WO2020051924A1 - Tmr array scanning type rock magnetic detector - Google Patents

Tmr array scanning type rock magnetic detector Download PDF

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Publication number
WO2020051924A1
WO2020051924A1 PCT/CN2018/105903 CN2018105903W WO2020051924A1 WO 2020051924 A1 WO2020051924 A1 WO 2020051924A1 CN 2018105903 W CN2018105903 W CN 2018105903W WO 2020051924 A1 WO2020051924 A1 WO 2020051924A1
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tmr
sample
magnetic
demagnetization
rock
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PCT/CN2018/105903
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French (fr)
Chinese (zh)
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刘双迟
秦华峰
刘青松
李金华
潘永信
朱日祥
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中国科学院地质与地球物理研究所
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Publication of WO2020051924A1 publication Critical patent/WO2020051924A1/en

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00Arrangements or instruments for measuring magnetic variables
    • G01R33/12Measuring magnetic properties of articles or specimens of solids or fluids

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  • the invention relates to the technical field of magnetic measurement, in particular to a TMR array scanning type rock magnetic detector.
  • Rock contains magnetic minerals, and its magnetic properties are of great significance in geological research.
  • a special mineral using its type, particle size, and content information, it can sensitively track a variety of geological and environmental processes, such as mineral generation, migration, and transformation processes (called environmental magnetism).
  • magnetic minerals can be oriented in a geomagnetic field environment. The geomagnetic field at that time is recorded by mechanisms such as thermal remanence (volcanic rocks) and sedimentary remanence (sedimentary rocks or sediments). Information can restore the information of the geomagnetic field at that time (called paleomagnetism). Therefore, the magnetic properties of rocks can be widely used to study geological structure and environmental evolution, petroleum and mineral exploration, deep earth dynamics, sedimentary sequence dating, and archeology.
  • Paleomagnetic research generally uses superconducting magnetometers, rotating magnetometers, vibrating sample magnetometers, and variable gradient magnetometers to measure the magnetic properties of rock samples. These systems measure the residual magnetism carried by the entire rock sample, which is the superposition of information of all magnetic particles in the sample, but cannot distinguish and extract the information of a single magnetic particle in the sample. With the deepening of the research, in practical applications, we need to know exactly the spatial distribution of magnetic particles and the particle size distribution characteristics of magnetic particles in the sample at the micron level.
  • the distribution pattern of magnetic particles in meteorites carries rich meteorite evolution information; stalagmites and deep-sea manganese stones have lower deposition rates. If it can recognize the magnetism at the micron level, it can construct high-precision environmental evolution information, which will greatly promote the development of related disciplines, which has important scientific significance.
  • the magnetic field scanning technology came into being, which can sensitively measure the magnetic field distribution on the surface of rock samples, and further calculate the distribution characteristics of magnetic particles in the rock.
  • the residual magnetism of the entire sample can also be calculated statistically.
  • the superconducting technology is expensive; the second is limited by the need to equip a low temperature system, and the probe must be separated from the sample by a distance to reduce its spatial resolution.
  • TMR (TunnelMagnetoResistance) element is a new type of magnetoresistance effect sensor that has begun industrial applications in recent years. It uses the tunnel magnetoresistance effect of magnetic multilayer film materials to induce magnetic fields, which is more than previously discovered and practically applied.
  • AMR (Anisotropic Magneto Resistance) and GMR (Giant Magneto Resistance) elements have greater resistance change rates.
  • TMR element has better temperature stability, higher sensitivity, lower power consumption, better linearity than Hall element, and does not require additional magnetic ring structure; better temperature than AMR element Stability, higher sensitivity, wider linear range, no need for additional set / reset coil structure; better temperature stability, higher sensitivity, lower power consumption, wider Linear range. Based on the above advantages, this sensor has begun to be gradually applied to high-precision technology fields such as information technology, automotive electronics, and biomedicine.
  • the general rock magnetic scanning system can only measure the surface magnetism, and does not have the function of in-situ magnetization and demagnetization of the sample.
  • the sample needs to be taken out of the magnetic shielding room and processed by a special magnetization and demagnetization device. After putting it back into the scanning system, it is difficult to ensure that the rocks are placed in the same position before and after the processing, which is not conducive to comparing the magnetic distribution before and after.
  • the technical problem to be solved by the present invention is to provide a TMR array scanning type rock magnetic detector for one or more of the defects in the prior art.
  • the present invention provides a TMR array scanning rock magnetic detector, including:
  • a sample positioning system includes a three-dimensional sample moving stage for placing a rock specimen, and a sample stage controller for adjusting the position of the three-dimensional sample moving stage; a sample support rod is provided on the three-dimensional sample moving stage;
  • a TMR magnetic field detection system includes a TMR probe array and a TMR circuit for driving the TMR probe array for magnetic field detection;
  • Magnetization demagnetization system including a magnetization demagnetization coil set outside a rock specimen, and a coil control circuit connected thereto;
  • a data processing control system which is connected to the TMR circuit, the coil control circuit, and the sample stage controller, and is used to accept user input and send TMR scanning instructions, magnetization or demagnetization instructions, and sample stage movement instructions to the TMR circuit, coil control, respectively. Circuit and sample stage controller.
  • the coil control circuit includes:
  • a pulse power supply connected to the data processing control system through a data acquisition card, and configured to generate a magnetization pulse current corresponding to a current intensity according to a magnetization instruction issued by the data processing control system;
  • a signal source connected to the data processing control system, and configured to generate a sine wave demagnetizing electrical signal of a corresponding frequency according to a demagnetization instruction issued by the data processing control system;
  • a power amplifier connected to the signal source and configured to amplify the sine wave demagnetized electrical signal generated by the signal source to a corresponding amplitude and output;
  • a switch is connected to the pulse power source and the power amplifier, and is used to switch the magnetization pulse current or the amplified sine wave demagnetization electric signal to the magnetization demagnetization coil to generate a magnetic field of a predetermined strength, and to perform the function of switching magnetization or demagnetization the goal of.
  • the three-dimensional sample moving stage is provided with a stepping motor and a grating scale displacement sensor;
  • the sample stage controller includes: a motor controller, connected to the data processing control system, for receiving a movement command of the sample stage to generate a motor control signal, and using the position information fed back by the grating scale displacement sensor to implement closed-loop control.
  • the positioning of the sample support rod a motor driver connected to the motor controller and configured to receive a motor control electrical signal and generate a driving signal to the stepper motor.
  • the sample supporting rods are horizontally arranged; there are three stepping motors, which are respectively used to control the sample supporting rods to move in three dimensions. .
  • the length of the sample support rod is 30 cm to 100 cm.
  • the three-dimensional sample moving stage and the sample support rod are made of non-magnetic materials.
  • the stepping motor is a piezoelectric ceramic ultrasonic motor.
  • the TMR probe array, the three-dimensional sample moving stage, and the magnetization demagnetization coil are all placed in a magnetic shielding room.
  • the TMR array scanning type rock magnetic detector further includes a TMR probe array and a sample support rod that are sleeved outside the TMR probe array and the sample support rod during magnetic field detection.
  • Magnetic shielding cylinder the magnetic shielding chamber is used to shield the internal magnetic field to 100nT and below; the magnetic shielding cylinder is used to shield the internal magnetic field to 10nT and below.
  • the implementation of the TMR array scanning rock magnetic detector of the present invention has the following beneficial effects:
  • the present invention uses the TMR sensor array and a mobile platform to construct the TMR array scanning rock magnetic detector, which can realize high-precision and high-resolution magnetic scanning of rock specimens.
  • a special magnetization demagnetization system is set up to perform in-situ magnetization and demagnetization without moving the rock specimen, which is convenient for comparing the magnetic distribution before and after.
  • FIG. 1 is a schematic structural diagram of a TMR array scanning rock magnetic detector according to a first embodiment of the present invention
  • FIG. 2 is a schematic structural diagram of a TMR array scanning rock magnetic detector according to a second embodiment of the present invention.
  • FIG. 3 is a schematic diagram of a magnetizing circuit in a TMR array scanning rock magnetic detector according to a second embodiment of the present invention.
  • FIG. 4 is a schematic diagram of a demagnetization circuit in a TMR array scanning rock magnetic detector according to a second embodiment of the present invention.
  • FIG. 5 is a schematic structural diagram of a magnetization demagnetization coil in a TMR array scanning rock magnetic detector according to a second embodiment of the present invention.
  • FIG. 6 is a schematic structural diagram of a three-dimensional sample moving stage in a TMR array scanning rock magnetic detector according to the present invention.
  • FIG. 1 is a schematic structural diagram of a TMR array scanning rock magnetic detector according to a first embodiment of the present invention.
  • the TMR array scanning rock magnetic detector provided in this embodiment includes at least: a sample positioning system, a TMR magnetic field detection system, a magnetization demagnetization system, and a data processing control system.
  • the sample positioning system includes a three-dimensional sample moving stage 10 for placing a rock specimen 1, and a sample stage controller 20 for adjusting the position of the three-dimensional sample moving stage 10.
  • the three-dimensional sample moving stage is provided with a sample support rod 11 for placing a rock specimen 1.
  • the TMR magnetic field detection system includes a TMR probe array 30 and a TMR circuit 40 for driving the TMR probe array 30 for magnetic field detection.
  • the number of TMR sensors in the TMR probe array 30 is n * n.
  • the magnetization demagnetization system includes a magnetization demagnetization coil 50 sleeved outside the rock specimen 30 and a coil control circuit 60 connected to the magnetization demagnetization coil 50.
  • the data processing control system 70 is connected to the TMR circuit 40, the coil control circuit 60, and the sample stage controller 20, and is used to accept user input and send TMR scan instructions, magnetization or demagnetization instructions, and sample stage movement instructions to the TMR circuit 40, coil control, respectively. Circuit 60 and sample stage controller 20.
  • the data processing control system 70 can be implemented by, for example, a computer.
  • FIG. 2 is a schematic structural diagram of a TMR array scanning rock magnetic detector according to a second embodiment of the present invention. As shown in FIG. 2, on the basis of the first embodiment, a specific implementation manner of each system is provided.
  • the TMR circuit 40 includes a TMR controller 41 and a preamplifier 42.
  • the TMR controller 41 is connected to the data processing control system 70 through a data acquisition card 71, and is configured to receive a TMR scan instruction issued by the data processing control system 70 and generate a TMR control signal.
  • the preamplifier 42 is connected to the TMR controller 41 and is used to amplify and filter the TMR control signal and output a voltage proportional to the magnetic field signal to the TMR probe array 30.
  • the TMR probe array 30 in the present invention may be selected from a plurality of TMR sensors and arranged in a matrix.
  • the TMR sensor has a linear measurement range of ⁇ 50Oe, a magnetic field resolution of 2nT / Hz 1/2 @ 100Hz, and a measurement area of 1 ⁇ 2 microns, which is very suitable for scanning weak magnetic samples.
  • This TMR sensor will form a TMR matrix with a total of 16 sensors arranged in a matrix of 4 ⁇ 4.
  • the collection of array data can accelerate the measurement speed and achieve spatial resolution on the micrometer scale.
  • the preamplifier 42 can use a power supply with noise attenuation of more than 100 dB to reduce noise.
  • the coil control circuit 60 includes a pulse power source 61, a signal source 62, a power amplifier 63, and a circuit breaker 64.
  • the pulse power source 61 is connected to the data processing control system 70 through the data acquisition card 71, and is configured to generate a magnetized pulse current corresponding to the current intensity according to the magnetization instruction issued by the data processing control system 70.
  • FIG. 3 is a schematic diagram of a magnetizing circuit in a TMR array scanning rock magnetic detector according to a second embodiment of the present invention.
  • the pulse magnetization of the present invention can use a capacitor discharge pulse magnetization technique. Pulse power supply, the maximum voltage can reach 1500V, charge the internal capacitor balance current, the current is 1-1.5A, the magnetization demagnetizing coil inductance is 32.4mH, the resistance is 1.727ohm, when the capacitance value is 300 ⁇ F, the capacitor can be charged to 1300V.
  • the pulse power supply can have four signal interfaces, as shown in the figure:
  • Analog voltage input used to set the voltage across the capacitor. When the capacitor voltage reaches the set value, the hardware turns off the charging circuit;
  • Analog voltage output the voltage sensor returns the voltage across the capacitor to the data acquisition card 71;
  • the signal source 62 is connected to the data processing control system 70, and is configured to generate a sine wave demagnetizing electrical signal with a corresponding frequency according to a demagnetization instruction issued by the data processing control system 70.
  • the power amplifier 63 is connected to the signal source 62 and is used to amplify the sine wave demagnetized electrical signal generated by the signal source 62 to a corresponding amplitude and output.
  • FIG. 4 is a schematic diagram of a demagnetization circuit in a TMR array scanning rock magnetic detector according to a second embodiment of the present invention.
  • the AC demagnetization field uses a signal source 62 and a power amplifier 63 to drive the magnetization demagnetization coil.
  • the signal source 62 is realized by a single-chip microcomputer 622 and an AD9854 chip 621, and the output frequency is 400 Hz, and the voltage amplitude decreases linearly with a sine wave (the magnetic field 200mT is attenuated to 0mT).
  • the single-chip microcomputer 622 communicates with the computer 72 through the RS232 serial port and waits for the computer's demagnetization instruction.
  • the demagnetization instruction set by the PC can change the amplitude and frequency of the output signal, and the output instruction control signal source 62 outputs a signal to the power amplifier for demagnetization.
  • an audio power amplifier 631 can be used as the power amplifier.
  • the professional amplifier CA20 of commercial sound precision company is used, 8ohm stereo power is 1300w, 4ohm stereo power is 2000w, and 2ohm stereo power is 2600w.
  • a maximum current of 36A can be achieved with a 2ohm load.
  • the maximum voltage calculated by 8ohm can reach 102V.
  • AD9854DDS chip can output sine wave with adjustable frequency, phase and amplitude.
  • 32-bit frequency control word, frequency accuracy can reach 0.0466Hz
  • 14-bit amplitude control word 21A maximum current (200mT magnetic field)
  • control accuracy can reach 0.0013A (12.2 ⁇ T).
  • the frequency of demagnetization is selected as 400Hz.
  • the resistance of the magnetization demagnetization coil 50 is affected by the proximity effect and becomes 2.499ohm. Due to the presence of the inductance, the impedance of the entire load is very large.
  • Use capacitors for tuning For resistance only, tuning is performed with CBB capacitors in series and parallel. The tuning capacitor is 1.221 ⁇ F.
  • the switch 64 is connected to the pulse power source 61 and the power amplifier 63, and is used to switch the magnetization pulse current or the amplified sine wave demagnetization electric signal to the magnetization demagnetization coil 50 to generate a magnetic field of a predetermined strength and to perform the function of switching the magnetization and demagnetization. purpose.
  • pulse power source 61 the pulse power source 61
  • the signal source 62 the signal source 62
  • the power amplifier 63 the power amplifier 63 that can be applied in the prior art.
  • FIG. 5 is a schematic structural diagram of a magnetization demagnetization coil in a TMR array scanning rock magnetic detector according to a second embodiment of the present invention.
  • the measurement of saturated isothermal remanence requires magnetization and demagnetization of the sample, and the TMR probe array is used to measure the remanence signal of the rock specimen.
  • This part mainly includes the design of DC magnetizing magnetic field coil and alternating magnetic field coil, so that the generated magnetic field has high uniformity and resolution.
  • the manufactured magnetized demagnetizing coil is placed on a coil bobbin, and the coil bobbin may be epoxy material. Rock specimens are placed in the internal cavity of the magnetized demagnetization coil.
  • the sample positioning system of the present invention can realize three-dimensional precise movement and positioning of a sample.
  • the three-dimensional sample moving stage 10 is provided with a stepping motor 13 and a scale displacement sensor 14.
  • the sample stage controller 20 further includes a motor controller 21 and a motor driver 22.
  • the motor controller 21 is connected to the data processing control system 70, and is used to receive the sample table movement instruction to generate a motor control signal, and use the position information fed back by the scale displacement sensor 14 to implement closed-loop control of the movement positioning of the rock specimen on the sample support rod 11.
  • the motor driver 22 is connected to the motor controller 21, and is used for receiving a motor control signal and generating a driving electric signal to the stepping motor 13.
  • the three-dimensional movement and positioning of the three-dimensional sample moving stage 10 are realized by three stepping motors 13 respectively.
  • the stepping motor 13 is preferably a piezoelectric ceramic ultrasonic motor to reduce the residual magnetism of the motor itself.
  • the motor driver of the piezoelectric ceramic ultrasonic motor can be an AB1A driver.
  • the motor driver receives an analog signal instruction of +/- 10V from the motor controller and converts the control signal into an AC voltage to drive the motor.
  • the motor controller 21 uses the motion control card DMC 18X2, and the DMC18X2 control card is directly inserted into the PCI card slot of the computer. These two control cards can control 1-4 axes respectively, which can meet the control requirements of the three-dimensional mobile platform . It can provide +/- 10V analog signal command for standard servo system.
  • the design and production of the rock specimen rack of the present invention requires that the sample support rod 11 be non-magnetic material and is very close to the superconducting receiving coil of the TMR probe array, so as to reduce the attenuation loss of the residual magnetic signal of the rock specimen.
  • the invention can realize accurate X-Y-Z three-dimensional movement of the sample, and realize the residual magnetic measurement and scanning imaging of the biological sample. Mobile resolution: 20nm, mobile accuracy: 100nm.
  • both the three-dimensional sample moving stage 10 and the sample support rod 11 are made of non-magnetic material. Such as ceramics, organic plastics, quartz glass and so on.
  • the TMR probe array 30, the three-dimensional sample moving stage 10, and the magnetized demagnetizing coil 50 of the present invention are all placed in a magnetic shielding room 9.
  • the invention designs a special magnetic shielding room 9 to provide a zero magnetic field space experimental environment for the entire system, and realize shielding of the ambient static magnetic field and alternating magnetic field.
  • a high-permeability material is used to build a square shielded chamber, which can sufficiently accommodate the rock specimen magnetic detection system, experimental samples and experimental operators.
  • the internal magnetic field of the magnetically shielded chamber 9 constructed by the present invention is a high-standard zero magnetic space below 100 nT and a uniform area lower than 50 nT, which can provide an excellent test environment for the magnetic detection and analyzer of the scanning TMR array rock specimen.
  • the present invention further includes a magnetic shielding tube 8 sleeved outside the TMR probe array 30 and the sample support rod 11 during magnetic field detection.
  • This magnetic shield cylinder 8 is used only when detecting the magnetic field of the rock sample 1, and is withdrawn when it is demagnetized.
  • the above magnetic shielding room 9 is used to shield the internal magnetic field to 100nT and below, which removes the interference of the surrounding environment on the test; magnetic shielding, 8 is used to shield the internal magnetic field to 10nT and below, which can reduce the background magnetic field of the test more low.
  • FIG. 6 is a schematic structural diagram of a three-dimensional sample moving stage of a TMR array scanning rock magnetic detector according to the present invention.
  • the three-dimensional sample moving stage 10 is composed of a three-dimensional moving mechanism, and a horizontal sample supporting rod 12 is provided above.
  • the horizontal sample support rod 12 has a length of 50 cm to 70 cm.
  • the horizontal sample support rod 12 larger than 50cm can reduce the influence of the motor itself and the magnetic field generated during the movement on the measurement.
  • the TMR array scanning rock magnetic detector of the present invention can achieve the following technical indicators:
  • Magnetization field strength 0-1T, uniformity ⁇ 2%;
  • Demagnetization intensity 0-0.3T, uniformity ⁇ 2%;
  • Magnetic shielding index of test area 0-5 ⁇ 10-8T.
  • the TMR array scanning rock magnetic detector of the present invention has the following characteristics:
  • the present invention provides a scanning rock specimen magnetic detection and analyzer with in-situ magnetization and demagnetization functions.
  • a scanning rock specimen magnetic detection and analyzer with in-situ magnetization and demagnetization functions.
  • magnetometers are used to measure the magnetic moment of the entire sample, and the existing scanning magnetometers do not have the functions of magnetizing and demagnetizing the samples.
  • the present invention proposes to use a TMR probe array to perform two-dimensional scanning on rock specimens, and can use the obtained magnetic signals and the least squares algorithm and deconvolution to realize the measurement of natural remanence and saturated isothermal remanence. Perspective development on data parsing.
  • the TMR array scanning rock magnetic detector of the present invention can provide a powerful tool for China's geological and geophysical research, not only can it provide new research tools for traditional geosciences such as paleomagnetism, environmental magnetism, etc., but it can also promote biomagnetism
  • the development of such interdisciplinary subjects as meteorite magnetism also has broad application prospects in integrated circuit detection analysis and non-destructive testing of magnetic materials.

Abstract

A TMR array scanning type rock magnetic detector, comprising: a sample positioning system, comprising a three-dimensional sample moving table (10) for placing a rock sample (1), and a sample table controller (20) for adjusting a position of the three-dimensional sample moving table (10); a TMR magnetic field detection system, comprising a TMR probe array (30), and a TMR circuit (40) for driving the TMR probe array (30) to perform magnetic field detection; a magnetizing demagnetization system, comprising a magnetizing demagnetization coil (50) sleeved outside the rock sample (1) and a coil control circuit (60) connected thereto; a data processing control system (70), connected to the TMR circuit (40), the coil control circuit (60), and the sample table controller (20), and configured to receive an input of a user and send a TMR scanning instruction, a magnetization or demagnetization instruction, and a sample table moving instruction, separately. The rock sample (1) can be subjected to magnetic scanning with high magnetic measurement precision and high spatial resolution; moreover, a special magnetizing demagnetization system is provided, and in-situ magnetization and demagnetization can be performed without moving the rock sample (1).

Description

一种TMR阵列扫描式岩石磁性检测仪TMR array scanning type rock magnetic detector 技术领域Technical field
本发明涉及磁性测量技术领域,尤其涉及一种TMR阵列扫描式岩石磁性检测仪。The invention relates to the technical field of magnetic measurement, in particular to a TMR array scanning type rock magnetic detector.
背景技术Background technique
岩石中含有磁性矿物,其磁学特性在地学研究中具有重要意义。一方面,作为特殊的矿物,利用其种类、粒径以及含量信息,可以灵敏地追踪多种地质与环境过程,比如矿物的生成、运移与转化过程等(称之为环境磁学)。另一方面,磁性矿物在地磁场环境下,可以被定向排列,通过热剩磁(火山岩)以及沉积剩磁(沉积岩或者沉积物)等机制把当时的地磁场记录下来,通过测定岩石的剩磁信息,可以恢复当时地磁场的信息(称之为古地磁学)。因此,岩石的磁学性质可以被广泛地用于研究地质构造与环境演化、石油矿物勘察、地球深部动力学过程、沉积序列定年、以及考古等。Rock contains magnetic minerals, and its magnetic properties are of great significance in geological research. On the one hand, as a special mineral, using its type, particle size, and content information, it can sensitively track a variety of geological and environmental processes, such as mineral generation, migration, and transformation processes (called environmental magnetism). On the other hand, magnetic minerals can be oriented in a geomagnetic field environment. The geomagnetic field at that time is recorded by mechanisms such as thermal remanence (volcanic rocks) and sedimentary remanence (sedimentary rocks or sediments). Information can restore the information of the geomagnetic field at that time (called paleomagnetism). Therefore, the magnetic properties of rocks can be widely used to study geological structure and environmental evolution, petroleum and mineral exploration, deep earth dynamics, sedimentary sequence dating, and archeology.
目前,磁场扫描技术正在成为岩石标本磁性测量的一个重要研究手段。古地磁学研究一般采用超导磁力仪、旋转磁力仪、振动样品磁力仪、变梯度磁力仪等测量岩石样品磁性。这些系统均测量整个岩石样品携带的剩磁,它是样品中所有磁性颗粒信息的叠加,而无法分辨与提取样品中单个磁性颗粒的信息。随着研究的深入,在实际应用中,我们需要确切地知道样品中在微米级上,磁性颗粒的空间分布以及磁性颗粒的粒径分布特征等。比如,陨石中磁性颗粒的分布模式携带着丰富的陨石演化信息;石笋和深海锰结石具有较低的沉积速率。如果能够识别微米级别上的磁性,就可以构建高精度的环境演化信息,从而极大地推动相关学科的发展,具有重要的科学意义。At present, magnetic field scanning technology is becoming an important research method for magnetic measurement of rock specimens. Paleomagnetic research generally uses superconducting magnetometers, rotating magnetometers, vibrating sample magnetometers, and variable gradient magnetometers to measure the magnetic properties of rock samples. These systems measure the residual magnetism carried by the entire rock sample, which is the superposition of information of all magnetic particles in the sample, but cannot distinguish and extract the information of a single magnetic particle in the sample. With the deepening of the research, in practical applications, we need to know exactly the spatial distribution of magnetic particles and the particle size distribution characteristics of magnetic particles in the sample at the micron level. For example, the distribution pattern of magnetic particles in meteorites carries rich meteorite evolution information; stalagmites and deep-sea manganese stones have lower deposition rates. If it can recognize the magnetism at the micron level, it can construct high-precision environmental evolution information, which will greatly promote the development of related disciplines, which has important scientific significance.
为了实现这一目的,磁场扫描技术应运而生,该技术可以灵敏地 测量岩石样品表面分布的磁场,并进一步计算出岩石中磁性颗粒的分布特征。通过同级叠加所有磁性颗粒携带的磁学信息,还可以统计地计算出整个样品的剩磁。但超导技术一则价格昂贵;二则受到必须配备低温系统所限,探头与样品必须隔离一部分距离降低了其空间分辨率。In order to achieve this purpose, the magnetic field scanning technology came into being, which can sensitively measure the magnetic field distribution on the surface of rock samples, and further calculate the distribution characteristics of magnetic particles in the rock. By superposing the magnetic information carried by all magnetic particles at the same level, the residual magnetism of the entire sample can also be calculated statistically. However, the superconducting technology is expensive; the second is limited by the need to equip a low temperature system, and the probe must be separated from the sample by a distance to reduce its spatial resolution.
TMR(Tunnel Magneto Resistance,隧道磁电阻)元件是近年来开始工业应用的新型磁电阻效应传感器,其利用的是磁性多层膜材料的隧道磁电阻效应对磁场进行感应,比之前所发现并实际应用的AMR(Anisotropic Magneto Resistance,各项异性磁电阻)元件和GMR(Giant Magneto Resistance,巨磁电阻)元件具有更大的电阻变化率。TMR元件相对于霍尔元件具有更好的温度稳定性,更高的灵敏度,更低的功耗,更好的线性度,不需要额外的聚磁环结构;相对于AMR元件具有更好的温度稳定性,更高的灵敏度,更宽的线性范围,不需要额外的set/reset线圈结构;相对于GMR元件具有更好的温度稳定性,更高的灵敏度,更低的功耗,更宽的线性范围。基于以上诸多优点,该传感器已开始逐步应用于信息技术、汽车电子、生物医学等高精技术领域。TMR (TunnelMagnetoResistance) element is a new type of magnetoresistance effect sensor that has begun industrial applications in recent years. It uses the tunnel magnetoresistance effect of magnetic multilayer film materials to induce magnetic fields, which is more than previously discovered and practically applied. AMR (Anisotropic Magneto Resistance) and GMR (Giant Magneto Resistance) elements have greater resistance change rates. TMR element has better temperature stability, higher sensitivity, lower power consumption, better linearity than Hall element, and does not require additional magnetic ring structure; better temperature than AMR element Stability, higher sensitivity, wider linear range, no need for additional set / reset coil structure; better temperature stability, higher sensitivity, lower power consumption, wider Linear range. Based on the above advantages, this sensor has begun to be gradually applied to high-precision technology fields such as information technology, automotive electronics, and biomedicine.
目前,现有技术中还缺乏基于TMR来构建的岩石磁性扫描系统。并且一般的岩石磁性扫描系统也统只能测量表面的磁性,还不具有对样品进行原位磁化和退磁的功能,通常需要将样品从磁屏蔽室中取出,使用专门的磁化和退磁装置进行处理后再放回扫描系统中,难以保障处理前后扫描的岩石摆放位置一致,不利于对前后的磁性分布进行比对。At present, there is a lack of a magnetic magnetic scanning system based on TMR in the prior art. In addition, the general rock magnetic scanning system can only measure the surface magnetism, and does not have the function of in-situ magnetization and demagnetization of the sample. Usually, the sample needs to be taken out of the magnetic shielding room and processed by a special magnetization and demagnetization device. After putting it back into the scanning system, it is difficult to ensure that the rocks are placed in the same position before and after the processing, which is not conducive to comparing the magnetic distribution before and after.
发明内容Summary of the Invention
本发明要解决的技术问题在于,针对现有技术中的以上一个或者多个缺陷,提供一种TMR阵列扫描式岩石磁性检测仪。The technical problem to be solved by the present invention is to provide a TMR array scanning type rock magnetic detector for one or more of the defects in the prior art.
为了解决上述技术问题,本发明提供了一种TMR阵列扫描式岩石磁性检测仪,包括:In order to solve the above technical problems, the present invention provides a TMR array scanning rock magnetic detector, including:
样品定位系统,包括用于放置岩石标本的三维样品移动台,以及用于调节所述三维样品移动台位置的样品台控制器;所述三维样品移动台上设置有样品支撑杆;A sample positioning system includes a three-dimensional sample moving stage for placing a rock specimen, and a sample stage controller for adjusting the position of the three-dimensional sample moving stage; a sample support rod is provided on the three-dimensional sample moving stage;
TMR磁场检测系统,包括TMR探头阵列,以及用于驱动所述TMR探头阵列进行磁场检测的TMR电路;A TMR magnetic field detection system includes a TMR probe array and a TMR circuit for driving the TMR probe array for magnetic field detection;
磁化退磁系统,包括套设在岩石标本外的磁化退磁线圈,以及与之连接的线圈控制电路;Magnetization demagnetization system, including a magnetization demagnetization coil set outside a rock specimen, and a coil control circuit connected thereto;
数据处理控制系统,与所述TMR电路、线圈控制电路和样品台控制器连接,用于接受用户输入并分别发送TMR扫描指令、磁化或退磁指令、样品台移动指令给所述TMR电路、线圈控制电路和样品台控制器。A data processing control system, which is connected to the TMR circuit, the coil control circuit, and the sample stage controller, and is used to accept user input and send TMR scanning instructions, magnetization or demagnetization instructions, and sample stage movement instructions to the TMR circuit, coil control, respectively. Circuit and sample stage controller.
在根据本发明所述的TMR阵列扫描式岩石磁性检测仪中,优选地,所述线圈控制电路包括:In the TMR array scanning rock magnetic detector according to the present invention, preferably, the coil control circuit includes:
脉冲电源,通过数据采集卡与所述数据处理控制系统连接,用于根据数据处理控制系统发出的磁化指令生成对应电流强度的磁化脉冲电流;A pulse power supply, connected to the data processing control system through a data acquisition card, and configured to generate a magnetization pulse current corresponding to a current intensity according to a magnetization instruction issued by the data processing control system;
信号源,与所述数据处理控制系统连接,用于根据数据处理控制系统发出的退磁指令生成对应频率的正弦波退磁电信号;A signal source, connected to the data processing control system, and configured to generate a sine wave demagnetizing electrical signal of a corresponding frequency according to a demagnetization instruction issued by the data processing control system;
功率放大器,与所述信号源连接,用于将信号源生成的正弦波退磁电信号放大成对应幅值后输出;A power amplifier connected to the signal source and configured to amplify the sine wave demagnetized electrical signal generated by the signal source to a corresponding amplitude and output;
换路开关,与所述脉冲电源和功率放大器连接,用于切换磁化脉冲电流或者放大后的正弦波退磁电信号给所述磁化退磁线圈,以产生预定强度的磁场,起到切换磁化或退磁功能的目的。A switch is connected to the pulse power source and the power amplifier, and is used to switch the magnetization pulse current or the amplified sine wave demagnetization electric signal to the magnetization demagnetization coil to generate a magnetic field of a predetermined strength, and to perform the function of switching magnetization or demagnetization the goal of.
在根据本发明所述的TMR阵列扫描式岩石磁性检测仪中,优选地,所述三维样品移动台上设置有步进电机和光栅尺位移传感器;In the TMR array scanning rock magnetic detector according to the present invention, preferably, the three-dimensional sample moving stage is provided with a stepping motor and a grating scale displacement sensor;
所述样品台控制器包括:电机控制器,与所述数据处理控制系统连接,用于接收所述样品台移动指令生成电机控制信号,并利用所述 光栅尺位移传感器反馈的位置信息实现闭环控制样品支撑杆的移动定位;电机驱动器,与所述电机控制器连接,用于接收电机控制电信号并能生成驱动信号给所述步进电机。The sample stage controller includes: a motor controller, connected to the data processing control system, for receiving a movement command of the sample stage to generate a motor control signal, and using the position information fed back by the grating scale displacement sensor to implement closed-loop control. The positioning of the sample support rod; a motor driver connected to the motor controller and configured to receive a motor control electrical signal and generate a driving signal to the stepper motor.
在根据本发明所述的TMR阵列扫描式岩石磁性检测仪中,优选地,所述样品支撑杆水平设置;所述步进电机为三个,分别用于控制样品支撑杆在三个维度上移动。In the TMR array scanning rock magnetic detector according to the present invention, preferably, the sample supporting rods are horizontally arranged; there are three stepping motors, which are respectively used to control the sample supporting rods to move in three dimensions. .
在根据本发明所述的TMR阵列扫描式岩石磁性检测仪中,优选地,所述样品支撑杆的长度为30cm~100cm。In the TMR array scanning type rock magnetic detector according to the present invention, preferably, the length of the sample support rod is 30 cm to 100 cm.
在根据本发明所述的TMR阵列扫描式岩石磁性检测仪中,优选地,所述三维样品移动台及样品支撑杆均选用无磁性材料制作。In the TMR array scanning rock magnetic detector according to the present invention, preferably, the three-dimensional sample moving stage and the sample support rod are made of non-magnetic materials.
在根据本发明所述的TMR阵列扫描式岩石磁性检测仪中,优选地,所述步进电机为压电陶瓷超声电机。In the TMR array scanning rock magnetic detector according to the present invention, preferably, the stepping motor is a piezoelectric ceramic ultrasonic motor.
在根据本发明所述的TMR阵列扫描式岩石磁性检测仪中,优选地,所述TMR探头阵列、三维样品移动台和磁化退磁线圈均置于磁屏蔽室中。In the TMR array scanning rock magnetic detector according to the present invention, preferably, the TMR probe array, the three-dimensional sample moving stage, and the magnetization demagnetization coil are all placed in a magnetic shielding room.
在根据本发明所述的TMR阵列扫描式岩石磁性检测仪中,优选地,所述TMR阵列扫描式岩石磁性检测仪还包括在磁场检测时套设于所述TMR探头阵列以及样品支撑杆外的磁屏蔽筒;所述磁屏蔽室用于将内部磁场屏蔽至100nT及以下;所述磁屏蔽筒用于将内部磁场屏蔽至10nT及以下。In the TMR array scanning type rock magnetic detector according to the present invention, preferably, the TMR array scanning type rock magnetic detector further includes a TMR probe array and a sample support rod that are sleeved outside the TMR probe array and the sample support rod during magnetic field detection. Magnetic shielding cylinder; the magnetic shielding chamber is used to shield the internal magnetic field to 100nT and below; the magnetic shielding cylinder is used to shield the internal magnetic field to 10nT and below.
实施本发明的TMR阵列扫描式岩石磁性检测仪,具有以下有益效果:本发明利用TMR传感器阵列和移动平台构建TMR阵列扫描式岩石磁性检测仪,可以对岩石标本实现高精度高分辨率的磁性扫描,并且其中设置了专门的磁化退磁系统,可以在不移动岩石标本的情况下进行原位磁化和退磁,便于对前后的磁性分布进行比。The implementation of the TMR array scanning rock magnetic detector of the present invention has the following beneficial effects: The present invention uses the TMR sensor array and a mobile platform to construct the TMR array scanning rock magnetic detector, which can realize high-precision and high-resolution magnetic scanning of rock specimens. And, a special magnetization demagnetization system is set up to perform in-situ magnetization and demagnetization without moving the rock specimen, which is convenient for comparing the magnetic distribution before and after.
附图说明BRIEF DESCRIPTION OF THE DRAWINGS
图1为根据本发明的第一实施例提供的TMR阵列扫描式岩石磁性 检测仪的结构示意图;1 is a schematic structural diagram of a TMR array scanning rock magnetic detector according to a first embodiment of the present invention;
图2为根据本发明的第二实施例提供的TMR阵列扫描式岩石磁性检测仪的结构示意图;2 is a schematic structural diagram of a TMR array scanning rock magnetic detector according to a second embodiment of the present invention;
图3为根据本发明第二实施例的TMR阵列扫描式岩石磁性检测仪中充磁电路的示意图;3 is a schematic diagram of a magnetizing circuit in a TMR array scanning rock magnetic detector according to a second embodiment of the present invention;
图4为根据本发明第二实施例的TMR阵列扫描式岩石磁性检测仪中退磁电路的示意图;4 is a schematic diagram of a demagnetization circuit in a TMR array scanning rock magnetic detector according to a second embodiment of the present invention;
图5为根据本发明第二实施例的TMR阵列扫描式岩石磁性检测仪中磁化退磁线圈的结构示意图;5 is a schematic structural diagram of a magnetization demagnetization coil in a TMR array scanning rock magnetic detector according to a second embodiment of the present invention;
图6为根据本发明的TMR阵列扫描式岩石磁性检测仪中三维样品移动台的结构示意图。FIG. 6 is a schematic structural diagram of a three-dimensional sample moving stage in a TMR array scanning rock magnetic detector according to the present invention.
具体实施方式detailed description
为使本发明实施例的目的、技术方案和优点更加清楚,下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例是本发明的一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动的前提下所获得的所有其他实施例,都属于本发明保护的范围。In order to make the objectives, technical solutions, and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described with reference to the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments These are part of the embodiments of the present invention, but not all of them. Based on the embodiments of the present invention, all other embodiments obtained by a person of ordinary skill in the art without creative efforts shall fall within the protection scope of the present invention.
请参阅图1,为根据本发明的第一实施例提供的TMR阵列扫描式岩石磁性检测仪的结构示意图。如图1所示,该实施例提供的TMR阵列扫描式岩石磁性检测仪至少包括:样品定位系统、TMR磁场检测系统、磁化退磁系统和数据处理控制系统。Please refer to FIG. 1, which is a schematic structural diagram of a TMR array scanning rock magnetic detector according to a first embodiment of the present invention. As shown in FIG. 1, the TMR array scanning rock magnetic detector provided in this embodiment includes at least: a sample positioning system, a TMR magnetic field detection system, a magnetization demagnetization system, and a data processing control system.
其中样品定位系统包括用于放置岩石标本1的三维样品移动台10,以及用于调节三维样品移动台10位置的样品台控制器20。该三维样品移动台上设置有样品支撑杆11,用于放置岩石标本1,。The sample positioning system includes a three-dimensional sample moving stage 10 for placing a rock specimen 1, and a sample stage controller 20 for adjusting the position of the three-dimensional sample moving stage 10. The three-dimensional sample moving stage is provided with a sample support rod 11 for placing a rock specimen 1.
TMR磁场检测系统包括TMR探头阵列30,以及用于驱动TMR探头阵列30进行磁场检测的TMR电路40。TMR探头阵列30中TMR 传感器的个数为n*n。The TMR magnetic field detection system includes a TMR probe array 30 and a TMR circuit 40 for driving the TMR probe array 30 for magnetic field detection. The number of TMR sensors in the TMR probe array 30 is n * n.
磁化退磁系统包括套设在岩石标本30外的磁化退磁线圈50,以及与之连接的线圈控制电路60。The magnetization demagnetization system includes a magnetization demagnetization coil 50 sleeved outside the rock specimen 30 and a coil control circuit 60 connected to the magnetization demagnetization coil 50.
数据处理控制系统70与TMR电路40、线圈控制电路60和样品台控制器20连接,用于接受用户输入并分别发送TMR扫描指令、磁化或退磁指令、样品台移动指令给TMR电路40、线圈控制电路60和样品台控制器20。数据处理控制系统70可以通过例如计算机实现。The data processing control system 70 is connected to the TMR circuit 40, the coil control circuit 60, and the sample stage controller 20, and is used to accept user input and send TMR scan instructions, magnetization or demagnetization instructions, and sample stage movement instructions to the TMR circuit 40, coil control, respectively. Circuit 60 and sample stage controller 20. The data processing control system 70 can be implemented by, for example, a computer.
请参阅图2,为根据本发明的第二实施例提供的TMR阵列扫描式岩石磁性检测仪的结构示意图。如图2所示,在第一实施例的基础上,提供了每个系统的具体实现方式。Please refer to FIG. 2, which is a schematic structural diagram of a TMR array scanning rock magnetic detector according to a second embodiment of the present invention. As shown in FIG. 2, on the basis of the first embodiment, a specific implementation manner of each system is provided.
其中,TMR电路40包括:TMR控制器41和前置放大器42。TMR控制器41通过数据采集卡71与数据处理控制系统70连接,用于接收数据处理控制系统70发出的TMR扫描指令,并生成TMR控制信号。前置放大器42与TMR控制器41连接,用于对TMR控制信号进行放大和滤波后,输出一个正比于磁场信号的电压给TMR探头阵列30。优选地,本发明中的TMR探头阵列30可以选用多个TMR传感器以矩阵排列。例如选购拥有±50Oe的线性测量范围,2nT/Hz 1/2@100Hz的磁场分辨率,1×2微米的测量区域,非常适合弱磁样品扫描。将该TMR传感器将以矩阵排列4×4共16支传感器构成TMR矩阵,阵列数据的采集可以加快测量速度并达到微米尺度的空间分辨率。前置放大器42可以采用拥有超过100分贝的衰减的电源降噪。 The TMR circuit 40 includes a TMR controller 41 and a preamplifier 42. The TMR controller 41 is connected to the data processing control system 70 through a data acquisition card 71, and is configured to receive a TMR scan instruction issued by the data processing control system 70 and generate a TMR control signal. The preamplifier 42 is connected to the TMR controller 41 and is used to amplify and filter the TMR control signal and output a voltage proportional to the magnetic field signal to the TMR probe array 30. Preferably, the TMR probe array 30 in the present invention may be selected from a plurality of TMR sensors and arranged in a matrix. For example, it has a linear measurement range of ± 50Oe, a magnetic field resolution of 2nT / Hz 1/2 @ 100Hz, and a measurement area of 1 × 2 microns, which is very suitable for scanning weak magnetic samples. This TMR sensor will form a TMR matrix with a total of 16 sensors arranged in a matrix of 4 × 4. The collection of array data can accelerate the measurement speed and achieve spatial resolution on the micrometer scale. The preamplifier 42 can use a power supply with noise attenuation of more than 100 dB to reduce noise.
线圈控制电路60包括:脉冲电源61、信号源62、功率放大器63和换路开关64。The coil control circuit 60 includes a pulse power source 61, a signal source 62, a power amplifier 63, and a circuit breaker 64.
其中脉冲电源61通过数据采集卡71与数据处理控制系统70连接,用于根据数据处理控制系统70发出的磁化指令生成对应电流强度的磁化脉冲电流。请结合参阅图3,为根据本发明第二实施例的TMR阵列扫描式岩石磁性检测仪中充磁电路的示意图。The pulse power source 61 is connected to the data processing control system 70 through the data acquisition card 71, and is configured to generate a magnetized pulse current corresponding to the current intensity according to the magnetization instruction issued by the data processing control system 70. Please refer to FIG. 3 in combination, which is a schematic diagram of a magnetizing circuit in a TMR array scanning rock magnetic detector according to a second embodiment of the present invention.
本发明的脉冲充磁可以使用电容放电脉冲充磁技术。脉冲电源, 最大电压可达1500V,给内部的电容衡流充电,电流1-1.5A,磁化退磁线圈电感32.4mH,电阻1.727ohm,选用电容容值300μF时,将电容充到1300V即可。The pulse magnetization of the present invention can use a capacitor discharge pulse magnetization technique. Pulse power supply, the maximum voltage can reach 1500V, charge the internal capacitor balance current, the current is 1-1.5A, the magnetization demagnetizing coil inductance is 32.4mH, the resistance is 1.727ohm, when the capacitance value is 300μF, the capacitor can be charged to 1300V.
该脉冲电源可以有四个信号的接口,如图所示:The pulse power supply can have four signal interfaces, as shown in the figure:
1)模拟电压输入:用于设置电容两端电压,当电容电压值达到设定值时,硬件关断充电电路;1) Analog voltage input: used to set the voltage across the capacitor. When the capacitor voltage reaches the set value, the hardware turns off the charging circuit;
2)模拟电压输出:电压传感器传回电容两端电压给数据采集卡71;2) Analog voltage output: the voltage sensor returns the voltage across the capacitor to the data acquisition card 71;
3)数字信号输入:用于软件控制开关充电电路;3) Digital signal input: used for software control switch charging circuit;
4)数字信号输入:用于控制放电电路开关。4) Digital signal input: used to control the discharge circuit switch.
四个接口与数据采集卡的DO、D/A和A/D接口相连。Four interfaces are connected to the DO, D / A, and A / D interfaces of the data acquisition card.
信号源62与数据处理控制系统70连接,用于根据数据处理控制系统70发出的退磁指令生成对应频率的正弦波退磁电信号。功率放大器63与信号源62连接,用于将信号源62生成的正弦波退磁电信号放大成对应幅值后输出。请结合参阅图4,为根据本发明第二实施例的TMR阵列扫描式岩石磁性检测仪中退磁电路的示意图。The signal source 62 is connected to the data processing control system 70, and is configured to generate a sine wave demagnetizing electrical signal with a corresponding frequency according to a demagnetization instruction issued by the data processing control system 70. The power amplifier 63 is connected to the signal source 62 and is used to amplify the sine wave demagnetized electrical signal generated by the signal source 62 to a corresponding amplitude and output. Please refer to FIG. 4 together, which is a schematic diagram of a demagnetization circuit in a TMR array scanning rock magnetic detector according to a second embodiment of the present invention.
本发明中交流退磁场使用信号源62和功率放大器63来驱动磁化退磁线圈。信号源62由单片机622和AD9854芯片621来实现,输出频率400Hz、电压幅值线性减小的正弦波(磁场200mT衰减到0mT)。单片机622与计算机72通过RS232串口通信,等待计算机的退磁指令。PC机的设置的退磁指令可对输出信号幅值、频率进行改变,输出指令控制信号源62输出信号到功率放大器,进行退磁。功率放大器可以采用音频功率放大器631。例如选用商业声准公司的专业功放CA20,8ohm立体声功率1300w,4ohm立体声功率2000w,2ohm立体声立体声功率2600w。理论上,使用2ohm负载可以达到最大电流36A。8ohm算的最大电压可达102V。AD9854DDS芯片可输出频率,相位,幅度可调的正弦波。32位频率控制字,频率精度可达0.0466Hz,14位幅度控制字,21A最大电流(200mT磁场),控制精度可达0.0013A(12.2μT)。退磁的频率选为400Hz,在400Hz条件下,磁化退磁线圈50的 电阻受临近效应影响,变为2.499ohm,由于电感的存在整个负载的阻抗很大,使用电容进行调谐,使在400Hz时,负载只为电阻特性,用CBB电容串并联实现调谐,调谐电容1.221μF。In the present invention, the AC demagnetization field uses a signal source 62 and a power amplifier 63 to drive the magnetization demagnetization coil. The signal source 62 is realized by a single-chip microcomputer 622 and an AD9854 chip 621, and the output frequency is 400 Hz, and the voltage amplitude decreases linearly with a sine wave (the magnetic field 200mT is attenuated to 0mT). The single-chip microcomputer 622 communicates with the computer 72 through the RS232 serial port and waits for the computer's demagnetization instruction. The demagnetization instruction set by the PC can change the amplitude and frequency of the output signal, and the output instruction control signal source 62 outputs a signal to the power amplifier for demagnetization. As the power amplifier, an audio power amplifier 631 can be used. For example, the professional amplifier CA20 of commercial sound precision company is used, 8ohm stereo power is 1300w, 4ohm stereo power is 2000w, and 2ohm stereo power is 2600w. Theoretically, a maximum current of 36A can be achieved with a 2ohm load. The maximum voltage calculated by 8ohm can reach 102V. AD9854DDS chip can output sine wave with adjustable frequency, phase and amplitude. 32-bit frequency control word, frequency accuracy can reach 0.0466Hz, 14-bit amplitude control word, 21A maximum current (200mT magnetic field), control accuracy can reach 0.0013A (12.2μT). The frequency of demagnetization is selected as 400Hz. Under the condition of 400Hz, the resistance of the magnetization demagnetization coil 50 is affected by the proximity effect and becomes 2.499ohm. Due to the presence of the inductance, the impedance of the entire load is very large. Use capacitors for tuning. For resistance only, tuning is performed with CBB capacitors in series and parallel. The tuning capacitor is 1.221 μF.
换路开关64与脉冲电源61和功率放大器63连接,用于切换磁化脉冲电流或者放大后的正弦波退磁电信号给磁化退磁线圈50,以产生预定强度的磁场,起到切换磁化获退磁功能的目的。The switch 64 is connected to the pulse power source 61 and the power amplifier 63, and is used to switch the magnetization pulse current or the amplified sine wave demagnetization electric signal to the magnetization demagnetization coil 50 to generate a magnetic field of a predetermined strength and to perform the function of switching the magnetization and demagnetization. purpose.
虽然上述给出了脉冲电源61、信号源62和功率放大器63的具体实现方式,但是本领域基础技术人员也可以采用其它现有技术中能够适用的脉冲电源61、信号源62和功率放大器63。Although the specific implementations of the pulse power source 61, the signal source 62, and the power amplifier 63 are given above, those skilled in the art can also use other pulse power sources 61, the signal source 62, and the power amplifier 63 that can be applied in the prior art.
请结合参阅图5,为根据本发明第二实施例的TMR阵列扫描式岩石磁性检测仪中磁化退磁线圈的结构示意图。饱和等温剩磁的测量需要对样品进行磁化和退磁,并利用TMR探头阵列测量岩石标本的剩磁信号。这部分主要包括直流磁化磁场线圈和交变磁场线圈的设计,使得产生的磁场具有很高的均匀性与分辨率。本发明的磁化退磁线圈采用空心圆柱线圈结构,如图所示,内径R1=25mm,外径R2=67mm,长度l=30mm。漆包线线径1.77mm(铜芯1.68mm),绕24层,每层33匝,共792匝。计算可得,当脉冲电流I=105A时,B=1T;当交流电流I=21A时,B=0.2T。能够满足磁化退磁场的要求。制作完成的磁化退磁线圈置于线圈架上,该线圈架可以为环氧材料。岩石标本被置于该磁化退磁线圈的内部空腔中。Please refer to FIG. 5 in combination, which is a schematic structural diagram of a magnetization demagnetization coil in a TMR array scanning rock magnetic detector according to a second embodiment of the present invention. The measurement of saturated isothermal remanence requires magnetization and demagnetization of the sample, and the TMR probe array is used to measure the remanence signal of the rock specimen. This part mainly includes the design of DC magnetizing magnetic field coil and alternating magnetic field coil, so that the generated magnetic field has high uniformity and resolution. The magnetized demagnetizing coil of the present invention adopts a hollow cylindrical coil structure. As shown in the figure, the inner diameter R1 = 25mm, the outer diameter R2 = 67mm, and the length l = 30mm. The diameter of enameled wire is 1.77mm (copper core 1.68mm). It is wound in 24 layers, each layer is 33 turns, for a total of 792 turns. It can be calculated that when the pulse current I = 105A, B = 1T; when the AC current I = 21A, B = 0.2T. Can meet the requirements of magnetization demagnetization. The manufactured magnetized demagnetizing coil is placed on a coil bobbin, and the coil bobbin may be epoxy material. Rock specimens are placed in the internal cavity of the magnetized demagnetization coil.
本发明的样品定位系统可以实现对样品的三维精密运动和定位。优选地,三维样品移动台10上设置有步进电机13和光栅尺位移传感器14。The sample positioning system of the present invention can realize three-dimensional precise movement and positioning of a sample. Preferably, the three-dimensional sample moving stage 10 is provided with a stepping motor 13 and a scale displacement sensor 14.
样品台控制器20进一步包括:电机控制器21和电机驱动器22。其中,电机控制器21与数据处理控制系统70连接,用于接收样品台移动指令生成电机控制信号,并利用光栅尺位移传感器14反馈的位置信息实现闭环控制样品支撑杆11上岩石标本的移动定位。电机驱动器22与电机控制器21连接,用于接收电机控制信号并能生成驱动电信号 给步进电机13。三维样品移动台10的三个方向的移动和定位分别通过三个步进电机13来实现。步进电机13优选采用压电陶瓷超声电机,以减少电机本身剩磁。压电陶瓷超声电机的电机驱动器可以采用AB1A驱动器。当操作于闭环伺服系统时,电机驱动器从电机控制器接收+/-10V的模拟信号指令,将控制信号转换为交流电压驱动电机。电机控制器21控制器选用运动控制卡DMC 18X2,DMC18X2控制卡直接插到计算机的PCI卡槽上,这两种控制卡分别可实现1-4个轴的控制,可以满足三维移动平台的控制要求。可为标准的伺服系统提供+/-10V的模拟信号指令。The sample stage controller 20 further includes a motor controller 21 and a motor driver 22. Among them, the motor controller 21 is connected to the data processing control system 70, and is used to receive the sample table movement instruction to generate a motor control signal, and use the position information fed back by the scale displacement sensor 14 to implement closed-loop control of the movement positioning of the rock specimen on the sample support rod 11. . The motor driver 22 is connected to the motor controller 21, and is used for receiving a motor control signal and generating a driving electric signal to the stepping motor 13. The three-dimensional movement and positioning of the three-dimensional sample moving stage 10 are realized by three stepping motors 13 respectively. The stepping motor 13 is preferably a piezoelectric ceramic ultrasonic motor to reduce the residual magnetism of the motor itself. The motor driver of the piezoelectric ceramic ultrasonic motor can be an AB1A driver. When operating in a closed-loop servo system, the motor driver receives an analog signal instruction of +/- 10V from the motor controller and converts the control signal into an AC voltage to drive the motor. The motor controller 21 uses the motion control card DMC 18X2, and the DMC18X2 control card is directly inserted into the PCI card slot of the computer. These two control cards can control 1-4 axes respectively, which can meet the control requirements of the three-dimensional mobile platform . It can provide +/- 10V analog signal command for standard servo system.
本发明的岩石标本架的设计与制作,要求样本支撑杆11为无磁材料并且与TMR探头阵列的超导接收线圈距离非常近,以减少岩石标本剩磁信号的衰减损耗。并且本发明可以实现对样品精准X-Y-Z三维运动,实现对生物样品的剩磁测量和扫描成像。移动分辨率:20nm,移动精度:100nm。优选地,三维样品移动台10及样品支撑杆11均选用无磁性材料制作。如陶瓷、有机塑料、石英玻璃等。The design and production of the rock specimen rack of the present invention requires that the sample support rod 11 be non-magnetic material and is very close to the superconducting receiving coil of the TMR probe array, so as to reduce the attenuation loss of the residual magnetic signal of the rock specimen. In addition, the invention can realize accurate X-Y-Z three-dimensional movement of the sample, and realize the residual magnetic measurement and scanning imaging of the biological sample. Mobile resolution: 20nm, mobile accuracy: 100nm. Preferably, both the three-dimensional sample moving stage 10 and the sample support rod 11 are made of non-magnetic material. Such as ceramics, organic plastics, quartz glass and so on.
本发明的TMR探头阵列30、三维样品移动台10和磁化退磁线圈50均置于磁屏蔽室9中。本发明设计了专用的磁屏蔽室9,为整个系统提供一个零磁场空间实验环境,实现对环境静磁场和交变磁场的屏蔽。优选地,利用高磁导率材料搭建立方形屏蔽室,能足够容纳岩石标本磁检测系统、实验样品和实验操作人员。The TMR probe array 30, the three-dimensional sample moving stage 10, and the magnetized demagnetizing coil 50 of the present invention are all placed in a magnetic shielding room 9. The invention designs a special magnetic shielding room 9 to provide a zero magnetic field space experimental environment for the entire system, and realize shielding of the ambient static magnetic field and alternating magnetic field. Preferably, a high-permeability material is used to build a square shielded chamber, which can sufficiently accommodate the rock specimen magnetic detection system, experimental samples and experimental operators.
本发明构建的磁屏蔽室9的内部磁场在100nT以下,均匀区低于50nT的高标准零磁空间,可以为扫描式TMR阵列岩石标本磁性检测与分析仪提供极佳的测试环境。The internal magnetic field of the magnetically shielded chamber 9 constructed by the present invention is a high-standard zero magnetic space below 100 nT and a uniform area lower than 50 nT, which can provide an excellent test environment for the magnetic detection and analyzer of the scanning TMR array rock specimen.
更优选地,本发明还包括在磁场检测时套设于所述TMR探头阵列30以及样品支撑杆11外的磁屏蔽筒8。该磁屏蔽筒8只在对岩石样本1进行磁场检测时使用,在退磁时撤开。上述磁屏蔽室9用于将内部磁场屏蔽至100nT及以下,去除了周围环境对测试的干扰;磁屏蔽,8则用于将内部磁场屏蔽至10nT及以下,可以将测试的背景磁场降得更低。More preferably, the present invention further includes a magnetic shielding tube 8 sleeved outside the TMR probe array 30 and the sample support rod 11 during magnetic field detection. This magnetic shield cylinder 8 is used only when detecting the magnetic field of the rock sample 1, and is withdrawn when it is demagnetized. The above magnetic shielding room 9 is used to shield the internal magnetic field to 100nT and below, which removes the interference of the surrounding environment on the test; magnetic shielding, 8 is used to shield the internal magnetic field to 10nT and below, which can reduce the background magnetic field of the test more low.
虽然上述图1和图2中样品支撑杆11为竖直的支撑杆,但是本发明不仅限于此,该样品支撑杆11更优选为水平设置的支撑杆。请参阅图6,为根据本发明的TMR阵列扫描式岩石磁性检测仪的三维样品移动台的结构示意图。如图6所示,其中三维样品移动台10由三维移动机构组成,且在上方设置有水平样品支撑杆12。该水平样品支撑杆12的长度为50cm~70cm。水平样品支撑杆12大于50cm可以减少电机本身及运动时产生的磁场对测量造成的影响。Although the sample support rod 11 in FIG. 1 and FIG. 2 is a vertical support rod, the present invention is not limited thereto, and the sample support rod 11 is more preferably a horizontally disposed support rod. Please refer to FIG. 6, which is a schematic structural diagram of a three-dimensional sample moving stage of a TMR array scanning rock magnetic detector according to the present invention. As shown in FIG. 6, the three-dimensional sample moving stage 10 is composed of a three-dimensional moving mechanism, and a horizontal sample supporting rod 12 is provided above. The horizontal sample support rod 12 has a length of 50 cm to 70 cm. The horizontal sample support rod 12 larger than 50cm can reduce the influence of the motor itself and the magnetic field generated during the movement on the measurement.
本发明的TMR阵列扫描式岩石磁性检测仪可以达到以下技术指标:The TMR array scanning rock magnetic detector of the present invention can achieve the following technical indicators:
1)、系统灵敏度:2nT/Hz1/2@100Hz;1) System sensitivity: 2nT / Hz1 / 2 @ 100Hz;
2)、测量范围:±50Oe;2) Measurement range: ± 50Oe;
3)、单TMR灵敏度:2-4mV/V/Oe;3), single TMR sensitivity: 2-4mV / V / Oe;
4)、磁化场强度:0-1T,均匀性±2%;4) Magnetization field strength: 0-1T, uniformity ± 2%;
5)、退磁场强度:0-0.3T,均匀性±2%;5) Demagnetization intensity: 0-0.3T, uniformity ± 2%;
6)、系统空间分辨率达到5×10-6m;6) The system spatial resolution reaches 5 × 10-6m;
7)、测试区磁屏蔽指标:0-5×10-8T。7) Magnetic shielding index of test area: 0-5 × 10-8T.
综上所述,本发明的TMR阵列扫描式岩石磁性检测仪具有以下特点:In summary, the TMR array scanning rock magnetic detector of the present invention has the following characteristics:
1)本发明针对岩石标本的磁性检测与分析需求,提供了一种具有原位磁化和退磁功能的扫描式岩石标本磁性检测与分析仪。现有技术中还没有这种商用的扫描式岩石标本磁检测系统,通常都是采用各类磁力仪测量整块样品的磁矩,而已有的扫描式磁力仪没有对样品的磁化和退磁功能。1) In accordance with the magnetic detection and analysis requirements of rock specimens, the present invention provides a scanning rock specimen magnetic detection and analyzer with in-situ magnetization and demagnetization functions. There is no such commercial scanning rock specimen magnetic detection system in the prior art. Generally, various types of magnetometers are used to measure the magnetic moment of the entire sample, and the existing scanning magnetometers do not have the functions of magnetizing and demagnetizing the samples.
2)本发明提出利用TMR探头阵列对岩石标本进行二维扫描,并可利用得到的磁信号和最小二乘算法及反卷积实现对天然剩磁和饱和等温剩磁的测量,同时从地学应用的角度开发对数据解析。2) The present invention proposes to use a TMR probe array to perform two-dimensional scanning on rock specimens, and can use the obtained magnetic signals and the least squares algorithm and deconvolution to realize the measurement of natural remanence and saturated isothermal remanence. Perspective development on data parsing.
本发明的TMR阵列扫描式岩石磁性检测仪可以为我国地质与地球物理研究提供有力的工具,不仅可以为古地磁学、环境磁学等传统 地球科学提供新的研究工具,还可以推动生物磁学、陨石磁学等交叉学科的发展,在集成电路检测分析、磁性材料无损检测等方面也具有广阔的应用前景。The TMR array scanning rock magnetic detector of the present invention can provide a powerful tool for China's geological and geophysical research, not only can it provide new research tools for traditional geosciences such as paleomagnetism, environmental magnetism, etc., but it can also promote biomagnetism The development of such interdisciplinary subjects as meteorite magnetism also has broad application prospects in integrated circuit detection analysis and non-destructive testing of magnetic materials.
最后应说明的是:以上实施例仅用以说明本发明的技术方案,而非对其限制;尽管参照前述实施例对本发明进行了详细的说明,本领域的普通技术人员应当理解:其依然可以对前述各实施例所记载的技术方案进行修改,或者对其中部分技术特征进行等同替换;而这些修改或者替换,并不使相应技术方案的本质脱离本发明各实施例技术方案的精神和范围。Finally, it should be noted that the above embodiments are only used to illustrate the technical solution of the present invention, rather than limiting them. Although the present invention has been described in detail with reference to the foregoing embodiments, those skilled in the art should understand that they can still Modifications to the technical solutions described in the foregoing embodiments, or equivalent replacements of some of the technical features thereof; and these modifications or replacements do not depart from the spirit and scope of the technical solutions of the embodiments of the present invention.

Claims (10)

  1. 一种TMR阵列扫描式岩石磁性检测仪,其特征在于,包括:A TMR array scanning type rock magnetic detector is characterized in that it includes:
    样品定位系统,包括用于放置岩石标本的三维样品移动台,以及用于调节所述三维样品移动台位置的样品台控制器;所述三维样品移动台上设置有样品支撑杆;A sample positioning system includes a three-dimensional sample moving stage for placing a rock specimen, and a sample stage controller for adjusting the position of the three-dimensional sample moving stage; a sample support rod is provided on the three-dimensional sample moving stage;
    TMR磁场检测系统,包括TMR探头阵列,以及用于驱动所述TMR探头阵列进行磁场检测的TMR电路;A TMR magnetic field detection system includes a TMR probe array and a TMR circuit for driving the TMR probe array for magnetic field detection;
    磁化退磁系统,包括套设在岩石标本外的磁化退磁线圈,以及与之连接的线圈控制电路;Magnetization demagnetization system, including a magnetization demagnetization coil set outside a rock specimen, and a coil control circuit connected thereto;
    数据处理控制系统,与所述TMR电路、线圈控制电路和样品台控制器连接,用于接受用户输入并分别发送TMR扫描指令、磁化或退磁指令、样品台移动指令给所述TMR电路、线圈控制电路和样品台控制器。A data processing control system, which is connected to the TMR circuit, the coil control circuit, and the sample stage controller, and is used to accept user input and send TMR scanning instructions, magnetization or demagnetization instructions, and sample stage movement instructions to the TMR circuit, coil control, respectively. Circuit and sample stage controller.
  2. 根据权利要求1所述的TMR阵列扫描式岩石磁性检测仪,其特征在于,所述线圈控制电路包括:The TMR array scanning rock magnetic detector according to claim 1, wherein the coil control circuit comprises:
    脉冲电源,通过数据采集卡与所述数据处理控制系统连接,用于根据数据处理控制系统发出的磁化指令生成对应电流强度的磁化脉冲电流;A pulse power supply, connected to the data processing control system through a data acquisition card, and configured to generate a magnetization pulse current corresponding to a current intensity according to a magnetization instruction issued by the data processing control system;
    信号源,与所述数据处理控制系统连接,用于根据数据处理控制系统发出的退磁指令生成对应频率的正弦波退磁电信号;A signal source, connected to the data processing control system, and configured to generate a sine wave demagnetizing electrical signal of a corresponding frequency according to a demagnetization instruction issued by the data processing control system;
    功率放大器,与所述信号源连接,用于将信号源生成的正弦波退磁电信号放大成对应幅值后输出;A power amplifier connected to the signal source and configured to amplify the sine wave demagnetized electrical signal generated by the signal source to a corresponding amplitude and output;
    换路开关,与所述脉冲电源和功率放大器连接,用于切换磁化脉冲电流或者放大后的正弦波退磁电信号给所述磁化退磁线圈,以产生预定强度的磁场,起到切换磁化或退磁功能的目的。A switch is connected to the pulse power source and the power amplifier, and is used to switch the magnetization pulse current or the amplified sine wave demagnetization electric signal to the magnetization demagnetization coil to generate a magnetic field of a predetermined strength, and perform the function of switching the magnetization or demagnetization. the goal of.
  3. 根据权利要求1或2所述的TMR阵列扫描式岩石磁性检测仪,其特征在于:The TMR array scanning rock magnetic detector according to claim 1 or 2, wherein:
    所述三维样品移动台上设置有步进电机和光栅尺位移传感器;A stepping motor and a grating scale displacement sensor are arranged on the three-dimensional sample moving stage;
    所述样品台控制器包括:The sample stage controller includes:
    电机控制器,与所述数据处理控制系统连接,用于接收数据处理控制系统的样品台移动指令生成电机控制信号,并利用所述光栅尺位移传感器反馈的位置信息实现闭环控制样品支撑杆的移动定位;The motor controller is connected to the data processing control system, and is configured to receive a sample stage movement instruction of the data processing control system to generate a motor control signal, and use the position information fed back by the scale displacement sensor to implement closed-loop control of the movement of the sample support rod Positioning
    电机驱动器,与所述电机控制器连接,用于接收电机控制信号并能生成驱动电信号给所述步进电机。The motor driver is connected to the motor controller and is configured to receive a motor control signal and generate a driving electric signal to the stepping motor.
  4. 根据权利要求3所述的TMR阵列扫描式岩石磁性检测仪,其特征在于,所述步进电机为三个,分别用于控制样品支撑杆在三个维度上移动。The TMR array scanning type rock magnetic detector according to claim 3, wherein there are three stepping motors for controlling the movement of the sample support rod in three dimensions, respectively.
  5. 根据权利要求4所述的TMR阵列扫描式岩石磁性检测仪,其特征在于,所述样品支撑杆水平设置。The TMR array scanning type rock magnetic detector according to claim 4, wherein the sample supporting rod is horizontally arranged.
  6. 根据权利要求4所述的TMR阵列扫描式岩石磁性检测仪,其特征在于,所述样品支撑杆的长度为30cm~100cm。The TMR array scanning type rock magnetic detector according to claim 4, wherein the length of the sample supporting rod is 30 cm to 100 cm.
  7. 根据权利要求3所述的TMR阵列扫描式岩石磁性检测仪,其特征在于,所述三维样品移动台及样品支撑杆均选用无磁性材料制作。The TMR array scanning type rock magnetic detector according to claim 3, wherein the three-dimensional sample moving stage and the sample supporting rod are both made of non-magnetic material.
  8. 根据权利要求3所述的TMR阵列扫描式岩石磁性检测仪,其特征在于,所述步进电机为压电陶瓷电机。The TMR array scanning rock magnetic detector according to claim 3, wherein the stepping motor is a piezoelectric ceramic motor.
  9. 根据权利要求1所述的TMR阵列扫描式岩石磁性检测仪,其特征在于,所述TMR探头阵列、三维样品移动台和磁化退磁线圈均置于磁屏蔽室中。The TMR array scanning rock magnetic detector according to claim 1, wherein the TMR probe array, the three-dimensional sample moving stage, and the magnetization demagnetization coil are all placed in a magnetic shielding room.
  10. 根据权利要求9所述的TMR阵列扫描式岩石磁性检测仪,其特征在于,所述TMR阵列扫描式岩石磁性检测仪还包括在磁场检测时套设于所述TMR探头阵列以及样品支撑杆外的磁屏蔽筒;The TMR array scanning rock magnetic detector according to claim 9, further comprising: Magnetic shield tube
    所述磁屏蔽室用于将内部磁场屏蔽至100nT及以下;所述磁屏蔽筒用于将内部磁场屏蔽至10nT及以下。The magnetic shielding room is used to shield the internal magnetic field to 100nT and below; the magnetic shielding cylinder is used to shield the internal magnetic field to 10nT and below.
PCT/CN2018/105903 2018-09-12 2018-09-17 Tmr array scanning type rock magnetic detector WO2020051924A1 (en)

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