 화합물은 유기 전계 발광 소자의 유기물층(30) 재료, 바람직하게는 전자 수송층(34), 전자 수송 보조층(35) 재료로 사용될 수 있다. 또한, 상기 화학식 1의 화합물을 포함하는 유기 전계 발광 소자는 성능 및 수명 특성이 크게 향상될 수 있고, 이러한 유기 전계 발광 소자가 적용된 풀 칼라 유기 발광 패널도 성능이 극대화될 수 있다.The compound represented by Chemical Formula 1 of the present invention may be used as a material for the organic material layer 30, preferably the electron transport layer 34 and the electron transport auxiliary layer 35 of the organic electroluminescent device. In addition, the organic electroluminescent device including the compound of Formula 1 may have significantly improved performance and lifetime characteristics, and a full-color organic light-emitting panel to which such an organic electroluminescent device is applied may also maximize performance.
또한, 본 발명에서 상기 유기 전계 발광 소자는 상기한 바와 같이 양극, 1층 이상의 유기물층 및 음극이 순차적으로 적층될 뿐만 아니라, 전극과 유기물층 계면에 절연층 또는 접착층을 추가로 포함할 수 있다.Further, in the present invention, the organic electroluminescent device may include an anode, one or more organic material layers, and a cathode sequentially stacked as described above, and further include an insulating layer or an adhesive layer at the interface between the electrode and the organic material layer.
본 발명의 유기 전계 발광 소자는 상기 유기물층 중 적어도 하나 이상(예컨대, 전자 수송층)이 상기 화학식 1로 표시되는 화합물을 포함하도록 형성하는 것을 제외하고는, 당 기술 분야에 알려져 있는 재료 및 방법을 이용하여 다른 유기물층 및 전극을 형성하여 제조될 수 있다.The organic electroluminescent device of the present invention uses materials and methods known in the art, except that at least one of the organic material layers (eg, an electron transport layer) is formed to include the compound represented by Formula 1 It can be manufactured by forming other organic material layers and electrodes.
상기 유기물층은 진공 증착법이나 용액 도포법에 의하여 형성될 수 있다. 상기 용액 도포법의 예로는 스핀 코팅, 딥코팅, 닥터 블레이딩, 잉크젯 프린팅 또는 열 전사법 등이 있으나, 이에 한정되지 않는다.The organic material layer may be formed by a vacuum deposition method or a solution coating method. Examples of the solution coating method include, but are not limited to, spin coating, dip coating, doctor blading, inkjet printing, or thermal transfer method.
본 발명에서 사용 가능한 기판으로는 특별히 한정되지 않으며, 실리콘 웨이퍼, 석영, 유리판, 금속판, 플라스틱 필름 및 시트 등이 사용될 수 있다.The substrate usable in the present invention is not particularly limited, and a silicon wafer, quartz, glass plate, metal plate, plastic film and sheet, and the like may be used.
또, 양극 물질로는 예컨대 정공 주입이 원활하도록 일 함수가 높은 도전체로 만들어질 수 있으며, 바나듐, 크롬, 구리, 아연, 금과 같은 금속 또는 이들의 합금; 아연산화물, 인듐산화물, 인듐 주석 산화물(ITO), 인듐 아연 산화물(IZO)과 같은 금속 산화물; ZnO:Al 또는 SnO2:Sb와 같은 금속과 산화물의 조합; 폴리티오펜, 폴리(3-메틸티오펜), 폴리[3,4-(에틸렌-1,2-디옥시)티오펜](PEDT), 폴리피롤 또는 폴리아닐린과 같은 전도성 고분자; 및 카본블랙 등이 있으나, 이에 한정되지는 않는다.In addition, the anode material may be made of a conductor having a high work function to facilitate hole injection, for example, and may include metals such as vanadium, chromium, copper, zinc, and gold, or alloys thereof; Metal oxides such as zinc oxide, indium oxide, indium tin oxide (ITO), and indium zinc oxide (IZO); Combinations of metals and oxides such as ZnO:Al or SnO 2 :Sb; Conductive polymers such as polythiophene, poly(3-methylthiophene), poly[3,4-(ethylene-1,2-dioxy)thiophene] (PEDT), polypyrrole or polyaniline; And carbon black, but are not limited thereto.
또, 음극 물질로는 예컨대 전자 주입이 원활하도록 일 함수가 낮은 도전체로 만들어질 수 있으며, 마그네슘, 칼슘, 나트륨, 칼륨, 타이타늄, 인듐, 이트륨, 리튬, 가돌리늄, 알루미늄, 은, 주석, 또는 납과 같은 금속 또는 이들의 합금; 및 LiF/Al 또는 LiO2/Al과 같은 다층 구조 물질 등이 있으나, 이에 한정되지는 않는다.In addition, as a negative electrode material, for example, it may be made of a conductor having a low work function to facilitate electron injection, and magnesium, calcium, sodium, potassium, titanium, indium, yttrium, lithium, gadolinium, aluminum, silver, tin, or lead The same metal or alloys thereof; And a multilayered material such as LiF/Al or LiO 2 /Al, but is not limited thereto.
이하 본 발명을 실시예를 통하여 상세히 설명하면 다음과 같다. 단, 하기 실시예는 본 발명을 예시하는 것일 뿐, 본 발명이 하기 실시예에 의해 한정되는 것은 아니다.Hereinafter, the present invention will be described in detail through examples. However, the following examples are only illustrative of the present invention, and the present invention is not limited by the following examples.
[준비예 1][Preparation Example 1]
4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(pyridin-3-yl)pyrimidine의 합성Synthesis of 4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(pyridin-3-yl)pyrimidine
Figure PCTKR2020004924-appb-I000026
Figure PCTKR2020004924-appb-I000026
4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(pyridin-3-yl)pyrimidine 50g(92.2mmol)과 pyridin-3-ylboronic acid 11.3g(92.2mmol)에 1,4-dioxane 250 mL를 가하였다. Pd(PPh3)4 5.32g(4.61mmol), K2CO3 31.85g(230mol)을 첨가 후 120℃에서 24시간 가열환류하였다. 상온으로 온도를 냉각하고 반응액에 염화암모늄 수용액 500 mL로 반응을 종결시켰다. 혼합액을 M.C 500 mL로 추출한 후, 증류수로 세척하였다. 얻어진 유기층을 무수 MgSO4로 건조하고, 감압증류하고 실리카겔 컬럼크로마토그래피로 정제하여 목적 화합물 30g(수율 61%)을 얻었다. 1H-NMR: 9.24(s, 1H), 8.73(s, 1H), 8.70(dd, 2H), 8.42(dd, 2H), 8.30(dd, 2H), 7.88(s, 1H), 7.85(dd, 2H), 7.57~7.45(m, 7H); HRMS [M]+: 542.454-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(pyridin-3-yl)pyrimidine 50g(92.2mmol) and pyridin-3-ylboronic acid 11.3 250 mL of 1,4-dioxane was added to g (92.2 mmol). Pd(PPh 3 ) 4 5.32g (4.61mmol) and K 2 CO 3 31.85g (230mol) were added and then heated to reflux at 120° C. for 24 hours. The temperature was cooled to room temperature, and the reaction was terminated with 500 mL of an aqueous ammonium chloride solution in the reaction solution. The mixed solution was extracted with 500 mL of MC, and then washed with distilled water. The obtained organic layer was dried over anhydrous MgSO 4 , distilled under reduced pressure, and purified by silica gel column chromatography to obtain 30 g of the title compound (yield 61%). 1H-NMR: 9.24 (s, 1H), 8.73 (s, 1H), 8.70 (dd, 2H), 8.42 (dd, 2H), 8.30 (dd, 2H), 7.88 (s, 1H), 7.85 (dd, 2H), 7.57-7.45 (m, 7H); HRMS [M] + : 542.45
[준비예 2][Preparation Example 2]
4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidine의 합성Synthesis of 4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidine
Figure PCTKR2020004924-appb-I000027
Figure PCTKR2020004924-appb-I000027
반응물로 4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(pyridin-4-yl)pyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 26g을 얻었다.; HRMS [M]+: 542.45[Preparation Example 1] except that 4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(pyridin-4-yl)pyrimidine was used as a reactant 26g of the title compound was obtained by performing the same procedure as described above.; HRMS [M]+: 542.45
[준비예 3][Preparation Example 3]
4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-phenyl-6-(4-(pyridin-3-yl)phenyl)pyrimidine의 합성Synthesis of 4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-phenyl-6-(4-(pyridin-3-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000028
Figure PCTKR2020004924-appb-I000028
반응물로 4-(3,5-dibromophenyl)-2-phenyl-6-(4-(pyridin-3-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 30g을 얻었다.; HRMS [M]+: 542.45Except for using 4-(3,5-dibromophenyl)-2-phenyl-6-(4-(pyridin-3-yl)phenyl)pyrimidine as a reactant, the target compound was performed in the same manner as in [Preparation Example 1] 30g was obtained.; HRMS [M]+: 542.45
[준비예 4][Preparation Example 4]
4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-phenyl-6-(4-(pyridin-4-yl)phenyl)pyrimidine의 합성Synthesis of 4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-phenyl-6-(4-(pyridin-4-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000029
Figure PCTKR2020004924-appb-I000029
반응물로 4-(3,5-dibromophenyl)-2-phenyl-6-(4-(pyridin-4-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 25g을 얻었다.; HRMS [M]+: 542.45Except for using 4-(3,5-dibromophenyl)-2-phenyl-6-(4-(pyridin-4-yl)phenyl)pyrimidine as a reactant, the target compound was carried out in the same manner as in [Preparation Example 1] 25g was obtained.; HRMS [M]+: 542.45
[준비예 5][Preparation Example 5]
4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine의 합성Synthesis of 4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000030
Figure PCTKR2020004924-appb-I000030
반응물로 4-(3,5-dibromophenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 543.44The same as in [Preparation Example 1], except that 4-(3,5-dibromophenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine was used as a reactant. The procedure was carried out to obtain 32 g of the title compound.; HRMS [M]+: 543.44
[준비예 6][Preparation Example 6]
4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine의 합성Synthesis of 4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000031
Figure PCTKR2020004924-appb-I000031
반응물로 4-(3,5-dibromophenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 543.44The same as in [Preparation Example 1] except for using 4-(3,5-dibromophenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine as a reactant The procedure was carried out to obtain 32 g of the title compound.; HRMS [M]+: 543.44
[준비예 7][Preparation Example 7]
4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidine의 합성 Synthesis of 4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidine
Figure PCTKR2020004924-appb-I000032
Figure PCTKR2020004924-appb-I000032
반응물로 4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 543.44The same as in [Preparation Example 1] except for using 4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidine as a reactant 39g of the title compound was obtained by performing the procedure.; HRMS [M]+: 543.44
[준비예 8][Preparation Example 8]
4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine의 합성 Synthesis of 4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000033
Figure PCTKR2020004924-appb-I000033
반응물로 4-(3,5-dibromophenyl)-2-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 543.44The same as in [Preparation Example 1], except that 4-(3,5-dibromophenyl)-2-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine was used as a reactant. 39g of the title compound was obtained by performing the procedure.; HRMS [M]+: 543.44
[준비예 9][Preparation Example 9]
4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(4-(pyridin-3-yl)phenyl)pyrimidine의 합성 4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(4-(pyridin-3-yl)phenyl) synthesis of pyrimidine
Figure PCTKR2020004924-appb-I000034
Figure PCTKR2020004924-appb-I000034
반응물로 4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(4-(pyridin-3-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 618.55Except for using 4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(4-(pyridin-3-yl)phenyl)pyrimidine as a reactant 39g of the title compound was obtained by performing the same procedure as in [Preparation Example 1].; HRMS [M]+: 618.55
[준비예 10][Preparation Example 10]
4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(4-(pyridin-4-yl)phenyl)pyrimidine의 합성 4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(4-(pyridin-4-yl)phenyl) synthesis of pyrimidine
Figure PCTKR2020004924-appb-I000035
Figure PCTKR2020004924-appb-I000035
반응물로 4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(4-(pyridin-4-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 618.55Except for using 4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(4-(pyridin-4-yl)phenyl)pyrimidine as a reactant 45g of the target compound was obtained by performing the same procedure as in [Preparation Example 1].; HRMS [M]+: 618.55
[준비예 11][Preparation Example 11]
4-(3-bromo-5-(pyridin-3-yl)phenyl)-2,6-bis(4-(pyridin-3-yl)phenyl)pyrimidine의 합성 Synthesis of 4-(3-bromo-5-(pyridin-3-yl)phenyl)-2,6-bis(4-(pyridin-3-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000036
Figure PCTKR2020004924-appb-I000036
반응물로 4-(3,5-dibromophenyl)-2,6-bis(4-(pyridin-3-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 619.5445g of the target compound by performing the same procedure as in [Preparation Example 1], except that 4-(3,5-dibromophenyl)-2,6-bis(4-(pyridin-3-yl)phenyl)pyrimidine was used as the reactant Got HRMS [M]+: 619.54
[준비예 12][Preparation Example 12]
4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine의 합성 4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine synthesis
Figure PCTKR2020004924-appb-I000037
Figure PCTKR2020004924-appb-I000037
반응물로 4-(3,5-dibromophenyl)-2-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 619.54[Preparation] except for using 4-(3,5-dibromophenyl)-2-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine as the reactant 45g of the title compound was obtained by performing the same procedure as in Example 1].; HRMS [M]+: 619.54
[준비예 13][Preparation Example 13]
4-(3-bromo-5-(pyridin-3-yl)phenyl)-2,6-bis(4-(pyridin-4-yl)phenyl)pyrimidine의 합성 Synthesis of 4-(3-bromo-5-(pyridin-3-yl)phenyl)-2,6-bis(4-(pyridin-4-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000038
Figure PCTKR2020004924-appb-I000038
반응물로 4-(3,5-dibromophenyl)-2,6-bis(4-(pyridin-4-yl)phenyl)pyrimidineyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 619.54Except for using 4-(3,5-dibromophenyl)-2,6-bis(4-(pyridin-4-yl)phenyl)pyrimidineyrimidine as a reactant, the target compound 45g by performing the same procedure as in [Preparation Example 1] Got HRMS [M]+: 619.54
[준비예 14][Preparation Example 14]
4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine의 합성 Synthesis of 4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000039
Figure PCTKR2020004924-appb-I000039
반응물로 4-(3,5-dibromophenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 592.51The same as in [Preparation Example 1], except that 4-(3,5-dibromophenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine was used as the reactant. The procedure was carried out to obtain 45 g of the title compound.; HRMS [M]+: 592.51
[준비예 15][Preparation Example 15]
4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine의 합성 Synthesis of 4-(3-bromo-5-(pyridin-3-yl)phenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000040
Figure PCTKR2020004924-appb-I000040
반응물로 4-(3,5-dibromophenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 592.51Same as [Preparation Example 1] except for using 4-(3,5-dibromophenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine as a reactant The procedure was carried out to obtain 45 g of the title compound.; HRMS [M]+: 592.51
[준비예 16][Preparation Example 16]
6-(4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-3-yl)phenyl)pyrimidin-2-yl)quinoline의 합성 Synthesis of 6-(4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-3-yl)phenyl)pyrimidin-2-yl)quinoline
Figure PCTKR2020004924-appb-I000041
Figure PCTKR2020004924-appb-I000041
반응물로 6-(4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)pyrimidin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 592.51[Preparation Example 1] and except for using 6-(4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)pyrimidin-2-yl)quinoline as a reactant 45g of the title compound was obtained by performing the same procedure.; HRMS [M]+: 592.51
[준비예 17][Preparation Example 17]
6-(4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-2-yl)quinoline의 합성 Synthesis of 6-(4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-2-yl)quinoline
Figure PCTKR2020004924-appb-I000042
Figure PCTKR2020004924-appb-I000042
반응물로 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 593.50The same process as in [Preparation Example 1], except that 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-2-yl)quinoline was used as the reactant To obtain 45 g of the title compound.; HRMS [M]+: 593.50
[준비예 18][Preparation Example 18]
6-(4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-2-yl)quinoline의 합성 Synthesis of 6-(4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-2-yl)quinoline
Figure PCTKR2020004924-appb-I000043
Figure PCTKR2020004924-appb-I000043
반응물로 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 593.50The same process as in [Preparation Example 1], except that 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-2-yl)quinoline was used as the reactant To obtain 45 g of the title compound.; HRMS [M]+: 593.50
[준비예 19][Preparation Example 19]
4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(pyridin-3-yl)pyrimidine의 합성Synthesis of 4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(pyridin-3-yl)pyrimidine
Figure PCTKR2020004924-appb-I000044
Figure PCTKR2020004924-appb-I000044
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 26g을 얻었다.; HRMS [M]+: 542.45Except that pyridin-4-ylboronic acid was used as a reactant, the target compound 26g was obtained by performing the same procedure as in [Preparation Example 1].; HRMS [M]+: 542.45
[준비예 20][Preparation Example 20]
4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(pyridin-4-yl)pyrimidine의 합성Synthesis of 4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(pyridin-4-yl)pyrimidine
Figure PCTKR2020004924-appb-I000045
Figure PCTKR2020004924-appb-I000045
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 2]과 동일한 과정을 수행하여 목적 화합물 26g을 얻었다.; HRMS [M]+: 542.45Except that pyridin-4-ylboronic acid was used as the reactant, the target compound 26g was obtained by performing the same procedure as in [Preparation Example 2].; HRMS [M]+: 542.45
[준비예 21][Preparation Example 21]
4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-phenyl-6-(4-(pyridin-3-yl)phenyl)pyrimidine의 합성Synthesis of 4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-phenyl-6-(4-(pyridin-3-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000046
Figure PCTKR2020004924-appb-I000046
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 3]과 동일한 과정을 수행하여 목적 화합물 30g을 얻었다.; HRMS [M]+: 542.4530g of the target compound was obtained by performing the same procedure as in [Preparation Example 3], except that pyridin-4-ylboronic acid was used as the reactant.; HRMS [M]+: 542.45
[준비예 22][Preparation Example 22]
4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-phenyl-6-(4-(pyridin-4-yl)phenyl)pyrimidine의 합성Synthesis of 4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-phenyl-6-(4-(pyridin-4-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000047
Figure PCTKR2020004924-appb-I000047
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 4]과 동일한 과정을 수행하여 목적 화합물 25g을 얻었다.; HRMS [M]+: 542.45Except that pyridin-4-ylboronic acid was used as a reactant, 25g of the target compound was obtained by performing the same procedure as in [Preparation Example 4].; HRMS [M]+: 542.45
[준비예 23][Preparation Example 23]
4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine의 합성Synthesis of 4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000048
Figure PCTKR2020004924-appb-I000048
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 5]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 543.44Except that pyridin-4-ylboronic acid was used as a reactant, 32g of the target compound was obtained by performing the same procedure as in [Preparation Example 5].; HRMS [M]+: 543.44
[준비예 24][Preparation Example 24]
4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine의 합성Synthesis of 4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000049
Figure PCTKR2020004924-appb-I000049
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 6]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 543.44Except that pyridin-4-ylboronic acid was used as a reactant, the target compound 32g was obtained by performing the same procedure as in [Preparation Example 6].; HRMS [M]+: 543.44
[준비예 25][Preparation Example 25]
4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidine의 합성 Synthesis of 4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidine
Figure PCTKR2020004924-appb-I000050
Figure PCTKR2020004924-appb-I000050
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 7]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 543.4439g of the target compound was obtained by performing the same procedure as in [Preparation Example 7], except that pyridin-4-ylboronic acid was used as the reactant.; HRMS [M]+: 543.44
[준비예 26][Preparation Example 26]
4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine의 합성 Synthesis of 4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000051
Figure PCTKR2020004924-appb-I000051
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 8]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 543.4439g of the target compound was obtained by performing the same procedure as in [Preparation Example 8], except that pyridin-4-ylboronic acid was used as the reactant.; HRMS [M]+: 543.44
[준비예 27][Preparation Example 27]
4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(4-(pyridin-3-yl)phenyl)pyrimidine의 합성 4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(4-(pyridin-3-yl)phenyl) synthesis of pyrimidine
Figure PCTKR2020004924-appb-I000052
Figure PCTKR2020004924-appb-I000052
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 9]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 618.5539g of the target compound was obtained by performing the same procedure as in [Preparation Example 9], except that pyridin-4-ylboronic acid was used as the reactant.; HRMS [M]+: 618.55
[준비예 28][Preparation Example 28]
4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(4-(pyridin-4-yl)phenyl)pyrimidine의 합성 4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(4-(pyridin-4-yl)phenyl) synthesis of pyrimidine
Figure PCTKR2020004924-appb-I000053
Figure PCTKR2020004924-appb-I000053
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 10]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 618.5545g of the target compound was obtained by performing the same procedure as in [Preparation Example 10], except that pyridin-4-ylboronic acid was used as the reactant.; HRMS [M]+: 618.55
[준비예 29][Preparation Example 29]
4-(3-bromo-5-(pyridin-4-yl)phenyl)-2,6-bis(4-(pyridin-3-yl)phenyl)pyrimidine의 합성 Synthesis of 4-(3-bromo-5-(pyridin-4-yl)phenyl)-2,6-bis(4-(pyridin-3-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000054
Figure PCTKR2020004924-appb-I000054
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 11]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 619.5445g of the target compound was obtained by performing the same procedure as in [Preparation Example 11], except that pyridin-4-ylboronic acid was used as the reactant.; HRMS [M]+: 619.54
[준비예 30][Preparation Example 30]
4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine의 합성 4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine synthesis
Figure PCTKR2020004924-appb-I000055
Figure PCTKR2020004924-appb-I000055
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 12]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 619.5445g of the target compound was obtained by performing the same procedure as in [Preparation Example 12], except that pyridin-4-ylboronic acid was used as the reactant.; HRMS [M]+: 619.54
[준비예 31][Preparation Example 31]
4-(3-bromo-5-(pyridin-4-yl)phenyl)-2,6-bis(4-(pyridin-4-yl)phenyl)pyrimidine의 합성 Synthesis of 4-(3-bromo-5-(pyridin-4-yl)phenyl)-2,6-bis(4-(pyridin-4-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000056
Figure PCTKR2020004924-appb-I000056
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 13]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 619.5445g of the target compound was obtained by performing the same procedure as in [Preparation Example 13], except that pyridin-4-ylboronic acid was used as the reactant.; HRMS [M]+: 619.54
[준비예 32][Preparation Example 32]
4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine의 합성 Synthesis of 4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000057
Figure PCTKR2020004924-appb-I000057
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 14]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 592.5145g of the target compound was obtained by performing the same procedure as in [Preparation Example 14], except that pyridin-4-ylboronic acid was used as the reactant.; HRMS [M]+: 592.51
[준비예 33][Preparation Example 33]
4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine의 합성 Synthesis of 4-(3-bromo-5-(pyridin-4-yl)phenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine
Figure PCTKR2020004924-appb-I000058
Figure PCTKR2020004924-appb-I000058
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 15]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 592.5145g of the target compound was obtained by performing the same procedure as in [Preparation Example 15], except that pyridin-4-ylboronic acid was used as the reactant.; HRMS [M]+: 592.51
[준비예 34][Preparation Example 34]
6-(4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-4-yl)phenyl)pyrimidin-2-yl)quinoline의 합성 Synthesis of 6-(4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-4-yl)phenyl)pyrimidin-2-yl)quinoline
Figure PCTKR2020004924-appb-I000059
Figure PCTKR2020004924-appb-I000059
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 16]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 592.5145g of the target compound was obtained by performing the same procedure as in [Preparation Example 16], except that pyridin-4-ylboronic acid was used as the reactant.; HRMS [M]+: 592.51
[준비예 35][Preparation Example 35]
6-(4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-2-yl)quinoline의 합성 Synthesis of 6-(4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-2-yl)quinoline
Figure PCTKR2020004924-appb-I000060
Figure PCTKR2020004924-appb-I000060
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 17]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 593.5045g of the target compound was obtained by performing the same procedure as in [Preparation Example 17], except that pyridin-4-ylboronic acid was used as the reactant.; HRMS [M]+: 593.50
[준비예 36][Preparation Example 36]
6-(4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-2-yl)quinoline의 합성 Synthesis of 6-(4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-2-yl)quinoline
Figure PCTKR2020004924-appb-I000061
Figure PCTKR2020004924-appb-I000061
반응물로 pyridin-4-ylboronic acid을 사용한 것을 제외하고는 [준비예 18]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 593.5045g of the target compound was obtained by performing the same procedure as in [Preparation Example 18], except that pyridin-4-ylboronic acid was used as the reactant.; HRMS [M]+: 593.50
[준비예 37][Preparation Example 37]
5-(3-(6-([1,1'-biphenyl]-4-yl)-2-(pyridin-3-yl)pyrimidin-4-yl)-5-bromophenyl)quinoline의 합성Synthesis of 5-(3-(6-([1,1'-biphenyl]-4-yl)-2-(pyridin-3-yl)pyrimidin-4-yl)-5-bromophenyl)quinoline
Figure PCTKR2020004924-appb-I000062
Figure PCTKR2020004924-appb-I000062
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 26g을 얻었다.; HRMS [M]+: 591.1126g of the target compound was obtained by performing the same procedure as in [Preparation Example 1], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 591.11
[준비예 38][Preparation Example 38]
5-(3-(6-([1,1'-biphenyl]-4-yl)-2-(pyridin-4-yl)pyrimidin-4-yl)-5-bromophenyl)quinoline의 합성Synthesis of 5-(3-(6-([1,1'-biphenyl]-4-yl)-2-(pyridin-4-yl)pyrimidin-4-yl)-5-bromophenyl)quinoline
Figure PCTKR2020004924-appb-I000063
Figure PCTKR2020004924-appb-I000063
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 2]과 동일한 과정을 수행하여 목적 화합물 26g을 얻었다.; HRMS [M]+: 591.1126g of the title compound was obtained by performing the same procedure as in [Preparation Example 2], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 591.11
[준비예 39][Preparation Example 39]
5-(3-bromo-5-(2-phenyl-6-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline의 합성Synthesis of 5-(3-bromo-5-(2-phenyl-6-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000064
Figure PCTKR2020004924-appb-I000064
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 3]과 동일한 과정을 수행하여 목적 화합물 30g을 얻었다.; HRMS [M]+: 591.1130g of the target compound was obtained by performing the same procedure as in [Preparation Example 3], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 591.11
[준비예 40][Preparation Example 40]
5-(3-bromo-5-(2-phenyl-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline의 합성Synthesis of 5-(3-bromo-5-(2-phenyl-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000065
Figure PCTKR2020004924-appb-I000065
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 4]과 동일한 과정을 수행하여 목적 화합물 25g을 얻었다.; HRMS [M]+: 591.11Except that quinolin-5-ylboronic acid was used as a reactant, 25g of the target compound was obtained by performing the same procedure as in [Preparation Example 4].; HRMS [M]+: 591.11
[준비예 41][Preparation Example 41]
5-(3-bromo-5-(2-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline의 합성Synthesis of 5-(3-bromo-5-(2-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000066
Figure PCTKR2020004924-appb-I000066
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 5]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 592.11The target compound 32g was obtained by performing the same procedure as in [Preparation Example 5], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 592.11
[준비예 42][Preparation Example 42]
5-(3-bromo-5-(2-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline의 합성Synthesis of 5-(3-bromo-5-(2-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000067
Figure PCTKR2020004924-appb-I000067
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 6]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 592.11The target compound 32g was obtained by performing the same procedure as in [Preparation Example 6], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 592.11
[준비예 43][Preparation Example 43]
5-(3-bromo-5-(6-(4-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidin-4-yl)phenyl)quinoline의 합성 Synthesis of 5-(3-bromo-5-(6-(4-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidin-4-yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000068
Figure PCTKR2020004924-appb-I000068
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 7]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 592.1139g of the title compound was obtained by performing the same procedure as in [Preparation Example 7], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 592.11
[준비예 44][Preparation Example 44]
5-(3-bromo-5-(2-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline의 합성 Synthesis of 5-(3-bromo-5-(2-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000069
Figure PCTKR2020004924-appb-I000069
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 8]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 592.1139g of the target compound was obtained by performing the same procedure as in [Preparation Example 8], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 592.11
[준비예 45][Preparation Example 45]
5-(3-(6-([1,1'-biphenyl]-4-yl)-2-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)quinoline의 합성 5-(3-(6-([1,1'-biphenyl]-4-yl)-2-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)quinoline synthesis
Figure PCTKR2020004924-appb-I000070
Figure PCTKR2020004924-appb-I000070
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 9]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 667.1439g of the target compound was obtained by performing the same procedure as in [Preparation Example 9], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 667.14
[준비예 46][Preparation Example 46]
5-(3-(6-([1,1'-biphenyl]-4-yl)-2-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)quinoline의 합성 5-(3-(6-([1,1'-biphenyl]-4-yl)-2-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)quinoline synthesis
Figure PCTKR2020004924-appb-I000071
Figure PCTKR2020004924-appb-I000071
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 10]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 667.1445g of the target compound was obtained by performing the same procedure as in [Preparation Example 10], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 667.14
[준비예 47][Preparation Example 47]
5-(3-(2,6-bis(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)quinoline의 합성 Synthesis of 5-(3-(2,6-bis(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)quinoline
Figure PCTKR2020004924-appb-I000072
Figure PCTKR2020004924-appb-I000072
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 11]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 668.1445g of the target compound was obtained by performing the same procedure as in [Preparation Example 11], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 668.14
[준비예 48][Preparation Example 48]
5-(3-bromo-5-(2-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline의 합성 Synthesis of 5-(3-bromo-5-(2-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000073
Figure PCTKR2020004924-appb-I000073
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 12]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 668.1445g of the target compound was obtained by performing the same procedure as in [Preparation Example 12], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 668.14
[준비예 49][Preparation Example 49]
5-(3-(2,6-bis(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)quinoline의 합성 Synthesis of 5-(3-(2,6-bis(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)quinoline
Figure PCTKR2020004924-appb-I000074
Figure PCTKR2020004924-appb-I000074
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 13]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 668.1445g of the target compound was obtained by performing the same procedure as in [Preparation Example 13], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 668.14
[준비예 50][Preparation Example 50]
5-(3-bromo-5-(2-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline의 합성 Synthesis of 5-(3-bromo-5-(2-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000075
Figure PCTKR2020004924-appb-I000075
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 14]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 641.1345g of the target compound was obtained by performing the same procedure as in [Preparation Example 14], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 641.13
[준비예 51][Preparation Example 51]
5-(3-bromo-5-(2-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline의 합성 Synthesis of 5-(3-bromo-5-(2-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000076
Figure PCTKR2020004924-appb-I000076
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 15]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 641.1345g of the target compound was obtained by performing the same procedure as in [Preparation Example 15], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 641.13
[준비예 52][Preparation Example 52]
5-(3-(6-([1,1'-biphenyl]-4-yl)-2-(quinolin-6-yl)pyrimidin-4-yl)-5-bromophenyl)quinoline의 합성 Synthesis of 5-(3-(6-([1,1'-biphenyl]-4-yl)-2-(quinolin-6-yl)pyrimidin-4-yl)-5-bromophenyl)quinoline
Figure PCTKR2020004924-appb-I000077
Figure PCTKR2020004924-appb-I000077
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 16]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 641.1345g of the title compound was obtained by performing the same procedure as in [Preparation Example 16], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 641.13
[준비예 53][Preparation Example 53]
5-(3-bromo-5-(6-(4-(pyridin-3-yl)phenyl)-2-(quinolin-6-yl)pyrimidin-4-yl)phenyl)quinoline의 합성 Synthesis of 5-(3-bromo-5-(6-(4-(pyridin-3-yl)phenyl)-2-(quinolin-6-yl)pyrimidin-4-yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000078
Figure PCTKR2020004924-appb-I000078
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 17]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 642.1245g of the title compound was obtained by performing the same procedure as in [Preparation Example 17], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 642.12
[준비예 54][Preparation Example 54]
5-(3-bromo-5-(6-(4-(pyridin-4-yl)phenyl)-2-(quinolin-6-yl)pyrimidin-4-yl)phenyl)quinoline의 합성 Synthesis of 5-(3-bromo-5-(6-(4-(pyridin-4-yl)phenyl)-2-(quinolin-6-yl)pyrimidin-4-yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000079
Figure PCTKR2020004924-appb-I000079
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 18]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 642.1245g of the target compound was obtained by performing the same procedure as in [Preparation Example 18], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 642.12
[준비예 55][Preparation Example 55]
9-(3-(6-([1,1'-biphenyl]-4-yl)-2-(pyridin-3-yl)pyrimidin-4-yl)-5-bromophenyl)-9H-carbazole의 합성Synthesis of 9-(3-(6-([1,1'-biphenyl]-4-yl)-2-(pyridin-3-yl)pyrimidin-4-yl)-5-bromophenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000080
Figure PCTKR2020004924-appb-I000080
4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(pyridin-3-yl)pyrimidine5g(9.25mmol)과 Carbazole 5.5g(10.17mmol)에 xylene 250 mL를 가하였다. Pd2(dba)3 0.42g (0.46mmol), Xphos 0.44g(0.92mmol), NaOtBu 2.2g(23.1mol)을 첨가 후 120℃에서 24시간 가열환류하였다. 상온으로 온도를 냉각하고 반응액에 염화암모늄 수용액 500 mL로 반응을 종결시켰다. 혼합액을 M.C 500 mL로 추출한 후, 증류수로 세척하였다. 얻어진 유기층을 무수 MgSO4로 건조하고, 감압증류하고 실리카겔 컬럼크로마토그래피로 정제하여 목적 화합물 4.46g(수율 77%)을 얻었다. 1H-NMR: 9.24(s, 1H), 8.73(s, 1H), 8.70(d, 1H), 8.55(d, 1H), 8.42(d, 1H), 8.30(dd, 2H), 8.15(s, 1H), 7.94~7.75(m, 5H), 7.49~7.35(m, 9H), 7.20~7.16(dd, 2H); HRMS [M]+: 629.134-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(pyridin-3-yl)pyrimidine5g(9.25mmol) and Carbazole 5.5g(10.17mmol) 250 mL of xylene was added. Pd 2 (dba) 3 0.42g (0.46mmol), Xphos 0.44g (0.92mmol), and NaOtBu 2.2g (23.1mol) were added and heated to reflux at 120° C. for 24 hours. The temperature was cooled to room temperature, and the reaction was terminated with 500 mL of an aqueous ammonium chloride solution in the reaction solution. The mixed solution was extracted with 500 mL of MC and washed with distilled water. The obtained organic layer was dried over anhydrous MgSO 4 , distilled under reduced pressure, and purified by silica gel column chromatography to obtain 4.46 g (yield 77%) of the title compound. 1H-NMR: 9.24 (s, 1H), 8.73 (s, 1H), 8.70 (d, 1H), 8.55 (d, 1H), 8.42 (d, 1H), 8.30 (dd, 2H), 8.15 (s, 1H), 7.94 to 7.75 (m, 5H), 7.49 to 7.35 (m, 9H), 7.20 to 7.16 (dd, 2H); HRMS [M] + : 629.13
[준비예 56][Preparation Example 56]
5-(3-(6-([1,1'-biphenyl]-4-yl)-2-(pyridin-4-yl)pyrimidin-4-yl)-5-bromophenyl)quinoline의 합성Synthesis of 5-(3-(6-([1,1'-biphenyl]-4-yl)-2-(pyridin-4-yl)pyrimidin-4-yl)-5-bromophenyl)quinoline
Figure PCTKR2020004924-appb-I000081
Figure PCTKR2020004924-appb-I000081
반응물로 4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(pyridin-4-yl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 26g을 얻었다.; HRMS [M]+: 629.13[Preparation Example 55] except that 4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(pyridin-4-yl)pyrimidine was used as the reactant 26g of the title compound was obtained by performing the same procedure as described above.; HRMS [M]+: 629.13
[준비예 57][Preparation Example 57]
9-(3-bromo-5-(2-phenyl-6-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole의 합성Synthesis of 9-(3-bromo-5-(2-phenyl-6-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000082
Figure PCTKR2020004924-appb-I000082
반응물로 4-(3,5-dibromophenyl)-2-phenyl-6-(4-(pyridin-3-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 30g을 얻었다.; HRMS [M]+: 629.13Except for using 4-(3,5-dibromophenyl)-2-phenyl-6-(4-(pyridin-3-yl)phenyl)pyrimidine as the reactant, the target compound was carried out in the same manner as in [Preparation Example 55] 30g was obtained.; HRMS [M]+: 629.13
[준비예 58][Preparation Example 58]
9-(3-bromo-5-(2-phenyl-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole의 합성Synthesis of 9-(3-bromo-5-(2-phenyl-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000083
Figure PCTKR2020004924-appb-I000083
반응물로 4-(3,5-dibromophenyl)-2-phenyl-6-(4-(pyridin-4-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 25g을 얻었다.; HRMS [M]+: 629.13Except for using 4-(3,5-dibromophenyl)-2-phenyl-6-(4-(pyridin-4-yl)phenyl)pyrimidine as a reactant, the target compound was carried out in the same manner as in [Preparation Example 55] 25g was obtained.; HRMS [M]+: 629.13
[준비예 59][Preparation Example 59]
9-(3-bromo-5-(2-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole의 합성Synthesis of 9-(3-bromo-5-(2-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000084
Figure PCTKR2020004924-appb-I000084
반응물로 4-(3,5-dibromophenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 630.12The same as in [Preparation Example 55], except that 4-(3,5-dibromophenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine was used as a reactant. The procedure was carried out to obtain 32 g of the title compound.; HRMS [M]+: 630.12
[준비예 60][Preparation Example 60]
9-(3-bromo-5-(2-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole의 합성Synthesis of 9-(3-bromo-5-(2-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000085
Figure PCTKR2020004924-appb-I000085
반응물로 4-(3,5-dibromophenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 630.12The same as in [Preparation Example 55], except that 4-(3,5-dibromophenyl)-2-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine was used as a reactant. The procedure was carried out to obtain 32 g of the title compound.; HRMS [M]+: 630.12
[준비예 61][Preparation Example 61]
9-(3-bromo-5-(6-(4-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidin-4-yl)phenyl)-9H-carbazole의 합성 Synthesis of 9-(3-bromo-5-(6-(4-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidin-4-yl)phenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000086
Figure PCTKR2020004924-appb-I000086
반응물로 4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 630.12The same as in [Preparation Example 55], except that 4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-2-(pyridin-4-yl)pyrimidine was used as a reactant. 39g of the title compound was obtained by performing the procedure.; HRMS [M]+: 630.12
[준비예 62][Preparation Example 62]
9-(3-bromo-5-(2-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole의 합성 Synthesis of 9-(3-bromo-5-(2-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000087
Figure PCTKR2020004924-appb-I000087
반응물로 4-(3,5-dibromophenyl)-2-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 630.12The same as in [Preparation Example 55], except that 4-(3,5-dibromophenyl)-2-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine was used as a reactant. 39g of the title compound was obtained by performing the procedure.; HRMS [M]+: 630.12
[준비예 63][Preparation Example 63]
9-(3-(6-([1,1'-biphenyl]-4-yl)-2-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)-9H-carbazole의 합성 9-(3-(6-([1,1'-biphenyl]-4-yl)-2-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)-9H Synthesis of -carbazole
Figure PCTKR2020004924-appb-I000088
Figure PCTKR2020004924-appb-I000088
반응물로 4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(4-(pyridin-3-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 705.16Except for using 4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(4-(pyridin-3-yl)phenyl)pyrimidine as a reactant 39g of the title compound was obtained by performing the same procedure as in [Preparation Example 55].; HRMS [M]+: 705.16
[준비예 64][Preparation Example 64]
9-(3-(6-([1,1'-biphenyl]-4-yl)-2-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)-9H-carbazole의 합성 9-(3-(6-([1,1'-biphenyl]-4-yl)-2-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)-9H Synthesis of -carbazole
Figure PCTKR2020004924-appb-I000089
Figure PCTKR2020004924-appb-I000089
반응물로 4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(4-(pyridin-4-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 705.16Except for using 4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-2-(4-(pyridin-4-yl)phenyl)pyrimidine as a reactant 45g of the title compound was obtained by performing the same procedure as in [Preparation Example 55].; HRMS [M]+: 705.16
[준비예 65][Preparation Example 65]
9-(3-(2,6-bis(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)-9H-carbazole의 합성 Synthesis of 9-(3-(2,6-bis(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000090
Figure PCTKR2020004924-appb-I000090
반응물로 4-(3,5-dibromophenyl)-2,6-bis(4-(pyridin-3-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 707,15The target compound 45g by performing the same procedure as in [Preparation Example 55], except that 4-(3,5-dibromophenyl)-2,6-bis(4-(pyridin-3-yl)phenyl)pyrimidine was used as the reactant Got HRMS [M]+: 707,15
[준비예 66][Preparation Example 66]
9-(3-bromo-5-(2-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole의 합성 9-(3-bromo-5-(2-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)-9H- synthesis of carbazole
Figure PCTKR2020004924-appb-I000091
Figure PCTKR2020004924-appb-I000091
반응물로 4-(3,5-dibromophenyl)-2-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 707,15[Preparation] except for using 4-(3,5-dibromophenyl)-2-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine as the reactant Example 55] was carried out in the same manner to obtain 45g of the title compound.; HRMS [M]+: 707,15
[준비예 67][Preparation Example 67]
9-(3-(2,6-bis(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)-9H-carbazole의 합성 Synthesis of 9-(3-(2,6-bis(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)-5-bromophenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000092
Figure PCTKR2020004924-appb-I000092
반응물로 4-(3,5-dibromophenyl)-2,6-bis(4-(pyridin-4-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 707,15The target compound 45g by performing the same procedure as in [Preparation Example 55], except that 4-(3,5-dibromophenyl)-2,6-bis(4-(pyridin-4-yl)phenyl)pyrimidine was used as the reactant Got HRMS [M]+: 707,15
[준비예 68][Preparation Example 68]
9-(3-bromo-5-(2-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole의 합성 Synthesis of 9-(3-bromo-5-(2-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000093
Figure PCTKR2020004924-appb-I000093
반응물로 4-(3,5-dibromophenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 679.14Same as [Preparation Example 55], except that 4-(3,5-dibromophenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)pyrimidine was used as the reactant The procedure was carried out to obtain 45 g of the title compound.; HRMS [M]+: 679.14
[준비예 69][Preparation Example 69]
9-(3-bromo-5-(2-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole의 합성 Synthesis of 9-(3-bromo-5-(2-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-4-yl)phenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000094
Figure PCTKR2020004924-appb-I000094
반응물로 4-(3,5-dibromophenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 679.14Same as [Preparation Example 55], except that 4-(3,5-dibromophenyl)-2-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)pyrimidine was used as the reactant. The procedure was carried out to obtain 45 g of the title compound.; HRMS [M]+: 679.14
[준비예 70][Preparation Example 70]
9-(3-(6-([1,1'-biphenyl]-4-yl)-2-(quinolin-6-yl)pyrimidin-4-yl)-5-bromophenyl)-9H-carbazole의 합성 Synthesis of 9-(3-(6-([1,1'-biphenyl]-4-yl)-2-(quinolin-6-yl)pyrimidin-4-yl)-5-bromophenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000095
Figure PCTKR2020004924-appb-I000095
반응물로 6-(4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)pyrimidin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 679.14[Preparation Example 55] and except for using 6-(4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)pyrimidin-2-yl)quinoline as a reactant 45g of the title compound was obtained by performing the same procedure.; HRMS [M]+: 679.14
[준비예 71][Preparation Example 71]
9-(3-bromo-5-(6-(4-(pyridin-3-yl)phenyl)-2-(quinolin-6-yl)pyrimidin-4-yl)phenyl)-9H-carbazole의 합성 Synthesis of 9-(3-bromo-5-(6-(4-(pyridin-3-yl)phenyl)-2-(quinolin-6-yl)pyrimidin-4-yl)phenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000096
Figure PCTKR2020004924-appb-I000096
반응물로 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 681.61The same procedure as in [Preparation Example 55], except that 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)pyrimidin-2-yl)quinoline was used as the reactant To obtain 45 g of the title compound.; HRMS [M]+: 681.61
[준비예 72][Preparation Example 72]
9-(3-bromo-5-(6-(4-(pyridin-4-yl)phenyl)-2-(quinolin-6-yl)pyrimidin-4-yl)phenyl)-9H-carbazole의 합성 Synthesis of 9-(3-bromo-5-(6-(4-(pyridin-4-yl)phenyl)-2-(quinolin-6-yl)pyrimidin-4-yl)phenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000097
Figure PCTKR2020004924-appb-I000097
반응물로 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 680.14The same process as in [Preparation Example 55], except that 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)pyrimidin-2-yl)quinoline was used as the reactant To obtain 45 g of the title compound.; HRMS [M]+: 680.14
[준비예 73][Preparation Example 73]
2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(pyridin-3-yl)-1,3,5-triazine의 합성2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(pyridin-3-yl)-1,3, Synthesis of 5-triazine
Figure PCTKR2020004924-appb-I000098
Figure PCTKR2020004924-appb-I000098
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-3-yl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 1]과 동일한 과정을 수행하여 목적 화합물 26g을 얻었다.; HRMS [M]+: 542.09Except for using 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-3-yl)-1,3,5-triazine as a reactant Then, 26g of the target compound was obtained by performing the same procedure as in [Preparation Example 1].; HRMS [M]+: 542.09
[준비예 74][Preparation Example 74]
2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazine의 합성2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3, Synthesis of 5-triazine
Figure PCTKR2020004924-appb-I000099
Figure PCTKR2020004924-appb-I000099
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-4-yl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 2]과 동일한 과정을 수행하여 목적 화합물 26g을 얻었다.; HRMS [M]+: 542.09Except for using 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-4-yl)-1,3,5-triazine as a reactant Then, 26g of the target compound was obtained by performing the same procedure as in [Preparation Example 2].; HRMS [M]+: 542.09
[준비예 75][Preparation Example 75]
2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine의 합성Synthesis of 2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine
Figure PCTKR2020004924-appb-I000100
Figure PCTKR2020004924-appb-I000100
반응물로 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 3]과 동일한 과정을 수행하여 목적 화합물 30g을 얻었다.; HRMS [M]+: 542.09[Preparation Example 3] and except for using 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine as a reactant The same procedure was carried out to obtain 30 g of the title compound.; HRMS [M]+: 542.09
[준비예 76][Preparation Example 76]
2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성Synthesis of 2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine
Figure PCTKR2020004924-appb-I000101
Figure PCTKR2020004924-appb-I000101
반응물로 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 4]과 동일한 과정을 수행하여 목적 화합물 25g을 얻었다.; HRMS [M]+: 542.09[Preparation Example 4] and except for using 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant The same procedure was carried out to obtain 25 g of the title compound.; HRMS [M]+: 542.09
[준비예 77][Preparation Example 77]
2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine의 합성2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5- synthesis of triazine
Figure PCTKR2020004924-appb-I000102
Figure PCTKR2020004924-appb-I000102
반응물로 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 5]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 543.09Except for using 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine as a reactant 32g of the target compound was obtained by performing the same procedure as in [Preparation Example 5].; HRMS [M]+: 543.09
[준비예 78][Preparation Example 78]
2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5- synthesis of triazine
Figure PCTKR2020004924-appb-I000103
Figure PCTKR2020004924-appb-I000103
반응물로 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 6]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 543.09Except for using 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 32g of the target compound was obtained by performing the same procedure as in [Preparation Example 6].; HRMS [M]+: 543.09
[준비예 79][Preparation Example 79]
2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazine의 합성 2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5- synthesis of triazine
Figure PCTKR2020004924-appb-I000104
Figure PCTKR2020004924-appb-I000104
반응물로 2-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 7]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 543.09Except for using 2-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazine as a reactant 39g of the title compound was obtained by performing the same procedure as in [Preparation Example 7].; HRMS [M]+: 543.09
[준비예 80][Preparation Example 80]
2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성 2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5- synthesis of triazine
Figure PCTKR2020004924-appb-I000105
Figure PCTKR2020004924-appb-I000105
반응물로 2-(3,5-dibromophenyl)-4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 8]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 543.09Except for using 2-(3,5-dibromophenyl)-4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 39g of the target compound was obtained by performing the same procedure as in [Preparation Example 8].; HRMS [M]+: 543.09
[준비예 81][Preparation Example 81]
2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine의 합성 2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl) Synthesis of -1,3,5-triazine
Figure PCTKR2020004924-appb-I000106
Figure PCTKR2020004924-appb-I000106
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 9]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 618.122-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5- 39g of the target compound was obtained by performing the same procedure as in [Preparation Example 9] except that triazine was used.; HRMS [M]+: 618.12
[준비예 82][Preparation Example 82]
2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성 2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl) Synthesis of -1,3,5-triazine
Figure PCTKR2020004924-appb-I000107
Figure PCTKR2020004924-appb-I000107
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 10]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 618.122-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5- 45g of the target compound was obtained by performing the same procedure as in [Preparation Example 10] except that triazine was used.; HRMS [M]+: 618.12
[준비예 83][Preparation Example 83]
2-(3-bromo-5-(pyridin-3-yl)phenyl)-4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazine의 합성 Synthesis of 2-(3-bromo-5-(pyridin-3-yl)phenyl)-4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazine
Figure PCTKR2020004924-appb-I000108
Figure PCTKR2020004924-appb-I000108
반응물로 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 11]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 619.12Same as [Preparation Example 11], except that 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazine was used as a reactant The procedure was carried out to obtain 45 g of the title compound.; HRMS [M]+: 619.12
[준비예 84][Preparation Example 84]
2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성 2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1 Synthesis of ,3,5-triazine
Figure PCTKR2020004924-appb-I000109
Figure PCTKR2020004924-appb-I000109
반응물로 2-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 12]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 619.122-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 45g of the title compound was obtained by performing the same procedure as in [Preparation Example 12], except that it was used.; HRMS [M]+: 619.12
[준비예 85][Preparation Example 85]
2-(3-bromo-5-(pyridin-3-yl)phenyl)-4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성 Synthesis of 2-(3-bromo-5-(pyridin-3-yl)phenyl)-4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazine
Figure PCTKR2020004924-appb-I000110
Figure PCTKR2020004924-appb-I000110
반응물로 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 13]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 619.12Same as [Preparation Example 13], except that 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazine was used as the reactant The procedure was carried out to obtain 45 g of the title compound.; HRMS [M]+: 619.12
[준비예 86][Preparation Example 86]
2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine의 합성 2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5- synthesis of triazine
Figure PCTKR2020004924-appb-I000111
Figure PCTKR2020004924-appb-I000111
반응물로 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 14]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 592.11Except for using 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine as a reactant 45g of the title compound was obtained by performing the same procedure as in [Preparation Example 14].; HRMS [M]+: 592.11
[준비예 87][Preparation Example 87]
2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성 2-(3-bromo-5-(pyridin-3-yl)phenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5- synthesis of triazine
Figure PCTKR2020004924-appb-I000112
Figure PCTKR2020004924-appb-I000112
반응물로 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 15]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 592.11Except for using 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 45g of the title compound was obtained by performing the same procedure as in [Preparation Example 15].; HRMS [M]+: 592.11
[준비예 88][Preparation Example 88]
6-(4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)quinoline의 합성 6-(4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl ) Synthesis of quinoline
Figure PCTKR2020004924-appb-I000113
Figure PCTKR2020004924-appb-I000113
반응물로 6-(4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-1,3,5-triazin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 16]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 592.11Except for using 6-(4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-1,3,5-triazin-2-yl)quinoline as a reactant Was carried out in the same manner as in [Preparation Example 16] to obtain 45g of the title compound.; HRMS [M]+: 592.11
[준비예 89][Preparation Example 89]
6-(4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)quinoline의 합성 6-(4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)quinoline Synthesis of
Figure PCTKR2020004924-appb-I000114
Figure PCTKR2020004924-appb-I000114
반응물로 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 17]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 593.10Except for using 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)quinoline as a reactant, [ Preparation Example 17] was carried out in the same manner to obtain 45g of the title compound.; HRMS [M]+: 593.10
[준비예 90][Preparation Example 90]
6-(4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)quinoline의 합성 6-(4-(3-bromo-5-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)quinoline Synthesis of
Figure PCTKR2020004924-appb-I000115
Figure PCTKR2020004924-appb-I000115
반응물로 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 18]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 593.10Except for using 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)quinoline as a reactant, [ Preparation Example 18] was carried out in the same manner to obtain 45g of the title compound.; HRMS [M]+: 593.10
[준비예 91][Preparation Example 91]
2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(pyridin-3-yl)-1,3,5-triazine의 합성2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(pyridin-3-yl)-1,3, Synthesis of 5-triazine
Figure PCTKR2020004924-appb-I000116
Figure PCTKR2020004924-appb-I000116
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-3-yl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 19]과 동일한 과정을 수행하여 목적 화합물 26g을 얻었다.; HRMS [M]+: 542.09Except for using 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-3-yl)-1,3,5-triazine as a reactant Then, 26g of the target compound was obtained by performing the same procedure as in [Preparation Example 19].; HRMS [M]+: 542.09
[준비예 92][Preparation Example 92]
2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazine의 합성2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(pyridin-4-yl)-1,3, Synthesis of 5-triazine
Figure PCTKR2020004924-appb-I000117
Figure PCTKR2020004924-appb-I000117
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-4-yl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 20]과 동일한 과정을 수행하여 목적 화합물 26g을 얻었다.; HRMS [M]+: 542.09Except for using 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-4-yl)-1,3,5-triazine as a reactant Then, 26g of the target compound was obtained by performing the same procedure as in [Preparation Example 20].; HRMS [M]+: 542.09
[준비예 93][Preparation Example 93]
2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine의 합성Synthesis of 2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine
Figure PCTKR2020004924-appb-I000118
Figure PCTKR2020004924-appb-I000118
반응물로 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 21]과 동일한 과정을 수행하여 목적 화합물 30g을 얻었다.; HRMS [M]+: 542.09Except for using 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine as a reactant, and [Preparation Example 21] The same procedure was carried out to obtain 30 g of the title compound.; HRMS [M]+: 542.09
[준비예 94][Preparation Example 94]
2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성Synthesis of 2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine
Figure PCTKR2020004924-appb-I000119
Figure PCTKR2020004924-appb-I000119
반응물로 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 22]과 동일한 과정을 수행하여 목적 화합물 25g을 얻었다.; HRMS [M]+: 542.09Except for using 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant, and [Preparation Example 22] The same procedure was carried out to obtain 25 g of the title compound.; HRMS [M]+: 542.09
[준비예 95][Preparation Example 95]
2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine의 합성2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5- synthesis of triazine
Figure PCTKR2020004924-appb-I000120
Figure PCTKR2020004924-appb-I000120
반응물로 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 23]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 543.09Except for using 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine as a reactant 32g of the target compound was obtained by performing the same procedure as in [Preparation Example 23].; HRMS [M]+: 543.09
[준비예 96][Preparation Example 96]
2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5- synthesis of triazine
Figure PCTKR2020004924-appb-I000121
Figure PCTKR2020004924-appb-I000121
반응물로 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 24]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 543.09Except for using 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 32g of the target compound was obtained by performing the same procedure as in [Preparation Example 24].; HRMS [M]+: 543.09
[준비예 97][Preparation Example 97]
2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazine의 합성 2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5- synthesis of triazine
Figure PCTKR2020004924-appb-I000122
Figure PCTKR2020004924-appb-I000122
반응물로 2-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 25]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 543.09Except for using 2-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazine as a reactant 39g of the title compound was obtained by performing the same procedure as in [Preparation Example 25].; HRMS [M]+: 543.09
[준비예 98][Preparation Example 98]
2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성 2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5- synthesis of triazine
Figure PCTKR2020004924-appb-I000123
Figure PCTKR2020004924-appb-I000123
반응물로 2-(3,5-dibromophenyl)-4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 26]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 543.09Except for using 2-(3,5-dibromophenyl)-4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 39g of the title compound was obtained by performing the same procedure as in [Preparation Example 26].; HRMS [M]+: 543.09
[준비예 99][Preparation Example 99]
2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine의 합성 2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl) Synthesis of -1,3,5-triazine
Figure PCTKR2020004924-appb-I000124
Figure PCTKR2020004924-appb-I000124
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 27]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 618.122-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5- 39g of the target compound was obtained by performing the same procedure as in [Preparation Example 27] except that triazine was used.; HRMS [M]+: 618.12
[준비예 100][Preparation Example 100]
2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성 2-([1,1'-biphenyl]-4-yl)-4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl) Synthesis of -1,3,5-triazine
Figure PCTKR2020004924-appb-I000125
Figure PCTKR2020004924-appb-I000125
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 28]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 618.122-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5- 45g of the target compound was obtained by performing the same procedure as in [Preparation Example 28] except that triazine was used.; HRMS [M]+: 618.12
[준비예 101][Preparation Example 101]
2-(3-bromo-5-(pyridin-4-yl)phenyl)-4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazine의 합성 Synthesis of 2-(3-bromo-5-(pyridin-4-yl)phenyl)-4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazine
Figure PCTKR2020004924-appb-I000126
Figure PCTKR2020004924-appb-I000126
반응물로 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 29]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 619.12The same as in [Preparation Example 29] except that 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazine was used as a reactant. The procedure was carried out to obtain 45 g of the title compound.; HRMS [M]+: 619.12
[준비예 102][Preparation Example 102]
2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성 2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1 Synthesis of ,3,5-triazine
Figure PCTKR2020004924-appb-I000127
Figure PCTKR2020004924-appb-I000127
반응물로 2-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 30]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 619.122-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 45g of the title compound was obtained by performing the same procedure as in [Preparation Example 30], except that it was used.; HRMS [M]+: 619.12
[준비예 103][Preparation Example 103]
2-(3-bromo-5-(pyridin-4-yl)phenyl)-4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성 Synthesis of 2-(3-bromo-5-(pyridin-4-yl)phenyl)-4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazine
Figure PCTKR2020004924-appb-I000128
Figure PCTKR2020004924-appb-I000128
반응물로 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 31]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 619.12Same as [Preparation Example 31], except that 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazine was used as a reactant The procedure was carried out to obtain 45 g of the title compound.; HRMS [M]+: 619.12
[준비예 104][Preparation Example 104]
2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine의 합성 2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5- synthesis of triazine
Figure PCTKR2020004924-appb-I000129
Figure PCTKR2020004924-appb-I000129
반응물로 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 32]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 592.11Except for using 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine as a reactant 45g of the title compound was obtained by performing the same procedure as in [Preparation Example 32].; HRMS [M]+: 592.11
[준비예 105][Preparation Example 105]
2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine의 합성 2-(3-bromo-5-(pyridin-4-yl)phenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5- synthesis of triazine
Figure PCTKR2020004924-appb-I000130
Figure PCTKR2020004924-appb-I000130
반응물로 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 33]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 592.11Except for using 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 45g of the title compound was obtained by performing the same procedure as in [Preparation Example 33].; HRMS [M]+: 592.11
[준비예 106][Preparation Example 106]
6-(4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)quinoline의 합성 6-(4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl ) Synthesis of quinoline
Figure PCTKR2020004924-appb-I000131
Figure PCTKR2020004924-appb-I000131
반응물로 6-(4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-1,3,5-triazin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 34]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 592.11Except for using 6-(4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-1,3,5-triazin-2-yl)quinoline as a reactant Was carried out in the same manner as in [Preparation Example 34] to obtain 45g of the title compound.; HRMS [M]+: 592.11
[준비예 107][Preparation Example 107]
6-(4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)quinoline의 합성 6-(4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)quinoline Synthesis of
Figure PCTKR2020004924-appb-I000132
Figure PCTKR2020004924-appb-I000132
반응물로 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 35]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 593.10Except for using 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)quinoline as a reactant, [ Preparation Example 35] was carried out in the same manner to obtain 45g of the title compound.; HRMS [M]+: 593.10
[준비예 108][Preparation Example 108]
6-(4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)quinoline의 합성 6-(4-(3-bromo-5-(pyridin-4-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)quinoline Synthesis of
Figure PCTKR2020004924-appb-I000133
Figure PCTKR2020004924-appb-I000133
반응물로 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 36]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 593.10Except for using 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)quinoline as a reactant, [ Preparation Example 36] was carried out in the same manner to obtain 45g of the title compound.; HRMS [M]+: 593.10
[준비예 109][Preparation Example 109]
5-(3-(4-([1,1'-biphenyl]-4-yl)-6-(pyridin-3-yl)-1,3,5-triazin-2-yl)-5-bromophenyl)quinoline의 합성5-(3-(4-([1,1'-biphenyl]-4-yl)-6-(pyridin-3-yl)-1,3,5-triazin-2-yl)-5-bromophenyl) synthesis of quinoline
Figure PCTKR2020004924-appb-I000134
Figure PCTKR2020004924-appb-I000134
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-3-yl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 37]과 동일한 과정을 수행하여 목적 화합물 26g을 얻었다.; HRMS [M]+: 592.11Except for using 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-3-yl)-1,3,5-triazine as a reactant Then, 26g of the target compound was obtained by performing the same procedure as in [Preparation Example 37].; HRMS [M]+: 592.11
[준비예 110][Preparation Example 110]
5-(3-(4-([1,1'-biphenyl]-4-yl)-6-(pyridin-4-yl)-1,3,5-triazin-2-yl)-5-bromophenyl)quinoline의 합성5-(3-(4-([1,1'-biphenyl]-4-yl)-6-(pyridin-4-yl)-1,3,5-triazin-2-yl)-5-bromophenyl) synthesis of quinoline
Figure PCTKR2020004924-appb-I000135
Figure PCTKR2020004924-appb-I000135
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-4-yl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 38]과 동일한 과정을 수행하여 목적 화합물 26g을 얻었다.; HRMS [M]+: 592.11Except for using 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-4-yl)-1,3,5-triazine as a reactant Then, 26g of the target compound was obtained by performing the same procedure as in [Preparation Example 38].; HRMS [M]+: 592.11
[준비예 111][Preparation Example 111]
5-(3-bromo-5-(4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline의 합성Synthesis of 5-(3-bromo-5-(4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000136
Figure PCTKR2020004924-appb-I000136
반응물로 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 39]과 동일한 과정을 수행하여 목적 화합물 30g을 얻었다.; HRMS [M]+: 592.11Except for using 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine as a reactant, and [Preparation Example 39] 30 g of the target compound was obtained by performing the same procedure.; HRMS [M]+: 592.11
[준비예 112][Preparation Example 112]
5-(3-bromo-5-(4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline의 합성Synthesis of 5-(3-bromo-5-(4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000137
Figure PCTKR2020004924-appb-I000137
반응물로 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 40]과 동일한 과정을 수행하여 목적 화합물 25g을 얻었다.; HRMS [M]+: 592.11Except for using 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant, and [Preparation Example 40] The same procedure was performed to obtain 25 g of the target compound.; HRMS [M]+: 592.11
[준비예 113][Preparation Example 113]
5-(3-bromo-5-(4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline의 합성5-(3-bromo-5-(4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline Synthesis of
Figure PCTKR2020004924-appb-I000138
Figure PCTKR2020004924-appb-I000138
반응물로 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 41]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 593.10Except for using 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine as a reactant 32g of the target compound was obtained by performing the same procedure as in [Preparation Example 41].; HRMS [M]+: 593.10
[준비예 114][Preparation Example 114]
5-(3-bromo-5-(4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline의 합성5-(3-bromo-5-(4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline Synthesis of
Figure PCTKR2020004924-appb-I000139
Figure PCTKR2020004924-appb-I000139
반응물로 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 42]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 593.10Except for using 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 32g of the target compound was obtained by performing the same procedure as in [Preparation Example 42].; HRMS [M]+: 593.10
[준비예 115][Preparation Example 115]
5-(3-bromo-5-(4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazin-2-yl)phenyl)quinoline의 합성 5-(3-bromo-5-(4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazin-2-yl)phenyl)quinoline Synthesis of
Figure PCTKR2020004924-appb-I000140
Figure PCTKR2020004924-appb-I000140
반응물로 2-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 43]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 593.10Except for using 2-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazine as a reactant 39g of the title compound was obtained by performing the same procedure as in [Preparation Example 43].; HRMS [M]+: 593.10
[준비예 116][Preparation Example 116]
5-(3-bromo-5-(4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline의 합성 5-(3-bromo-5-(4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline Synthesis of
Figure PCTKR2020004924-appb-I000141
Figure PCTKR2020004924-appb-I000141
반응물로 2-(3,5-dibromophenyl)-4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 44]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 593.10Except for using 2-(3,5-dibromophenyl)-4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 39g of the title compound was obtained by performing the same procedure as in [Preparation Example 44].; HRMS [M]+: 593.10
[준비예 117][Preparation Example 117]
5-(3-(4-([1,1'-biphenyl]-4-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)-5-bromophenyl)quinoline의 합성 5-(3-(4-([1,1'-biphenyl]-4-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl) Synthesis of -5-bromophenyl)quinoline
Figure PCTKR2020004924-appb-I000142
Figure PCTKR2020004924-appb-I000142
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 45]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 668.142-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5- 39g of the target compound was obtained by performing the same procedure as in [Preparation Example 45] except that triazine was used.; HRMS [M]+: 668.14
[준비예 118][Preparation Example 118]
5-(3-(4-([1,1'-biphenyl]-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)-5-bromophenyl)quinoline의 합성 5-(3-(4-([1,1'-biphenyl]-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl) Synthesis of -5-bromophenyl)quinoline
Figure PCTKR2020004924-appb-I000143
Figure PCTKR2020004924-appb-I000143
반응물로 5-(3-(4-([1,1'-biphenyl]-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)-5-bromophenyl)quinoline을 사용한 것을 제외하고는 [준비예 46]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 668.145-(3-(4-([1,1'-biphenyl]-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2- 45g of the target compound was obtained by performing the same procedure as in [Preparation Example 46], except that yl)-5-bromophenyl)quinoline was used.; HRMS [M]+: 668.14
[준비예 119][Preparation Example 119]
5-(3-(4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)-5-bromophenyl)quinoline의 합성 Synthesis of 5-(3-(4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)-5-bromophenyl)quinoline
Figure PCTKR2020004924-appb-I000144
Figure PCTKR2020004924-appb-I000144
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [준비예 47]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 669.1345g of the title compound was obtained by performing the same procedure as in [Preparation Example 47], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 669.13
[준비예 120][Preparation Example 120]
5-(3-bromo-5-(4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline의 합성 5-(3-bromo-5-(4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2- Synthesis of yl)phenyl)quinoline
Figure PCTKR2020004924-appb-I000145
Figure PCTKR2020004924-appb-I000145
반응물로 2-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 48]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 669.132-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 45g of the target compound was obtained by performing the same procedure as in [Preparation Example 48], except that it was used.; HRMS [M]+: 669.13
[준비예 121][Preparation Example 121]
5-(3-(4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)-5-bromophenyl)quinoline의 합성 Synthesis of 5-(3-(4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)-5-bromophenyl)quinoline
Figure PCTKR2020004924-appb-I000146
Figure PCTKR2020004924-appb-I000146
반응물로 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 49]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 669.13The same as in [Preparation Example 49] except that 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazine was used as a reactant. The procedure was carried out to obtain 45 g of the title compound.; HRMS [M]+: 669.13
[준비예 122][Preparation Example 122]
5-(3-bromo-5-(4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline의 합성 5-(3-bromo-5-(4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline Synthesis of
Figure PCTKR2020004924-appb-I000147
Figure PCTKR2020004924-appb-I000147
반응물로 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 50]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 642.12Except for using 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine as a reactant 45g of the title compound was obtained by performing the same procedure as in [Preparation Example 50].; HRMS [M]+: 642.12
[준비예 123][Preparation Example 123]
5-(3-bromo-5-(4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline의 합성 5-(3-bromo-5-(4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)quinoline Synthesis of
Figure PCTKR2020004924-appb-I000148
Figure PCTKR2020004924-appb-I000148
반응물로 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 51]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 642.12Except for using 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 45g of the title compound was obtained by performing the same procedure as in [Preparation Example 51].; HRMS [M]+: 642.12
[준비예 124][Preparation Example 124]
6-(4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(quinolin-5-yl)phenyl)-1,3,5-triazin-2-yl)quinoline의 합성 6-(4-([1,1'-biphenyl]-4-yl)-6-(3-bromo-5-(quinolin-5-yl)phenyl)-1,3,5-triazin-2-yl ) Synthesis of quinoline
Figure PCTKR2020004924-appb-I000149
Figure PCTKR2020004924-appb-I000149
반응물로 6-(4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-1,3,5-triazin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 52]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 642.12Except for using 6-(4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-1,3,5-triazin-2-yl)quinoline as a reactant Was carried out in the same manner as in [Preparation Example 52] to obtain 45g of the title compound.; HRMS [M]+: 642.12
[준비예 125][Preparation Example 125]
5-(3-bromo-5-(4-(4-(pyridin-3-yl)phenyl)-6-(quinolin-6-yl)-1,3,5-triazin-2-yl)phenyl)quinoline의 합성 5-(3-bromo-5-(4-(4-(pyridin-3-yl)phenyl)-6-(quinolin-6-yl)-1,3,5-triazin-2-yl)phenyl)quinoline Synthesis of
Figure PCTKR2020004924-appb-I000150
Figure PCTKR2020004924-appb-I000150
반응물로 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 53]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 643.12Except for using 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)quinoline as a reactant, [ Preparation Example 53] was carried out in the same manner to obtain 45g of the title compound.; HRMS [M]+: 643.12
[준비예 126][Preparation Example 126]
5-(3-bromo-5-(4-(4-(pyridin-4-yl)phenyl)-6-(quinolin-6-yl)-1,3,5-triazin-2-yl)phenyl)quinoline의 합성 5-(3-bromo-5-(4-(4-(pyridin-4-yl)phenyl)-6-(quinolin-6-yl)-1,3,5-triazin-2-yl)phenyl)quinoline Synthesis of
Figure PCTKR2020004924-appb-I000151
Figure PCTKR2020004924-appb-I000151
반응물로 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 54]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 643.12Except for using 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)quinoline as a reactant, [ Preparation Example 54] was carried out in the same manner to obtain 45g of the title compound.; HRMS [M]+: 643.12
[준비예 127][Preparation Example 127]
9-(3-(4-([1,1'-biphenyl]-4-yl)-6-(pyridin-3-yl)-1,3,5-triazin-2-yl)-5-bromophenyl)-9H-carbazole의 합성9-(3-(4-([1,1'-biphenyl]-4-yl)-6-(pyridin-3-yl)-1,3,5-triazin-2-yl)-5-bromophenyl) Synthesis of -9H-carbazole
Figure PCTKR2020004924-appb-I000152
Figure PCTKR2020004924-appb-I000152
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-3-yl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 55]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 630.12Except for using 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-3-yl)-1,3,5-triazine as a reactant Then, 45g of the target compound was obtained by performing the same procedure as in [Preparation Example 55].; HRMS [M]+: 630.12
[준비예 128][Preparation Example 128]
9-(3-(4-([1,1'-biphenyl]-4-yl)-6-(pyridin-4-yl)-1,3,5-triazin-2-yl)-5-bromophenyl)-9H-carbazole의 합성9-(3-(4-([1,1'-biphenyl]-4-yl)-6-(pyridin-4-yl)-1,3,5-triazin-2-yl)-5-bromophenyl) Synthesis of -9H-carbazole
Figure PCTKR2020004924-appb-I000153
Figure PCTKR2020004924-appb-I000153
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-4-yl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 56]과 동일한 과정을 수행하여 목적 화합물 26g을 얻었다.; HRMS [M]+: 630.12Except for using 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(pyridin-4-yl)-1,3,5-triazine as a reactant Then, 26g of the target compound was obtained by performing the same procedure as in [Preparation Example 56].; HRMS [M]+: 630.12
[준비예 129][Preparation Example 129]
9-(3-bromo-5-(4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)-9H-carbazole의 합성Synthesis of 9-(3-bromo-5-(4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000154
Figure PCTKR2020004924-appb-I000154
반응물로 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 57]과 동일한 과정을 수행하여 목적 화합물 30g을 얻었다.; HRMS [M]+: 630.12[Preparation Example 57] and except for using 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine as a reactant 30 g of the target compound was obtained by performing the same procedure.; HRMS [M]+: 630.12
[준비예 130][Preparation Example 130]
9-(3-bromo-5-(4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)-9H-carbazole의 합성Synthesis of 9-(3-bromo-5-(4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000155
Figure PCTKR2020004924-appb-I000155
반응물로 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 58]과 동일한 과정을 수행하여 목적 화합물 25g을 얻었다.; HRMS [M]+: 630.12[Preparation Example 58] and except for using 2-(3,5-dibromophenyl)-4-phenyl-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant The same procedure was performed to obtain 25 g of the target compound.; HRMS [M]+: 630.12
[준비예 131][Preparation Example 131]
9-(3-bromo-5-(4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)-9H-carbazole의 합성9-(3-bromo-5-(4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)- Synthesis of 9H-carbazole
Figure PCTKR2020004924-appb-I000156
Figure PCTKR2020004924-appb-I000156
반응물로 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 59]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 631.12Except for using 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine as a reactant 32g of the title compound was obtained by performing the same procedure as in [Preparation Example 59].; HRMS [M]+: 631.12
[준비예 132][Preparation Example 132]
9-(3-bromo-5-(4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)-9H-carbazole의 합성9-(3-bromo-5-(4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)- Synthesis of 9H-carbazole
Figure PCTKR2020004924-appb-I000157
Figure PCTKR2020004924-appb-I000157
반응물로 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 60]과 동일한 과정을 수행하여 목적 화합물 32g을 얻었다.; HRMS [M]+: 631.12Except for using 2-(3,5-dibromophenyl)-4-(pyridin-3-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 32g of the target compound was obtained by performing the same procedure as in [Preparation Example 60].; HRMS [M]+: 631.12
[준비예 133][Preparation Example 133]
9-(3-bromo-5-(4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazin-2-yl)phenyl)-9H-carbazole의 합성 9-(3-bromo-5-(4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazin-2-yl)phenyl)- Synthesis of 9H-carbazole
Figure PCTKR2020004924-appb-I000158
Figure PCTKR2020004924-appb-I000158
반응물로 2-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 61]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 631.12Except for using 2-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(pyridin-4-yl)-1,3,5-triazine as a reactant 39g of the title compound was obtained by performing the same procedure as in [Preparation Example 61].; HRMS [M]+: 631.12
[준비예 134][Preparation Example 134]
9-(3-bromo-5-(4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)-9H-carbazole의 합성 9-(3-bromo-5-(4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)- Synthesis of 9H-carbazole
Figure PCTKR2020004924-appb-I000159
Figure PCTKR2020004924-appb-I000159
반응물로 2-(3,5-dibromophenyl)-4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 62]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 631.12Except for using 2-(3,5-dibromophenyl)-4-(pyridin-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 39g of the title compound was obtained by performing the same procedure as in [Preparation Example 62].; HRMS [M]+: 631.12
[준비예 135][Preparation Example 135]
9-(3-(4-([1,1'-biphenyl]-4-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)-5-bromophenyl)-9H-carbazole의 합성 9-(3-(4-([1,1'-biphenyl]-4-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl) Synthesis of -5-bromophenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000160
Figure PCTKR2020004924-appb-I000160
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 63]과 동일한 과정을 수행하여 목적 화합물 39g을 얻었다.; HRMS [M]+: 706.152-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5- 39g of the target compound was obtained by performing the same procedure as in [Preparation Example 63] except that triazine was used.; HRMS [M]+: 706.15
[준비예 136][Preparation Example 136]
9-(3-(4-([1,1'-biphenyl]-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)-5-bromophenyl)-9H-carbazole의 합성 9-(3-(4-([1,1'-biphenyl]-4-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl) Synthesis of -5-bromophenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000161
Figure PCTKR2020004924-appb-I000161
반응물로 2-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 64]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 706.152-([1,1'-biphenyl]-4-yl)-4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5- 45g of the target compound was obtained by performing the same procedure as in [Preparation Example 64] except that triazine was used.; HRMS [M]+: 706.15
[준비예 137][Preparation Example 137]
9-(3-(4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)-5-bromophenyl)-9H-carbazole의 합성 Synthesis of 9-(3-(4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)-5-bromophenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000162
Figure PCTKR2020004924-appb-I000162
반응물로 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 65]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 707.15The same as in [Preparation Example 65] except that 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-3-yl)phenyl)-1,3,5-triazine was used as the reactant. The procedure was carried out to obtain 45 g of the title compound.; HRMS [M]+: 707.15
[준비예 138][Preparation Example 138]
9-(3-bromo-5-(4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)-9H-carbazole의 합성 9-(3-bromo-5-(4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2- Synthesis of yl)phenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000163
Figure PCTKR2020004924-appb-I000163
반응물로 2-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 66]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 707.152-(3,5-dibromophenyl)-4-(4-(pyridin-3-yl)phenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 45g of the title compound was obtained by performing the same procedure as in [Preparation Example 66], except that it was used.; HRMS [M]+: 707.15
[준비예 139][Preparation Example 139]
9-(3-(4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)-5-bromophenyl)-9H-carbazole의 합성 Synthesis of 9-(3-(4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)-5-bromophenyl)-9H-carbazole
Figure PCTKR2020004924-appb-I000164
Figure PCTKR2020004924-appb-I000164
반응물로 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 67]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 707.15Same as [Preparation Example 67], except that 2-(3,5-dibromophenyl)-4,6-bis(4-(pyridin-4-yl)phenyl)-1,3,5-triazine was used as a reactant The procedure was carried out to obtain 45 g of the title compound.; HRMS [M]+: 707.15
[준비예 140][Preparation Example 140]
9-(3-bromo-5-(4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)-9H-carbazole의 합성 9-(3-bromo-5-(4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)- Synthesis of 9H-carbazole
Figure PCTKR2020004924-appb-I000165
Figure PCTKR2020004924-appb-I000165
반응물로 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 68]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 680.14Except for using 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazine as a reactant 45g of the title compound was obtained by performing the same procedure as in [Preparation Example 68].; HRMS [M]+: 680.14
[준비예 141][Preparation Example 141]
9-(3-bromo-5-(4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)-9H-carbazole의 합성 9-(3-bromo-5-(4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)phenyl)- Synthesis of 9H-carbazole
Figure PCTKR2020004924-appb-I000166
Figure PCTKR2020004924-appb-I000166
반응물로 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine을 사용한 것을 제외하고는 [준비예 69]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 680.14Except for using 2-(3,5-dibromophenyl)-4-(naphthalen-2-yl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazine as a reactant 45g of the title compound was obtained by performing the same procedure as in [Preparation Example 69].; HRMS [M]+: 680.14
[준비예 142][Preparation Example 142]
9-(3-(4-([1,1'-biphenyl]-4-yl)-6-(quinolin-6-yl)-1,3,5-triazin-2-yl)-5-bromophenyl)-9H-carbazole의 합성 9-(3-(4-([1,1'-biphenyl]-4-yl)-6-(quinolin-6-yl)-1,3,5-triazin-2-yl)-5-bromophenyl) Synthesis of -9H-carbazole
Figure PCTKR2020004924-appb-I000167
Figure PCTKR2020004924-appb-I000167
반응물로 6-(4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-1,3,5-triazin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 70]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 680.14Except for using 6-(4-([1,1'-biphenyl]-4-yl)-6-(3,5-dibromophenyl)-1,3,5-triazin-2-yl)quinoline as a reactant Was carried out in the same manner as in [Preparation Example 70] to obtain 45g of the title compound.; HRMS [M]+: 680.14
[준비예 143][Preparation Example 143]
9-(3-bromo-5-(4-(4-(pyridin-3-yl)phenyl)-6-(quinolin-6-yl)-1,3,5-triazin-2-yl)phenyl)-9H-carbazole의 합성 9-(3-bromo-5-(4-(4-(pyridin-3-yl)phenyl)-6-(quinolin-6-yl)-1,3,5-triazin-2-yl)phenyl)- Synthesis of 9H-carbazole
Figure PCTKR2020004924-appb-I000168
Figure PCTKR2020004924-appb-I000168
반응물로 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 71]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 681.13Except for using 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-3-yl)phenyl)-1,3,5-triazin-2-yl)quinoline as a reactant, [ Preparation Example 71] was carried out in the same manner to obtain 45g of the title compound.; HRMS [M]+: 681.13
[준비예 144][Preparation Example 144]
9-(3-bromo-5-(4-(4-(pyridin-4-yl)phenyl)-6-(quinolin-6-yl)-1,3,5-triazin-2-yl)phenyl)-9H-carbazole의 합성 9-(3-bromo-5-(4-(4-(pyridin-4-yl)phenyl)-6-(quinolin-6-yl)-1,3,5-triazin-2-yl)phenyl)- Synthesis of 9H-carbazole
Figure PCTKR2020004924-appb-I000169
Figure PCTKR2020004924-appb-I000169
반응물로 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)quinoline을 사용한 것을 제외하고는 [준비예 72]과 동일한 과정을 수행하여 목적 화합물 45g을 얻었다.; HRMS [M]+: 681.13Except for using 6-(4-(3,5-dibromophenyl)-6-(4-(pyridin-4-yl)phenyl)-1,3,5-triazin-2-yl)quinoline as a reactant, [ Preparation Example 72] was carried out in the same manner to obtain 45g of the title compound.; HRMS [M]+: 681.13
[합성예 1] Mat 1의 합성[Synthesis Example 1] Synthesis of Mat 1
Figure PCTKR2020004924-appb-I000170
Figure PCTKR2020004924-appb-I000170
[준비예 1] 5g(9.25mmol)과 phenanthren-9-ylboronic acid 2.2g(10.17mmol)에 1,4-dioxane 250 mL를 가하였다. Pd(PPh3)4 0.53g(0.46mmol), K2CO3 3.19g(23.1mol)을 첨가 후 120℃에서 24시간 가열환류하였다. 상온으로 온도를 냉각하고 반응액에 염화암모늄 수용액 500 mL로 반응을 종결시켰다. 혼합액을 M.C 200 mL로 추출한 후, 증류수로 세척하였다. 얻어진 유기층을 무수 MgSO4로 건조하고, 감압증류하고 실리카겔 컬럼크로마토그래피로 정제하여 목적 화합물 4.37g(수율 88%)을 얻었다. 1H-NMR: 9.24(s, 2H), 9.08(d, 1H), 8.84(d, 1H), 8.73(s, 1H), 8.70(dd, 2H), 8.42(dd, 2H), 8.30(m, 3H), 8.04(s, 4H), 7.90~7.85(m, 3H), 7.70~7.41(m, 11H); HRMS [M]+: 639.25[Preparation Example 1] 250 mL of 1,4-dioxane was added to 5g (9.25mmol) and 2.2g (10.17mmol) of phenanthren-9-ylboronic acid. Pd(PPh 3 ) 4 0.53g (0.46mmol), K 2 CO 3 3.19g (23.1mol) was added and then heated to reflux at 120° C. for 24 hours. The temperature was cooled to room temperature, and the reaction was terminated with 500 mL of an aqueous ammonium chloride solution in the reaction solution. After extracting the mixed solution with 200 mL of MC, it was washed with distilled water. The obtained organic layer was dried over anhydrous MgSO 4 , distilled under reduced pressure, and purified by silica gel column chromatography to obtain 4.37 g (yield 88%) of the title compound. 1H-NMR: 9.24 (s, 2H), 9.08 (d, 1H), 8.84 (d, 1H), 8.73 (s, 1H), 8.70 (dd, 2H), 8.42 (dd, 2H), 8.30 (m, 3H), 8.04 (s, 4H), 7.90-7.85 (m, 3H), 7.70-7.41 (m, 11H); HRMS [M] + : 639.25
[합성예 2] Mat 2의 합성[Synthesis Example 2] Synthesis of Mat 2
반응물로 (9-phenyl-9H-carbazol-3-yl)boronic acid을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 704.27Except for using (9-phenyl-9H-carbazol-3-yl) boronic acid as a reactant, the target compound was obtained by performing the same procedure as in [Synthesis Example 1].; HRMS [M]+: 704.27
[합성예 3] Mat 3의 합성[Synthesis Example 3] Synthesis of Mat 3
반응물로 dibenzo[b,d]furan-2-ylboronic acid을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.23The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that dibenzo[b,d]furan-2-ylboronic acid was used as the reactant.; HRMS [M]+: 629.23
[합성예 4] Mat 4의 합성[Synthesis Example 4] Synthesis of Mat 4
Figure PCTKR2020004924-appb-I000171
Figure PCTKR2020004924-appb-I000171
[준비예 1] 5g(9.25mmol)과 Carbazole 1.7g(10.17mmol)에 xylene 250 mL를 가하였다. Pd2(dba)3 0.42g (0.46mmol), Xphos 0.44g(0.92mmol), NaOtBu 2.2g(23.1mol)을 첨가 후 120℃에서 24시간 가열환류하였다. 상온으로 온도를 냉각하고 반응액에 염화암모늄 수용액 500 mL로 반응을 종결시켰다. 혼합액을 M.C 500 mL로 추출한 후, 증류수로 세척하였다. 얻어진 유기층을 무수 MgSO4로 건조하고, 감압증류하고 실리카겔 컬럼크로마토그래피로 정제하여 목적 화합물 4.46g(수율 77%)을 얻었다. 1H-NMR: 9.24(s, 2H), 8.73(s, 1H), 8.70(d, 2H), 8.55(d, 1H), 8.42(dd, 2H), 8.31~8.30(m, 4H), 8.19(d, 1H), 7.9~7.85(m, 4H), 7.57~7.41(m, 8H), 7.20(dd, 2H); HRMS [M]+: 628.24[Preparation Example 1] 250 mL of xylene was added to 5g (9.25mmol) and 1.7g (10.17mmol) of Carbazole. Pd 2 (dba) 3 0.42g (0.46mmol), Xphos 0.44g (0.92mmol), and NaOtBu 2.2g (23.1mol) were added and heated to reflux at 120° C. for 24 hours. The temperature was cooled to room temperature, and the reaction was terminated with 500 mL of an aqueous ammonium chloride solution in the reaction solution. The mixed solution was extracted with 500 mL of MC, and then washed with distilled water. The obtained organic layer was dried over anhydrous MgSO 4 , distilled under reduced pressure, and purified by silica gel column chromatography to obtain 4.46 g (yield 77%) of the title compound. 1H-NMR: 9.24(s, 2H), 8.73(s, 1H), 8.70(d, 2H), 8.55(d, 1H), 8.42(dd, 2H), 8.31~8.30(m, 4H), 8.19( d, 1H), 7.9 to 7.85 (m, 4H), 7.57 to 7.41 (m, 8H), 7.20 (dd, 2H); HRMS [M] + : 628.24
[합성예 5] Mat 5의 합성[Synthesis Example 5] Synthesis of Mat 5
반응물로 pyridin-3-ylboronic acid을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 540.21The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that pyridin-3-ylboronic acid was used as the reactant.; HRMS [M]+: 540.21
[합성예 6] Mat 6의 합성[Synthesis Example 6] Synthesis of Mat 6
반응물로 quinolin-5-ylboronic acid을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that quinolin-5-ylboronic acid was used as the reactant.; HRMS [M]+: 590.23
[합성예 7] Mat 7의 합성[Synthesis Example 7] Synthesis of Mat 7
반응물로 [준비예 2]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 639.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 2] was used as the reactant.; HRMS [M]+: 639.25
[합성예 8] Mat 8의 합성[Synthesis Example 8] Synthesis of Mat 8
반응물로 [준비예 2]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 704.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 2] was used as the reactant.; HRMS [M]+: 704.27
[합성예 9] Mat 9의 합성[Synthesis Example 9] Synthesis of Mat 9
반응물로 [준비예 2]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 2] was used as the reactant.; HRMS [M]+: 629.23
[합성예 10] Mat 10의 합성[Synthesis Example 10] Synthesis of Mat 10
반응물로 [준비예 2]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 628.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 2] was used as the reactant.; HRMS [M]+: 628.24
[합성예 11] Mat 11의 합성[Synthesis Example 11] Synthesis of Mat 11
반응물로 [준비예 2]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 540.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 2] was used as the reactant.; HRMS [M]+: 540.21
[합성예 12] Mat 12의 합성[Synthesis Example 12] Synthesis of Mat 12
반응물로 [준비예 2]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 2] was used as the reactant.; HRMS [M]+: 590.23
[합성예 13] Mat 13의 합성[Synthesis Example 13] Synthesis of Mat 13
반응물로 [준비예 3]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 639.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 3] was used as the reactant.; HRMS [M]+: 639.25
[합성예 14] Mat 14의 합성[Synthesis Example 14] Synthesis of Mat 14
반응물로 [준비예 3]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 704.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 3] was used as the reactant.; HRMS [M]+: 704.27
[합성예 15] Mat 15의 합성[Synthesis Example 15] Synthesis of Mat 15
반응물로 [준비예 3]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 3] was used as the reactant.; HRMS [M]+: 629.23
[합성예 16] Mat 16의 합성[Synthesis Example 16] Synthesis of Mat 16
반응물로 [준비예 3]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 628.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 3] was used as the reactant.; HRMS [M]+: 628.24
[합성예 17] Mat 17의 합성[Synthesis Example 17] Synthesis of Mat 17
반응물로 [준비예 3]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 540.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 3] was used as the reactant.; HRMS [M]+: 540.21
[합성예 18] Mat 18의 합성[Synthesis Example 18] Synthesis of Mat 18
반응물로 [준비예 3]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 3] was used as the reactant.; HRMS [M]+: 590.23
[합성예 19] Mat 19의 합성[Synthesis Example 19] Synthesis of Mat 19
반응물로 [준비예 4]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 639.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 4] was used as the reactant.; HRMS [M]+: 639.25
[합성예 20] Mat 20의 합성[Synthesis Example 20] Synthesis of Mat 20
반응물로 [준비예 4]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 704.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 4] was used as the reactant.; HRMS [M]+: 704.27
[합성예 21] Mat 21의 합성[Synthesis Example 21] Synthesis of Mat 21
반응물로 [준비예 4]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 4] was used as the reactant.; HRMS [M]+: 629.23
[합성예 22] Mat 22의 합성[Synthesis Example 22] Synthesis of Mat 22
반응물로 [준비예 4]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 628.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 4] was used as the reactant.; HRMS [M]+: 628.24
[합성예 23] Mat 23의 합성[Synthesis Example 23] Synthesis of Mat 23
반응물로 [준비예 4]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 540.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 4] was used as the reactant.; HRMS [M]+: 540.21
[합성예 24] Mat 24의 합성[Synthesis Example 24] Synthesis of Mat 24
반응물로 [준비예 4]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 4] was used as the reactant.; HRMS [M]+: 590.23
[합성예 25] Mat 25의 합성[Synthesis Example 25] Synthesis of Mat 25
반응물로 [준비예 5]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 5] was used as the reactant.; HRMS [M]+: 640.24
[합성예 26] Mat 26의 합성[Synthesis Example 26] Synthesis of Mat 26
반응물로 [준비예 5]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 5] was used as the reactant.; HRMS [M]+: 705.27
[합성예 27] Mat 27의 합성[Synthesis Example 27] Synthesis of Mat 27
반응물로 [준비예 5]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 5] was used as the reactant.; HRMS [M]+: 630.22
[합성예 28] Mat 28의 합성[Synthesis Example 28] Synthesis of Mat 28
반응물로 [준비예 5]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 5] was used as the reactant.; HRMS [M]+: 629.24
[합성예 29] Mat 29의 합성[Synthesis Example 29] Synthesis of Mat 29
반응물로 [준비예 5]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 5] was used as the reactant.; HRMS [M]+: 541.21
[합성예 30] Mat 30의 합성[Synthesis Example 30] Synthesis of Mat 30
반응물로 [준비예 5]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 5] was used as the reactant.; HRMS [M]+: 591.23
[합성예 31] Mat 31의 합성[Synthesis Example 31] Synthesis of Mat 31
반응물로 [준비예 6]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 6] was used as the reactant.; HRMS [M]+: 640.24
[합성예 32] Mat 32의 합성[Synthesis Example 32] Synthesis of Mat 32
반응물로 [준비예 6]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 6] was used as the reactant.; HRMS [M]+: 705.27
[합성예 33] Mat 33의 합성[Synthesis Example 33] Synthesis of Mat 33
반응물로 [준비예 6]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 6] was used as the reactant.; HRMS [M]+: 630.22
[합성예 34] Mat 34의 합성[Synthesis Example 34] Synthesis of Mat 34
반응물로 [준비예 6]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 6] was used as the reactant.; HRMS [M]+: 629.24
[합성예 35] Mat 35의 합성[Synthesis Example 35] Synthesis of Mat 35
반응물로 [준비예 6]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 6] was used as the reactant.; HRMS [M]+: 541.21
[합성예 36] Mat 36의 합성[Synthesis Example 36] Synthesis of Mat 36
반응물로 [준비예 6]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 6] was used as the reactant.; HRMS [M]+: 591.23
[합성예 37] Mat 37의 합성[Synthesis Example 37] Synthesis of Mat 37
반응물로 [준비예 7]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 7] was used as the reactant.; HRMS [M]+: 640.24
[합성예 38] Mat 38의 합성[Synthesis Example 38] Synthesis of Mat 38
반응물로 [준비예 7]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 7] was used as the reactant.; HRMS [M]+: 705.27
[합성예 39] Mat 39의 합성[Synthesis Example 39] Synthesis of Mat 39
반응물로 [준비예 7]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 7] was used as the reactant.; HRMS [M]+: 630.22
[합성예 40] Mat 40의 합성[Synthesis Example 40] Synthesis of Mat 40
반응물로 [준비예 7]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 7] was used as the reactant.; HRMS [M]+: 629.24
[합성예 41] Mat 41의 합성[Synthesis Example 41] Synthesis of Mat 41
반응물로 [준비예 7]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 7] was used as the reactant.; HRMS [M]+: 541.21
[합성예 42] Mat 42의 합성[Synthesis Example 42] Synthesis of Mat 42
반응물로 [준비예 7]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 7] was used as the reactant.; HRMS [M]+: 591.23
[합성예 43] Mat 43의 합성[Synthesis Example 43] Synthesis of Mat 43
반응물로 [준비예 8]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 8] was used as the reactant.; HRMS [M]+: 640.24
[합성예 44] Mat 44의 합성[Synthesis Example 44] Synthesis of Mat 44
반응물로 [준비예 8]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 8] was used as the reactant.; HRMS [M]+: 705.27
[합성예 45] Mat 45의 합성[Synthesis Example 45] Synthesis of Mat 45
반응물로 [준비예 8]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 8] was used as the reactant.; HRMS [M]+: 630.22
[합성예 46] Mat 46의 합성[Synthesis Example 46] Synthesis of Mat 46
반응물로 [준비예 8]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 8] was used as the reactant.; HRMS [M]+: 629.24
[합성예 47] Mat 47의 합성[Synthesis Example 47] Synthesis of Mat 47
반응물로 [준비예 8]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 8] was used as the reactant.; HRMS [M]+: 541.21
[합성예 48] Mat 48의 합성[Synthesis Example 48] Synthesis of Mat 48
반응물로 [준비예 8]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 8] was used as the reactant.; HRMS [M]+: 591.23
[합성예 49] Mat 49의 합성[Synthesis Example 49] Synthesis of Mat 49
반응물로 [준비예 9]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 715.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 9] was used as the reactant.; HRMS [M]+: 715.28
[합성예 50] Mat 50의 합성[Synthesis Example 50] Synthesis of Mat 50
반응물로 [준비예 9]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 780.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 9] was used as the reactant.; HRMS [M]+: 780.30
[합성예 51] Mat 51의 합성[Synthesis Example 51] Synthesis of Mat 51
반응물로 [준비예 9]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 9] was used as the reactant.; HRMS [M]+: 705.26
[합성예 52] Mat 52의 합성[Synthesis Example 52] Synthesis of Mat 52
반응물로 [준비예 9]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 704.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 9] was used as the reactant.; HRMS [M]+: 704.27
[합성예 53] Mat 53의 합성[Synthesis Example 53] Synthesis of Mat 53
반응물로 [준비예 9]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 616.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 9] was used as the reactant.; HRMS [M]+: 616.24
[합성예 54] Mat 54의 합성[Synthesis Example 54] Synthesis of Mat 54
반응물로 [준비예 9]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 666.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 9] was used as the reactant.; HRMS [M]+: 666.26
[합성예 55] Mat 55의 합성[Synthesis Example 55] Synthesis of Mat 55
반응물로 [준비예 10]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 715.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 10] was used as the reactant.; HRMS [M]+: 715.28
[합성예 56] Mat 56의 합성[Synthesis Example 56] Synthesis of Mat 56
반응물로 [준비예 10]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 780.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 10] was used as the reactant.; HRMS [M]+: 780.30
[합성예 57] Mat 57의 합성[Synthesis Example 57] Synthesis of Mat 57
반응물로 [준비예 10]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 10] was used as the reactant.; HRMS [M]+: 705.26
[합성예 58] Mat 58의 합성[Synthesis Example 58] Synthesis of Mat 58
반응물로 [준비예 10]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 704.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 10] was used as the reactant.; HRMS [M]+: 704.27
[합성예 59] Mat 59의 합성[Synthesis Example 59] Synthesis of Mat 59
반응물로 [준비예 10]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 616.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 10] was used as the reactant.; HRMS [M]+: 616.24
[합성예 60] Mat 60의 합성[Synthesis Example 60] Synthesis of Mat 60
반응물로 [준비예 10]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 666.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 10] was used as the reactant.; HRMS [M]+: 666.26
[합성예 61] Mat 61의 합성[Synthesis Example 61] Synthesis of Mat 61
반응물로 [준비예 11]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 11] was used as the reactant.; HRMS [M]+: 716.28
[합성예 62] Mat 62의 합성[Synthesis Example 62] Synthesis of Mat 62
반응물로 [준비예 11]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 781.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 11] was used as the reactant.; HRMS [M]+: 781.30
[합성예 63] Mat 63의 합성[Synthesis Example 63] Synthesis of Mat 63
반응물로 [준비예 11]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 11] was used as the reactant.; HRMS [M]+: 706.26
[합성예 64] Mat 64의 합성[Synthesis Example 64] Synthesis of Mat 64
반응물로 [준비예 11]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 11] was used as the reactant.; HRMS [M]+: 705.27
[합성예 65] Mat 65의 합성[Synthesis Example 65] Synthesis of Mat 65
반응물로 [준비예 11]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 617.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 11] was used as the reactant.; HRMS [M]+: 617.24
[합성예 66] Mat 66의 합성[Synthesis Example 66] Synthesis of Mat 66
반응물로 [준비예 11]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 11] was used as the reactant.; HRMS [M]+: 667.26
[합성예 67] Mat 67의 합성[Synthesis Example 67] Synthesis of Mat 67
반응물로 [준비예 12]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 12] was used as the reactant.; HRMS [M]+: 716.28
[합성예 68] Mat 68의 합성[Synthesis Example 68] Synthesis of Mat 68
반응물로 [준비예 12]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 781.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 12] was used as the reactant.; HRMS [M]+: 781.30
[합성예 69] Mat 69의 합성[Synthesis Example 69] Synthesis of Mat 69
반응물로 [준비예 12]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 12] was used as the reactant.; HRMS [M]+: 706.26
[합성예 70] Mat 70의 합성[Synthesis Example 70] Synthesis of Mat 70
반응물로 [준비예 12]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 12] was used as the reactant.; HRMS [M]+: 705.27
[합성예 71] Mat 71의 합성[Synthesis Example 71] Synthesis of Mat 71
반응물로 [준비예 12]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 617.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 12] was used as the reactant.; HRMS [M]+: 617.24
[합성예 72] Mat 72의 합성[Synthesis Example 72] Synthesis of Mat 72
반응물로 [준비예 12]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 12] was used as the reactant.; HRMS [M]+: 667.26
[합성예 73] Mat 73의 합성[Synthesis Example 73] Synthesis of Mat 73
반응물로 [준비예 13]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 13] was used as the reactant.; HRMS [M]+: 716.28
[합성예 74] Mat 74의 합성[Synthesis Example 74] Synthesis of Mat 74
반응물로 [준비예 13]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 781.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 13] was used as the reactant.; HRMS [M]+: 781.30
[합성예 75] Mat 75의 합성[Synthesis Example 75] Synthesis of Mat 75
반응물로 [준비예 13]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 13] was used as the reactant.; HRMS [M]+: 706.26
[합성예 76] Mat 76의 합성[Synthesis Example 76] Synthesis of Mat 76
반응물로 [준비예 13]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 13] was used as the reactant.; HRMS [M]+: 705.27
[합성예 77] Mat 77의 합성[Synthesis Example 77] Synthesis of Mat 77
반응물로 [준비예 13]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 617.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 13] was used as the reactant.; HRMS [M]+: 617.24
[합성예 78] Mat 78의 합성[Synthesis Example 78] Synthesis of Mat 78
반응물로 [준비예 13]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 13] was used as the reactant.; HRMS [M]+: 667.26
[합성예 79] Mat 79의 합성[Synthesis Example 79] Synthesis of Mat 79
반응물로 [준비예 14]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 689.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 14] was used as the reactant.; HRMS [M]+: 689.26
[합성예 80] Mat 80의 합성[Synthesis Example 80] Synthesis of Mat 80
반응물로 [준비예 14]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 754.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 14] was used as the reactant.; HRMS [M]+: 754.29
[합성예 81] Mat 81의 합성[Synthesis Example 81] Synthesis of Mat 81
반응물로 [준비예 14]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 14] was used as the reactant.; HRMS [M]+: 629.25
[합성예 82] Mat 82의 합성[Synthesis Example 82] Synthesis of Mat 82
반응물로 [준비예 14]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 678.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 14] was used as the reactant.; HRMS [M]+: 678.26
[합성예 83] Mat 83의 합성[Synthesis Example 83] Synthesis of Mat 83
반응물로 [준비예 14]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 14] was used as the reactant.; HRMS [M]+: 590.23
[합성예 84] Mat 84의 합성[Synthesis Example 84] Synthesis of Mat 84
반응물로 [준비예 14]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 14] was used as the reactant.; HRMS [M]+: 640.24
[합성예 85] Mat 85의 합성[Synthesis Example 85] Synthesis of Mat 85
반응물로 [준비예 15]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 689.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 15] was used as the reactant.; HRMS [M]+: 689.26
[합성예 86] Mat 86의 합성[Synthesis Example 86] Synthesis of Mat 86
반응물로 [준비예 15]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 754.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 15] was used as the reactant.; HRMS [M]+: 754.29
[합성예 87] Mat 87의 합성[Synthesis Example 87] Synthesis of Mat 87
반응물로 [준비예 15]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 15] was used as the reactant.; HRMS [M]+: 629.25
[합성예 88] Mat 88의 합성[Synthesis Example 88] Synthesis of Mat 88
반응물로 [준비예 15]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 678.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 15] was used as the reactant.; HRMS [M]+: 678.26
[합성예 89] Mat 89의 합성[Synthesis Example 89] Synthesis of Mat 89
반응물로 [준비예 15]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 15] was used as the reactant.; HRMS [M]+: 590.23
[합성예 90] Mat 90의 합성[Synthesis Example 90] Synthesis of Mat 90
반응물로 [준비예 15]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 15] was used as the reactant.; HRMS [M]+: 640.24
[합성예 91] Mat 91의 합성[Synthesis Example 91] Synthesis of Mat 91
반응물로 [준비예 16]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 689.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 16] was used as the reactant.; HRMS [M]+: 689.26
[합성예 92] Mat 92의 합성[Synthesis Example 92] Synthesis of Mat 92
반응물로 [준비예 16]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 754.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 16] was used as the reactant.; HRMS [M]+: 754.29
[합성예 93] Mat 93의 합성[Synthesis Example 93] Synthesis of Mat 93
반응물로 [준비예 16]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 16] was used as the reactant.; HRMS [M]+: 629.25
[합성예 94] Mat 94의 합성[Synthesis Example 94] Synthesis of Mat 94
반응물로 [준비예 16]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 678.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 16] was used as the reactant.; HRMS [M]+: 678.26
[합성예 95] Mat 95의 합성[Synthesis Example 95] Synthesis of Mat 95
반응물로 [준비예 16]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 16] was used as the reactant.; HRMS [M]+: 590.23
[합성예 96] Mat 96의 합성[Synthesis Example 96] Synthesis of Mat 96
반응물로 [준비예 16]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 16] was used as the reactant.; HRMS [M]+: 640.24
[합성예 97] Mat 97의 합성[Synthesis Example 97] Synthesis of Mat 97
반응물로 [준비예 17]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 17] was used as the reactant.; HRMS [M]+: 690.26
[합성예 98] Mat 98의 합성[Synthesis Example 98] Synthesis of Mat 98
반응물로 [준비예 17]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 17] was used as the reactant.; HRMS [M]+: 755.29
[합성예 99] Mat 99의 합성[Synthesis Example 99] Synthesis of Mat 99
반응물로 [준비예 17]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 17] was used as the reactant.; HRMS [M]+: 630.25
[합성예 100] Mat 100의 합성[Synthesis Example 100] Synthesis of Mat 100
반응물로 [준비예 17]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 17] was used as the reactant.; HRMS [M]+: 679.26
[합성예 101] Mat 101의 합성[Synthesis Example 101] Synthesis of Mat 101
반응물로 [준비예 17]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 17] was used as the reactant.; HRMS [M]+: 591.23
[합성예 102] Mat 102의 합성[Synthesis Example 102] Synthesis of Mat 102
반응물로 [준비예 17]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 17] was used as the reactant.; HRMS [M]+: 641.24
[합성예 103] Mat 103의 합성[Synthesis Example 103] Synthesis of Mat 103
반응물로 [준비예 18]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 18] was used as the reactant.; HRMS [M]+: 690.26
[합성예 104] Mat 104의 합성[Synthesis Example 104] Synthesis of Mat 104
반응물로 [준비예 18]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 18] was used as the reactant.; HRMS [M]+: 755.29
[합성예 105] Mat 105의 합성[Synthesis Example 105] Synthesis of Mat 105
반응물로 [준비예 18]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 18] was used as the reactant.; HRMS [M]+: 630.25
[합성예 106] Mat 106의 합성[Synthesis Example 106] Synthesis of Mat 106
반응물로 [준비예 18]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 18] was used as the reactant.; HRMS [M]+: 679.26
[합성예 107] Mat 107의 합성[Synthesis Example 107] Synthesis of Mat 107
반응물로 [준비예 18]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 18] was used as the reactant.; HRMS [M]+: 591.23
[합성예 108] Mat 108의 합성[Synthesis Example 108] Synthesis of Mat 108
반응물로 [준비예 18]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 18] was used as the reactant.; HRMS [M]+: 641.24
[합성예 109] Mat 109의 합성[Synthesis Example 109] Synthesis of Mat 109
반응물로 [준비예 19]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 639.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 19] was used as the reactant.; HRMS [M]+: 639.25
[합성예 110] Mat 110의 합성[Synthesis Example 110] Synthesis of Mat 110
반응물로 [준비예 19]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 704.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 19] was used as the reactant.; HRMS [M]+: 704.27
[합성예 111] Mat 111의 합성[Synthesis Example 111] Synthesis of Mat 111
반응물로 [준비예 19]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 19] was used as the reactant.; HRMS [M]+: 629.23
[합성예 112] Mat 112의 합성[Synthesis Example 112] Synthesis of Mat 112
반응물로 [준비예 19]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 628.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 19] was used as the reactant.; HRMS [M]+: 628.24
[합성예 113] Mat 113의 합성[Synthesis Example 113] Synthesis of Mat 113
반응물로 [준비예 19]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 540.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 19] was used as the reactant.; HRMS [M]+: 540.21
[합성예 114] Mat 114의 합성[Synthesis Example 114] Synthesis of Mat 114
반응물로 [준비예 19]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 19] was used as the reactant.; HRMS [M]+: 590.23
[합성예 115] Mat 115의 합성[Synthesis Example 115] Synthesis of Mat 115
반응물로 [준비예 20]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 639.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 20] was used as the reactant.; HRMS [M]+: 639.25
[합성예 116] Mat 116의 합성[Synthesis Example 116] Synthesis of Mat 116
반응물로 [준비예 20]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 704.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 20] was used as the reactant.; HRMS [M]+: 704.27
[합성예 117] Mat 117의 합성[Synthesis Example 117] Synthesis of Mat 117
반응물로 [준비예 20]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 20] was used as the reactant.; HRMS [M]+: 629.23
[합성예 118] Mat 118의 합성[Synthesis Example 118] Synthesis of Mat 118
반응물로 [준비예 20]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 628.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 20] was used as the reactant.; HRMS [M]+: 628.24
[합성예 119] Mat 119의 합성[Synthesis Example 119] Synthesis of Mat 119
반응물로 [준비예 20]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 540.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 20] was used as the reactant.; HRMS [M]+: 540.21
[합성예 120] Mat 120의 합성[Synthesis Example 120] Synthesis of Mat 120
반응물로 [준비예 20]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 20] was used as the reactant.; HRMS [M]+: 590.23
[합성예 121] Mat 121의 합성[Synthesis Example 121] Synthesis of Mat 121
반응물로 [준비예 21]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 639.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 21] was used as the reactant.; HRMS [M]+: 639.25
[합성예 122] Mat 122의 합성[Synthesis Example 122] Synthesis of Mat 122
반응물로 [준비예 21]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 704.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 21] was used as the reactant.; HRMS [M]+: 704.27
[합성예 123] Mat 123의 합성[Synthesis Example 123] Synthesis of Mat 123
반응물로 [준비예 21]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 21] was used as the reactant.; HRMS [M]+: 629.23
[합성예 124] Mat 124의 합성[Synthesis Example 124] Synthesis of Mat 124
반응물로 [준비예 21]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 628.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 21] was used as the reactant.; HRMS [M]+: 628.24
[합성예 125] Mat 125의 합성[Synthesis Example 125] Synthesis of Mat 125
반응물로 [준비예 21]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 540.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 21] was used as the reactant.; HRMS [M]+: 540.21
[합성예 126] Mat 126의 합성[Synthesis Example 126] Synthesis of Mat 126
반응물로 [준비예 21]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 21] was used as the reactant.; HRMS [M]+: 590.23
[합성예 127] Mat 127의 합성[Synthesis Example 127] Synthesis of Mat 127
반응물로 [준비예 22]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 639.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 22] was used as the reactant.; HRMS [M]+: 639.25
[합성예 128] Mat 128의 합성[Synthesis Example 128] Synthesis of Mat 128
반응물로 [준비예 22]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 704.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 22] was used as the reactant.; HRMS [M]+: 704.27
[합성예 129] Mat 129의 합성[Synthesis Example 129] Synthesis of Mat 129
반응물로 [준비예 22]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 22] was used as the reactant.; HRMS [M]+: 629.23
[합성예 130] Mat 130의 합성[Synthesis Example 130] Synthesis of Mat 130
반응물로 [준비예 22]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 628.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 22] was used as the reactant.; HRMS [M]+: 628.24
[합성예 131] Mat 131의 합성[Synthesis Example 131] Synthesis of Mat 131
반응물로 [준비예 22]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 540.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 22] was used as the reactant.; HRMS [M]+: 540.21
[합성예 132] Mat 132의 합성[Synthesis Example 132] Synthesis of Mat 132
반응물로 [준비예 22]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 22] was used as the reactant.; HRMS [M]+: 590.23
[합성예 133] Mat 133의 합성[Synthesis Example 133] Synthesis of Mat 133
반응물로 [준비예 23]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 23] was used as the reactant.; HRMS [M]+: 640.24
[합성예 134] Mat 134의 합성[Synthesis Example 134] Synthesis of Mat 134
반응물로 [준비예 23]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 23] was used as the reactant.; HRMS [M]+: 705.27
[합성예 135] Mat 135의 합성[Synthesis Example 135] Synthesis of Mat 135
반응물로 [준비예 23]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 23] was used as the reactant.; HRMS [M]+: 630.22
[합성예 136] Mat 136의 합성[Synthesis Example 136] Synthesis of Mat 136
반응물로 [준비예 23]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 23] was used as the reactant.; HRMS [M]+: 629.24
[합성예 137] Mat 137의 합성[Synthesis Example 137] Synthesis of Mat 137
반응물로 [준비예 23]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 23] was used as the reactant.; HRMS [M]+: 541.21
[합성예 138] Mat 138의 합성[Synthesis Example 138] Synthesis of Mat 138
반응물로 [준비예 23]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 23] was used as the reactant.; HRMS [M]+: 591.23
[합성예 139] Mat 139의 합성[Synthesis Example 139] Synthesis of Mat 139
반응물로 [준비예 24]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 24] was used as the reactant.; HRMS [M]+: 640.24
[합성예 140] Mat 140의 합성[Synthesis Example 140] Synthesis of Mat 140
반응물로 [준비예 24]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 24] was used as the reactant.; HRMS [M]+: 705.27
[합성예 141] Mat 141의 합성[Synthesis Example 141] Synthesis of Mat 141
반응물로 [준비예 24]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 24] was used as the reactant.; HRMS [M]+: 630.22
[합성예 142] Mat 142의 합성[Synthesis Example 142] Synthesis of Mat 142
반응물로 [준비예 24]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 24] was used as the reactant.; HRMS [M]+: 629.24
[합성예 143] Mat 143의 합성[Synthesis Example 143] Synthesis of Mat 143
반응물로 [준비예 24]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 24] was used as the reactant.; HRMS [M]+: 541.21
[합성예 144] Mat 144의 합성[Synthesis Example 144] Synthesis of Mat 144
반응물로 [준비예 24]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 24] was used as the reactant.; HRMS [M]+: 591.23
[합성예 145] Mat 145의 합성[Synthesis Example 145] Synthesis of Mat 145
반응물로 [준비예 25]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 25] was used as the reactant.; HRMS [M]+: 640.24
[합성예 146] Mat 146의 합성[Synthesis Example 146] Synthesis of Mat 146
반응물로 [준비예 25]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 25] was used as the reactant.; HRMS [M]+: 705.27
[합성예 147] Mat 147의 합성[Synthesis Example 147] Synthesis of Mat 147
반응물로 [준비예 25]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 25] was used as the reactant.; HRMS [M]+: 630.22
[합성예 148] Mat 148의 합성[Synthesis Example 148] Synthesis of Mat 148
반응물로 [준비예 25]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 25] was used as the reactant.; HRMS [M]+: 629.24
[합성예 149] Mat 149의 합성[Synthesis Example 149] Synthesis of Mat 149
반응물로 [준비예 25]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 25] was used as the reactant.; HRMS [M]+: 541.21
[합성예 150] Mat 150의 합성[Synthesis Example 150] Synthesis of Mat 150
반응물로 [준비예 25]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 25] was used as the reactant.; HRMS [M]+: 591.23
[합성예 151] Mat 151의 합성[Synthesis Example 151] Synthesis of Mat 151
반응물로 [준비예 26]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 26] was used as the reactant.; HRMS [M]+: 640.24
[합성예 152] Mat 152의 합성[Synthesis Example 152] Synthesis of Mat 152
반응물로 [준비예 26]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 26] was used as the reactant.; HRMS [M]+: 705.27
[합성예 153] Mat 153의 합성[Synthesis Example 153] Synthesis of Mat 153
반응물로 [준비예 26]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 26] was used as the reactant.; HRMS [M]+: 630.22
[합성예 154] Mat 154의 합성[Synthesis Example 154] Synthesis of Mat 154
반응물로 [준비예 26]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 26] was used as the reactant.; HRMS [M]+: 629.24
[합성예 155] Mat 155의 합성[Synthesis Example 155] Synthesis of Mat 155
반응물로 [준비예 26]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 26] was used as the reactant.; HRMS [M]+: 541.21
[합성예 156] Mat 156의 합성[Synthesis Example 156] Synthesis of Mat 156
반응물로 [준비예 26]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 26] was used as the reactant.; HRMS [M]+: 591.23
[합성예 157] Mat 157의 합성[Synthesis Example 157] Synthesis of Mat 157
반응물로 [준비예 27]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 715.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 27] was used as the reactant.; HRMS [M]+: 715.28
[합성예 158] Mat 158의 합성[Synthesis Example 158] Synthesis of Mat 158
반응물로 [준비예 27]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 780.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 27] was used as the reactant.; HRMS [M]+: 780.30
[합성예 159] Mat 159의 합성[Synthesis Example 159] Synthesis of Mat 159
반응물로 [준비예 27]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 27] was used as the reactant.; HRMS [M]+: 705.26
[합성예 160] Mat 160의 합성[Synthesis Example 160] Synthesis of Mat 160
반응물로 [준비예 27]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 704.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 27] was used as the reactant.; HRMS [M]+: 704.27
[합성예 161] Mat 161의 합성[Synthesis Example 161] Synthesis of Mat 161
반응물로 [준비예 27]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 616.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 27] was used as the reactant.; HRMS [M]+: 616.24
[합성예 162] Mat 162의 합성[Synthesis Example 162] Synthesis of Mat 162
반응물로 [준비예 27]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 666.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 27] was used as the reactant.; HRMS [M]+: 666.26
[합성예 163] Mat 163의 합성[Synthesis Example 163] Synthesis of Mat 163
반응물로 [준비예 28]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 715.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 28] was used as the reactant.; HRMS [M]+: 715.28
[합성예 164] Mat 164의 합성[Synthesis Example 164] Synthesis of Mat 164
반응물로 [준비예 28]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 780.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 28] was used as the reactant.; HRMS [M]+: 780.30
[합성예 165] Mat 165의 합성[Synthesis Example 165] Synthesis of Mat 165
반응물로 [준비예 28]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 28] was used as the reactant.; HRMS [M]+: 705.26
[합성예 166] Mat 166의 합성[Synthesis Example 166] Synthesis of Mat 166
반응물로 [준비예 28]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 704.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 28] was used as the reactant.; HRMS [M]+: 704.27
[합성예 167] Mat 167의 합성[Synthesis Example 167] Synthesis of Mat 167
반응물로 [준비예 28]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 616.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 28] was used as the reactant.; HRMS [M]+: 616.24
[합성예 168] Mat 168의 합성[Synthesis Example 168] Synthesis of Mat 168
반응물로 [준비예 28]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 666.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 28] was used as the reactant.; HRMS [M]+: 666.26
[합성예 169] Mat 169의 합성[Synthesis Example 169] Synthesis of Mat 169
반응물로 [준비예 29]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 29] was used as the reactant.; HRMS [M]+: 716.28
[합성예 170] Mat 170의 합성[Synthesis Example 170] Synthesis of Mat 170
반응물로 [준비예 29]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 781.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 29] was used as the reactant.; HRMS [M]+: 781.30
[합성예 171] Mat 171의 합성[Synthesis Example 171] Synthesis of Mat 171
반응물로 [준비예 29]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 29] was used as the reactant.; HRMS [M]+: 706.26
[합성예 172] Mat 172의 합성[Synthesis Example 172] Synthesis of Mat 172
반응물로 [준비예 29]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 29] was used as the reactant.; HRMS [M]+: 705.27
[합성예 173] Mat 173의 합성[Synthesis Example 173] Synthesis of Mat 173
반응물로 [준비예 29]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 617.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 29] was used as the reactant.; HRMS [M]+: 617.24
[합성예 174] Mat 174의 합성[Synthesis Example 174] Synthesis of Mat 174
반응물로 [준비예 29]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 29] was used as the reactant.; HRMS [M]+: 667.26
[합성예 175] Mat 175의 합성[Synthesis Example 175] Synthesis of Mat 175
반응물로 [준비예 30]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 30] was used as the reactant.; HRMS [M]+: 716.28
[합성예 176] Mat 176의 합성[Synthesis Example 176] Synthesis of Mat 176
반응물로 [준비예 30]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 781.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 30] was used as the reactant.; HRMS [M]+: 781.30
[합성예 177] Mat 177의 합성[Synthesis Example 177] Synthesis of Mat 177
반응물로 [준비예 30]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 30] was used as the reactant.; HRMS [M]+: 706.26
[합성예 178] Mat 178의 합성[Synthesis Example 178] Synthesis of Mat 178
반응물로 [준비예 30]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 30] was used as the reactant.; HRMS [M]+: 705.27
[합성예 179] Mat 179의 합성[Synthesis Example 179] Synthesis of Mat 179
반응물로 [준비예 30]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 617.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 30] was used as the reactant.; HRMS [M]+: 617.24
[합성예 180] Mat 180의 합성[Synthesis Example 180] Synthesis of Mat 180
반응물로 [준비예 30]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 30] was used as the reactant.; HRMS [M]+: 667.26
[합성예 181] Mat 181의 합성[Synthesis Example 181] Synthesis of Mat 181
반응물로 [준비예 31]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 31] was used as the reactant.; HRMS [M]+: 716.28
[합성예 182] Mat 182의 합성[Synthesis Example 182] Synthesis of Mat 182
반응물로 [준비예 31]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 781.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 31] was used as the reactant.; HRMS [M]+: 781.30
[합성예 183] Mat 183의 합성[Synthesis Example 183] Synthesis of Mat 183
반응물로 [준비예 31]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 31] was used as the reactant.; HRMS [M]+: 706.26
[합성예 184] Mat 184의 합성[Synthesis Example 184] Synthesis of Mat 184
반응물로 [준비예 31]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 31] was used as the reactant.; HRMS [M]+: 705.27
[합성예 185] Mat 185의 합성[Synthesis Example 185] Synthesis of Mat 185
반응물로 [준비예 31]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 617.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 31] was used as the reactant.; HRMS [M]+: 617.24
[합성예 186] Mat 186의 합성[Synthesis Example 186] Synthesis of Mat 186
반응물로 [준비예 31]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 31] was used as the reactant.; HRMS [M]+: 667.26
[합성예 187] Mat 187의 합성[Synthesis Example 187] Synthesis of Mat 187
반응물로 [준비예 32]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 689.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 32] was used as the reactant.; HRMS [M]+: 689.26
[합성예 188] Mat 188의 합성[Synthesis Example 188] Synthesis of Mat 188
반응물로 [준비예 32]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 754.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 32] was used as the reactant.; HRMS [M]+: 754.29
[합성예 189] Mat 189의 합성[Synthesis Example 189] Synthesis of Mat 189
반응물로 [준비예 32]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 32] was used as the reactant.; HRMS [M]+: 629.25
[합성예 190] Mat 190의 합성[Synthesis Example 190] Synthesis of Mat 190
반응물로 [준비예 32]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 678.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 32] was used as the reactant.; HRMS [M]+: 678.26
[합성예 191] Mat 191의 합성[Synthesis Example 191] Synthesis of Mat 191
반응물로 [준비예 32]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 32] was used as the reactant.; HRMS [M]+: 590.23
[합성예 192] Mat 192의 합성[Synthesis Example 192] Synthesis of Mat 192
반응물로 [준비예 32]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 32] was used as the reactant.; HRMS [M]+: 640.24
[합성예 193] Mat 193의 합성[Synthesis Example 193] Synthesis of Mat 193
반응물로 [준비예 33]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 689.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 33] was used as the reactant.; HRMS [M]+: 689.26
[합성예 194] Mat 194의 합성[Synthesis Example 194] Synthesis of Mat 194
반응물로 [준비예 33]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 754.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 33] was used as the reactant.; HRMS [M]+: 754.29
[합성예 195] Mat 195의 합성[Synthesis Example 195] Synthesis of Mat 195
반응물로 [준비예 33]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 33] was used as the reactant.; HRMS [M]+: 629.25
[합성예 196] Mat 196의 합성[Synthesis Example 196] Synthesis of Mat 196
반응물로 [준비예 33]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 678.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 33] was used as the reactant.; HRMS [M]+: 678.26
[합성예 197] Mat 197의 합성[Synthesis Example 197] Synthesis of Mat 197
반응물로 [준비예 33]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 33] was used as the reactant.; HRMS [M]+: 590.23
[합성예 198] Mat 198의 합성[Synthesis Example 198] Synthesis of Mat 198
반응물로 [준비예 33]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 33] was used as the reactant.; HRMS [M]+: 640.24
[합성예 199] Mat 199의 합성[Synthesis Example 199] Synthesis of Mat 199
반응물로 [준비예 34]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 689.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 34] was used as the reactant.; HRMS [M]+: 689.26
[합성예 200] Mat 200의 합성[Synthesis Example 200] Synthesis of Mat 200
반응물로 [준비예 34]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 754.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 34] was used as the reactant.; HRMS [M]+: 754.29
[합성예 201] Mat 201의 합성[Synthesis Example 201] Synthesis of Mat 201
반응물로 [준비예 34]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 34] was used as the reactant.; HRMS [M]+: 629.25
[합성예 202] Mat 202의 합성[Synthesis Example 202] Synthesis of Mat 202
반응물로 [준비예 34]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 678.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 34] was used as the reactant.; HRMS [M]+: 678.26
[합성예 203] Mat 203의 합성[Synthesis Example 203] Synthesis of Mat 203
반응물로 [준비예 34]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 34] was used as the reactant.; HRMS [M]+: 590.23
[합성예 204] Mat 204의 합성[Synthesis Example 204] Synthesis of Mat 204
반응물로 [준비예 34]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 34] was used as the reactant.; HRMS [M]+: 640.24
[합성예 205] Mat 205의 합성[Synthesis Example 205] Synthesis of Mat 205
반응물로 [준비예 35]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 35] was used as the reactant.; HRMS [M]+: 690.26
[합성예 206] Mat 206의 합성[Synthesis Example 206] Synthesis of Mat 206
반응물로 [준비예 35]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 35] was used as the reactant.; HRMS [M]+: 755.29
[합성예 207] Mat 207의 합성[Synthesis Example 207] Synthesis of Mat 207
반응물로 [준비예 35]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 35] was used as the reactant.; HRMS [M]+: 630.25
[합성예 208] Mat 208의 합성[Synthesis Example 208] Synthesis of Mat 208
반응물로 [준비예 35]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 35] was used as the reactant.; HRMS [M]+: 679.26
[합성예 209] Mat 209의 합성[Synthesis Example 209] Synthesis of Mat 209
반응물로 [준비예 35]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 35] was used as the reactant.; HRMS [M]+: 591.23
[합성예 210] Mat 210의 합성[Synthesis Example 210] Synthesis of Mat 210
반응물로 [준비예 35]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 35] was used as the reactant.; HRMS [M]+: 641.24
[합성예 211] Mat 211의 합성[Synthesis Example 211] Synthesis of Mat 211
반응물로 [준비예 36]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 36] was used as the reactant.; HRMS [M]+: 690.26
[합성예 212] Mat 212의 합성[Synthesis Example 212] Synthesis of Mat 212
반응물로 [준비예 36]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 36] was used as the reactant.; HRMS [M]+: 755.29
[합성예 213] Mat 213의 합성[Synthesis Example 213] Synthesis of Mat 213
반응물로 [준비예 36]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 36] was used as the reactant.; HRMS [M]+: 630.25
[합성예 214] Mat 214의 합성[Synthesis Example 214] Synthesis of Mat 214
반응물로 [준비예 36]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 36] was used as the reactant.; HRMS [M]+: 679.26
[합성예 215] Mat 215의 합성[Synthesis Example 215] Synthesis of Mat 215
반응물로 [준비예 36]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 36] was used as the reactant.; HRMS [M]+: 591.23
[합성예 216] Mat 216의 합성[Synthesis Example 216] Synthesis of Mat 216
반응물로 [준비예 36]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 36] was used as the reactant.; HRMS [M]+: 641.24
[합성예 217] Mat 217의 합성[Synthesis Example 217] Synthesis of Mat 217
반응물로 [준비예 37]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 689.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 37] was used as the reactant.; HRMS [M]+: 689.26
[합성예 218] Mat 218의 합성[Synthesis Example 218] Synthesis of Mat 218
반응물로 [준비예 37]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 754.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 37] was used as the reactant.; HRMS [M]+: 754.29
[합성예 219] Mat 219의 합성[Synthesis Example 219] Synthesis of Mat 219
반응물로 [준비예 37]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.24The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 37] was used as the reactant.; HRMS [M]+: 679.24
[합성예 220] Mat 220의 합성[Synthesis Example 220] Synthesis of Mat 220
반응물로 [준비예 37]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 678.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 37] was used as the reactant.; HRMS [M]+: 678.24
[합성예 221] Mat 221의 합성[Synthesis Example 221] Synthesis of Mat 221
반응물로 [준비예 37]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 37] was used as the reactant.; HRMS [M]+: 590.23
[합성예 222] Mat 222의 합성[Synthesis Example 222] Synthesis of Mat 222
반응물로 [준비예 37]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 37] was used as the reactant.; HRMS [M]+: 590.23
[합성예 223] Mat 223의 합성[Synthesis Example 223] Synthesis of Mat 223
반응물로 [준비예 38]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 689.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 38] was used as the reactant.; HRMS [M]+: 689.26
[합성예 224] Mat 224의 합성[Synthesis Example 224] Synthesis of Mat 224
반응물로 [준비예 38]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 754.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 38] was used as the reactant.; HRMS [M]+: 754.29
[합성예 225] Mat 225의 합성[Synthesis Example 225] Synthesis of Mat 225
반응물로 [준비예 38]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 38] was used as the reactant.; HRMS [M]+: 679.23
[합성예 226] Mat 226의 합성[Synthesis Example 226] Synthesis of Mat 226
반응물로 [준비예 38]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 678.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 38] was used as the reactant.; HRMS [M]+: 678.24
[합성예 227] Mat 227의 합성[Synthesis Example 227] Synthesis of Mat 227
반응물로 [준비예 38]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 38] was used as the reactant.; HRMS [M]+: 590.21
[합성예 228] Mat 228의 합성[Synthesis Example 228] Synthesis of Mat 228
반응물로 [준비예 38]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 38] was used as the reactant.; HRMS [M]+: 640.23
[합성예 229] Mat 229의 합성[Synthesis Example 229] Synthesis of Mat 229
반응물로 [준비예 39]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 689.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 39] was used as the reactant.; HRMS [M]+: 689.25
[합성예 230] Mat 230의 합성[Synthesis Example 230] Synthesis of Mat 230
반응물로 [준비예 39]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 754.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 39] was used as the reactant.; HRMS [M]+: 754.27
[합성예 231] Mat 231의 합성[Synthesis Example 231] Synthesis of Mat 231
반응물로 [준비예 39]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 39] was used as the reactant.; HRMS [M]+: 679.23
[합성예 232] Mat 232의 합성[Synthesis Example 232] Synthesis of Mat 232
반응물로 [준비예 39]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 678.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 39] was used as the reactant.; HRMS [M]+: 678.24
[합성예 233] Mat 233의 합성[Synthesis Example 233] Synthesis of Mat 233
반응물로 [준비예 39]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 39] was used as the reactant.; HRMS [M]+: 590.21
[합성예 234] Mat 234의 합성[Synthesis Example 234] Synthesis of Mat 234
반응물로 [준비예 39]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 39] was used as the reactant.; HRMS [M]+: 640.23
[합성예 235] Mat 235의 합성[Synthesis Example 235] Synthesis of Mat 235
반응물로 [준비예 40]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 689.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 40] was used as the reactant.; HRMS [M]+: 689.25
[합성예 236] Mat 236의 합성[Synthesis Example 236] Synthesis of Mat 236
반응물로 [준비예 40]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 754.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 40] was used as the reactant.; HRMS [M]+: 754.27
[합성예 237] Mat 237의 합성[Synthesis Example 237] Synthesis of Mat 237
반응물로 [준비예 40]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 40] was used as the reactant.; HRMS [M]+: 679.23
[합성예 238] Mat 238의 합성[Synthesis Example 238] Synthesis of Mat 238
반응물로 [준비예 40]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 678.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 40] was used as the reactant.; HRMS [M]+: 678.24
[합성예 239] Mat 239의 합성[Synthesis Example 239] Synthesis of Mat 239
반응물로 [준비예 40]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 590.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 40] was used as the reactant.; HRMS [M]+: 590.21
[합성예 240] Mat 240의 합성[Synthesis Example 240] Synthesis of Mat 240
반응물로 [준비예 40]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 40] was used as the reactant.; HRMS [M]+: 640.23
[합성예 241] Mat 241의 합성[Synthesis Example 241] Synthesis of Mat 241
반응물로 [준비예 41]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 41] was used as the reactant.; HRMS [M]+: 690.24
[합성예 242] Mat 242의 합성[Synthesis Example 242] Synthesis of Mat 242
반응물로 [준비예 41]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 41] was used as the reactant.; HRMS [M]+: 755.27
[합성예 243] Mat 243의 합성[Synthesis Example 243] Synthesis of Mat 243
반응물로 [준비예 41]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 41] was used as the reactant.; HRMS [M]+: 680.22
[합성예 244] Mat 244의 합성[Synthesis Example 244] Synthesis of Mat 244
반응물로 [준비예 41]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 41] was used as the reactant.; HRMS [M]+: 679.24
[합성예 245] Mat 245의 합성[Synthesis Example 245] Synthesis of Mat 245
반응물로 [준비예 41]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 41] was used as the reactant.; HRMS [M]+: 591.21
[합성예 246] Mat 246의 합성[Synthesis Example 246] Synthesis of Mat 246
반응물로 [준비예 41]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 41] was used as the reactant.; HRMS [M]+: 641.23
[합성예 247] Mat 247의 합성[Synthesis Example 247] Synthesis of Mat 247
반응물로 [준비예 42]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 42] was used as the reactant.; HRMS [M]+: 690.24
[합성예 248] Mat 248의 합성[Synthesis Example 248] Synthesis of Mat 248
반응물로 [준비예 42]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 42] was used as the reactant.; HRMS [M]+: 755.27
[합성예 249] Mat 249의 합성[Synthesis Example 249] Synthesis of Mat 249
반응물로 [준비예 42]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 42] was used as the reactant.; HRMS [M]+: 680.22
[합성예 250] Mat 250의 합성[Synthesis Example 250] Synthesis of Mat 250
반응물로 [준비예 42]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 42] was used as the reactant.; HRMS [M]+: 679.24
[합성예 251] Mat 251의 합성[Synthesis Example 251] Synthesis of Mat 251
반응물로 [준비예 42]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 42] was used as the reactant.; HRMS [M]+: 591.21
[합성예 252] Mat 252의 합성[Synthesis Example 252] Synthesis of Mat 252
반응물로 [준비예 42]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 42] was used as the reactant.; HRMS [M]+: 641.23
[합성예 253] Mat 253의 합성[Synthesis Example 253] Synthesis of Mat 253
반응물로 [준비예 43]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 43] was used as the reactant.; HRMS [M]+: 690.24
[합성예 254] Mat 254의 합성[Synthesis Example 254] Synthesis of Mat 254
반응물로 [준비예 43]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 43] was used as the reactant.; HRMS [M]+: 755.27
[합성예 255] Mat 255의 합성[Synthesis Example 255] Synthesis of Mat 255
반응물로 [준비예 43]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 43] was used as the reactant.; HRMS [M]+: 680.22
[합성예 1256] Mat 256의 합성[Synthesis Example 1256] Synthesis of Mat 256
반응물로 [준비예 43]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 43] was used as the reactant.; HRMS [M]+: 679.24
[합성예 257] Mat 257의 합성[Synthesis Example 257] Synthesis of Mat 257
반응물로 [준비예 43]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 43] was used as the reactant.; HRMS [M]+: 591.21
[합성예 258] Mat 258의 합성[Synthesis Example 258] Synthesis of Mat 258
반응물로 [준비예 43]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 43] was used as the reactant.; HRMS [M]+: 641.23
[합성예 259] Mat 259의 합성[Synthesis Example 259] Synthesis of Mat 259
반응물로 [준비예 44]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 44] was used as the reactant.; HRMS [M]+: 690.24
[합성예 260] Mat 260의 합성[Synthesis Example 260] Synthesis of Mat 260
반응물로 [준비예 44]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 44] was used as the reactant.; HRMS [M]+: 755.27
[합성예 261] Mat 261의 합성[Synthesis Example 261] Synthesis of Mat 261
반응물로 [준비예 44]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 44] was used as the reactant.; HRMS [M]+: 680.22
[합성예 262] Mat 262의 합성[Synthesis Example 262] Synthesis of Mat 262
반응물로 [준비예 44]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 44] was used as the reactant.; HRMS [M]+: 679.24
[합성예 263] Mat 263의 합성[Synthesis Example 263] Synthesis of Mat 263
반응물로 [준비예 44]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 44] was used as the reactant.; HRMS [M]+: 591.21
[합성예 264] Mat 264의 합성[Synthesis Example 264] Synthesis of Mat 264
반응물로 [준비예 44]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 44] was used as the reactant.; HRMS [M]+: 641.23
[합성예 265] Mat 265의 합성[Synthesis Example 265] Synthesis of Mat 265
반응물로 [준비예 45]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 765.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 45] was used as the reactant.; HRMS [M]+: 765.28
[합성예 266] Mat 266의 합성[Synthesis Example 266] Synthesis of Mat 266
반응물로 [준비예 45]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 830.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 45] was used as the reactant.; HRMS [M]+: 830.30
[합성예 267] Mat 267의 합성[Synthesis Example 267] Synthesis of Mat 267
반응물로 [준비예 45]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 45] was used as the reactant.; HRMS [M]+: 755.26
[합성예 268] Mat 268의 합성[Synthesis Example 268] Synthesis of Mat 268
반응물로 [준비예 45]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 754.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 45] was used as the reactant.; HRMS [M]+: 754.27
[합성예 269] Mat 269의 합성[Synthesis Example 269] Synthesis of Mat 269
반응물로 [준비예 45]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 666.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 45] was used as the reactant.; HRMS [M]+: 666.24
[합성예 270] Mat 270의 합성[Synthesis Example 270] Synthesis of Mat 270
반응물로 [준비예 45]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 45] was used as the reactant.; HRMS [M]+: 716.26
[합성예 271] Mat 271의 합성[Synthesis Example 271] Synthesis of Mat 271
반응물로 [준비예 46]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 765.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 46] was used as the reactant.; HRMS [M]+: 765.28
[합성예 272] Mat 272의 합성[Synthesis Example 272] Synthesis of Mat 272
반응물로 [준비예 46]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 830.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 46] was used as the reactant.; HRMS [M]+: 830.30
[합성예 273] Mat 273의 합성[Synthesis Example 273] Synthesis of Mat 273
반응물로 [준비예 46]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 46] was used as the reactant.; HRMS [M]+: 755.26
[합성예 274] Mat 274의 합성[Synthesis Example 274] Synthesis of Mat 274
반응물로 [준비예 46]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 754.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 46] was used as the reactant.; HRMS [M]+: 754.27
[합성예 275] Mat 275의 합성[Synthesis Example 275] Synthesis of Mat 275
반응물로 [준비예 46]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 666.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 46] was used as the reactant.; HRMS [M]+: 666.24
[합성예 276] Mat 276의 합성[Synthesis Example 276] Synthesis of Mat 276
반응물로 [준비예 46]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 46] was used as the reactant.; HRMS [M]+: 716.26
[합성예 277] Mat 277의 합성[Synthesis Example 277] Synthesis of Mat 277
반응물로 [준비예 47]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 766.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 47] was used as the reactant.; HRMS [M]+: 766.28
[합성예 278] Mat 278의 합성[Synthesis Example 278] Synthesis of Mat 278
반응물로 [준비예 47]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 831.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 47] was used as the reactant.; HRMS [M]+: 831.30
[합성예 279] Mat 279의 합성[Synthesis Example 279] Synthesis of Mat 279
반응물로 [준비예 47]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 47] was used as the reactant.; HRMS [M]+: 756.26
[합성예 280] Mat 280의 합성[Synthesis Example 280] Synthesis of Mat 280
반응물로 [준비예 47]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 47] was used as the reactant.; HRMS [M]+: 755.27
[합성예 281] Mat 281의 합성[Synthesis Example 281] Synthesis of Mat 281
반응물로 [준비예 47]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 47] was used as the reactant.; HRMS [M]+: 667.24
[합성예 282] Mat 282의 합성[Synthesis Example 282] Synthesis of Mat 282
반응물로 [준비예 47]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 47] was used as the reactant.; HRMS [M]+: 717.26
[합성예 283] Mat 283의 합성[Synthesis Example 283] Synthesis of Mat 283
반응물로 [준비예 48]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 766.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 48] was used as the reactant.; HRMS [M]+: 766.28
[합성예 284] Mat 284의 합성[Synthesis Example 284] Synthesis of Mat 284
반응물로 [준비예 48]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 831.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 48] was used as the reactant.; HRMS [M]+: 831.30
[합성예 285] Mat 285의 합성[Synthesis Example 285] Synthesis of Mat 285
반응물로 [준비예 48]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 48] was used as the reactant.; HRMS [M]+: 756.26
[합성예 286] Mat 286의 합성[Synthesis Example 286] Synthesis of Mat 286
반응물로 [준비예 48]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 48] was used as the reactant.; HRMS [M]+: 755.27
[합성예 287] Mat 287의 합성[Synthesis Example 287] Synthesis of Mat 287
반응물로 [준비예 48]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 48] was used as the reactant.; HRMS [M]+: 667.24
[합성예 288] Mat 288의 합성[Synthesis Example 288] Synthesis of Mat 288
반응물로 [준비예 48]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 48] was used as the reactant.; HRMS [M]+: 717.26
[합성예 289] Mat 289의 합성[Synthesis Example 289] Synthesis of Mat 289
반응물로 [준비예 49]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 766.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 49] was used as the reactant.; HRMS [M]+: 766.28
[합성예 290] Mat 290의 합성[Synthesis Example 290] Synthesis of Mat 290
반응물로 [준비예 49]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 831.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 49] was used as the reactant.; HRMS [M]+: 831.30
[합성예 291] Mat 291의 합성[Synthesis Example 291] Synthesis of Mat 291
반응물로 [준비예 49]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 49] was used as the reactant.; HRMS [M]+: 756.26
[합성예 292] Mat 292의 합성[Synthesis Example 292] Synthesis of Mat 292
반응물로 [준비예 49]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 49] was used as the reactant.; HRMS [M]+: 755.27
[합성예 293] Mat 293의 합성[Synthesis Example 293] Synthesis of Mat 293
반응물로 [준비예 49]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 49] was used as the reactant.; HRMS [M]+: 667.24
[합성예 294] Mat 294의 합성[Synthesis Example 294] Synthesis of Mat 294
반응물로 [준비예 49]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 49] was used as the reactant.; HRMS [M]+: 717.26
[합성예 295] Mat 295의 합성[Synthesis Example 295] Synthesis of Mat 295
반응물로 [준비예 50]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 739.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 50] was used as the reactant.; HRMS [M]+: 739.26
[합성예 296] Mat 296의 합성[Synthesis Example 296] Synthesis of Mat 296
반응물로 [준비예 50]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 804.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 50] was used as the reactant.; HRMS [M]+: 804.29
[합성예 297] Mat 297의 합성[Synthesis Example 297] Synthesis of Mat 297
반응물로 [준비예 50]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 50] was used as the reactant.; HRMS [M]+: 679.25
[합성예 298] Mat 298의 합성[Synthesis Example 298] Synthesis of Mat 298
반응물로 [준비예 50]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 728.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 50] was used as the reactant.; HRMS [M]+: 728.26
[합성예 299] Mat 299의 합성[Synthesis Example 299] Synthesis of Mat 299
반응물로 [준비예 50]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 50] was used as the reactant.; HRMS [M]+: 640.23
[합성예 300] Mat 300의 합성[Synthesis Example 300] Synthesis of Mat 300
반응물로 [준비예 50]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 50] was used as the reactant.; HRMS [M]+: 690.24
[합성예 301] Mat 301의 합성[Synthesis Example 301] Synthesis of Mat 301
반응물로 [준비예 51]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 739.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 51] was used as the reactant.; HRMS [M]+: 739.26
[합성예 302] Mat 302의 합성[Synthesis Example 302] Synthesis of Mat 302
반응물로 [준비예 51]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 804.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 51] was used as the reactant.; HRMS [M]+: 804.29
[합성예 303] Mat 303의 합성[Synthesis Example 303] Synthesis of Mat 303
반응물로 [준비예 51]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 51] was used as the reactant.; HRMS [M]+: 679.25
[합성예 304] Mat 304의 합성[Synthesis Example 304] Synthesis of Mat 304
반응물로 [준비예 51]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 738.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 51] was used as the reactant.; HRMS [M]+: 738.26
[합성예 305] Mat 305의 합성[Synthesis Example 305] Synthesis of Mat 305
반응물로 [준비예 51]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 51] was used as the reactant.; HRMS [M]+: 640.23
[합성예 306] Mat 306의 합성[Synthesis Example 306] Synthesis of Mat 306
반응물로 [준비예 51]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 51] was used as the reactant.; HRMS [M]+: 690.24
[합성예 307] Mat 307의 합성[Synthesis Example 307] Synthesis of Mat 307
반응물로 [준비예 52]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 739.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 52] was used as the reactant.; HRMS [M]+: 739.26
[합성예 308] Mat 308의 합성[Synthesis Example 308] Synthesis of Mat 308
반응물로 [준비예 52]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 804.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 52] was used as the reactant.; HRMS [M]+: 804.29
[합성예 309] Mat 309의 합성[Synthesis Example 309] Synthesis of Mat 309
반응물로 [준비예 52]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 52] was used as the reactant.; HRMS [M]+: 679.25
[합성예 310] Mat 310의 합성[Synthesis Example 310] Synthesis of Mat 310
반응물로 [준비예 52]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 728.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 52] was used as the reactant.; HRMS [M]+: 728.26
[합성예 311] Mat 311의 합성[Synthesis Example 311] Synthesis of Mat 311
반응물로 [준비예 52]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 52] was used as the reactant.; HRMS [M]+: 640.23
[합성예 312] Mat 312의 합성[Synthesis Example 312] Synthesis of Mat 312
반응물로 [준비예 52]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 52] was used as the reactant.; HRMS [M]+: 690.24
[합성예 313] Mat 313의 합성[Synthesis Example 313] Synthesis of Mat 313
반응물로 [준비예 53]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 740.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 53] was used as the reactant.; HRMS [M]+: 740.26
[합성예 314] Mat 314의 합성[Synthesis Example 314] Synthesis of Mat 314
반응물로 [준비예 53]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 805.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 53] was used as the reactant.; HRMS [M]+: 805.29
[합성예 315] Mat 315의 합성[Synthesis Example 315] Synthesis of Mat 315
반응물로 [준비예 53]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 53] was used as the reactant.; HRMS [M]+: 680.25
[합성예 316] Mat 316의 합성[Synthesis Example 316] Synthesis of Mat 316
반응물로 [준비예 53]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 729.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 53] was used as the reactant.; HRMS [M]+: 729.26
[합성예 317] Mat 317의 합성[Synthesis Example 317] Synthesis of Mat 317
반응물로 [준비예 53]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 53] was used as the reactant.; HRMS [M]+: 641.23
[합성예 318] Mat 318의 합성[Synthesis Example 318] Synthesis of Mat 318
반응물로 [준비예 53]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 691.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 53] was used as the reactant.; HRMS [M]+: 691.24
[합성예 319] Mat 319의 합성[Synthesis Example 319] Synthesis of Mat 319
반응물로 [준비예 54]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 740.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 54] was used as the reactant.; HRMS [M]+: 740.26
[합성예 320] Mat 320의 합성[Synthesis Example 320] Synthesis of Mat 320
반응물로 [준비예 54]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 805.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 54] was used as the reactant.; HRMS [M]+: 805.29
[합성예 321] Mat 321의 합성[Synthesis Example 321] Synthesis of Mat 321
반응물로 [준비예 54]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 54] was used as the reactant.; HRMS [M]+: 680.25
[합성예 322] Mat 322의 합성[Synthesis Example 322] Synthesis of Mat 322
반응물로 [준비예 54]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 729.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 54] was used as the reactant.; HRMS [M]+: 729.26
[합성예 323] Mat 323의 합성[Synthesis Example 323] Synthesis of Mat 323
반응물로 [준비예 54]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 54] was used as the reactant.; HRMS [M]+: 641.23
[합성예 324] Mat 324의 합성[Synthesis Example 324] Synthesis of Mat 324
반응물로 [준비예 54]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 691.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 54] was used as the reactant.; HRMS [M]+: 691.24
[합성예 325] Mat 325의 합성[Synthesis Example 325] Synthesis of Mat 325
반응물로 [준비예 55]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 727.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 55] was used as the reactant.; HRMS [M]+: 727.25
[합성예 326] Mat 326의 합성[Synthesis Example 326] Synthesis of Mat 326
반응물로 [준비예 55]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 743.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 55] was used as the reactant.; HRMS [M]+: 743.27
[합성예 327] Mat 327의 합성[Synthesis Example 327] Synthesis of Mat 327
반응물로 [준비예 55]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 792.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 55] was used as the reactant.; HRMS [M]+: 792.23
[합성예 328] Mat 328의 합성[Synthesis Example 328] Synthesis of Mat 328
반응물로 [준비예 55]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 55] was used as the reactant.; HRMS [M]+: 717.24
[합성예 329] Mat 329의 합성 [Synthesis Example 329] Synthesis of Mat 329
반응물로 [준비예 55]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 726.27The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 55] was used as the reactant.; HRMS [M]+: 726.27
[합성예 330] Mat 330의 합성[Synthesis Example 330] Synthesis of Mat 330
반응물로 [준비예 55]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 733.25The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 55] was used as the reactant.; HRMS [M]+: 733.25
[합성예 331] Mat 331의 합성[Synthesis Example 331] Synthesis of Mat 331
반응물로 [준비예 56]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 727.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 56] was used as the reactant.; HRMS [M]+: 727.25
[합성예 332] Mat 332의 합성[Synthesis Example 332] Synthesis of Mat 332
반응물로 [준비예 56]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 743.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 56] was used as the reactant.; HRMS [M]+: 743.27
[합성예 333] Mat 333의 합성[Synthesis Example 333] Synthesis of Mat 333
반응물로 [준비예 56]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 792.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 56] was used as the reactant.; HRMS [M]+: 792.23
[합성예 334] Mat 334의 합성[Synthesis Example 334] Synthesis of Mat 334
반응물로 [준비예 56]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 56] was used as the reactant.; HRMS [M]+: 717.24
[합성예 335] Mat 335의 합성[Synthesis Example 335] Synthesis of Mat 335
반응물로 [준비예 56]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 56] was used as the reactant.; HRMS [M]+: 716.21
[합성예 336] Mat 336의 합성[Synthesis Example 336] Synthesis of Mat 336
반응물로 [준비예 56]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 733.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 56] was used as the reactant.; HRMS [M]+: 733.23
[합성예 337] Mat 337의 합성[Synthesis Example 337] Synthesis of Mat 337
반응물로 [준비예 57]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 727.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 57] was used as the reactant.; HRMS [M]+: 727.25
[합성예 338] Mat 338의 합성[Synthesis Example 338] Synthesis of Mat 338
반응물로 [준비예 57]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 743.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 57] was used as the reactant.; HRMS [M]+: 743.27
[합성예 339] Mat 339의 합성[Synthesis Example 339] Synthesis of Mat 339
반응물로 [준비예 57]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 792.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 57] was used as the reactant.; HRMS [M]+: 792.23
[합성예 340] Mat 340의 합성[Synthesis Example 340] Synthesis of Mat 340
반응물로 [준비예 57]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 57] was used as the reactant.; HRMS [M]+: 717.24
[합성예 341] Mat 341의 합성[Synthesis Example 341] Synthesis of Mat 341
반응물로 [준비예 57]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 540.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 57] was used as the reactant.; HRMS [M]+: 540.21
[합성예 342] Mat 342의 합성[Synthesis Example 342] Synthesis of Mat 342
반응물로 [준비예 57]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 57] was used as the reactant.; HRMS [M]+: 716.23
[합성예 343] Mat 343의 합성[Synthesis Example 343] Synthesis of Mat 343
반응물로 [준비예 58]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 727.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 58] was used as the reactant.; HRMS [M]+: 727.25
[합성예 344] Mat 344의 합성[Synthesis Example 344] Synthesis of Mat 344
반응물로 [준비예 58]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 743.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 58] was used as the reactant.; HRMS [M]+: 743.27
[합성예 345] Mat 345의 합성[Synthesis Example 345] Synthesis of Mat 345
반응물로 [준비예 58]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 792.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 58] was used as the reactant.; HRMS [M]+: 792.23
[합성예 346] Mat 346의 합성[Synthesis Example 346] Synthesis of Mat 346
반응물로 [준비예 58]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 58] was used as the reactant.; HRMS [M]+: 716.24
[합성예 347] Mat 347의 합성[Synthesis Example 347] Synthesis of Mat 347
반응물로 [준비예 58]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 58] was used as the reactant.; HRMS [M]+: 716.21
[합성예 348] Mat 348의 합성[Synthesis Example 348] Synthesis of Mat 348
반응물로 [준비예 58]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 733.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 58] was used as the reactant.; HRMS [M]+: 733.23
[합성예 349] Mat 349의 합성[Synthesis Example 349] Synthesis of Mat 349
반응물로 [준비예 59]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 728.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 59] was used as the reactant.; HRMS [M]+: 728.24
[합성예 350] Mat 350의 합성[Synthesis Example 350] Synthesis of Mat 350
반응물로 [준비예 59]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 744.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 59] was used as the reactant.; HRMS [M]+: 744.27
[합성예 351] Mat 351의 합성[Synthesis Example 351] Synthesis of Mat 351
반응물로 [준비예 59]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 59] was used as the reactant.; HRMS [M]+: 793.22
[합성예 352] Mat 352의 합성[Synthesis Example 352] Synthesis of Mat 352
반응물로 [준비예 59]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 718.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 59] was used as the reactant.; HRMS [M]+: 718.24
[합성예 353] Mat 353의 합성[Synthesis Example 353] Synthesis of Mat 353
반응물로 [준비예 59]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 59] was used as the reactant.; HRMS [M]+: 716.21
[합성예 354] Mat 354의 합성[Synthesis Example 354] Synthesis of Mat 354
반응물로 [준비예 59]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 734.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 59] was used as the reactant.; HRMS [M]+: 734.23
[합성예 355] Mat 355의 합성[Synthesis Example 355] Synthesis of Mat 355
반응물로 [준비예 60]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 728.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 60] was used as the reactant.; HRMS [M]+: 728.24
[합성예 356] Mat 356의 합성[Synthesis Example 356] Synthesis of Mat 356
반응물로 [준비예 60]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 744.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 60] was used as the reactant.; HRMS [M]+: 744.27
[합성예 357] Mat 357의 합성[Synthesis Example 357] Synthesis of Mat 357
반응물로 [준비예 60]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 60] was used as the reactant.; HRMS [M]+: 793.22
[합성예 358] Mat 358의 합성[Synthesis Example 358] Synthesis of Mat 358
반응물로 [준비예 60]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 718.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 60] was used as the reactant.; HRMS [M]+: 718.24
[합성예 359] Mat 359의 합성[Synthesis Example 359] Synthesis of Mat 359
반응물로 [준비예 60]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 60] was used as the reactant.; HRMS [M]+: 716.21
[합성예 360] Mat 360의 합성[Synthesis Example 360] Synthesis of Mat 360
반응물로 [준비예 60]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 734.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 60] was used as the reactant.; HRMS [M]+: 734.23
[합성예 361] Mat 361의 합성[Synthesis Example 361] Synthesis of Mat 361
반응물로 [준비예 61]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 728.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 61] was used as the reactant.; HRMS [M]+: 728.24
[합성예 362] Mat 362의 합성[Synthesis Example 362] Synthesis of Mat 362
반응물로 [준비예 61]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 744.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 61] was used as the reactant.; HRMS [M]+: 744.27
[합성예 363] Mat 363의 합성[Synthesis Example 363] Synthesis of Mat 363
반응물로 [준비예 61]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 61] was used as the reactant.; HRMS [M]+: 793.22
[합성예 364] Mat 364의 합성[Synthesis Example 364] Synthesis of Mat 364
반응물로 [준비예 61]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 718.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 61] was used as the reactant.; HRMS [M]+: 718.24
[합성예 365] Mat 365의 합성[Synthesis Example 365] Synthesis of Mat 365
반응물로 [준비예 61]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 816.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 61] was used as the reactant.; HRMS [M]+: 816.21
[합성예 366] Mat 366의 합성[Synthesis Example 366] Synthesis of Mat 366
반응물로 [준비예 61]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 734.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 61] was used as the reactant.; HRMS [M]+: 734.23
[합성예 367] Mat 367의 합성[Synthesis Example 367] Synthesis of Mat 367
반응물로 [준비예 62]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 728.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 62] was used as the reactant.; HRMS [M]+: 728.24
[합성예 368] Mat 368의 합성[Synthesis Example 368] Synthesis of Mat 368
반응물로 [준비예 62]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 744.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 62] was used as the reactant.; HRMS [M]+: 744.27
[합성예 369] Mat 369의 합성[Synthesis Example 369] Synthesis of Mat 369
반응물로 [준비예 62]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 62] was used as the reactant.; HRMS [M]+: 793.22
[합성예 370] Mat 370의 합성[Synthesis Example 370] Synthesis of Mat 370
반응물로 [준비예 62]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 718.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 62] was used as the reactant.; HRMS [M]+: 718.24
[합성예 371] Mat 371의 합성[Synthesis Example 371] Synthesis of Mat 371
반응물로 [준비예 62]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 62] was used as the reactant.; HRMS [M]+: 716.21
[합성예 372] Mat 372의 합성[Synthesis Example 372] Synthesis of Mat 372
반응물로 [준비예 62]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 734.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 62] was used as the reactant.; HRMS [M]+: 734.23
[합성예 373] Mat 373의 합성[Synthesis Example 373] Synthesis of Mat 373
반응물로 [준비예 63]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 803.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 63] was used as the reactant.; HRMS [M]+: 803.28
[합성예 374] Mat 374의 합성[Synthesis Example 374] Synthesis of Mat 374
반응물로 [준비예 63]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 819.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 63] was used as the reactant.; HRMS [M]+: 819.30
[합성예 375] Mat 375의 합성[Synthesis Example 375] Synthesis of Mat 375
반응물로 [준비예 63]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 868.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 63] was used as the reactant.; HRMS [M]+: 868.26
[합성예 376] Mat 376의 합성[Synthesis Example 376] Synthesis of Mat 376
반응물로 [준비예 63]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 63] was used as the reactant.; HRMS [M]+: 793.27
[합성예 377] Mat 377의 합성[Synthesis Example 377] Synthesis of Mat 377
반응물로 [준비예 63]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 792.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 63] was used as the reactant.; HRMS [M]+: 792.24
[합성예 378] Mat 378의 합성[Synthesis Example 378] Synthesis of Mat 378
반응물로 [준비예 63]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 809.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 63] was used as the reactant.; HRMS [M]+: 809.26
[합성예 379] Mat 379의 합성[Synthesis Example 379] Synthesis of Mat 379
반응물로 [준비예 64]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 803.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 64] was used as the reactant.; HRMS [M]+: 803.28
[합성예 380] Mat 380의 합성[Synthesis Example 380] Synthesis of Mat 380
반응물로 [준비예 64]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 819.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 64] was used as the reactant.; HRMS [M]+: 819.30
[합성예 381] Mat 381의 합성[Synthesis Example 381] Synthesis of Mat 381
반응물로 [준비예 64]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 868.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 64] was used as the reactant.; HRMS [M]+: 868.26
[합성예 382] Mat 382의 합성[Synthesis Example 382] Synthesis of Mat 382
반응물로 [준비예 64]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 64] was used as the reactant.; HRMS [M]+: 793.27
[합성예 383] Mat 383의 합성[Synthesis Example 383] Synthesis of Mat 383
반응물로 [준비예 64]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 792.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 64] was used as the reactant.; HRMS [M]+: 792.24
[합성예 384] Mat 384의 합성[Synthesis Example 384] Synthesis of Mat 384
반응물로 [준비예 64]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 809.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 64] was used as the reactant.; HRMS [M]+: 809.26
[합성예 385] Mat 385의 합성[Synthesis Example 385] Synthesis of Mat 385
반응물로 [준비예 65]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 804.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 65] was used as the reactant.; HRMS [M]+: 804.28
[합성예 386] Mat 386의 합성[Synthesis Example 386] Synthesis of Mat 386
반응물로 [준비예 65]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 820.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 65] was used as the reactant.; HRMS [M]+: 820.30
[합성예 387] Mat 387의 합성[Synthesis Example 387] Synthesis of Mat 387
반응물로 [준비예 65]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 869.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 65] was used as the reactant.; HRMS [M]+: 869.26
[합성예 388] Mat 388의 합성[Synthesis Example 388] Synthesis of Mat 388
반응물로 [준비예 65]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 65] was used as the reactant.; HRMS [M]+: 794.27
[합성예 389] Mat 389의 합성[Synthesis Example 389] Synthesis of Mat 389
반응물로 [준비예 65]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 65] was used as the reactant.; HRMS [M]+: 793.24
[합성예 390] Mat 390의 합성[Synthesis Example 390] Synthesis of Mat 390
반응물로 [준비예 65]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 810.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 65] was used as the reactant.; HRMS [M]+: 810.26
[합성예 391] Mat 391의 합성[Synthesis Example 391] Synthesis of Mat 391
반응물로 [준비예 66]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 804.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 66] was used as the reactant.; HRMS [M]+: 804.28
[합성예 392] Mat 392의 합성[Synthesis Example 392] Synthesis of Mat 392
반응물로 [준비예 66]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 820.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 66] was used as the reactant.; HRMS [M]+: 820.30
[합성예 393] Mat 393의 합성[Synthesis Example 393] Synthesis of Mat 393
반응물로 [준비예 66]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 869.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 66] was used as the reactant.; HRMS [M]+: 869.26
[합성예 394] Mat 394의 합성[Synthesis Example 394] Synthesis of Mat 394
반응물로 [준비예 66]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 66] was used as the reactant.; HRMS [M]+: 794.27
[합성예 395] Mat 395의 합성[Synthesis Example 395] Synthesis of Mat 395
반응물로 [준비예 66]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 66] was used as the reactant.; HRMS [M]+: 793.24
[합성예 396] Mat 396의 합성[Synthesis Example 396] Synthesis of Mat 396
반응물로 [준비예 66]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 810.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 66] was used as the reactant.; HRMS [M]+: 810.26
[합성예 397] Mat 397의 합성[Synthesis Example 397] Synthesis of Mat 397
반응물로 [준비예 67]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 804.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 67] was used as the reactant.; HRMS [M]+: 804.28
[합성예 398] Mat 398의 합성[Synthesis Example 398] Synthesis of Mat 398
반응물로 [준비예 67]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 820.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 67] was used as the reactant.; HRMS [M]+: 820.30
[합성예 399] Mat 399의 합성[Synthesis Example 399] Synthesis of Mat 399
반응물로 [준비예 67]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 869.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 67] was used as the reactant.; HRMS [M]+: 869.26
[합성예 400] Mat 400의 합성[Synthesis Example 400] Synthesis of Mat 400
반응물로 [준비예 67]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 67] was used as the reactant.; HRMS [M]+: 794.27
[합성예 401] Mat 401의 합성[Synthesis Example 401] Synthesis of Mat 401
반응물로 [준비예 67]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 67] was used as the reactant.; HRMS [M]+: 793.24
[합성예 402] Mat 402의 합성[Synthesis Example 402] Synthesis of Mat 402
반응물로 [준비예 67]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 810.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 67] was used as the reactant.; HRMS [M]+: 810.26
[합성예 403] Mat 403의 합성[Synthesis Example 403] Synthesis of Mat 403
반응물로 [준비예 68]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 777.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 68] was used as the reactant.; HRMS [M]+: 777.26
[합성예 404] Mat 404의 합성[Synthesis Example 404] Synthesis of Mat 404
반응물로 [준비예 68]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 68] was used as the reactant.; HRMS [M]+: 793.29
[합성예 405] Mat 405의 합성[Synthesis Example 405] Synthesis of Mat 405
반응물로 [준비예 68]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 842.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 68] was used as the reactant.; HRMS [M]+: 842.25
[합성예 406] Mat 406의 합성[Synthesis Example 406] Synthesis of Mat 406
반응물로 [준비예 68]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 767.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 68] was used as the reactant.; HRMS [M]+: 767.26
[합성예 407] Mat 407의 합성[Synthesis Example 407] Synthesis of Mat 407
반응물로 [준비예 68]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 766.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 68] was used as the reactant.; HRMS [M]+: 766.23
[합성예 408] Mat 408의 합성[Synthesis Example 408] Synthesis of Mat 408
반응물로 [준비예 68]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 733.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 68] was used as the reactant.; HRMS [M]+: 733.24
[합성예 409] Mat 409의 합성[Synthesis Example 409] Synthesis of Mat 409
반응물로 [준비예 69]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 777.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 69] was used as the reactant.; HRMS [M]+: 777.26
[합성예 410] Mat 410의 합성[Synthesis Example 410] Synthesis of Mat 410
반응물로 [준비예 69]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 69] was used as the reactant.; HRMS [M]+: 793.29
[합성예 411] Mat 411의 합성[Synthesis Example 411] Synthesis of Mat 411
반응물로 [준비예 69]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 842.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 69] was used as the reactant.; HRMS [M]+: 842.25
[합성예 412] Mat 412의 합성[Synthesis Example 412] Synthesis of Mat 412
반응물로 [준비예 69]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 767.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 69] was used as the reactant.; HRMS [M]+: 767.26
[합성예 413] Mat 413의 합성[Synthesis Example 413] Synthesis of Mat 413
반응물로 [준비예 69]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 766.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 69] was used as the reactant.; HRMS [M]+: 766.23
[합성예 414] Mat 414의 합성[Synthesis Example 414] Synthesis of Mat 414
반응물로 [준비예 69]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 733.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 69] was used as the reactant.; HRMS [M]+: 733.24
[합성예 415] Mat 415의 합성[Synthesis Example 415] Synthesis of Mat 415
반응물로 [준비예 70]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 777.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 70] was used as the reactant.; HRMS [M]+: 777.26
[합성예 416] Mat 416의 합성[Synthesis Example 416] Synthesis of Mat 416
반응물로 [준비예 70]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 70] was used as the reactant.; HRMS [M]+: 793.29
[합성예 417] Mat 417의 합성[Synthesis Example 417] Synthesis of Mat 417
반응물로 [준비예 70]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 842.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 70] was used as the reactant.; HRMS [M]+: 842.25
[합성예 418] Mat 418의 합성[Synthesis Example 418] Synthesis of Mat 418
반응물로 [준비예 70]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 767.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 70] was used as the reactant.; HRMS [M]+: 767.26
[합성예 419] Mat 419의 합성[Synthesis Example 419] Synthesis of Mat 419
반응물로 [준비예 70]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 766.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 70] was used as the reactant.; HRMS [M]+: 766.23
[합성예 420] Mat 420의 합성[Synthesis Example 420] Synthesis of Mat 420
반응물로 [준비예 70]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 733.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 70] was used as the reactant.; HRMS [M]+: 733.24
[합성예 421] Mat 421의 합성[Synthesis Example 421] Synthesis of Mat 421
반응물로 [준비예 71]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 778.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 71] was used as the reactant.; HRMS [M]+: 778.26
[합성예 422] Mat 422의 합성[Synthesis Example 422] Synthesis of Mat 422
반응물로 [준비예 71]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 71] was used as the reactant.; HRMS [M]+: 794.29
[합성예 423] Mat 423의 합성[Synthesis Example 423] Synthesis of Mat 423
반응물로 [준비예 71]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 843.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 71] was used as the reactant.; HRMS [M]+: 843.25
[합성예 424] Mat 424의 합성[Synthesis Example 424] Synthesis of Mat 424
반응물로 [준비예 71]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 768.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 71] was used as the reactant.; HRMS [M]+: 768.26
[합성예 425] Mat 425의 합성[Synthesis Example 425] Synthesis of Mat 425
반응물로 [준비예 71]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 767.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 71] was used as the reactant.; HRMS [M]+: 767.23
[합성예 426] Mat 426의 합성[Synthesis Example 426] Synthesis of Mat 426
반응물로 [준비예 71]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 734.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 71] was used as the reactant.; HRMS [M]+: 734.24
[합성예 427] Mat 427의 합성[Synthesis Example 427] Synthesis of Mat 427
반응물로 [준비예 72]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 778.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 72] was used as the reactant.; HRMS [M]+: 778.26
[합성예 428] Mat 428의 합성[Synthesis Example 428] Synthesis of Mat 428
반응물로 [준비예 72]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 72] was used as the reactant.; HRMS [M]+: 794.29
[합성예 429] Mat 429의 합성[Synthesis Example 429] Synthesis of Mat 429
반응물로 [준비예 72]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 843.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 72] was used as the reactant.; HRMS [M]+: 843.25
[합성예 430] Mat 430의 합성[Synthesis Example 430] Synthesis of Mat 430
반응물로 [준비예 72]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 768.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 72] was used as the reactant.; HRMS [M]+: 768.26
[합성예 431] Mat 431의 합성[Synthesis Example 431] Synthesis of Mat 431
반응물로 [준비예 72]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 767.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 72] was used as the reactant.; HRMS [M]+: 767.23
[합성예 432] Mat 432의 합성[Synthesis Example 432] Synthesis of Mat 432
반응물로 [준비예 72]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 734.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 72] was used as the reactant.; HRMS [M]+: 734.24
[합성예 433] Mat 433의 합성[Synthesis Example 433] Synthesis of Mat 433
반응물로 [준비예 73]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 73] was used as the reactant.; HRMS [M]+: 640.24
[합성예 434] Mat 434의 합성[Synthesis Example 434] Synthesis of Mat 434
반응물로 [준비예 73]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 73] was used as the reactant.; HRMS [M]+: 705.27
[합성예 435] Mat 435의 합성[Synthesis Example 435] Synthesis of Mat 435
반응물로 [준비예 73]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 73] was used as the reactant.; HRMS [M]+: 630.23
[합성예 436] Mat 436의 합성[Synthesis Example 436] Synthesis of Mat 436
반응물로 [준비예 73]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 729.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 73] was used as the reactant.; HRMS [M]+: 729.27
[합성예 437] Mat 437의 합성[Synthesis Example 437] Synthesis of Mat 437
반응물로 [준비예 73]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 73] was used as the reactant.; HRMS [M]+: 541.21
[합성예 438] Mat 438의 합성[Synthesis Example 438] Synthesis of Mat 438
반응물로 [준비예 73]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 73] was used as the reactant.; HRMS [M]+: 591.23
[합성예 439] Mat 439의 합성[Synthesis Example 439] Synthesis of Mat 439
반응물로 [준비예 74]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 74] was used as the reactant.; HRMS [M]+: 640.25
[합성예 440] Mat 440의 합성[Synthesis Example 440] Synthesis of Mat 440
반응물로 [준비예 74]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 74] was used as the reactant.; HRMS [M]+: 705.27
[합성예 441] Mat 441의 합성[Synthesis Example 441] Synthesis of Mat 441
반응물로 [준비예 74]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 74] was used as the reactant.; HRMS [M]+: 630.23
[합성예 442] Mat 442의 합성[Synthesis Example 442] Synthesis of Mat 442
반응물로 [준비예 74]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 74] was used as the reactant.; HRMS [M]+: 629.24
[합성예 443] Mat 443의 합성[Synthesis Example 443] Synthesis of Mat 443
반응물로 [준비예 74]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 74] was used as the reactant.; HRMS [M]+: 541.21
[합성예 444] Mat 444의 합성[Synthesis Example 444] Synthesis of Mat 444
반응물로 [준비예 74]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 74] was used as the reactant.; HRMS [M]+: 591.23
[합성예 445] Mat 445의 합성[Synthesis Example 445] Synthesis of Mat 445
반응물로 [준비예 75]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 75] was used as the reactant.; HRMS [M]+: 640.25
[합성예 446] Mat 446의 합성[Synthesis Example 446] Synthesis of Mat 446
반응물로 [준비예 75]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 75] was used as the reactant.; HRMS [M]+: 705.27
[합성예 447] Mat 447의 합성[Synthesis Example 447] Synthesis of Mat 447
반응물로 [준비예 75]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 75] was used as the reactant.; HRMS [M]+: 630.23
[합성예 448] Mat 448의 합성[Synthesis Example 448] Synthesis of Mat 448
반응물로 [준비예 75]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 75] was used as the reactant.; HRMS [M]+: 629.24
[합성예 449] Mat 449의 합성[Synthesis Example 449] Synthesis of Mat 449
반응물로 [준비예 75]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 75] was used as the reactant.; HRMS [M]+: 541.21
[합성예 450] Mat 450의 합성[Synthesis Example 450] Synthesis of Mat 450
반응물로 [준비예 75]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 75] was used as the reactant.; HRMS [M]+: 591.23
[합성예 451] Mat 451의 합성[Synthesis Example 451] Synthesis of Mat 451
반응물로 [준비예 76]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 76] was used as the reactant.; HRMS [M]+: 640.25
[합성예 452] Mat 452의 합성[Synthesis Example 452] Synthesis of Mat 452
반응물로 [준비예 76]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 76] was used as the reactant.; HRMS [M]+: 705.27
[합성예 453] Mat 453의 합성[Synthesis Example 453] Synthesis of Mat 453
반응물로 [준비예 76]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 76] was used as the reactant.; HRMS [M]+: 630.23
[합성예 454] Mat 454의 합성[Synthesis Example 454] Synthesis of Mat 454
반응물로 [준비예 76]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 76] was used as the reactant.; HRMS [M]+: 629.24
[합성예 455] Mat 455의 합성[Synthesis Example 455] Synthesis of Mat 455
반응물로 [준비예 76]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 76] was used as the reactant.; HRMS [M]+: 541.21
[합성예 456] Mat 456의 합성[Synthesis Example 456] Synthesis of Mat 456
반응물로 [준비예 76]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 76] was used as the reactant.; HRMS [M]+: 591.23
[합성예 457] Mat 457의 합성[Synthesis Example 457] Synthesis of Mat 457
반응물로 [준비예 77]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 77] was used as the reactant.; HRMS [M]+: 641.24
[합성예 458] Mat 458의 합성[Synthesis Example 458] Synthesis of Mat 458
반응물로 [준비예 77]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 77] was used as the reactant.; HRMS [M]+: 706.27
[합성예 459] Mat 459의 합성[Synthesis Example 459] Synthesis of Mat 459
반응물로 [준비예 77]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 631.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 77] was used as the reactant.; HRMS [M]+: 631.22
[합성예 460] Mat 460의 합성[Synthesis Example 460] Synthesis of Mat 460
반응물로 [준비예 77]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 77] was used as the reactant.; HRMS [M]+: 630.24
[합성예 461] Mat 461의 합성[Synthesis Example 461] Synthesis of Mat 461
반응물로 [준비예 77]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 542.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 77] was used as the reactant.; HRMS [M]+: 542.21
[합성예 462] Mat 462의 합성[Synthesis Example 462] Synthesis of Mat 462
반응물로 [준비예 77]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 77] was used as the reactant.; HRMS [M]+: 592.23
[합성예 463] Mat 463의 합성[Synthesis Example 463] Synthesis of Mat 463
반응물로 [준비예 78]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 78] was used as the reactant.; HRMS [M]+: 641.24
[합성예 464] Mat 464의 합성[Synthesis Example 464] Synthesis of Mat 464
반응물로 [준비예 78]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 78] was used as the reactant.; HRMS [M]+: 706.27
[합성예 465] Mat 465의 합성[Synthesis Example 465] Synthesis of Mat 465
반응물로 [준비예 78]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 631.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 78] was used as the reactant.; HRMS [M]+: 631.22
[합성예 466] Mat 466의 합성[Synthesis Example 466] Synthesis of Mat 466
반응물로 [준비예 78]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 78] was used as the reactant.; HRMS [M]+: 630.24
[합성예 467] Mat 467의 합성[Synthesis Example 467] Synthesis of Mat 467
반응물로 [준비예 78]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 542.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 78] was used as the reactant.; HRMS [M]+: 542.21
[합성예 468] Mat 468의 합성[Synthesis Example 468] Synthesis of Mat 468
반응물로 [준비예 78]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 78] was used as the reactant.; HRMS [M]+: 592.23
[합성예 469] Mat 469의 합성[Synthesis Example 469] Synthesis of Mat 469
반응물로 [준비예 79]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 79] was used as the reactant.; HRMS [M]+: 641.24
[합성예 470] Mat 470의 합성[Synthesis Example 470] Synthesis of Mat 470
반응물로 [준비예 79]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 79] was used as the reactant.; HRMS [M]+: 706.27
[합성예 471] Mat 471의 합성[Synthesis Example 471] Synthesis of Mat 471
반응물로 [준비예 79]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 631.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 79] was used as the reactant.; HRMS [M]+: 631.22
[합성예 472] Mat 472의 합성[Synthesis Example 472] Synthesis of Mat 472
반응물로 [준비예 79]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 79] was used as the reactant.; HRMS [M]+: 630.24
[합성예 473] Mat 473의 합성[Synthesis Example 473] Synthesis of Mat 473
반응물로 [준비예 79]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 542.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 79] was used as the reactant.; HRMS [M]+: 542.21
[합성예 474] Mat 474의 합성[Synthesis Example 474] Synthesis of Mat 474
반응물로 [준비예 79]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 79] was used as the reactant.; HRMS [M]+: 592.23
[합성예 475] Mat 475의 합성[Synthesis Example 475] Synthesis of Mat 475
반응물로 [준비예 80]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 80] was used as the reactant.; HRMS [M]+: 641.24
[합성예 476] Mat 476의 합성[Synthesis Example 476] Synthesis of Mat 476
반응물로 [준비예 80]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 80] was used as the reactant.; HRMS [M]+: 706.27
[합성예 477] Mat 477의 합성[Synthesis Example 477] Synthesis of Mat 477
반응물로 [준비예 80]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 631.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 80] was used as the reactant.; HRMS [M]+: 631.22
[합성예 478] Mat 478의 합성[Synthesis Example 478] Synthesis of Mat 478
반응물로 [준비예 80]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 80] was used as the reactant.; HRMS [M]+: 630.24
[합성예 479] Mat 479의 합성[Synthesis Example 479] Synthesis of Mat 479
반응물로 [준비예 80]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 542.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 80] was used as the reactant.; HRMS [M]+: 542.21
[합성예 480] Mat 480의 합성[Synthesis Example 480] Synthesis of Mat 480
반응물로 [준비예 80]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 80] was used as the reactant.; HRMS [M]+: 592.23
[합성예 481] Mat 481의 합성[Synthesis Example 481] Synthesis of Mat 481
반응물로 [준비예 81]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 81] was used as the reactant.; HRMS [M]+: 716.28
[합성예 482] Mat 482의 합성[Synthesis Example 482] Synthesis of Mat 482
반응물로 [준비예 81]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 781.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 81] was used as the reactant.; HRMS [M]+: 781.30
[합성예 483] Mat 483의 합성[Synthesis Example 483] Synthesis of Mat 483
반응물로 [준비예 81]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 81] was used as the reactant.; HRMS [M]+: 706.26
[합성예 484] Mat 484의 합성[Synthesis Example 484] Synthesis of Mat 484
반응물로 [준비예 81]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 81] was used as the reactant.; HRMS [M]+: 705.27
[합성예 485] Mat 485의 합성[Synthesis Example 485] Synthesis of Mat 485
반응물로 [준비예 81]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 617.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 81] was used as the reactant.; HRMS [M]+: 617.24
[합성예 486] Mat 486의 합성[Synthesis Example 486] Synthesis of Mat 486
반응물로 [준비예 81]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 81] was used as the reactant.; HRMS [M]+: 667.26
[합성예 487] Mat 487의 합성[Synthesis Example 487] Synthesis of Mat 487
반응물로 [준비예 82]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 82] was used as the reactant.; HRMS [M]+: 716.28
[합성예 488] Mat 488의 합성[Synthesis Example 488] Synthesis of Mat 488
반응물로 [준비예 82]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 781.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 82] was used as the reactant.; HRMS [M]+: 781.30
[합성예 489] Mat 489의 합성[Synthesis Example 489] Synthesis of Mat 489
반응물로 [준비예 82]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 82] was used as the reactant.; HRMS [M]+: 706.26
[합성예 490] Mat 490의 합성[Synthesis Example 490] Synthesis of Mat 490
반응물로 [준비예 82]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 82] was used as the reactant.; HRMS [M]+: 705.27
[합성예 491] Mat 491의 합성[Synthesis Example 491] Synthesis of Mat 491
반응물로 [준비예 82]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 617.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 82] was used as the reactant.; HRMS [M]+: 617.24
[합성예 492] Mat 492의 합성[Synthesis Example 492] Synthesis of Mat 492
반응물로 [준비예 82]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 82] was used as the reactant.; HRMS [M]+: 667.26
[합성예 493] Mat 493의 합성[Synthesis Example 493] Synthesis of Mat 493
반응물로 [준비예 83]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 83] was used as the reactant.; HRMS [M]+: 717.28
[합성예 494] Mat 494의 합성[Synthesis Example 494] Synthesis of Mat 494
반응물로 [준비예 83]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 782.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 83] was used as the reactant.; HRMS [M]+: 782.30
[합성예 495] Mat 495의 합성[Synthesis Example 495] Synthesis of Mat 495
반응물로 [준비예 83]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 707.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 83] was used as the reactant.; HRMS [M]+: 707.26
[합성예 496] Mat 496의 합성[Synthesis Example 496] Synthesis of Mat 496
반응물로 [준비예 83]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 83] was used as the reactant.; HRMS [M]+: 706.27
[합성예 497] Mat 497의 합성[Synthesis Example 497] Synthesis of Mat 497
반응물로 [준비예 83]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 618.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 83] was used as the reactant.; HRMS [M]+: 618.24
[합성예 498] Mat 498의 합성[Synthesis Example 498] Synthesis of Mat 498
반응물로 [준비예 83]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 668.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 83] was used as the reactant.; HRMS [M]+: 668.26
[합성예 499] Mat 499의 합성[Synthesis Example 499] Synthesis of Mat 499
반응물로 [준비예 84]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 84] was used as the reactant.; HRMS [M]+: 717.28
[합성예 500] Mat 500의 합성[Synthesis Example 500] Synthesis of Mat 500
반응물로 [준비예 84]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 782.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 84] was used as the reactant.; HRMS [M]+: 782.30
[합성예 501] Mat 501의 합성[Synthesis Example 501] Synthesis of Mat 501
반응물로 [준비예 84]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 707.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 84] was used as the reactant.; HRMS [M]+: 707.26
[합성예 502] Mat 502의 합성[Synthesis Example 502] Synthesis of Mat 502
반응물로 [준비예 84]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 84] was used as the reactant.; HRMS [M]+: 706.27
[합성예 503] Mat 503의 합성[Synthesis Example 503] Synthesis of Mat 503
반응물로 [준비예 84]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 618.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 84] was used as the reactant.; HRMS [M]+: 618.24
[합성예 504] Mat 504의 합성[Synthesis Example 504] Synthesis of Mat 504
반응물로 [준비예 84]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 668.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 84] was used as the reactant.; HRMS [M]+: 668.26
[합성예 505] Mat 505의 합성[Synthesis Example 505] Synthesis of Mat 505
반응물로 [준비예 85]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 85] was used as the reactant.; HRMS [M]+: 717.28
[합성예 506] Mat 506의 합성[Synthesis Example 506] Synthesis of Mat 506
반응물로 [준비예 85]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 782.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 85] was used as the reactant.; HRMS [M]+: 782.30
[합성예 507] Mat 507의 합성[Synthesis Example 507] Synthesis of Mat 507
반응물로 [준비예 85]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 707.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 85] was used as the reactant.; HRMS [M]+: 707.26
[합성예 508] Mat 508의 합성[Synthesis Example 508] Synthesis of Mat 508
반응물로 [준비예 85]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 85] was used as the reactant.; HRMS [M]+: 706.27
[합성예 509] Mat 509의 합성[Synthesis Example 509] Synthesis of Mat 509
반응물로 [준비예 85]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 618.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 85] was used as the reactant.; HRMS [M]+: 618.24
[합성예 510] Mat 510의 합성[Synthesis Example 510] Synthesis of Mat 510
반응물로 [준비예 85]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 668.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 85] was used as the reactant.; HRMS [M]+: 668.26
[합성예 511] Mat 511의 합성[Synthesis Example 511] Synthesis of Mat 511
반응물로 [준비예 86]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 86] was used as the reactant.; HRMS [M]+: 690.26
[합성예 512] Mat 512의 합성[Synthesis Example 512] Synthesis of Mat 512
반응물로 [준비예 86]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 86] was used as the reactant.; HRMS [M]+: 755.29
[합성예 513] Mat 513의 합성[Synthesis Example 513] Synthesis of Mat 513
반응물로 [준비예 86]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 86] was used as the reactant.; HRMS [M]+: 630.25
[합성예 514] Mat 514의 합성[Synthesis Example 514] Synthesis of Mat 514
반응물로 [준비예 86]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 86] was used as the reactant.; HRMS [M]+: 679.26
[합성예 515] Mat 515의 합성[Synthesis Example 515] Synthesis of Mat 515
반응물로 [준비예 86]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 86] was used as the reactant.; HRMS [M]+: 591.23
[합성예 516] Mat 516의 합성[Synthesis Example 516] Synthesis of Mat 516
반응물로 [준비예 86]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 86] was used as the reactant.; HRMS [M]+: 641.24
[합성예 517] Mat 517의 합성[Synthesis Example 517] Synthesis of Mat 517
반응물로 [준비예 87]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 87] was used as the reactant.; HRMS [M]+: 690.26
[합성예 518] Mat 518의 합성[Synthesis Example 518] Synthesis of Mat 518
반응물로 [준비예 87]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 87] was used as the reactant.; HRMS [M]+: 755.29
[합성예 519] Mat 519의 합성[Synthesis Example 519] Synthesis of Mat 519
반응물로 [준비예 87]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 87] was used as the reactant.; HRMS [M]+: 630.25
[합성예 520] Mat 520의 합성[Synthesis Example 520] Synthesis of Mat 520
반응물로 [준비예 87]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 87] was used as the reactant.; HRMS [M]+: 679.26
[합성예 521] Mat 521의 합성[Synthesis Example 521] Synthesis of Mat 521
반응물로 [준비예 87]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 87] was used as the reactant.; HRMS [M]+: 591.23
[합성예 522] Mat 522의 합성[Synthesis Example 522] Synthesis of Mat 522
반응물로 [준비예 87]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 87] was used as the reactant.; HRMS [M]+: 641.24
[합성예 523] Mat 523의 합성[Synthesis Example 523] Synthesis of Mat 523
반응물로 [준비예 88]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 88] was used as the reactant.; HRMS [M]+: 690.26
[합성예 524] Mat 524의 합성[Synthesis Example 524] Synthesis of Mat 524
반응물로 [준비예 88]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 88] was used as the reactant.; HRMS [M]+: 755.29
[합성예 525] Mat 525의 합성[Synthesis Example 525] Synthesis of Mat 525
반응물로 [준비예 88]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 88] was used as the reactant.; HRMS [M]+: 630.25
[합성예 526] Mat 526의 합성[Synthesis Example 526] Synthesis of Mat 526
반응물로 [준비예 88]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 88] was used as the reactant.; HRMS [M]+: 679.26
[합성예 527] Mat 527의 합성[Synthesis Example 527] Synthesis of Mat 527
반응물로 [준비예 88]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 88] was used as the reactant.; HRMS [M]+: 591.23
[합성예 528] Mat 528의 합성[Synthesis Example 528] Synthesis of Mat 528
반응물로 [준비예 88]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 88] was used as the reactant.; HRMS [M]+: 641.24
[합성예 529] Mat 529의 합성[Synthesis Example 529] Synthesis of Mat 529
반응물로 [준비예 89]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 691.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 89] was used as the reactant.; HRMS [M]+: 691.26
[합성예 530] Mat 530의 합성[Synthesis Example 530] Synthesis of Mat 530
반응물로 [준비예 89]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 89] was used as the reactant.; HRMS [M]+: 756.29
[합성예 531] Mat 531의 합성[Synthesis Example 531] Synthesis of Mat 531
반응물로 [준비예 89]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 631.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 89] was used as the reactant.; HRMS [M]+: 631.25
[합성예 532] Mat 532의 합성[Synthesis Example 532] Synthesis of Mat 532
반응물로 [준비예 89]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 89] was used as the reactant.; HRMS [M]+: 680.26
[합성예 533] Mat 533의 합성[Synthesis Example 533] Synthesis of Mat 533
반응물로 [준비예 89]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 89] was used as the reactant.; HRMS [M]+: 592.23
[합성예 534] Mat 534의 합성[Synthesis Example 534] Synthesis of Mat 534
반응물로 [준비예 89]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 642.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 89] was used as the reactant.; HRMS [M]+: 642.24
[합성예 535] Mat 535의 합성[Synthesis Example 535] Synthesis of Mat 535
반응물로 [준비예 90]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 691.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 90] was used as the reactant.; HRMS [M]+: 691.26
[합성예 536] Mat 536의 합성[Synthesis Example 536] Synthesis of Mat 536
반응물로 [준비예 90]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 90] was used as the reactant.; HRMS [M]+: 756.29
[합성예 537] Mat 537의 합성[Synthesis Example 537] Synthesis of Mat 537
반응물로 [준비예 90]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 631.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 90] was used as the reactant.; HRMS [M]+: 631.25
[합성예 538] Mat 538의 합성[Synthesis Example 538] Synthesis of Mat 538
반응물로 [준비예 90]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 90] was used as the reactant.; HRMS [M]+: 680.26
[합성예 539] Mat 539의 합성[Synthesis Example 539] Synthesis of Mat 539
반응물로 [준비예 90]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 90] was used as the reactant.; HRMS [M]+: 592.23
[합성예 540] Mat 540의 합성[Synthesis Example 540] Synthesis of Mat 540
반응물로 [준비예 90]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 642.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 90] was used as the reactant.; HRMS [M]+: 642.24
[합성예 541] Mat 541의 합성[Synthesis Example 541] Synthesis of Mat 541
반응물로 [준비예 91]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 91] was used as the reactant.; HRMS [M]+: 640.25
[합성예 542] Mat 542의 합성[Synthesis Example 542] Synthesis of Mat 542
반응물로 [준비예 91]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 91] was used as the reactant.; HRMS [M]+: 705.27
[합성예 543] Mat 543의 합성[Synthesis Example 543] Synthesis of Mat 543
반응물로 [준비예 91]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 91] was used as the reactant.; HRMS [M]+: 630.23
[합성예 544] Mat 544의 합성[Synthesis Example 544] Synthesis of Mat 544
반응물로 [준비예 91]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 91] was used as the reactant.; HRMS [M]+: 629.24
[합성예 545] Mat 545의 합성[Synthesis Example 545] Synthesis of Mat 545
반응물로 [준비예 91]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 91] was used as the reactant.; HRMS [M]+: 541.21
[합성예 546] Mat 546의 합성[Synthesis Example 546] Synthesis of Mat 546
반응물로 [준비예 91]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 91] was used as the reactant.; HRMS [M]+: 591.23
[합성예 547] Mat 547의 합성[Synthesis Example 547] Synthesis of Mat 547
반응물로 [준비예 92]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 92] was used as the reactant.; HRMS [M]+: 640.25
[합성예 548] Mat 548의 합성[Synthesis Example 548] Synthesis of Mat 548
반응물로 [준비예 92]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 92] was used as the reactant.; HRMS [M]+: 705.27
[합성예 549] Mat 549의 합성[Synthesis Example 549] Synthesis of Mat 549
반응물로 [준비예 92]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 92] was used as the reactant.; HRMS [M]+: 630.23
[합성예 550] Mat 550의 합성[Synthesis Example 550] Synthesis of Mat 550
반응물로 [준비예 92]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 92] was used as the reactant.; HRMS [M]+: 629.24
[합성예 551] Mat 551의 합성[Synthesis Example 551] Synthesis of Mat 551
반응물로 [준비예 92]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 92] was used as the reactant.; HRMS [M]+: 541.21
[합성예 552] Mat 552의 합성[Synthesis Example 552] Synthesis of Mat 552
반응물로 [준비예 92]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 92] was used as the reactant.; HRMS [M]+: 591.23
[합성예 553] Mat 553의 합성[Synthesis Example 553] Synthesis of Mat 553
반응물로 [준비예 93]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 93] was used as the reactant.; HRMS [M]+: 640.25
[합성예 554] Mat 554의 합성[Synthesis Example 554] Synthesis of Mat 554
반응물로 [준비예 93]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 93] was used as the reactant.; HRMS [M]+: 705.27
[합성예 555] Mat 555의 합성[Synthesis Example 555] Synthesis of Mat 555
반응물로 [준비예 93]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 93] was used as the reactant.; HRMS [M]+: 630.23
[합성예 556] Mat 556의 합성[Synthesis Example 556] Synthesis of Mat 556
반응물로 [준비예 93]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 93] was used as the reactant.; HRMS [M]+: 629.24
[합성예 557] Mat 557의 합성[Synthesis Example 557] Synthesis of Mat 557
반응물로 [준비예 93]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 93] was used as the reactant.; HRMS [M]+: 541.21
[합성예 558] Mat 558의 합성[Synthesis Example 558] Synthesis of Mat 558
반응물로 [준비예 93]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 93] was used as the reactant.; HRMS [M]+: 591.23
[합성예 559] Mat 559의 합성[Synthesis Example 559] Synthesis of Mat 559
반응물로 [준비예 94]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 640.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 94] was used as the reactant.; HRMS [M]+: 640.25
[합성예 560] Mat 560의 합성[Synthesis Example 560] Synthesis of Mat 560
반응물로 [준비예 94]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 94] was used as the reactant.; HRMS [M]+: 705.27
[합성예 561] Mat 561의 합성[Synthesis Example 561] Synthesis of Mat 561
반응물로 [준비예 94]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 94] was used as the reactant.; HRMS [M]+: 630.23
[합성예 562] Mat 562의 합성[Synthesis Example 562] Synthesis of Mat 562
반응물로 [준비예 94]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 629.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 94] was used as the reactant.; HRMS [M]+: 629.24
[합성예 563] Mat 563의 합성[Synthesis Example 563] Synthesis of Mat 563
반응물로 [준비예 94]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 94] was used as the reactant.; HRMS [M]+: 541.21
[합성예 564] Mat 564의 합성[Synthesis Example 564] Synthesis of Mat 564
반응물로 [준비예 94]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 94] was used as the reactant.; HRMS [M]+: 591.23
[합성예 565] Mat 565의 합성[Synthesis Example 565] Synthesis of Mat 565
반응물로 [준비예 95]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 95] was used as the reactant.; HRMS [M]+: 641.24
[합성예 566] Mat 566의 합성[Synthesis Example 566] Synthesis of Mat 566
반응물로 [준비예 95]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 95] was used as the reactant.; HRMS [M]+: 706.27
[합성예 567] Mat 567의 합성[Synthesis Example 567] Synthesis of Mat 567
반응물로 [준비예 95]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 631.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 95] was used as the reactant.; HRMS [M]+: 631.22
[합성예 568] Mat 568의 합성[Synthesis Example 568] Synthesis of Mat 568
반응물로 [준비예 95]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 95] was used as the reactant.; HRMS [M]+: 630.24
[합성예 569] Mat 569의 합성[Synthesis Example 569] Synthesis of Mat 569
반응물로 [준비예 95]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 542.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 95] was used as the reactant.; HRMS [M]+: 542.21
[합성예 570] Mat 570의 합성[Synthesis Example 570] Synthesis of Mat 570
반응물로 [준비예 95]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 95] was used as the reactant.; HRMS [M]+: 592.23
[합성예 571] Mat 571의 합성[Synthesis Example 571] Synthesis of Mat 571
반응물로 [준비예 96]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 96] was used as the reactant.; HRMS [M]+: 641.24
[합성예 572] Mat 572의 합성[Synthesis Example 572] Synthesis of Mat 572
반응물로 [준비예 96]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 96] was used as the reactant.; HRMS [M]+: 706.27
[합성예 573] Mat 573의 합성[Synthesis Example 573] Synthesis of Mat 573
반응물로 [준비예 96]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 631.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 96] was used as the reactant.; HRMS [M]+: 631.22
[합성예 574] Mat 574의 합성[Synthesis Example 574] Synthesis of Mat 574
반응물로 [준비예 96]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 96] was used as the reactant.; HRMS [M]+: 630.24
[합성예 575] Mat 575의 합성[Synthesis Example 575] Synthesis of Mat 575
반응물로 [준비예 96]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 542.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 96] was used as the reactant.; HRMS [M]+: 542.21
[합성예 576] Mat 576의 합성[Synthesis Example 576] Synthesis of Mat 576
반응물로 [준비예 96]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 96] was used as the reactant.; HRMS [M]+: 592.23
[합성예 577] Mat 577의 합성[Synthesis Example 577] Synthesis of Mat 577
반응물로 [준비예 97]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 97] was used as the reactant.; HRMS [M]+: 641.24
[합성예 578] Mat 578의 합성[Synthesis Example 578] Synthesis of Mat 578
반응물로 [준비예 97]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 97] was used as the reactant.; HRMS [M]+: 706.27
[합성예 579] Mat 579의 합성[Synthesis Example 579] Synthesis of Mat 579
반응물로 [준비예 97]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 631.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 97] was used as the reactant.; HRMS [M]+: 631.22
[합성예 580] Mat 580의 합성[Synthesis Example 580] Synthesis of Mat 580
반응물로 [준비예 97]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 97] was used as the reactant.; HRMS [M]+: 630.24
[합성예 581] Mat 581의 합성[Synthesis Example 581] Synthesis of Mat 581
반응물로 [준비예 97]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 542.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 97] was used as the reactant.; HRMS [M]+: 542.21
[합성예 582] Mat 582의 합성[Synthesis Example 582] Synthesis of Mat 582
반응물로 [준비예 97]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 97] was used as the reactant.; HRMS [M]+: 592.23
[합성예 583] Mat 583의 합성[Synthesis Example 583] Synthesis of Mat 583
반응물로 [준비예 98]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 98] was used as the reactant.; HRMS [M]+: 641.24
[합성예 584] Mat 584의 합성[Synthesis Example 584] Synthesis of Mat 584
반응물로 [준비예 98]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 98] was used as the reactant.; HRMS [M]+: 706.27
[합성예 585] Mat 585의 합성[Synthesis Example 585] Synthesis of Mat 585
반응물로 [준비예 98]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 631.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 98] was used as the reactant.; HRMS [M]+: 631.22
[합성예 586] Mat 586의 합성[Synthesis Example 586] Synthesis of Mat 586
반응물로 [준비예 98]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 98] was used as the reactant.; HRMS [M]+: 630.24
[합성예 587] Mat 587의 합성[Synthesis Example 587] Synthesis of Mat 587
반응물로 [준비예 98]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 542.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 98] was used as the reactant.; HRMS [M]+: 542.21
[합성예 588] Mat 588의 합성[Synthesis Example 588] Synthesis of Mat 588
반응물로 [준비예 98]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 98] was used as the reactant.; HRMS [M]+: 592.23
[합성예 589] Mat 589의 합성[Synthesis Example 589] Synthesis of Mat 589
반응물로 [준비예 99]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 99] was used as the reactant.; HRMS [M]+: 716.28
[합성예 590] Mat 590의 합성[Synthesis Example 590] Synthesis of Mat 590
반응물로 [준비예 99]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 781.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 99] was used as the reactant.; HRMS [M]+: 781.30
[합성예 591] Mat 591의 합성[Synthesis Example 591] Synthesis of Mat 591
반응물로 [준비예 99]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 99] was used as the reactant.; HRMS [M]+: 706.26
[합성예 592] Mat 592의 합성[Synthesis Example 592] Synthesis of Mat 592
반응물로 [준비예 99]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 99] was used as the reactant.; HRMS [M]+: 705.27
[합성예 593] Mat 593의 합성[Synthesis Example 593] Synthesis of Mat 593
반응물로 [준비예 99]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 617.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 99] was used as the reactant.; HRMS [M]+: 617.24
[합성예 594] Mat 594의 합성[Synthesis Example 594] Synthesis of Mat 594
반응물로 [준비예 99]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 99] was used as the reactant.; HRMS [M]+: 667.26
[합성예 595] Mat 595의 합성[Synthesis Example 595] Synthesis of Mat 595
반응물로 [준비예 100]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 716.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 100] was used as the reactant.; HRMS [M]+: 716.28
[합성예 596] Mat 596의 합성[Synthesis Example 596] Synthesis of Mat 596
반응물로 [준비예 100]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 781.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 100] was used as the reactant.; HRMS [M]+: 781.30
[합성예 597] Mat 597의 합성[Synthesis Example 597] Synthesis of Mat 597
반응물로 [준비예 100]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 100] was used as the reactant.; HRMS [M]+: 706.26
[합성예 598] Mat 598의 합성[Synthesis Example 598] Synthesis of Mat 598
반응물로 [준비예 100]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 705.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 100] was used as the reactant.; HRMS [M]+: 705.27
[합성예 599] Mat 599의 합성[Synthesis Example 599] Synthesis of Mat 599
반응물로 [준비예 100]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 617.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 100] was used as the reactant.; HRMS [M]+: 617.24
[합성예 600] Mat 600의 합성[Synthesis Example 600] Synthesis of Mat 600
반응물로 [준비예 100]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 100] was used as the reactant.; HRMS [M]+: 667.26
[합성예 601] Mat 601의 합성[Synthesis Example 601] Synthesis of Mat 601
반응물로 [준비예 101]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 101] was used as the reactant.; HRMS [M]+: 717.28
[합성예 602] Mat 602의 합성[Synthesis Example 602] Synthesis of Mat 602
반응물로 [준비예 101]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 782.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 101] was used as the reactant.; HRMS [M]+: 782.30
[합성예 603] Mat 603의 합성[Synthesis Example 603] Synthesis of Mat 603
반응물로 [준비예 101]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 707.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 101] was used as the reactant.; HRMS [M]+: 707.26
[합성예 604] Mat 604의 합성[Synthesis Example 604] Synthesis of Mat 604
반응물로 [준비예 101]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 101] was used as the reactant.; HRMS [M]+: 706.27
[합성예 605] Mat 605의 합성[Synthesis Example 605] Synthesis of Mat 605
반응물로 [준비예 101]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 618.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 101] was used as the reactant.; HRMS [M]+: 618.24
[합성예 606] Mat 606의 합성[Synthesis Example 606] Synthesis of Mat 606
반응물로 [준비예 101]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 668.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 101] was used as the reactant.; HRMS [M]+: 668.26
[합성예 607] Mat 607의 합성[Synthesis Example 607] Synthesis of Mat 607
반응물로 [준비예 102]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 102] was used as the reactant.; HRMS [M]+: 717.28
[합성예 608] Mat 608의 합성[Synthesis Example 608] Synthesis of Mat 608
반응물로 [준비예 102]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 782.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 102] was used as the reactant.; HRMS [M]+: 782.30
[합성예 609] Mat 609의 합성[Synthesis Example 609] Synthesis of Mat 609
반응물로 [준비예 102]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 707.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 102] was used as the reactant.; HRMS [M]+: 707.26
[합성예 610] Mat 610의 합성[Synthesis Example 610] Synthesis of Mat 610
반응물로 [준비예 102]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 102] was used as the reactant.; HRMS [M]+: 706.27
[합성예 611] Mat 611의 합성[Synthesis Example 611] Synthesis of Mat 611
반응물로 [준비예 102]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 618.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 102] was used as the reactant.; HRMS [M]+: 618.24
[합성예 612] Mat 612의 합성[Synthesis Example 612] Synthesis of Mat 612
반응물로 [준비예 102]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 668.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 102] was used as the reactant.; HRMS [M]+: 668.26
[합성예 613] Mat 613의 합성[Synthesis Example 613] Synthesis of Mat 613
반응물로 [준비예 103]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 103] was used as the reactant.; HRMS [M]+: 717.28
[합성예 614] Mat 614의 합성[Synthesis Example 614] Synthesis of Mat 614
반응물로 [준비예 103]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 782.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 103] was used as the reactant.; HRMS [M]+: 782.30
[합성예 615] Mat 615의 합성[Synthesis Example 615] Synthesis of Mat 615
반응물로 [준비예 103]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 707.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 103] was used as the reactant.; HRMS [M]+: 707.26
[합성예 616] Mat 616의 합성[Synthesis Example 616] Synthesis of Mat 616
반응물로 [준비예 103]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 706.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 103] was used as the reactant.; HRMS [M]+: 706.27
[합성예 617] Mat 617의 합성[Synthesis Example 617] Synthesis of Mat 617
반응물로 [준비예 103]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 618.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 103] was used as the reactant.; HRMS [M]+: 618.24
[합성예 618] Mat 618의 합성[Synthesis Example 618] Synthesis of Mat 618
반응물로 [준비예 103]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 668.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 103] was used as the reactant.; HRMS [M]+: 668.26
[합성예 619] Mat 619의 합성[Synthesis Example 619] Synthesis of Mat 619
반응물로 [준비예 104]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 104] was used as the reactant.; HRMS [M]+: 690.26
[합성예 620] Mat 620의 합성[Synthesis Example 620] Synthesis of Mat 620
반응물로 [준비예 104]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 104] was used as the reactant.; HRMS [M]+: 755.29
[합성예 621] Mat 621의 합성[Synthesis Example 621] Synthesis of Mat 621
반응물로 [준비예 104]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 104] was used as the reactant.; HRMS [M]+: 630.25
[합성예 622] Mat 622의 합성[Synthesis Example 622] Synthesis of Mat 622
반응물로 [준비예 104]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 104] was used as the reactant.; HRMS [M]+: 679.26
[합성예 623] Mat 623의 합성[Synthesis Example 623] Synthesis of Mat 623
반응물로 [준비예 104]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 104] was used as the reactant.; HRMS [M]+: 591.23
[합성예 624] Mat 624의 합성[Synthesis Example 624] Synthesis of Mat 624
반응물로 [준비예 104]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 104] was used as the reactant.; HRMS [M]+: 641.24
[합성예 625] Mat 625의 합성[Synthesis Example 625] Synthesis of Mat 625
반응물로 [준비예 105]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 105] was used as the reactant.; HRMS [M]+: 690.26
[합성예 626] Mat 626의 합성[Synthesis Example 626] Synthesis of Mat 626
반응물로 [준비예 105]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 105] was used as the reactant.; HRMS [M]+: 755.29
[합성예 627] Mat 627의 합성[Synthesis Example 627] Synthesis of Mat 627
반응물로 [준비예 105]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 105] was used as the reactant.; HRMS [M]+: 630.25
[합성예 628] Mat 628의 합성[Synthesis Example 628] Synthesis of Mat 628
반응물로 [준비예 105]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 105] was used as the reactant.; HRMS [M]+: 679.26
[합성예 629] Mat 629의 합성[Synthesis Example 629] Synthesis of Mat 629
반응물로 [준비예 105]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 105] was used as the reactant.; HRMS [M]+: 591.23
[합성예 630] Mat 630의 합성[Synthesis Example 630] Synthesis of Mat 630
반응물로 [준비예 105]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 105] was used as the reactant.; HRMS [M]+: 641.24
[합성예 631] Mat 631의 합성[Synthesis Example 631] Synthesis of Mat 631
반응물로 [준비예 106]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 106] was used as the reactant.; HRMS [M]+: 690.26
[합성예 632] Mat 632의 합성[Synthesis Example 632] Synthesis of Mat 632
반응물로 [준비예 106]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 106] was used as the reactant.; HRMS [M]+: 755.29
[합성예 633] Mat 633의 합성[Synthesis Example 633] Synthesis of Mat 633
반응물로 [준비예 106]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 630.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 106] was used as the reactant.; HRMS [M]+: 630.25
[합성예 634] Mat 634의 합성[Synthesis Example 634] Synthesis of Mat 634
반응물로 [준비예 106]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 106] was used as the reactant.; HRMS [M]+: 679.26
[합성예 635] Mat 635의 합성[Synthesis Example 635] Synthesis of Mat 635
반응물로 [준비예 106]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 106] was used as the reactant.; HRMS [M]+: 591.23
[합성예 636] Mat 636의 합성[Synthesis Example 636] Synthesis of Mat 636
반응물로 [준비예 106]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 106] was used as the reactant.; HRMS [M]+: 641.24
[합성예 637] Mat 637의 합성[Synthesis Example 637] Synthesis of Mat 637
반응물로 [준비예 106]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 691.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 106] was used as the reactant.; HRMS [M]+: 691.26
[합성예 638] Mat 638의 합성[Synthesis Example 638] Synthesis of Mat 638
반응물로 [준비예 106]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 106] was used as the reactant.; HRMS [M]+: 756.29
[합성예 639] Mat 639의 합성[Synthesis Example 639] Synthesis of Mat 639
반응물로 [준비예 106]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 631.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 106] was used as the reactant.; HRMS [M]+: 631.25
[합성예 640] Mat 640의 합성[Synthesis Example 640] Synthesis of Mat 640
반응물로 [준비예 106]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 106] was used as the reactant.; HRMS [M]+: 680.26
[합성예 641] Mat 641의 합성[Synthesis Example 641] Synthesis of Mat 641
반응물로 [준비예 106]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 106] was used as the reactant.; HRMS [M]+: 592.23
[합성예 642] Mat 642의 합성[Synthesis Example 642] Synthesis of Mat 642
반응물로 [준비예 106]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 642.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 106] was used as the reactant.; HRMS [M]+: 642.24
[합성예 643] Mat 643의 합성[Synthesis Example 643] Synthesis of Mat 643
반응물로 [준비예 107]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 691.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 107] was used as the reactant.; HRMS [M]+: 691.26
[합성예 644] Mat 644의 합성[Synthesis Example 644] Synthesis of Mat 644
반응물로 [준비예 107]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 107] was used as the reactant.; HRMS [M]+: 756.29
[합성예 645] Mat 645의 합성[Synthesis Example 645] Synthesis of Mat 645
반응물로 [준비예 107]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 631.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 107] was used as the reactant.; HRMS [M]+: 631.25
[합성예 646] Mat 646의 합성[Synthesis Example 646] Synthesis of Mat 646
반응물로 [준비예 107]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 107] was used as the reactant.; HRMS [M]+: 680.26
[합성예 647] Mat 647의 합성[Synthesis Example 647] Synthesis of Mat 647
반응물로 [준비예 107]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 107] was used as the reactant.; HRMS [M]+: 592.23
[합성예 648] Mat 648의 합성[Synthesis Example 648] Synthesis of Mat 648
반응물로 [준비예 107]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 642.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 107] was used as the reactant.; HRMS [M]+: 642.24
[합성예 649] Mat 649의 합성[Synthesis Example 649] Synthesis of Mat 649
반응물로 [준비예 108]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 108] was used as the reactant.; HRMS [M]+: 690.26
[합성예 650] Mat 650의 합성[Synthesis Example 650] Synthesis of Mat 650
반응물로 [준비예 108]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 108] was used as the reactant.; HRMS [M]+: 755.29
[합성예 651] Mat 651의 합성[Synthesis Example 651] Synthesis of Mat 651
반응물로 [준비예 108]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.24The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 108] was used as the reactant.; HRMS [M]+: 680.24
[합성예 652] Mat 652의 합성[Synthesis Example 652] Synthesis of Mat 652
반응물로 [준비예 108]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 108] was used as the reactant.; HRMS [M]+: 679.24
[합성예 653] Mat 653의 합성[Synthesis Example 653] Synthesis of Mat 653
반응물로 [준비예 108]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 108] was used as the reactant.; HRMS [M]+: 591.23
[합성예 654] Mat 654의 합성[Synthesis Example 654] Synthesis of Mat 654
반응물로 [준비예 108]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 108] was used as the reactant.; HRMS [M]+: 591.23
[합성예 655] Mat 655의 합성[Synthesis Example 655] Synthesis of Mat 655
반응물로 [준비예 109]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 109] was used as the reactant.; HRMS [M]+: 690.26
[합성예 656] Mat 656의 합성[Synthesis Example 656] Synthesis of Mat 656
반응물로 [준비예 109]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 109] was used as the reactant.; HRMS [M]+: 755.29
[합성예 657] Mat 657의 합성[Synthesis Example 657] Synthesis of Mat 657
반응물로 [준비예 109]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 109] was used as the reactant.; HRMS [M]+: 680.23
[합성예 658] Mat 658의 합성[Synthesis Example 658] Synthesis of Mat 658
반응물로 [준비예 109]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 109] was used as the reactant.; HRMS [M]+: 679.24
[합성예 659] Mat 659의 합성[Synthesis Example 659] Synthesis of Mat 659
반응물로 [준비예 109]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 109] was used as the reactant.; HRMS [M]+: 591.21
[합성예 660] Mat 660의 합성[Synthesis Example 660] Synthesis of Mat 660
반응물로 [준비예 109]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 109] was used as the reactant.; HRMS [M]+: 641.23
[합성예 661] Mat 661의 합성[Synthesis Example 661] Synthesis of Mat 661
반응물로 [준비예 110]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 110] was used as the reactant.; HRMS [M]+: 690.25
[합성예 662] Mat 662의 합성[Synthesis Example 662] Synthesis of Mat 662
반응물로 [준비예 110]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 110] was used as the reactant.; HRMS [M]+: 755.27
[합성예 663] Mat 663의 합성[Synthesis Example 663] Synthesis of Mat 663
반응물로 [준비예 110]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 110] was used as the reactant.; HRMS [M]+: 680.23
[합성예 664] Mat 664의 합성[Synthesis Example 664] Synthesis of Mat 664
반응물로 [준비예 110]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 110] was used as the reactant.; HRMS [M]+: 679.24
[합성예 665] Mat 665의 합성[Synthesis Example 665] Synthesis of Mat 665
반응물로 [준비예 110]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 110] was used as the reactant.; HRMS [M]+: 591.21
[합성예 666] Mat 666의 합성[Synthesis Example 666] Synthesis of Mat 666
반응물로 [준비예 110]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 110] was used as the reactant.; HRMS [M]+: 641.23
[합성예 667] Mat 667의 합성[Synthesis Example 667] Synthesis of Mat 667
반응물로 [준비예 111]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 690.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 111] was used as the reactant.; HRMS [M]+: 690.25
[합성예 668] Mat 668의 합성[Synthesis Example 668] Synthesis of Mat 668
반응물로 [준비예 111]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 111] was used as the reactant.; HRMS [M]+: 755.27
[합성예 669] Mat 669의 합성[Synthesis Example 669] Synthesis of Mat 669
반응물로 [준비예 111]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 111] was used as the reactant.; HRMS [M]+: 680.23
[합성예 670] Mat 670의 합성[Synthesis Example 670] Synthesis of Mat 670
반응물로 [준비예 111]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 679.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 111] was used as the reactant.; HRMS [M]+: 679.24
[합성예 671] Mat 671의 합성[Synthesis Example 671] Synthesis of Mat 671
반응물로 [준비예 111]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 591.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 111] was used as the reactant.; HRMS [M]+: 591.21
[합성예 672] Mat 672의 합성[Synthesis Example 672] Synthesis of Mat 672
반응물로 [준비예 111]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 111] was used as the reactant.; HRMS [M]+: 641.23
[합성예 673] Mat 673의 합성[Synthesis Example 673] Synthesis of Mat 673
반응물로 [준비예 112]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 691.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 112] was used as the reactant.; HRMS [M]+: 691.24
[합성예 674] Mat 674의 합성[Synthesis Example 674] Synthesis of Mat 674
반응물로 [준비예 112]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 112] was used as the reactant.; HRMS [M]+: 756.27
[합성예 675] Mat 675의 합성[Synthesis Example 675] Synthesis of Mat 675
반응물로 [준비예 112]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 681.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 112] was used as the reactant.; HRMS [M]+: 681.22
[합성예 676] Mat 676의 합성[Synthesis Example 676] Synthesis of Mat 676
반응물로 [준비예 112]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 112] was used as the reactant.; HRMS [M]+: 680.24
[합성예 677] Mat 677의 합성[Synthesis Example 677] Synthesis of Mat 677
반응물로 [준비예 112]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 112] was used as the reactant.; HRMS [M]+: 592.21
[합성예 678] Mat 678의 합성[Synthesis Example 678] Synthesis of Mat 678
반응물로 [준비예 112]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 642.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 112] was used as the reactant.; HRMS [M]+: 642.23
[합성예 679] Mat 679의 합성[Synthesis Example 679] Synthesis of Mat 679
반응물로 [준비예 113]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 691.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 113] was used as the reactant.; HRMS [M]+: 691.24
[합성예 680] Mat 680의 합성[Synthesis Example 680] Synthesis of Mat 680
반응물로 [준비예 113]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 113] was used as the reactant.; HRMS [M]+: 756.27
[합성예 681] Mat 681의 합성[Synthesis Example 681] Synthesis of Mat 681
반응물로 [준비예 113]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 681.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 113] was used as the reactant.; HRMS [M]+: 681.22
[합성예 682] Mat 682의 합성[Synthesis Example 682] Synthesis of Mat 682
반응물로 [준비예 113]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 113] was used as the reactant.; HRMS [M]+: 680.24
[합성예 683] Mat 683의 합성[Synthesis Example 683] Synthesis of Mat 683
반응물로 [준비예 113]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 113] was used as the reactant.; HRMS [M]+: 592.21
[합성예 684] Mat 684의 합성[Synthesis Example 684] Synthesis of Mat 684
반응물로 [준비예 113]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 642.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 113] was used as the reactant.; HRMS [M]+: 642.23
[합성예 685] Mat 685의 합성[Synthesis Example 685] Synthesis of Mat 685
반응물로 [준비예 114]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 691.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 114] was used as the reactant.; HRMS [M]+: 691.24
[합성예 686] Mat 686의 합성[Synthesis Example 686] Synthesis of Mat 686
반응물로 [준비예 114]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 114] was used as the reactant.; HRMS [M]+: 756.27
[합성예 687] Mat 687의 합성[Synthesis Example 687] Synthesis of Mat 687
반응물로 [준비예 114]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 681.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 114] was used as the reactant.; HRMS [M]+: 681.22
[합성예 688] Mat 688의 합성[Synthesis Example 688] Synthesis of Mat 688
반응물로 [준비예 114]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 114] was used as the reactant.; HRMS [M]+: 680.24
[합성예 689] Mat 689의 합성[Synthesis Example 689] Synthesis of Mat 689
반응물로 [준비예 114]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 114] was used as the reactant.; HRMS [M]+: 592.21
[합성예 690] Mat 690의 합성[Synthesis Example 690] Synthesis of Mat 690
반응물로 [준비예 114]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 642.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 114] was used as the reactant.; HRMS [M]+: 642.23
[합성예 691] Mat 691의 합성[Synthesis Example 691] Synthesis of Mat 691
반응물로 [준비예 115]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 691.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 115] was used as the reactant.; HRMS [M]+: 691.24
[합성예 692] Mat 692의 합성[Synthesis Example 692] Synthesis of Mat 692
반응물로 [준비예 115]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 115] was used as the reactant.; HRMS [M]+: 756.27
[합성예 693] Mat 693의 합성[Synthesis Example 693] Synthesis of Mat 693
반응물로 [준비예 115]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 681.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 115] was used as the reactant.; HRMS [M]+: 681.22
[합성예 694] Mat 694의 합성[Synthesis Example 694] Synthesis of Mat 694
반응물로 [준비예 115]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 115] was used as the reactant.; HRMS [M]+: 680.24
[합성예 695] Mat 695의 합성[Synthesis Example 695] Synthesis of Mat 695
반응물로 [준비예 115]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 592.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 115] was used as the reactant.; HRMS [M]+: 592.21
[합성예 696] Mat 696의 합성[Synthesis Example 696] Synthesis of Mat 696
반응물로 [준비예 115]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 642.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 115] was used as the reactant.; HRMS [M]+: 642.23
[합성예 697] Mat 697의 합성[Synthesis Example 697] Synthesis of Mat 697
반응물로 [준비예 116]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 766.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 116] was used as the reactant.; HRMS [M]+: 766.28
[합성예 698] Mat 698의 합성[Synthesis Example 698] Synthesis of Mat 698
반응물로 [준비예 116]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 831.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 116] was used as the reactant.; HRMS [M]+: 831.30
[합성예 699] Mat 699의 합성[Synthesis Example 699] Synthesis of Mat 699
반응물로 [준비예 116]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 116] was used as the reactant.; HRMS [M]+: 756.26
[합성예 700] Mat 700의 합성[Synthesis Example 700] Synthesis of Mat 700
반응물로 [준비예 116]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 116] was used as the reactant.; HRMS [M]+: 755.27
[합성예 701] Mat 701의 합성[Synthesis Example 701] Synthesis of Mat 701
반응물로 [준비예 116]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 116] was used as the reactant.; HRMS [M]+: 667.24
[합성예 702] Mat 702의 합성[Synthesis Example 702] Synthesis of Mat 702
반응물로 [준비예 116]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 116] was used as the reactant.; HRMS [M]+: 717.26
[합성예 703] Mat 703의 합성[Synthesis Example 703] Synthesis of Mat 703
반응물로 [준비예 117]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 766.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 117] was used as the reactant.; HRMS [M]+: 766.28
[합성예 704] Mat 704의 합성[Synthesis Example 704] Synthesis of Mat 704
반응물로 [준비예 117]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 831.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 117] was used as the reactant.; HRMS [M]+: 831.30
[합성예 705] Mat 705의 합성[Synthesis Example 705] Synthesis of Mat 705
반응물로 [준비예 117]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 117] was used as the reactant.; HRMS [M]+: 756.26
[합성예 706] Mat 706의 합성[Synthesis Example 706] Synthesis of Mat 706
반응물로 [준비예 117]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 755.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 117] was used as the reactant.; HRMS [M]+: 755.27
[합성예 707] Mat 707의 합성[Synthesis Example 707] Synthesis of Mat 707
반응물로 [준비예 117]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 667.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 117] was used as the reactant.; HRMS [M]+: 667.24
[합성예 708] Mat 708의 합성[Synthesis Example 708] Synthesis of Mat 708
반응물로 [준비예 117]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 117] was used as the reactant.; HRMS [M]+: 717.26
[합성예 709] Mat 709의 합성[Synthesis Example 709] Synthesis of Mat 709
반응물로 [준비예 118]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 767.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 118] was used as the reactant.; HRMS [M]+: 767.28
[합성예 710] Mat 710의 합성[Synthesis Example 710] Synthesis of Mat 710
반응물로 [준비예 118]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 832.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 118] was used as the reactant.; HRMS [M]+: 832.30
[합성예 711] Mat 711의 합성[Synthesis Example 711] Synthesis of Mat 711
반응물로 [준비예 118]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 757.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 118] was used as the reactant.; HRMS [M]+: 757.26
[합성예 712] Mat 712의 합성[Synthesis Example 712] Synthesis of Mat 712
반응물로 [준비예 118]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 118] was used as the reactant.; HRMS [M]+: 756.27
[합성예 713] Mat 713의 합성[Synthesis Example 713] Synthesis of Mat 713
반응물로 [준비예 118]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 668.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 118] was used as the reactant.; HRMS [M]+: 668.24
[합성예 714] Mat 714의 합성[Synthesis Example 714] Synthesis of Mat 714
반응물로 [준비예 118]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 718.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 118] was used as the reactant.; HRMS [M]+: 718.26
[합성예 715] Mat 715의 합성[Synthesis Example 715] Synthesis of Mat 715
반응물로 [준비예 119]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 767.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 119] was used as the reactant.; HRMS [M]+: 767.28
[합성예 716] Mat 716의 합성[Synthesis Example 716] Synthesis of Mat 716
반응물로 [준비예 119]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 832.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 119] was used as the reactant.; HRMS [M]+: 832.30
[합성예 717] Mat 717의 합성[Synthesis Example 717] Synthesis of Mat 717
반응물로 [준비예 119]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 757.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 119] was used as the reactant.; HRMS [M]+: 757.26
[합성예 718] Mat 718의 합성[Synthesis Example 718] Synthesis of Mat 718
반응물로 [준비예 119]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 119] was used as the reactant.; HRMS [M]+: 756.27
[합성예 719] Mat 719의 합성[Synthesis Example 719] Synthesis of Mat 719
반응물로 [준비예 119]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 668.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 119] was used as the reactant.; HRMS [M]+: 668.24
[합성예 720] Mat 720의 합성[Synthesis Example 720] Synthesis of Mat 720
반응물로 [준비예 119]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 718.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 119] was used as the reactant.; HRMS [M]+: 718.26
[합성예 721] Mat 721의 합성[Synthesis Example 721] Synthesis of Mat 721
반응물로 [준비예 120]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 767.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 120] was used as the reactant.; HRMS [M]+: 767.28
[합성예 722] Mat 722의 합성[Synthesis Example 722] Synthesis of Mat 722
반응물로 [준비예 120]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 832.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 120] was used as the reactant.; HRMS [M]+: 832.30
[합성예 723] Mat 723의 합성[Synthesis Example 723] Synthesis of Mat 723
반응물로 [준비예 120]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 757.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 120] was used as the reactant.; HRMS [M]+: 757.26
[합성예 724] Mat 724의 합성[Synthesis Example 724] Synthesis of Mat 724
반응물로 [준비예 120]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 756.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 120] was used as the reactant.; HRMS [M]+: 756.27
[합성예 725] Mat 725의 합성[Synthesis Example 725] Synthesis of Mat 725
반응물로 [준비예 120]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 668.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 120] was used as the reactant.; HRMS [M]+: 668.24
[합성예 726] Mat 726의 합성[Synthesis Example 726] Synthesis of Mat 726
반응물로 [준비예 120]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 718.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 120] was used as the reactant.; HRMS [M]+: 718.26
[합성예 727] Mat 727의 합성[Synthesis Example 727] Synthesis of Mat 727
반응물로 [준비예 121]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 740.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 121] was used as the reactant.; HRMS [M]+: 740.26
[합성예 728] Mat 728의 합성[Synthesis Example 728] Synthesis of Mat 728
반응물로 [준비예 121]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 805.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 121] was used as the reactant.; HRMS [M]+: 805.29
[합성예 729] Mat 729의 합성[Synthesis Example 729] Synthesis of Mat 729
반응물로 [준비예 121]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 121] was used as the reactant.; HRMS [M]+: 680.25
[합성예 730] Mat 730의 합성[Synthesis Example 730] Synthesis of Mat 730
반응물로 [준비예 121]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 729.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 121] was used as the reactant.; HRMS [M]+: 729.26
[합성예 731] Mat 731의 합성[Synthesis Example 731] Synthesis of Mat 731
반응물로 [준비예 121]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 121] was used as the reactant.; HRMS [M]+: 641.23
[합성예 732] Mat 732의 합성[Synthesis Example 732] Synthesis of Mat 732
반응물로 [준비예 121]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 691.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 121] was used as the reactant.; HRMS [M]+: 691.24
[합성예 733] Mat 733의 합성[Synthesis Example 733] Synthesis of Mat 733
반응물로 [준비예 121]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 740.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 121] was used as the reactant.; HRMS [M]+: 740.26
[합성예 734] Mat 734의 합성[Synthesis Example 734] Synthesis of Mat 734
반응물로 [준비예 121]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 805.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 121] was used as the reactant.; HRMS [M]+: 805.29
[합성예 735] Mat 735의 합성[Synthesis Example 735] Synthesis of Mat 735
반응물로 [준비예 121]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 121] was used as the reactant.; HRMS [M]+: 680.25
[합성예 736] Mat 736의 합성[Synthesis Example 736] Synthesis of Mat 736
반응물로 [준비예 121]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 739.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 121] was used as the reactant.; HRMS [M]+: 739.26
[합성예 737] Mat 737의 합성[Synthesis Example 737] Synthesis of Mat 737
반응물로 [준비예 121]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 121] was used as the reactant.; HRMS [M]+: 641.23
[합성예 738] Mat 738의 합성[Synthesis Example 738] Synthesis of Mat 738
반응물로 [준비예 121]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 691.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 121] was used as the reactant.; HRMS [M]+: 691.24
[합성예 739] Mat 739의 합성[Synthesis Example 739] Synthesis of Mat 739
반응물로 [준비예 122]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 740.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 122] was used as the reactant.; HRMS [M]+: 740.26
[합성예 740] Mat 740의 합성[Synthesis Example 740] Synthesis of Mat 740
반응물로 [준비예 122]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 805.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 122] was used as the reactant.; HRMS [M]+: 805.29
[합성예 741] Mat 741의 합성[Synthesis Example 741] Synthesis of Mat 741
반응물로 [준비예 122]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 680.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 122] was used as the reactant.; HRMS [M]+: 680.25
[합성예 742] Mat 742의 합성[Synthesis Example 742] Synthesis of Mat 742
반응물로 [준비예 122]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 729.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 122] was used as the reactant.; HRMS [M]+: 729.26
[합성예 743] Mat 743의 합성[Synthesis Example 743] Synthesis of Mat 743
반응물로 [준비예 122]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 641.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 122] was used as the reactant.; HRMS [M]+: 641.23
[합성예 744] Mat 744의 합성[Synthesis Example 744] Synthesis of Mat 744
반응물로 [준비예 122]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 691.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 122] was used as the reactant.; HRMS [M]+: 691.24
[합성예 745] Mat 745의 합성[Synthesis Example 745] Synthesis of Mat 745
반응물로 [준비예 123]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 741.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 123] was used as the reactant.; HRMS [M]+: 741.26
[합성예 746] Mat 746의 합성[Synthesis Example 746] Synthesis of Mat 746
반응물로 [준비예 123]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 806.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 123] was used as the reactant.; HRMS [M]+: 806.29
[합성예 747] Mat 747의 합성[Synthesis Example 747] Synthesis of Mat 747
반응물로 [준비예 123]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 681.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 123] was used as the reactant.; HRMS [M]+: 681.25
[합성예 748] Mat 748의 합성[Synthesis Example 748] Synthesis of Mat 748
반응물로 [준비예 123]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 730.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 123] was used as the reactant.; HRMS [M]+: 730.26
[합성예 749] Mat 749의 합성[Synthesis Example 749] Synthesis of Mat 749
반응물로 [준비예 123]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 642.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 123] was used as the reactant.; HRMS [M]+: 642.23
[합성예 750] Mat 750의 합성[Synthesis Example 750] Synthesis of Mat 750
반응물로 [준비예 123]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 692.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 123] was used as the reactant.; HRMS [M]+: 692.24
[합성예 751] Mat 751의 합성[Synthesis Example 751] Synthesis of Mat 751
반응물로 [준비예 124]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 741.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 124] was used as the reactant.; HRMS [M]+: 741.26
[합성예 752] Mat 752의 합성[Synthesis Example 752] Synthesis of Mat 752
반응물로 [준비예 124]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 806.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 124] was used as the reactant.; HRMS [M]+: 806.29
[합성예 753] Mat 753의 합성[Synthesis Example 753] Synthesis of Mat 753
반응물로 [준비예 124]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 681.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 124] was used as the reactant.; HRMS [M]+: 681.25
[합성예 754] Mat 754의 합성[Synthesis Example 754] Synthesis of Mat 754
반응물로 [준비예 124]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 730.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 124] was used as the reactant.; HRMS [M]+: 730.26
[합성예 755] Mat 755의 합성[Synthesis Example 755] Synthesis of Mat 755
반응물로 [준비예 124]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 642.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 124] was used as the reactant.; HRMS [M]+: 642.23
[합성예 756] Mat 756의 합성[Synthesis Example 756] Synthesis of Mat 756
반응물로 [준비예 124]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 692.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 124] was used as the reactant.; HRMS [M]+: 692.24
[합성예 757] Mat 757의 합성[Synthesis Example 757] Synthesis of Mat 757
반응물로 [준비예 125]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 728.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 125] was used as the reactant.; HRMS [M]+: 728.25
[합성예 758] Mat 578의 합성[Synthesis Example 758] Synthesis of Mat 578
반응물로 [준비예 125]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 744.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 125] was used as the reactant.; HRMS [M]+: 744.27
[합성예 759] Mat 759의 합성[Synthesis Example 759] Synthesis of Mat 759
반응물로 [준비예 125]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 125] was used as the reactant.; HRMS [M]+: 793.23
[합성예 760] Mat 760의 합성[Synthesis Example 760] Synthesis of Mat 760
반응물로 [준비예 125]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 718.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 125] was used as the reactant.; HRMS [M]+: 718.24
[합성예 761] Mat 761의 합성[Synthesis Example 761] Synthesis of Mat 761
반응물로 [준비예 125]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 727.27The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 125] was used as the reactant.; HRMS [M]+: 727.27
[합성예 762] Mat 762의 합성[Synthesis Example 762] Synthesis of Mat 762
반응물로 [준비예 125]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 734.25The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 125] was used as the reactant.; HRMS [M]+: 734.25
[합성예 763] Mat 763의 합성[Synthesis Example 763] Synthesis of Mat 763
반응물로 [준비예 126]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 728.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 126] was used as the reactant.; HRMS [M]+: 728.25
[합성예 764] Mat 764의 합성[Synthesis Example 764] Synthesis of Mat 764
반응물로 [준비예 126]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 744.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 126] was used as the reactant.; HRMS [M]+: 744.27
[합성예 765] Mat 765의 합성[Synthesis Example 765] Synthesis of Mat 765
반응물로 [준비예 126]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 126] was used as the reactant.; HRMS [M]+: 793.23
[합성예 766] Mat 766의 합성[Synthesis Example 766] Synthesis of Mat 766
반응물로 [준비예 126]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 718.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 126] was used as the reactant.; HRMS [M]+: 718.24
[합성예 767] Mat 767의 합성[Synthesis Example 767] Synthesis of Mat 767
반응물로 [준비예 126]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 126] was used as the reactant.; HRMS [M]+: 717.21
[합성예 768] Mat 768의 합성[Synthesis Example 768] Synthesis of Mat 768
반응물로 [준비예 126]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 734.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 126] was used as the reactant.; HRMS [M]+: 734.23
[합성예 769] Mat 769의 합성[Synthesis Example 769] Synthesis of Mat 769
반응물로 [준비예 127]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 728.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 127] was used as the reactant.; HRMS [M]+: 728.25
[합성예 770] Mat 770의 합성[Synthesis Example 770] Synthesis of Mat 770
반응물로 [준비예 127]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 744.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 127] was used as the reactant.; HRMS [M]+: 744.27
[합성예 771] Mat 771의 합성[Synthesis Example 771] Synthesis of Mat 771
반응물로 [준비예 127]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 127] was used as the reactant.; HRMS [M]+: 793.23
[합성예 772] Mat 772의 합성[Synthesis Example 772] Synthesis of Mat 772
반응물로 [준비예 127]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 718.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 127] was used as the reactant.; HRMS [M]+: 718.24
[합성예 773] Mat 773의 합성[Synthesis Example 773] Synthesis of Mat 773
반응물로 [준비예 127]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 541.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 127] was used as the reactant.; HRMS [M]+: 541.21
[합성예 774] Mat 774의 합성[Synthesis Example 774] Synthesis of Mat 774
반응물로 [준비예 127]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 127] was used as the reactant.; HRMS [M]+: 717.23
[합성예 775] Mat 775의 합성[Synthesis Example 775] Synthesis of Mat 775
반응물로 [준비예 128]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 728.25The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 128] was used as the reactant.; HRMS [M]+: 728.25
[합성예 776] Mat 776의 합성[Synthesis Example 776] Synthesis of Mat 776
반응물로 [준비예 128]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 744.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 128] was used as the reactant.; HRMS [M]+: 744.27
[합성예 777] Mat 777의 합성[Synthesis Example 777] Synthesis of Mat 777
반응물로 [준비예 128]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.23The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 128] was used as the reactant.; HRMS [M]+: 793.23
[합성예 778] Mat 778의 합성[Synthesis Example 778] Synthesis of Mat 778
반응물로 [준비예 128]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 128] was used as the reactant.; HRMS [M]+: 717.24
[합성예 779] Mat 779의 합성[Synthesis Example 779] Synthesis of Mat 779
반응물로 [준비예 128]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 128] was used as the reactant.; HRMS [M]+: 717.21
[합성예 780] Mat 780의 합성[Synthesis Example 780] Synthesis of Mat 780
반응물로 [준비예 128]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 734.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 128] was used as the reactant.; HRMS [M]+: 734.23
[합성예 781] Mat 781의 합성[Synthesis Example 781] Synthesis of Mat 781
반응물로 [준비예 129]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 729.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 129] was used as the reactant.; HRMS [M]+: 729.24
[합성예 782] Mat 782의 합성[Synthesis Example 782] Synthesis of Mat 782
반응물로 [준비예 129]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 745.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 129] was used as the reactant.; HRMS [M]+: 745.27
[합성예 783] Mat 783의 합성[Synthesis Example 783] Synthesis of Mat 783
반응물로 [준비예 129]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 129] was used as the reactant.; HRMS [M]+: 794.22
[합성예 784] Mat 784의 합성[Synthesis Example 784] Synthesis of Mat 784
반응물로 [준비예 129]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 719.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 129] was used as the reactant.; HRMS [M]+: 719.24
[합성예 785] Mat 785의 합성[Synthesis Example 785] Synthesis of Mat 785
반응물로 [준비예 129]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 129] was used as the reactant.; HRMS [M]+: 717.21
[합성예 786] Mat 786의 합성[Synthesis Example 786] Synthesis of Mat 786
반응물로 [준비예 129]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 735.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 129] was used as the reactant.; HRMS [M]+: 735.23
[합성예 787] Mat 787의 합성[Synthesis Example 787] Synthesis of Mat 787
반응물로 [준비예 130]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 729.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 130] was used as the reactant.; HRMS [M]+: 729.24
[합성예 788] Mat 788의 합성[Synthesis Example 788] Synthesis of Mat 788
반응물로 [준비예 130]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 745.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 130] was used as the reactant.; HRMS [M]+: 745.27
[합성예 789] Mat 789의 합성[Synthesis Example 789] Synthesis of Mat 789
반응물로 [준비예 130]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 130] was used as the reactant.; HRMS [M]+: 794.22
[합성예 790] Mat 790의 합성[Synthesis Example 790] Synthesis of Mat 790
반응물로 [준비예 130]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 719.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 130] was used as the reactant.; HRMS [M]+: 719.24
[합성예 791] Mat 791의 합성[Synthesis Example 791] Synthesis of Mat 791
반응물로 [준비예 130]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 130] was used as the reactant.; HRMS [M]+: 717.21
[합성예 792] Mat 792의 합성[Synthesis Example 792] Synthesis of Mat 792
반응물로 [준비예 130]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 735.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 130] was used as the reactant.; HRMS [M]+: 735.23
[합성예 793] Mat 793의 합성[Synthesis Example 793] Synthesis of Mat 793
반응물로 [준비예 131]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 729.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 131] was used as the reactant.; HRMS [M]+: 729.24
[합성예 794] Mat 794의 합성[Synthesis Example 794] Synthesis of Mat 794
반응물로 [준비예 131]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 745.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 131] was used as the reactant.; HRMS [M]+: 745.27
[합성예 795] Mat 795의 합성[Synthesis Example 795] Synthesis of Mat 795
반응물로 [준비예 131]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 131] was used as the reactant.; HRMS [M]+: 794.22
[합성예 796] Mat 796의 합성[Synthesis Example 796] Synthesis of Mat 796
반응물로 [준비예 131]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 719.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 131] was used as the reactant.; HRMS [M]+: 719.24
[합성예 797] Mat 797의 합성[Synthesis Example 797] Synthesis of Mat 797
반응물로 [준비예 131]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 817.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 131] was used as the reactant.; HRMS [M]+: 817.21
[합성예 798] Mat 798의 합성[Synthesis Example 798] Synthesis of Mat 798
반응물로 [준비예 131]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 735.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 131] was used as the reactant.; HRMS [M]+: 735.23
[합성예 799] Mat 799의 합성[Synthesis Example 799] Synthesis of Mat 799
반응물로 [준비예 132]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 729.24The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 132] was used as the reactant.; HRMS [M]+: 729.24
[합성예 800] Mat 800의 합성[Synthesis Example 800] Synthesis of Mat 800
반응물로 [준비예 132]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 745.27The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 132] was used as the reactant.; HRMS [M]+: 745.27
[합성예 801] Mat 801의 합성[Synthesis Example 801] Synthesis of Mat 801
반응물로 [준비예 132]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.22The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 132] was used as the reactant.; HRMS [M]+: 794.22
[합성예 802] Mat 802의 합성[Synthesis Example 802] Synthesis of Mat 802
반응물로 [준비예 132]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 719.24The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 132] was used as the reactant.; HRMS [M]+: 719.24
[합성예 803] Mat 803의 합성[Synthesis Example 803] Synthesis of Mat 803
반응물로 [준비예 132]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 717.21The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 132] was used as the reactant.; HRMS [M]+: 717.21
[합성예 804] Mat 804의 합성[Synthesis Example 804] Synthesis of Mat 804
반응물로 [준비예 132]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 735.23The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 132] was used as the reactant.; HRMS [M]+: 735.23
[합성예 805] Mat 805의 합성[Synthesis Example 805] Synthesis of Mat 805
반응물로 [준비예 133]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 804.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 133] was used as the reactant.; HRMS [M]+: 804.28
[합성예 806] Mat 806의 합성[Synthesis Example 806] Synthesis of Mat 806
반응물로 [준비예 133]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 820.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 133] was used as the reactant.; HRMS [M]+: 820.30
[합성예 807] Mat 807의 합성[Synthesis Example 807] Synthesis of Mat 807
반응물로 [준비예 133]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 869.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 133] was used as the reactant.; HRMS [M]+: 869.26
[합성예 808] Mat 808의 합성[Synthesis Example 808] Synthesis of Mat 808
반응물로 [준비예 133]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 133] was used as the reactant.; HRMS [M]+: 794.27
[합성예 809] Mat 809의 합성[Synthesis Example 809] Synthesis of Mat 809
반응물로 [준비예 133]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 133] was used as the reactant.; HRMS [M]+: 793.24
[합성예 810] Mat 810의 합성[Synthesis Example 810] Synthesis of Mat 810
반응물로 [준비예 133]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 810.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 133] was used as the reactant.; HRMS [M]+: 810.26
[합성예 811] Mat 811의 합성[Synthesis Example 811] Synthesis of Mat 811
반응물로 [준비예 134]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 804.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 134] was used as the reactant.; HRMS [M]+: 804.28
[합성예 812] Mat 812의 합성[Synthesis Example 812] Synthesis of Mat 812
반응물로 [준비예 134]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 820.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 134] was used as the reactant.; HRMS [M]+: 820.30
[합성예 813] Mat 813의 합성[Synthesis Example 813] Synthesis of Mat 813
반응물로 [준비예 134]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 869.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 134] was used as the reactant.; HRMS [M]+: 869.26
[합성예 814] Mat 814의 합성[Synthesis Example 814] Synthesis of Mat 814
반응물로 [준비예 134]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 134] was used as the reactant.; HRMS [M]+: 794.27
[합성예 815] Mat 815의 합성[Synthesis Example 815] Synthesis of Mat 815
반응물로 [준비예 134]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 793.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 134] was used as the reactant.; HRMS [M]+: 793.24
[합성예 816] Mat 816의 합성[Synthesis Example 816] Synthesis of Mat 816
반응물로 [준비예 134]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 810.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 134] was used as the reactant.; HRMS [M]+: 810.26
[합성예 817] Mat 817의 합성[Synthesis Example 817] Synthesis of Mat 817
반응물로 [준비예 135]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 805.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 135] was used as the reactant.; HRMS [M]+: 805.28
[합성예 818] Mat 818의 합성[Synthesis Example 818] Synthesis of Mat 818
반응물로 [준비예 135]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 821.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 135] was used as the reactant.; HRMS [M]+: 821.30
[합성예 819] Mat 819의 합성[Synthesis Example 819] Synthesis of Mat 819
반응물로 [준비예 135]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 870.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 135] was used as the reactant.; HRMS [M]+: 870.26
[합성예 820] Mat 820의 합성[Synthesis Example 820] Synthesis of Mat 820
반응물로 [준비예 135]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 795.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 135] was used as the reactant.; HRMS [M]+: 795.27
[합성예 821] Mat 821의 합성[Synthesis Example 821] Synthesis of Mat 821
반응물로 [준비예 135]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 135] was used as the reactant.; HRMS [M]+: 794.24
[합성예 822] Mat 822의 합성[Synthesis Example 822] Synthesis of Mat 822
반응물로 [준비예 135]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 811.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 135] was used as the reactant.; HRMS [M]+: 811.26
[합성예 823] Mat 823의 합성[Synthesis Example 823] Synthesis of Mat 823
반응물로 [준비예 136]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 805.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 136] was used as the reactant.; HRMS [M]+: 805.28
[합성예 824] Mat 824의 합성[Synthesis Example 824] Synthesis of Mat 824
반응물로 [준비예 136]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 821.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 136] was used as the reactant.; HRMS [M]+: 821.30
[합성예 825] Mat 825의 합성[Synthesis Example 825] Synthesis of Mat 825
반응물로 [준비예 136]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 870.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 136] was used as the reactant.; HRMS [M]+: 870.26
[합성예 826] Mat 826의 합성[Synthesis Example 826] Synthesis of Mat 826
반응물로 [준비예 136]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 795.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 136] was used as the reactant.; HRMS [M]+: 795.27
[합성예 827] Mat 827의 합성[Synthesis Example 827] Synthesis of Mat 827
반응물로 [준비예 136]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 136] was used as the reactant.; HRMS [M]+: 794.24
[합성예 828] Mat 828의 합성[Synthesis Example 828] Synthesis of Mat 828
반응물로 [준비예 136]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 811.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 136] was used as the reactant.; HRMS [M]+: 811.26
[합성예 829] Mat 829의 합성[Synthesis Example 829] Synthesis of Mat 829
반응물로 [준비예 137]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 805.28The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 137] was used as the reactant.; HRMS [M]+: 805.28
[합성예 830] Mat 830의 합성[Synthesis Example 830] Synthesis of Mat 830
반응물로 [준비예 137]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 821.30The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 137] was used as the reactant.; HRMS [M]+: 821.30
[합성예 831] Mat 831의 합성[Synthesis Example 831] Synthesis of Mat 831
반응물로 [준비예 137]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 870.26The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 137] was used as the reactant.; HRMS [M]+: 870.26
[합성예 832] Mat 832의 합성[Synthesis Example 832] Synthesis of Mat 832
반응물로 [준비예 137]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 795.27The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 137] was used as the reactant.; HRMS [M]+: 795.27
[합성예 833] Mat 833의 합성[Synthesis Example 833] Synthesis of Mat 833
반응물로 [준비예 137]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.24The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 137] was used as the reactant.; HRMS [M]+: 794.24
[합성예 834] Mat 834의 합성[Synthesis Example 834] Synthesis of Mat 834
반응물로 [준비예 137]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 811.26The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 137] was used as the reactant.; HRMS [M]+: 811.26
[합성예 835] Mat 835의 합성[Synthesis Example 835] Synthesis of Mat 835
반응물로 [준비예 138]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 778.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 138] was used as the reactant.; HRMS [M]+: 778.26
[합성예 836] Mat 836의 합성[Synthesis Example 836] Synthesis of Mat 836
반응물로 [준비예 138]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 138] was used as the reactant.; HRMS [M]+: 794.29
[합성예 837] Mat 837의 합성[Synthesis Example 837] Synthesis of Mat 837
반응물로 [준비예 138]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 843.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 138] was used as the reactant.; HRMS [M]+: 843.25
[합성예 838] Mat 838의 합성[Synthesis Example 838] Synthesis of Mat 838
반응물로 [준비예 138]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 768.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 138] was used as the reactant.; HRMS [M]+: 768.26
[합성예 839] Mat 839의 합성[Synthesis Example 839] Synthesis of Mat 839
반응물로 [준비예 138]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 767.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 138] was used as the reactant.; HRMS [M]+: 767.23
[합성예 840] Mat 840의 합성[Synthesis Example 840] Synthesis of Mat 840
반응물로 [준비예 138]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 734.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 138] was used as the reactant.; HRMS [M]+: 734.24
[합성예 841] Mat 841의 합성[Synthesis Example 841] Synthesis of Mat 841
반응물로 [준비예 139]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 778.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 139] was used as the reactant.; HRMS [M]+: 778.26
[합성예 842] Mat 842의 합성[Synthesis Example 842] Synthesis of Mat 842
반응물로 [준비예 139]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 139] was used as the reactant.; HRMS [M]+: 794.29
[합성예 843] Mat 843의 합성[Synthesis Example 843] Synthesis of Mat 843
반응물로 [준비예 139]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 843.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 139] was used as the reactant.; HRMS [M]+: 843.25
[합성예 844] Mat 844의 합성[Synthesis Example 844] Synthesis of Mat 844
반응물로 [준비예 139]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 768.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 139] was used as the reactant.; HRMS [M]+: 768.26
[합성예 845] Mat 845의 합성[Synthesis Example 845] Synthesis of Mat 845
반응물로 [준비예 139]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 767.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 139] was used as the reactant.; HRMS [M]+: 767.23
[합성예 846] Mat 846의 합성[Synthesis Example 846] Synthesis of Mat 846
반응물로 [준비예 139]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 734.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 139] was used as the reactant.; HRMS [M]+: 734.24
[합성예 847] Mat 847의 합성[Synthesis Example 847] Synthesis of Mat 847
반응물로 [준비예 140]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 778.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 140] was used as the reactant.; HRMS [M]+: 778.26
[합성예 848] Mat 848의 합성[Synthesis Example 848] Synthesis of Mat 848
반응물로 [준비예 140]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 794.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 140] was used as the reactant.; HRMS [M]+: 794.29
[합성예 849] Mat 849의 합성[Synthesis Example 849] Synthesis of Mat 849
반응물로 [준비예 140]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 843.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 140] was used as the reactant.; HRMS [M]+: 843.25
[합성예 850] Mat 850의 합성[Synthesis Example 850] Synthesis of Mat 850
반응물로 [준비예 140]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 768.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 140] was used as the reactant.; HRMS [M]+: 768.26
[합성예 851] Mat 851의 합성[Synthesis Example 851] Synthesis of Mat 851
반응물로 [준비예 140]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 767.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 140] was used as the reactant.; HRMS [M]+: 767.23
[합성예 852] Mat 852의 합성[Synthesis Example 852] Synthesis of Mat 852
반응물로 [준비예 140]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 734.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 140] was used as the reactant.; HRMS [M]+: 734.24
[합성예 853] Mat 853의 합성[Synthesis Example 853] Synthesis of Mat 853
반응물로 [준비예 141]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 779.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 141] was used as the reactant.; HRMS [M]+: 779.26
[합성예 854] Mat 854의 합성[Synthesis Example 854] Synthesis of Mat 854
반응물로 [준비예 141]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 795.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 141] was used as the reactant.; HRMS [M]+: 795.29
[합성예 855] Mat 855의 합성[Synthesis Example 855] Synthesis of Mat 855
반응물로 [준비예 141]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 844.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 141] was used as the reactant.; HRMS [M]+: 844.25
[합성예 856] Mat 856의 합성[Synthesis Example 856] Synthesis of Mat 856
반응물로 [준비예 141]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다.; HRMS [M]+: 769.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 141] was used as the reactant.; HRMS [M]+: 769.26
[합성예 857] Mat 857의 합성[Synthesis Example 857] Synthesis of Mat 857
반응물로 [준비예 141]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다; HRMS [M]+: 768.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 141] was used as the reactant; HRMS [M]+: 768.23
[합성예 858] Mat 858의 합성[Synthesis Example 858] Synthesis of Mat 858
반응물로 [준비예 141]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다; HRMS [M]+: 735.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 141] was used as the reactant; HRMS [M]+: 735.24
[합성예 859] Mat 859의 합성[Synthesis Example 859] Synthesis of Mat 859
반응물로 [준비예 142]을 사용한 것을 제외하고는 [합성예 1]과 동일한 과정을 수행하여 목적 화합물을 얻었다; HRMS [M]+: 779.26The target compound was obtained by performing the same procedure as in [Synthesis Example 1], except that [Preparation Example 142] was used as a reactant; HRMS [M]+: 779.26
[합성예 860] Mat 860의 합성[Synthesis Example 860] Synthesis of Mat 860
반응물로 [준비예 142]을 사용한 것을 제외하고는 [합성예 2]과 동일한 과정을 수행하여 목적 화합물을 얻었다; HRMS [M]+: 795.29The target compound was obtained by performing the same procedure as in [Synthesis Example 2], except that [Preparation Example 142] was used as a reactant; HRMS [M]+: 795.29
[합성예 861] Mat 861의 합성[Synthesis Example 861] Synthesis of Mat 861
반응물로 [준비예 142]을 사용한 것을 제외하고는 [합성예 3]과 동일한 과정을 수행하여 목적 화합물을 얻었다; HRMS [M]+: 844.25The target compound was obtained by performing the same procedure as in [Synthesis Example 3], except that [Preparation Example 142] was used as a reactant; HRMS [M]+: 844.25
[합성예 862] Mat 862의 합성[Synthesis Example 862] Synthesis of Mat 862
반응물로 [준비예 142]을 사용한 것을 제외하고는 [합성예 4]과 동일한 과정을 수행하여 목적 화합물을 얻었다; HRMS [M]+: 769.26The target compound was obtained by performing the same procedure as in [Synthesis Example 4], except that [Preparation Example 142] was used as a reactant; HRMS [M]+: 769.26
[합성예 863] Mat 863의 합성[Synthesis Example 863] Synthesis of Mat 863
반응물로 [준비예 142]을 사용한 것을 제외하고는 [합성예 5]과 동일한 과정을 수행하여 목적 화합물을 얻었다; HRMS [M]+: 768.23The target compound was obtained by performing the same procedure as in [Synthesis Example 5], except that [Preparation Example 142] was used as the reactant; HRMS [M]+: 768.23
[합성예 864] Mat 864의 합성[Synthesis Example 864] Synthesis of Mat 864
반응물로 [준비예 142]을 사용한 것을 제외하고는 [합성예 6]과 동일한 과정을 수행하여 목적 화합물을 얻었다; HRMS [M]+: 735.24The target compound was obtained by performing the same procedure as in [Synthesis Example 6], except that [Preparation Example 142] was used as a reactant; HRMS [M]+: 735.24
[실시예 1~28] 청색 유기 전계 발광 소자의 제조[Examples 1 to 28] Preparation of blue organic electroluminescent device
합성예에서 합성한 화합물 중 표 1에 있는 전자 수송층 물질을 통상적으로 알려진 방법으로 고순도 승화정제를 한 후 아래의 과정에 따라 청색 유기 EL 소자를 제작하였다.Among the compounds synthesized in Synthesis Example, the electron transport layer material in Table 1 was subjected to high-purity sublimation purification by a commonly known method, and then a blue organic EL device was manufactured according to the following procedure.
ITO (Indium tin oxide)가 1500
Figure PCTKR2020004924-appb-I000172
두께로 박막 코팅된 유리 기판을 증류수 초음파로 세척하였다. 증류수 세척이 끝나면, 이소프로필 알코올, 아세톤, 메탄올 등의 용제로 초음파 세척을 하고, 건조시킨 후, UV OZONE 세정기(Power sonic 405, 화신테크)로 이송시킨 다음, UV를 이용하여 상기 기판을 5분간 세정하고 진공 증착기로 기판을 이송하였다.
ITO (Indium tin oxide) is 1500
Figure PCTKR2020004924-appb-I000172
The glass substrate coated with a thin film to a thickness was washed with distilled water and ultrasonic waves. After washing with distilled water, ultrasonically clean with a solvent such as isopropyl alcohol, acetone, methanol, etc., dry, and transfer to a UV OZONE cleaner (Power Sonic 405, Hwashin Tech), and then use UV for 5 minutes. It was cleaned and the substrate was transferred to a vacuum evaporator.
상기와 같이 준비된 ITO 투명 전극 위에, DS-205 (80 nm)/NPB (15 nm)/ADN + 5 % DS-405 (30nm)/표 1에 기재된 화합물(30 nm)/LiF (1 nm)/Al (200 nm) 순으로 적층하여 유기 전계 발광 소자를 제조하였다.On the ITO transparent electrode prepared as above, DS-205 (80 nm)/NPB (15 nm)/ADN + 5% DS-405 (30 nm)/compounds described in Table 1 (30 nm)/LiF (1 nm)/ Al (200 nm) was sequentially stacked to prepare an organic electroluminescent device.
이때 사용된 NPB, ADN 및 Alq3의 구조는 다음과 같다.The structures of NPB, ADN and Alq 3 used at this time are as follows.
Figure PCTKR2020004924-appb-I000173
Figure PCTKR2020004924-appb-I000173
[비교예 1] 청색 유기 전계 발광 소자의 제조[Comparative Example 1] Preparation of blue organic electroluminescent device
전자 수송층 물질로 화합물 1 대신 Alq3을 30nm로 증착하는 것을 제외하고는, 실시예 1과 동일하게 수행하여 청색 유기 전계 발광 소자를 제작하였다.A blue organic electroluminescent device was manufactured in the same manner as in Example 1, except that Alq 3 was deposited at 30 nm instead of Compound 1 as an electron transport layer material.
[평가예 1][Evaluation Example 1]
실시예 1 내지 28및 비교예 1에서 각각 제조된 유기 전계 발광 소자에 대하여, 전류밀도 10 mA/㎠에서의 구동전압, 전류효율, 발광파장을 측정하였고, 그 결과를 하기 표 1에 나타내었다.For the organic electroluminescent devices prepared in Examples 1 to 28 and Comparative Example 1, respectively, the driving voltage, current efficiency, and emission wavelength at a current density of 10 mA/cm2 were measured, and the results are shown in Table 1 below.
Figure PCTKR2020004924-appb-T000001
Figure PCTKR2020004924-appb-T000001
상기 표1에 나타낸 바와 같이, 본 발명에 따른 화합물을 청색 유기 EL 소자의 전자 수송층 물질로 사용하였을 경우(실시예 1-28) 종래 Alq3를 사용한 청색 유기 EL 소자(비교예1)와 비교해 볼 때 효율 및 구동전압 면에서 보다 우수한 성능을 나타내는 것을 알 수 있다.As shown in Table 1 above, when the compound according to the present invention is used as an electron transport layer material of a blue organic EL device (Example 1-28), it will be compared with a blue organic EL device using Alq 3 (Comparative Example 1). It can be seen that it shows better performance in terms of efficiency and driving voltage.
[실시예 29 ~ 62] 녹색 유기 EL 소자의 제작[Examples 29 to 62] Fabrication of green organic EL device
합성예에서 합성한 화합물 중 표 2에 있는 물질을 통상적으로 알려진 방법으로 고순도 승화정제를 한 후 아래의 과정에 따라 녹색 유기 EL 소자를 제작하였다.Among the compounds synthesized in Synthesis Example, the materials in Table 2 were subjected to high-purity sublimation purification by a commonly known method, and then a green organic EL device was manufactured according to the following procedure.
먼저, ITO (Indium tin oxide)가 1500
Figure PCTKR2020004924-appb-I000174
두께로 박막 코팅된 유리 기판을 증류수 초음파로 세척하였다. 증류수 세척이 끝나면 이소프로필 알코올, 아세톤, 메탄올 등의 용제로 초음파 세척을 하고 건조시킨 후 UV OZONE 세정기 (Power sonic 405, 화신테크)로 이송시킨 다음 UV를 이용하여 상기 기판을 5분간 세정하고 진공 증착기로 기판을 이송하였다.
First, ITO (Indium tin oxide) is 1500
Figure PCTKR2020004924-appb-I000174
The glass substrate coated with a thin film to a thickness was washed with distilled water and ultrasonic waves. After washing with distilled water, ultrasonically clean with a solvent such as isopropyl alcohol, acetone, methanol, etc., dry, transfer to a UV OZONE cleaner (Power Sonic 405, Hwashin Tech), and clean the substrate for 5 minutes using UV and a vacuum evaporator. The substrate was transferred to the furnace.
이렇게 준비된 ITO 투명 전극 위에 m-MTDATA (60 nm)/TCTA (80 nm)/ 표 2의 각각의 화합물 + 10 % Ir(ppy)3 (300nm)/BCP (10 nm)/Alq3 (30 nm)/LiF (1 nm)/Al (200 nm) 순으로 적층하여 유기 EL 소자를 제작하였다.On the prepared ITO transparent electrode, m-MTDATA (60 nm)/TCTA (80 nm)/each compound of Table 2 + 10% Ir(ppy) 3 (300 nm)/BCP (10 nm)/Alq 3 (30 nm) /LiF (1 nm)/Al (200 nm) was stacked in order to fabricate an organic EL device.
m-MTDATA, TCTA, Ir(ppy)3, CBP 및 BCP의 구조는 하기와 같다.The structures of m-MTDATA, TCTA, Ir(ppy) 3 , CBP and BCP are as follows.
[규칙 제91조에 의한 정정 07.05.2020] 
Figure WO-DOC-FIGURE-cm2
[Correction 07.05.2020 pursuant to Rule 91]
Figure WO-DOC-FIGURE-cm2
[비교예 2] 녹색 유기 EL 소자의 제작[Comparative Example 2] Fabrication of green organic EL device
발광층 형성시 발광 호스트 물질로서 합성예에서 합성한 화합물대신 CBP를 사용하는 것을 제외하고는 실시예 29와 동일한 과정으로 녹색 유기 EL 소자를 제작하였다.A green organic EL device was manufactured in the same manner as in Example 29, except that CBP was used instead of the compound synthesized in Synthesis Example as a light emitting host material when forming the emission layer.
[평가예][Evaluation example]
실시예 29 ~ 62 및 비교예 2에서 제작한 각각의 녹색 유기 EL 소자에 대하여 전류밀도 10 mA/㎠에서의 구동전압, 전류효율 및 발광 피크를 측정하고, 그 결과를 하기 표 2에 나타내었다.For each of the green organic EL devices manufactured in Examples 29 to 62 and Comparative Example 2, the driving voltage, current efficiency, and emission peak at a current density of 10 mA/cm 2 were measured, and the results are shown in Table 2 below.
Figure PCTKR2020004924-appb-T000002
Figure PCTKR2020004924-appb-T000002
상기 표2에 나타낸 바와 같이, 본 발명에 따른 화합물을 녹색 유기 EL 소자의 발광층 호스트 물질로 사용하였을 경우(실시예 29-62) 종래 CBP를 사용한 녹색 유기 EL 소자(비교예2)와 비교해 볼 때 효율 및 구동전압 면에서 보다 우수한 성능을 나타내는 것을 알 수 있다.As shown in Table 2 above, when the compound according to the present invention was used as a host material for the emission layer of a green organic EL device (Examples 29-62) compared with a green organic EL device using a conventional CBP (Comparative Example 2). It can be seen that it shows better performance in terms of efficiency and driving voltage.
본 발명은 유기 전계 발광 소자용 재료로서 사용될 수 있는 신규 유기 화합물 및 이를 포함하는 유기 전계 발광 소자에 관한 것이다.The present invention relates to a novel organic compound that can be used as a material for an organic electroluminescent device and an organic electroluminescent device including the same.

Claims (10)

  1. 하기 화학식 1로 표시되는 화합물을 제공한다.It provides a compound represented by the following formula (1).
    [화학식 1][Formula 1]
    Figure PCTKR2020004924-appb-I000176
    Figure PCTKR2020004924-appb-I000176
    상기 화학식 1에서,In Formula 1,
    X1 내지 X3은 각각 독립적으로 N 또는 C(R1)이나, 이들 중 적어도 둘 이상은 N이고, R1은 수소이거나 치환 또는 비치환된 C1~C60의 알킬이고,X 1 to X 3 are each independently N or C (R 1 ), but at least two or more of them are N, and R 1 is hydrogen or a substituted or unsubstituted C 1 to C 60 alkyl,
    L1 내지 L4는 각각 독립적으로 직접결합, 또는 C6~C18의 아릴렌기 및 핵원자수 5 내지 18개의 헤테로아릴렌기로 이루어진 군에서 선택되며,L 1 to L 4 are each independently a direct bond, or selected from the group consisting of an arylene group of C 6 to C 18 and a heteroarylene group having 5 to 18 nuclear atoms,
    A와 B는 각각 독립적으로 치환 또는 비치환된 C6~C60의 아릴기 또는 핵원자수 5 내지 60개의 헤테로아릴기이며, 적어도 하나 이상은 함질소복소환을 포함하는 헤테로아릴기이며,A and B are each independently a substituted or unsubstituted C 6 to C 60 aryl group or a heteroaryl group having 5 to 60 nuclear atoms, and at least one is a heteroaryl group including a nitrogen-containing heterocycle,
    Ar1 과 Ar2는 C6~C60의 아릴기 또는 핵원자수 5 내지 60개의 헤테로아릴기이며, 적어도 하나 이상은 함질소복소환을 포함하는 헤테로아릴기이며,Ar 1 and Ar 2 are C 6 to C 60 aryl group or a heteroaryl group having 5 to 60 nuclear atoms, and at least one is a heteroaryl group including a nitrogen-containing heterocycle,
    상기 L1 내지 L4의 아릴렌기 및 헤테로아릴렌기와, 상기 A, B, Ar1 및 Ar2의 아릴기 및 헤테로아릴기는 각각 독립적으로 중수소, 할로겐, 시아노기, 니트로기, C1~C40의 알킬기, C2~C40의 알케닐기, C2~C40의 알키닐기, C6~C60의 아릴기, 핵원자수 5 내지 60개의 헤테로아릴기, C6~C60의 아릴옥시기, C1~C40의 알킬옥시기, C6~C60의 아릴아민기, C3~C40의 시클로알킬기, 핵원자수 3 내지 40개의 헤테로시클로알킬기, C1~C40의 알킬실릴기, C1~C40의 알킬보론기, C6~C60의 아릴보론기, C6~C60의 아릴포스핀기, C6~C60의 모노 또는 디아릴포스피닐기 및 C6~C60의 아릴실릴기로 이루어진 군에서 선택된 1종 이상의 치환기로 치환되거나 비치환되고, 복수 개의 치환기로 치환되는 경우, 이들은 서로 동일하거나 상이할 수 있다.The arylene group and heteroarylene group of L 1 to L 4, the aryl group and heteroaryl group of A, B, Ar 1 and Ar 2 are each independently deuterium, halogen, cyano group, nitro group, C 1 to C 40 Alkyl group, C 2 ~ C 40 alkenyl group, C 2 ~ C 40 alkynyl group, C 6 ~ C 60 aryl group, 5 to 60 nuclear atoms heteroaryl group, C 6 ~ C 60 aryloxy group , C 1 ~ C 40 alkyloxy group, C 6 ~ C 60 arylamine group, C 3 ~ C 40 cycloalkyl group, 3 to 40 nuclear atoms heterocycloalkyl group, C 1 ~ C 40 alkylsilyl group , C 1 ~ C 40 alkyl boron group, C 6 ~ C 60 aryl boron group, C 6 ~ C 60 arylphosphine group, C 6 ~ C 60 mono or diarylphosphine group and C 6 ~ C 60 When substituted or unsubstituted with one or more substituents selected from the group consisting of an arylsilyl group of, and when substituted with a plurality of substituents, they may be the same or different from each other.
  2. 제1항에 있어서,The method of claim 1,
    상기 화학식 1로 표시되는 화합물은 하기 화합식 1-1 또는 1-2로 표시되는 것을 특징으로 하는 화합물:The compound represented by Formula 1 is a compound characterized in that it is represented by the following Formula 1-1 or 1-2:
    [화학식 1-1][Formula 1-1]
    Figure PCTKR2020004924-appb-I000177
    Figure PCTKR2020004924-appb-I000177
    [화학식 1-2][Formula 1-2]
    Figure PCTKR2020004924-appb-I000178
    Figure PCTKR2020004924-appb-I000178
    상기 화학식 1-1 및 화학식 1-2에서,In Formula 1-1 and Formula 1-2,
    A, B, L1 내지 L4, Ar1 및 Ar2는 청구항 1에서 정의한 바와 같다.A, B, L1 to L4, Ar1 and Ar2 are as defined in claim 1.
  3. 제1항에 있어서,The method of claim 1,
    상기 A 및 B는 각각 독립적으로 하기 치환기 군으로부터 어느 하나 선택되며, 적어도 하나 이상은 함질소복소환을 포함하는 치환기인 것을 특징으로 하는 화합물:A compound, wherein A and B are each independently selected from the following substituent groups, and at least one is a substituent containing a nitrogen-containing heterocycle:
    Figure PCTKR2020004924-appb-I000179
    Figure PCTKR2020004924-appb-I000179
    상기 치환기 군에서 *는 결합이 이루어지는 부분이다.In the above substituent group, * is a moiety in which a bond is formed.
  4. 제1항에 있어서,The method of claim 1,
    상기 Ar1 및 Ar2는 각각 독립적으로 하기 치환기 군으로부터 어느 하나 선택되며, 적어도 하나 이상은 함질소복소환을 포함하는 치환기인 것을 특징으로 하는 화합물:Wherein Ar1 and Ar2 are each independently selected from the following substituent groups, and at least one is a compound characterized in that it is a substituent containing a nitrogen-containing heterocycle:
    Figure PCTKR2020004924-appb-I000180
    Figure PCTKR2020004924-appb-I000180
    상기 치환기 군에서 *는 결합이 이루어지는 부분이다.In the above substituent group, * is a moiety in which a bond is formed.
  5. 제1항에 있어서,The method of claim 1,
    상기 A, B, Ar1 및 Ar2는 서로 상이한 것을 특징으로 하는 화합물.A, B, Ar1 and Ar2 are a compound, characterized in that different from each other.
  6. 제1항에 있어서,The method of claim 1,
    상기 L1 내지 L4는 각각 독립적으로 직접결합 또는 아릴렌인 것을 특징으로 하는 화합물,The compound, characterized in that the L1 to L4 are each independently a direct bond or an arylene,
  7. 제1항에 있어서,The method of claim 1,
    상기 화합물은 하기 화합물로 이루어진 군에서 선택되는 것을 특징으로 하는 화합물.The compound is a compound, characterized in that selected from the group consisting of the following compounds.
    Figure PCTKR2020004924-appb-I000181
    Figure PCTKR2020004924-appb-I000181
    Figure PCTKR2020004924-appb-I000182
    Figure PCTKR2020004924-appb-I000182
    Figure PCTKR2020004924-appb-I000183
    Figure PCTKR2020004924-appb-I000183
    Figure PCTKR2020004924-appb-I000184
    Figure PCTKR2020004924-appb-I000184
    Figure PCTKR2020004924-appb-I000185
    Figure PCTKR2020004924-appb-I000185
    Figure PCTKR2020004924-appb-I000186
    Figure PCTKR2020004924-appb-I000186
    Figure PCTKR2020004924-appb-I000187
    Figure PCTKR2020004924-appb-I000187
    Figure PCTKR2020004924-appb-I000188
    Figure PCTKR2020004924-appb-I000188
    Figure PCTKR2020004924-appb-I000189
    Figure PCTKR2020004924-appb-I000189
    Figure PCTKR2020004924-appb-I000190
    Figure PCTKR2020004924-appb-I000190
    Figure PCTKR2020004924-appb-I000191
    Figure PCTKR2020004924-appb-I000191
    Figure PCTKR2020004924-appb-I000192
    Figure PCTKR2020004924-appb-I000192
    Figure PCTKR2020004924-appb-I000193
    Figure PCTKR2020004924-appb-I000193
    Figure PCTKR2020004924-appb-I000194
    Figure PCTKR2020004924-appb-I000194
    Figure PCTKR2020004924-appb-I000195
    Figure PCTKR2020004924-appb-I000195
    Figure PCTKR2020004924-appb-I000196
    Figure PCTKR2020004924-appb-I000196
    Figure PCTKR2020004924-appb-I000197
    Figure PCTKR2020004924-appb-I000197
    Figure PCTKR2020004924-appb-I000198
    Figure PCTKR2020004924-appb-I000198
  8. (i) 양극, (ii) 음극, 및 (iii) 상기 양극과 음극 사이에 개재(介在)된 1층 이상의 유기물층을 포함하는 유기 전계 발광 소자로서,An organic electroluminescent device comprising (i) an anode, (ii) a cathode, and (iii) at least one organic material layer interposed between the anode and the cathode,
    상기 1층 이상의 유기물층 중에서 적어도 하나는 제1항의 화학식 1로 표시되는 화합물을 포함하는 것을 특징으로 하는 유기 전계 발광 소자.At least one of the one or more organic material layers comprises a compound represented by Chemical Formula 1 of claim 1.
  9. 제8항에 있어서,The method of claim 8,
    상기 유기물층은 정공 주입층, 정공 수송층, 정공 수송 보조층, 전자 수송층, 전자 수송 보조층 및 발광층으로 이루어진 군에서 선택되는 하나 이상의 층을 포함하는, 유기 전계 발광 소자.The organic material layer includes at least one layer selected from the group consisting of a hole injection layer, a hole transport layer, a hole transport auxiliary layer, an electron transport layer, an electron transport auxiliary layer, and a light emitting layer.
  10. 제8항에 있어서,The method of claim 8,
    상기 유기물층은 전자 수송층, 전자 수송 보조층 및 발광층으로 이루어진 군에서 선택되는 하나 이상의 층을 포함하는, 유기 전계 발광 소자.The organic material layer includes at least one layer selected from the group consisting of an electron transport layer, an electron transport auxiliary layer, and an emission layer.
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KR20140087804A (en) * 2012-12-31 2014-07-09 제일모직주식회사 COMPOUND FOR ORGANIC OPTOELECTRONIC DEVICE, ORGANIC LiGHT EMITTING DIODE INCLUDING THE SAME AND DISPLAY INCLUDING THE ORGANIC LiGHT EMITTING DIODE
KR20150142822A (en) * 2014-06-11 2015-12-23 삼성디스플레이 주식회사 Organic light-emitting devices
KR20160007985A (en) * 2014-07-10 2016-01-21 삼성디스플레이 주식회사 Organic light emitting diode and organic light emitting display device including the same
KR20160090238A (en) * 2015-01-20 2016-07-29 삼성디스플레이 주식회사 Organic light-emitting device

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KR20230137903A (en) 2021-01-29 2023-10-05 이데미쓰 고산 가부시키가이샤 Compounds, materials for organic electroluminescent devices, organic electroluminescent devices and electronic devices
EP4043453A1 (en) 2021-02-11 2022-08-17 Idemitsu Kosan Co., Ltd. Compound, material for an organic electroluminescence device and an organic electroluminescence device comprising the compound

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