WO2018130008A1 - 一种茶按摩油及其制备方法与应用 - Google Patents

一种茶按摩油及其制备方法与应用 Download PDF

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Publication number
WO2018130008A1
WO2018130008A1 PCT/CN2017/112103 CN2017112103W WO2018130008A1 WO 2018130008 A1 WO2018130008 A1 WO 2018130008A1 CN 2017112103 W CN2017112103 W CN 2017112103W WO 2018130008 A1 WO2018130008 A1 WO 2018130008A1
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Prior art keywords
oil
tea
parts
massage
seed oil
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PCT/CN2017/112103
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English (en)
French (fr)
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叶勇
杨谦
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华南理工大学
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Priority to US16/334,364 priority Critical patent/US10702468B2/en
Publication of WO2018130008A1 publication Critical patent/WO2018130008A1/zh

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
    • A61N5/00—Radiation therapy
    • A61N5/06—Radiation therapy using light
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/592—Mixtures of compounds complementing their respective functions
    • A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
    • A61N5/00—Radiation therapy
    • A61N5/06—Radiation therapy using light
    • A61N2005/0658—Radiation therapy using light characterised by the wavelength of light used
    • A61N2005/0659—Radiation therapy using light characterised by the wavelength of light used infrared
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005—Antimicrobial preparations

Definitions

  • the invention belongs to the field of skin care products, and particularly relates to a tea massage oil and a preparation method and application thereof.
  • Massage is a physiotherapy method that stimulates acupoints, relaxes muscles, relieves fatigue and stress through massage.
  • Massage oil is a skin oil used in massage to enhance the massage effect, usually composed of essential oil and base oil.
  • Essential oils are volatile, stimulating the brain and relaxing; base oils are used to dilute essential oils and have nutritional functions.
  • Camellia oil has the effect of nourishing the skin.
  • the patent application of the application No. 200810066987.1, the patent application No. 201410758075.6 discloses a massage oil using tea seed oil as a matrix or component.
  • the tea oil is sticky and dispersible, and it is directly used as a massage base oil or in combination, which is not conducive to the penetration of the active ingredients in the massage oil into the skin, and it is difficult to activate the skin.
  • the invention adopts the dispersely good ethyl ester tea oil as the base oil, cooperates with the antibacterial essential oil and the plant nutrient oil, and utilizes the far-infrared action of the nanometer strontium to activate the skin, thereby playing a good role in promoting nutrient absorption and protecting the skin, especially Suitable for men's health protection.
  • Another object of the present invention is to provide a method for preparing the above tea massage oil.
  • the invention prepares the ethyl esterified tea oil under the mild condition by the enzymatic method, ensures that the nutrient composition of the tea oil is not destroyed, and exerts the multi-effect health care effect of the massage oil through reasonable compatibility.
  • a tea massage oil prepared from the following raw materials by weight:
  • each raw material 40 ⁇ 87 parts of ethylated tea oil, 5 ⁇ 15 parts of oregano oil, 2 ⁇ 12 parts of white leaf layer oil, pumpkin seeds 2 to 10 parts of oil, 2 to 10 parts of cactus seed oil, 1 to 10 parts of thyme seed oil, and 1 to 5 parts of nano-cerium oxide.
  • the sum of the parts by weight of each raw material is preferably 100.
  • the tea massage oil is preferably prepared from the following raw materials by weight:
  • ethylated tea oil 70 parts of ethylated tea oil, 10 parts of oregano oil, 5 parts of white leaf layer oil, 5 parts of pumpkin seed oil, 5 parts of cactus seed oil, 3 parts of thyme seed oil, and 2 parts of nano cerium oxide.
  • the ethylated tea oil is prepared by mixing tea seed oil with ethanol, adding immobilized lipase, reacting at a certain temperature, centrifuging, taking the supernatant, and using the saturated sodium chloride aqueous solution in the supernatant. The mixture was rinsed, allowed to stand for stratification, and the lower layer was removed to obtain ethyl esterified tea oil.
  • the volume ratio of the tea seed oil to ethanol is 1: (1 to 5), the amount of the immobilized lipase is 0.5 to 5% of the mass of the tea seed oil, and the temperature of the reaction is 30 to 70 ° C.
  • the time is 12 to 24 hours.
  • the immobilized lipase is one or more of Lipozyme TL IM or Lipozyme 435.
  • the centrifugal rotation speed is 1000-5000 rev / min, the centrifugation time is 20-60 min; the saturated sodium chloride aqueous solution is 0.5 to 3 times the mass of the tea seed oil.
  • the preparation method of the tea massage oil comprises the steps of: mixing ethyl esterified tea oil, oregano oil, mutual leaf white oil, pumpkin seed oil, cactus seed oil, thyme seed oil and nano cerium oxide, Get tea massage oil.
  • the massage oil has a viscosity of 27 to 45 mPa ⁇ s.
  • the tea massage oil is used as an anti-fatigue massage product, a male health massage product, a deodorant massage product, and/or an activated skin massage product.
  • the tea massage oil appliance eliminates fatigue and men's health care, defamation and far infrared activation of the skin.
  • Tea oil itself has nutritive and antibacterial effect, but its viscosity is large, which is not conducive to uniform application.
  • the present invention makes tea oil by ester exchange method to make ethylated tea oil, which improves the fluidity and comfort of tea oil; oregano oil It is a volatile oil of oregano grass, rich in carvacrol and thymol, with heat, dampness, heat, solution, qi and strong bactericidal and bacteriostatic effects; main components of F. sylvestris It has terpineol and terpineol, and has strong antibacterial ability against Staphylococcus aureus.
  • pumpkin seed oil contains various bioactive substances such as plant sterols, amino acids, vitamins and minerals. Especially high content of zinc, magnesium, calcium and phosphorus, it is a healthy nutrient oil with outstanding male health effects, can prevent prostate hyperplasia; cactus seed oil, mild, to eliminate facial fine lines, pigmentation, stretch marks, scars And acne and pimples have obvious effects; passion fruit oil is rich in linolenic acid, which is easily absorbed by the skin and can prevent the formation of melanin. It is non-toxic and can produce negative ions at body temperature and emit far infrared rays. It has the functions of promoting metabolism, blood circulation, anti-inflammatory and analgesic, and regulating immunity.
  • Nano-cerium oxide is used to enhance their affinity and far-infrared effect on the skin.
  • tea oil, pumpkin oil and cactus are used.
  • the nutritive action of seed oil and passion fruit seed oil and the antibacterial action of oregano oil and interlobular white leaf oil form a tea massage oil with various functions.
  • the components of the massage oil of the present invention are all natural products, and no preservatives, artificial flavors and hormones are added, and the skin is not irritated.
  • the present invention uses ethylated tea oil as a base oil, has low viscosity, good fluidity, clear and transparent appearance, and comfortable skin feeling.
  • the nano cerium oxide of the present invention can generate negative ions at body temperature, emit far infrared rays of the human body, activate the skin, and improve the therapeutic effect of the massage.
  • the present invention is a multifunctional massage oil which is suitable for male health care by distributing regeneration, promoting absorption, antibacterial and anti-inflammatory, health care, and other functions of the group to exert synergy between the components.
  • oregano oil oregano grass steam distilled oil, produced by Shenzhen Dingcheng Plant and Spice Co., Ltd.
  • Mutual Leaf White Thousand Layers of Oil Fahrenheit White Thousand Layers of Steam Distillation Oil, Ji'an Zhongxiang Natural Plant Co., Ltd.
  • pumpkin seed oil zucchini seed cold-pressed grade, produced by Jilinzhou Changbai Workshop Electronics Co., Ltd.
  • cactus seed oil cactus seed press oil, produced by Neptune Cosmetics Co., France
  • thyme seed oil Thime fruit pressed oil, produced by Shenzhen Guoxin Flavor & Fragrance Co., Ltd.
  • nano-cerium oxide nano-cerium oxide (nano-sized cerium oxide, produced by Linglong County Tianlong Mineral Processing Factory).
  • a tea massage oil prepared from the following raw materials by weight:
  • ethylated tea oil 70 parts of ethylated tea oil, 10 parts of oregano oil, 5 parts of white leaf layer oil, 5 parts of pumpkin seed oil, 5 parts of cactus seed oil, 3 parts of thyme seed oil, 2 parts of nano cerium oxide;
  • the preparation method of the tea massage oil comprises the following steps:
  • Ethylated tea oil, oregano oil, eucalyptus oil, pumpkin seed oil, cactus seed oil, thyme seed oil and nano cerium oxide are uniformly mixed to obtain tea massage oil.
  • the massage oil prepared in this embodiment has a density of 0.938 g/mL and a viscosity of 32 mPa.s, which is only 1/4 of the general vegetable oil, easy to disperse, good in bacteriostatic performance, stable, and has no obvious change after being sealed at room temperature for 18 months.
  • a tea massage oil prepared from the following raw materials by weight:
  • the preparation method of the tea massage oil comprises the following steps:
  • Ethylated tea oil, oregano oil, eucalyptus oil, pumpkin seed oil, cactus seed oil, thyme seed oil and nano cerium oxide are uniformly mixed to obtain tea massage oil.
  • the massage oil prepared in this embodiment has a density of 0.925 g/mL and a viscosity of 27 mPa.s, which is only 1/5 of the general vegetable oil, easy to disperse, good in bacteriostatic performance, stable, and has no obvious change after being sealed at room temperature for 18 months.
  • a tea massage oil prepared from the following raw materials by weight:
  • ethylated tea oil 15 parts of oregano oil, 10 parts of white leaf oil, 10 parts of pumpkin seed oil, 10 parts of cactus seed oil, 10 parts of thyme seed oil, 5 parts of nano-cerium oxide;
  • the preparation method of the tea massage oil comprises the following steps:
  • Ethyl acetate tea oil, oregano oil, Mutual leaf white oil, pumpkin seed oil, cactus seed oil, Thyme seed oil and nano cerium oxide are evenly mixed to obtain tea massage oil.
  • the massage oil prepared in this embodiment has a density of 0.963 g/mL and a viscosity of 45 mPa.s, which is only 1/3 of the general vegetable oil, easy to disperse, good in antibacterial performance, stable, and has no obvious change after being sealed at room temperature for 18 months.
  • a tea massage oil prepared from the following raw materials by weight:
  • ethylated tea oil 50 parts of ethylated tea oil, 8 parts of oregano oil, 6 parts of white leaf layer oil, 6 parts of pumpkin seed oil, 4 parts of cactus seed oil, 4 parts of thyme seed oil, 2 parts of nano cerium oxide;
  • the preparation method of the tea massage oil comprises the following steps:
  • Ethylated tea oil, oregano oil, eucalyptus oil, pumpkin seed oil, cactus seed oil, thyme seed oil and nano cerium oxide are uniformly mixed to obtain tea massage oil.
  • the massage oil prepared in this embodiment has a density of 0.947 g/mL and a viscosity of 41 mPa.s, which is only 1/3 of the general vegetable oil, easy to disperse, has good bacteriostatic performance, and is stable, and has no obvious change after being sealed at room temperature for 18 months.
  • a tea massage oil prepared from the following raw materials by weight:
  • ethylated tea oil 12 parts of oregano oil, 8 parts of succulent oil, 8 parts of pumpkin seed oil, 6 parts of cactus seed oil, 6 parts of thyme seed oil, 3 parts of nano cerium oxide;
  • the preparation method of the tea massage oil comprises the following steps:
  • Ethylated tea oil, oregano oil, eucalyptus oil, pumpkin seed oil, cactus seed oil, thyme seed oil and nano cerium oxide are uniformly mixed to obtain tea massage oil.
  • the massage oil prepared in this embodiment has a density of 0.942 g/mL and a viscosity of 37 mPa.s, which is only 1/4 of the general vegetable oil, easy to disperse, good in bacteriostatic performance, stable, and has no obvious change after being sealed at room temperature for 18 months.
  • a tea massage oil prepared from the following raw materials by weight:
  • the preparation method of the tea massage oil comprises the following steps:
  • Ethylated tea oil, oregano oil, eucalyptus oil, pumpkin seed oil, cactus seed oil, thyme seed oil and nano cerium oxide are uniformly mixed to obtain tea massage oil.
  • the massage oil prepared in this embodiment has a density of 0.940 g/mL and a viscosity of 34 mPa.s, which is only 1/4 of the general vegetable oil, easy to disperse, good in bacteriostatic performance, stable, and has no obvious change after being sealed at room temperature for 18 months.
  • mice 60 male volunteers were divided into 6 groups, and the tea massage oils prepared in Examples 1 to 6 were respectively used for 30 days, and their comfort ( ⁇ 25 points), fatigue elimination ( ⁇ 25 points), and reduction of color sputum. ( ⁇ 25 points), skin vitality ( ⁇ 25 points) score.

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Abstract

一种茶按摩油及其制备方法与应用，所述茶按摩油由以下按重量份数计的原料制备而成：乙酯化茶油40～87份，牛至油5～15份，互叶白千层油2～12份，南瓜子油2～10份，仙人掌种子油2～10份，百里香果籽油1～10份，纳米氧化锗1～5份。所述方法为：将乙酯化茶油，牛至油，互叶白千层油，南瓜子油，仙人掌种子油，百里香果籽油以及纳米氧化锗混合均匀，得到茶按摩油。所述茶按摩油具有消除疲劳及男性保健、去瘢和远红外活化肌肤作用。

Description

一种茶按摩油及其制备方法与应用 技术领域
本发明属于护肤品领域，具体涉及一种茶按摩油及其制备方法与应用。
背景技术
按摩是一种理疗手段，通过按摩进行穴位刺激、放松筋骨、舒缓疲劳和压力。按摩油是按摩时采用的，用以增强按摩效果的护肤油，通常由精油和基底油组成。精油具有挥发性，可刺激大脑，起到放松的作用；基底油用于精油的稀释，并具备营养功能。
目前市场上的按摩油种类众多，但大多为人工合成的基底油，含化学物质或激素，长期使用不利于人体健康。植物油和挥发油也被广泛用作按摩油，对人体和环境安全，但组方不合理，功效单一，没有用于男性健康的按摩油产品。
山茶油具有滋养肌肤的作用。申请号200810066987.1的专利申请、申请号为201410758075.6的专利申请公开了一种以茶籽油作为基质或组分的按摩油。但是茶油质粘、分散性差，直接作为按摩基质油或配伍使用，不利于按摩油中活性成分透入肌肤，难以起到激活肌肤作用。
发明内容
为了克服现有技术的缺点与不足，本发明的首要目的在于提供一种茶按摩油。本发明采用分散性好的乙酯化茶油为基底油，配合抗菌精油和植物营养油，并利用纳米锗的远红外作用，激活肌肤，起到良好的促进营养吸收和保护肌肤的作用，尤其适合于男性健康保护。
本发明的另一目的在于提供上述茶按摩油的制备方法。本发明通过酶法在温和条件下制备乙酯化茶油，保证茶油营养成分不被破坏；并通过合理配伍，发挥按摩油的多功效保健作用。
本发明的目的通过下述技术方案实现：
一种茶按摩油，由以下重量份计的原料制备而成：
乙酯化茶油40～87份，牛至油5～15份，互叶白千层油2～12份，南瓜子 油2～10份，仙人掌种子油2～10份，百里香果籽油1～10份，纳米氧化锗1～5份。各原料的重量份数之和优选为100。
所述茶按摩油，优选由以下重量份的原料制备而成：
乙酯化茶油70份，牛至油10份，互叶白千层油5份，南瓜子油5份，仙人掌种子油5份，百里香果籽油3份，纳米氧化锗2份。
所述乙酯化茶油通过以下方法制备得到：将茶籽油与乙醇混合，加入固定化脂肪酶，在一定温度下反应，离心，取上清液，将上清液用饱和氯化钠水溶液淋洗，静置分层，除去下层，得到乙酯化茶油。
所述茶籽油与乙醇的体积比1：(1～5)，所述固定化脂肪酶的用量为茶籽油质量的0.5～5％，所述反应的温度为30～70℃，反应的时间为12～24h。
所述固定化脂肪酶为Lipozyme TL IM或Lipozyme 435中的一种以上。
所述离心的转速为1000～5000转/min，离心时间为20～60min；所述饱和氯化钠水溶液的用量为茶籽油质量的0.5～3倍。
所述茶按摩油的制备方法，包括如下步骤：将乙酯化茶油，牛至油，互叶白千层油，南瓜子油，仙人掌种子油，百里香果籽油以及纳米氧化锗混合均匀，得到茶按摩油。所述按摩油的粘度为27～45mPa.s。
所述茶按摩油用作消除疲劳按摩产品、男性保健按摩产品、去瘢按摩产品和/或活化肌肤按摩产品。所述茶按摩油具消除疲劳及男性保健、去瘢和远红外活化肌肤作用。
原理：茶油本身具有营养抗菌功效，但其粘度大，不利于涂抹均匀，本发明将茶油通过酯交换法制成乙酯化茶油，改善了茶油的流动性和舒适性；牛至油是牛至草的挥发油，富含类香芹酚和欧百里香酚，具有清热、化湿、祛暑、解表、理气和极强的杀菌、抑菌作用；互叶白千层油主要组分有松油醇、松油烯等，对金黄色葡萄球菌等具有较强的抗菌能力，是一种优良的天然抗菌剂；南瓜子油含有植物甾醇、氨基酸、维生素、矿物质等多种生物活性物质，尤其是锌、镁、钙、磷含量极高，是有突出男性保健作用的健康营养油，可预防前列腺增生；仙人掌种子油，性温和，对消除面部细纹、色斑、妊娠纹、疤痕及痤疮、丘疹都有明显功效；百香果籽油含有丰富的亚麻酸，极易被皮肤吸收，可预防黑色素的形成。氧化锗无毒，能够在体温下产生负离子，发射远红外线， 具有促进新陈代谢、血液循环、抗炎镇痛和调节免疫等作用，采用纳米氧化锗，加强了它们对肌肤的亲和力和远红外作用；再与其他原料配伍使用，利用茶油、南瓜子油、仙人掌种子油、百香果籽油的营养作用和牛至油、互叶白叶层油的抗菌作用，形成多种功效为一体的茶按摩油。
本发明相对于现有技术具有如下的优点及效果：
(1)本发明按摩油的成分均为天然产物，不添加防腐剂，人工香料和激素，对皮肤无刺激。
(2)本发明使用乙酯化茶油作为基础油，粘度低，流动性好，外观澄清透明，皮肤感觉舒适。
(3)本发明使用纳米氧化锗能够在体温下产生负离子，发射人体远红外线，激活肌肤，提高按摩的疗效。
(4)本发明通过将修复再生，促进吸收，抗菌消炎，保健去瘢等不同功能的组分配伍，发挥各组分间的协同作用，是一种多功能按摩油，尤其适合于男性保健。
具体实施方式
下面结合实施例对本发明作进一步详细的描述，但本发明的实施方式不限于此。实施例中牛至油(牛至草水蒸汽蒸馏油，深圳市鼎诚植物香料有限公司生产)，互叶白千层油(互叶白千层嫩枝水蒸汽蒸馏油，吉安市中香天然植物有限公司生产)，南瓜子油(南瓜子冷榨一级，吉林省长白工坊科贸有限公司生产)，仙人掌种子油(仙人掌种子压榨油，法国奈洁化妆品公司生产)，百里香果籽油(百里香果压榨油，深圳市国鑫香精香料有限公司生产)，纳米氧化锗(纳米级二氧化锗，灵寿县天隆矿产品加工厂生产)。
实施例1
一种茶按摩油，由以下重量份计的原料制备而成：
乙酯化茶油70份，牛至油10份，互叶白千层油5份，南瓜子油5份，仙人掌种子油5份，百里香果籽油3份，纳米氧化锗2份；
所述茶按摩油的制备方法，包括如下步骤：
(1)乙酯化制备：将茶籽油(油茶籽油)与乙醇按体积比1：3混合，加入茶籽油质量1％的固定化脂肪酶Lipozyme TL IM，在40℃反应20h；3000转 /min离心30min，上清液再用茶籽油质量2倍的饱和氯化钠水溶液淋洗，静置分层，除去下层，即得乙酯化茶油；
(2)将乙酯化茶油，牛至油，互叶白千层油，南瓜子油，仙人掌种子油，百里香果籽油以及纳米氧化锗混合均匀，得到茶按摩油。
本实施例制备的按摩油的密度为0.938g/mL、粘度32mPa.s，仅为一般植物油的1/4、易分散、抑菌性能好、稳定，密封室温放置18个月无明显变化。
实施例2
一种茶按摩油，由以下重量份计的原料制备而成：
乙酯化茶油87份，牛至油5份，互叶白千层油2份，南瓜子油2份，仙人掌种子油2份，百里香果籽油1份，纳米氧化锗1份；
所述茶按摩油的制备方法，包括如下步骤：
(1)乙酯化制备：茶籽油与乙醇按体积比1：5混合，加入茶籽油质量5％的固定化脂肪酶Lipozyme 435，在30℃反应24h；1000转/min离心60min，上清液再用茶油质量3倍的饱和氯化钠水溶液淋洗，静置分层，除去下层，即得乙酯化茶油；
(2)将乙酯化茶油，牛至油，互叶白千层油，南瓜子油，仙人掌种子油，百里香果籽油以及纳米氧化锗混合均匀，得到茶按摩油。
本实施例制备的按摩油的密度为0.925g/mL、粘度27mPa.s，仅为一般植物油的1/5、易分散、抑菌性能好、稳定，密封室温放置18个月无明显变化。
实施例3
一种茶按摩油，由以下重量份计的原料制备而成：
乙酯化茶油40份，牛至油15份，互叶白千层油10份，南瓜子油10份，仙人掌种子油10份，百里香果籽油10份，纳米氧化锗5份；
所述茶按摩油的制备方法，包括如下步骤：
(1)乙酯化制备：茶籽油与乙醇按体积比1：1混合，加入茶籽油质量0.5％的固定化脂肪酶Lipozyme TL IM，在70℃反应12h；5000转/min离心20min，上清液再用茶籽油质量0.5倍的饱和氯化钠水溶液淋洗，静置分层，除去下层，即得乙酯化茶油；
(2)将乙酯化茶油，牛至油，互叶白千层油，南瓜子油，仙人掌种子油， 百里香果籽油以及纳米氧化锗混合均匀，得到茶按摩油。
本实施例制备的按摩油的密度为0.963g/mL、粘度45mPa.s，仅为一般植物油的1/3、易分散、抑菌性能好、稳定，密封室温放置18个月无明显变化。
实施例4
一种茶按摩油，由以下重量份计的原料制备而成：
乙酯化茶油50份，牛至油8份，互叶白千层油6份，南瓜子油6份，仙人掌种子油4份，百里香果籽油4份，纳米氧化锗2份；
所述茶按摩油的制备方法，包括如下步骤：
(1)乙酯化制备：茶籽油与乙醇按体积比1：2混合，加入茶油质量2％的固定化脂肪酶Lipozyme 435，在50℃反应16h；2000转/min离心30min，上清液再用茶油质量2倍的饱和氯化钠水溶液淋洗，静置分层，除去下层，即得乙酯化茶油；
(2)将乙酯化茶油，牛至油，互叶白千层油，南瓜子油，仙人掌种子油，百里香果籽油以及纳米氧化锗混合均匀，得到茶按摩油。
本实施例制备的按摩油的密度为0.947g/mL、粘度41mPa.s，仅为一般植物油的1/3、易分散、抑菌性能好、稳定，密封室温放置18个月无明显变化。
实施例5
一种茶按摩油，由以下重量份计的原料制备而成：
乙酯化茶油57份，牛至油12份，互叶白千层油8份，南瓜子油8份，仙人掌种子油6份，百里香果籽油6份，纳米氧化锗3份；
所述茶按摩油的制备方法，包括如下步骤：
(1)乙酯化制备：茶籽油与乙醇按体积比1：4混合，加入茶油质量4％的固定化脂肪酶Lipozyme 435，在36℃反应18h；3000转/min离心40min，上清液再用茶油质量3倍的饱和氯化钠水溶液淋洗，静置分层，除去下层，即得乙酯化茶油；
(2)将乙酯化茶油，牛至油，互叶白千层油，南瓜子油，仙人掌种子油，百里香果籽油以及纳米氧化锗混合均匀，得到茶按摩油。
本实施例制备的按摩油的密度为0.942g/mL、粘度37mPa.s，仅为一般植物油的1/4、易分散、抑菌性能好、稳定，密封室温放置18个月无明显变化。
实施例6
一种茶按摩油，由以下重量份计的原料制备而成：
乙酯化茶油64份，牛至油6份，互叶白千层油12份，南瓜子油5份，仙人掌种子油4份，百里香果籽油7份，纳米氧化锗2份；
所述茶按摩油的制备方法，包括如下步骤：
(1)乙酯化制备：茶籽油与乙醇按体积比1：3混合，加入茶籽油质量2.5％的固定化脂肪酶Lipozyme TL IM，在50℃反应15h；4000转/min离心25min，上清液用茶籽油质量2.5倍的饱和氯化钠水溶液淋洗，静置分层，除去下层，即得乙酯化茶油；
(2)将乙酯化茶油，牛至油，互叶白千层油，南瓜子油，仙人掌种子油，百里香果籽油以及纳米氧化锗混合均匀，得到茶按摩油。
本实施例制备的按摩油的密度为0.940g/mL、粘度34mPa.s，仅为一般植物油的1/4、易分散、抑菌性能好、稳定，密封室温放置18个月无明显变化。
实施例7效果评价
实施例1～6制得的茶按摩油使用效果的测定：
实验方法：60名男性志愿者分为6组，分别使用实施例1～6制得的茶按摩油30天，对其舒适性(≤25分)、消除疲劳(≤25分)、降低色瘢(≤25分)、肌肤活力(≤25分)评分。
实验结果见表1。结果表明，实施例1～6制得的茶按摩油使用效果优于市售国内茶油按摩油。
表1实施例1～6制得的茶按摩油应用效果评价(
Figure PCTCN2017112103-appb-000001
n＝10)
Figure PCTCN2017112103-appb-000002
上述实施例为本发明较佳的实施方式，但本发明的实施方式并不受上述实施例的限制，其他的任何未背离本发明的精神实质与原理下所作的改变、修饰、替代、组合、简化，均应为等效的置换方式，都包含在本发明的保护范围之内。

Claims (8)

  1. 一种茶按摩油，其特征在于：由以下重量份计的原料制备而成：
    乙酯化茶油40～87份，牛至油5～15份，互叶白千层油2～12份，南瓜子油2～10份，仙人掌种子油2～10份，百里香果籽油1～10份，纳米氧化锗1～5份。
  2. 根据权利要求1所述茶按摩油，其特征在于：由以下重量份的原料制备而成：
    乙酯化茶油70份，牛至油10份，互叶白千层油5份，南瓜子油5份，仙人掌种子油5份，百里香果籽油3份，纳米氧化锗2份。
  3. 根据权利要求1或2所述茶按摩油，其特征在于：所述乙酯化茶油通过以下方法制备得到：将茶籽油与乙醇混合，加入固定化脂肪酶，在一定温度下反应，离心，取上清液，将上清液用饱和氯化钠水溶液淋洗，静置分层，除去下层，得到乙酯化茶油。
  4. 根据权利要求3所述茶按摩油，其特征在于：所述茶籽油与乙醇的体积比1：(1～5)，所述固定化脂肪酶的用量为茶籽油质量的0.5～5％，所述反应的温度为30～70℃，反应的时间为12～24h。
  5. 根据权利要求3所述茶按摩油，其特征在于：
    所述固定化脂肪酶为Lipozyme TL IM或Lipozyme 435中的一种以上。
  6. 根据权利要求3所述茶按摩油，其特征在于：
    所述离心的转速为1000～5000转/min，离心时间为20～60min；所述饱和氯化钠水溶液的用量为茶籽油质量的0.5～3倍。
  7. 根据权利要求1～6任一项所述茶按摩油的制备方法，其特征在于包括如下步骤：将乙酯化茶油，牛至油，互叶白千层油，南瓜子油，仙人掌种子油，百里香果籽油以及纳米氧化锗混合均匀，得到茶按摩油。
  8. 根据权利要求1～6任一项所述茶按摩油的应用，其特征在于：所述茶按摩油用作消除疲劳按摩产品、男性保健按摩产品、去瘢按摩产品和/或活化肌肤按摩产品。
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