WO2017191851A1 - Device for generating saturated solution of calcined calcium - Google Patents

Device for generating saturated solution of calcined calcium Download PDF

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Publication number
WO2017191851A1
WO2017191851A1 PCT/JP2017/018757 JP2017018757W WO2017191851A1 WO 2017191851 A1 WO2017191851 A1 WO 2017191851A1 JP 2017018757 W JP2017018757 W JP 2017018757W WO 2017191851 A1 WO2017191851 A1 WO 2017191851A1
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Prior art keywords
calcined calcium
calcium
filter
main body
saturated solution
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PCT/JP2017/018757
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French (fr)
Japanese (ja)
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敏憲 森松
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株式会社オーノギ
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Priority claimed from JP2016257902A external-priority patent/JP6354113B2/en
Application filed by 株式会社オーノギ filed Critical 株式会社オーノギ
Publication of WO2017191851A1 publication Critical patent/WO2017191851A1/en

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F21/00—Dissolving
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2/00—Lime, magnesia or dolomite
    • C04B2/02—Lime
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof

Definitions

  • the present invention relates to an apparatus for continuously producing a strong alkaline calcined calcium saturated solution useful for disinfecting and deodorizing fresh food such as vegetables or tableware by dissolving calcined calcium without waste.
  • the present invention has been made to solve the above-mentioned problems, and the calcined calcium saturated solution generating device according to claim 1 is charged with granular calcined calcium above an apparatus main body comprising a cylindrical main body and an inverted frustoconical bottom. And a water inlet is provided below to introduce water in the circumferential direction of the apparatus main body, and a protrusion is provided on the bottom of the inverted truncated cone-shaped bottom, Is characterized in that an aqueous solution outlet provided with a filter is provided.
  • the calcined calcium saturated solution generating apparatus is provided with a granular calcined calcium inlet at the upper part of the apparatus main body comprising a cylindrical main body and an inverted frustoconical bottom, and a water introducing means below the circumference of the apparatus main body.
  • the bottom of the inverted frustoconical bottom is provided with a protrusion, and an aqueous solution outlet is provided at the top of the cylindrical body, on the downstream side of the aqueous solution outlet.
  • a filter housing is provided.
  • the present invention has an effect of generating a calcium saturated solution in an efficient and space-saving manner with granular calcined calcium
  • the apparatus main body has a cylindrical shape, has a protrusion at the center of the bottom portion, and the lower portion has an inverted trapezoidal conical cylinder.
  • a water flow control plate is provided on the dissolution tank and the side, and the upper trapezoidal conical cylinder from the upper part to the upper part is cylindrical, and the water supply supply port is directed in the circumferential direction on the lower side, with the uppermost sealing lid Filtration system on the lid: an apparatus comprising a water outlet through which a filter of 0.5 to 10 ⁇ m passes, and formed by a granular calcined calcium inlet and a sealing lid on the central side surface of the cylinder inclined upward.
  • the granular calcined calcium which is the raw material for the highly alkaline calcined calcium saturated solution, turns the water flow from the bottom to the top to rotate the water flow into the bottom flow through the water flow control plate. As the cylinder rises upward, the rotation speed becomes faster, and the calcium saturated solution is generated at a faster speed, and the granular calcined calcium that could not be dissolved settles from the center of the cylinder to the bottom and then flows due to water flow.
  • a device that can generate a saturated solution continuously by repeating rotational movement, and can efficiently generate a transparent highly alkaline calcined calcium saturated solution through a filter in the upper part of the device body.
  • generation apparatus which shows 1st embodiment of this invention.
  • generation state of the granular baking calcium saturated solution of 1st embodiment CC sectional view of FIG. A is a cross-sectional view taken along the line AA in FIG. 1, and B is a cross-sectional view taken along the line BB.
  • generation apparatus which shows 2nd embodiment of this invention.
  • the apparatus main body 1 includes a cylindrical main body 1a and an inverted conical bottom 1b.
  • An aqueous solution outlet 5 is provided on the upper portion of the cylindrical main body 1a, and a cylindrical filter 4 is provided in the aqueous solution outlet 5.
  • a protrusion 11 is provided on the bottom 17 of the inverted conical bottom 1b on the inverted conical bottom 1b.
  • a female screw 16 is screwed into the bottom portion 17, and a male screw 18 that is screwed into the female screw 16 is screwed into the rear end side of the protrusion 11.
  • a water introduction nozzle 9 as water introduction means is provided below the cylindrical main body 1a, and the discharge direction of the water introduction nozzle 9 faces the circumferential direction of the cylindrical main body 1a. Further, a granular calcined calcium charging hole 19 is provided at a substantially central portion of the cylindrical main body 1a, and a calcined calcium charging pipe 20 is connected to the calcined calcium charging hole 19, and a tip of the calcined calcium charging pipe 20 is provided.
  • the part is a calcined calcium inlet 2 and is closed with a lid 23.
  • An aqueous solution take-out pipe 21 is connected to the aqueous solution take-out port 5, a pressure gauge 12 is provided in the calcined calcium input pipe 20, and a water introduction valve 10 is provided with a water amount adjusting valve 10.
  • the pipe 3 is connected continuously. Further, two water flow adjusting plates 6 are provided on the inner peripheral surface of the inverted conical bottom 1b.
  • generation apparatus 22 of this invention is demonstrated.
  • the lid 23 of the granular calcined calcium inlet 2 is opened, the granular calcined calcium is introduced, the lid is closed, and the water amount adjustment valve 10 is opened to open the inside of the apparatus main body 1.
  • Water with water pressure is supplied from the water guide nozzle 9.
  • Undissolved granular calcined calcium descends toward the inverted conical bottom 1b via the central portion of the cylindrical main body 1a, and is dispersed in the circumferential direction by the protrusions 11, and the rotational water flow of the introduced water and the water flow adjusting plate 6 As a result, the granular calcined calcium rises again and repeats rising and falling.
  • the solution in contact with the filter 4 among the solutions in the apparatus main body 1 has high transparency.
  • the undissolved granular calcination calcium adhering to the side surface of the filter 4 is also peeled off and descends to the bottom. The clogging of the filter 4 can be grasped by the replacement guideline of the pressure gauge 12 and the apparatus can be replaced by opening the filter replacement lid 7. It is easy to check the remaining amount.
  • the invention of the device body is a device that can produce a calcium saturated solution without touching air due to the properties of calcined calcium, and the insoluble granular calcined calcium returns to the dissolving device to become a calcium saturated solution.
  • the present invention employs a small household device with a cylindrical outer diameter of 20 cm and a height of 60 cm.
  • the granulated calcined calcium 8 explains the process of producing a calcined calcium saturated solution.
  • About 1 liter of water is introduced into the apparatus body diameter 20 cm from the water inlet, and 100 g of granular calcined calcium is introduced from FIG. 2 l per minute from an inner diameter of 4 mm,
  • water with a water pressure of 0.3 Mpa is added, the granular calcined calcium that settles and accumulates at the bottom of the container starts to dissolve in the same rotational motion as water, and is filtered by the upper filter 4 while rotating to the top of the device body 1.
  • a strong alkaline solution having a pH value of 12 and 7 of an aqueous solution take-out pipe 21 was continuously generated from a calcium saturated solution and an aqueous solution outlet 5 inner diameter of 6 mm.
  • Filter Filtration accuracy: In the case of use of 1 micron, 90 l of a colorless transparent ph12.3 to 12.7 saturated solution is confirmed with respect to 100 g of granular calcined calcium.
  • Filter Filtration accuracy: When using 10 microns, a translucent saturated solution is confirmed for 100 g of granular calcined calcium, and it is necessary to wash away with fresh water for cleaning purposes. Can be used for purposes such as sandbox spraying, where calcium clogging is likely to occur.
  • the apparatus main body 101 includes an inverted conical main body 101a and a cylindrical bottom 101b, and an aqueous solution outlet 5 and a granular calcined calcium inlet 107 are provided on the upper portion of the inverted conical main body 101a.
  • a pipe 21 is provided.
  • a cyclone filter 102 is connected to the downstream side of the aqueous solution extraction pipe 21.
  • a calcined calcium solution extraction pipe 104 is connected to the upper part of the cyclone filter 102.
  • a pressure gauge 112 is attached to the calcined calcium solution extraction pipe 104.
  • a filter housing 103 is connected to the downstream side of the calcined calcium solution extraction pipe 104.
  • a ph electrode housing 105 is connected to the outlet side of the filter housing 103 so that the calcined calcium solution is discharged from the aqueous solution outlet 113.
  • the cylindrical bottom 101b is provided with a conical protrusion 119 on the bottom 17 of the cylindrical bottom 101b.
  • Three high-speed flow nozzles 120 as water introduction means are attached to the left side in FIG. 5 on the side wall of the cylindrical bottom portion 101b, two on the right side, and two on the right side are two high-speed flow rate nozzles on the left side. It is attached to face 120.
  • the discharge direction of the high-speed flow rate nozzle 120 faces the circumferential direction of the cylindrical bottom portion 101b.
  • a granular calcined calcium inlet 107 is provided at a substantially central portion of the inverted conical main body 101 a and is closed with a lid 23.
  • the cloudy aqueous solution outlet pipe 111 is connected to the cloudy aqueous solution outlet 111.
  • a water introduction branch pipe 118 having a water amount adjustment valve 115 is connected to the high-speed flow rate nozzle 120.
  • the water introduction branch pipe 118 is connected to the water introduction pipe 109 via a water amount adjustment valve 115.
  • An insoluble calcium recovery pipe 122 is connected to the lower part of the cyclone filter 102.
  • the insoluble calcium recovery pipe 122 is connected to an ejector 110 incorporated in a calcium mixing pipe 123.
  • a flow rate adjusting plate 106 is provided between the mounting position of the high-speed flow nozzle 120 and the mounting position of the high-speed flow nozzle 120 inside the cylindrical bottom 101b.
  • the flow rate adjusting plate 106 is provided in a state of being inclined downward toward the water introduction method.
  • the flow rate adjusting plate 106 is a punching plate, but is not necessarily a punching plate.
  • the device of the present invention is a space-saving and efficient high-calcin calcium-saturated calcium saturated solution that produces a colorless and transparent solution.
  • you can change the size of the device from a general home to a kindergarten sandbox, school, hotel, food factory,
  • the environment can be improved by washing and spraying food, kitchens, and toilets contaminated with bacteria, viruses, and mold in public facilities.
  • the device of the present invention is a sealed container, and it can generate a highly alkaline solution with very little contact with air, and can be used only when necessary to maintain a high alkali.

Abstract

In the prior art, a horn-shaped container was used in which the remaining amount of particulate calcined calcium as a starting material for a saturated solution of calcined calcium could not be known without removing a lid, the particulate calcined calcium could not be thoroughly dissolved, the dissolution rate was low, a filter was on the outside of the dissolving container, and the filter quickly became clogged. In the present invention, using a cylindrical container makes it possible to uniformly and quickly dissolve the particulate calcined calcium, using a transparent resin container makes it possible to confirm the remaining amount and the state of dissolution of the particulate calcined calcium, and a filter 4 is attached to a filter replacement lid, whereby particulate calcined calcium adhering to the filter comes off and falls to a bottom part, and a rotating water flow occurs and a saturated solution is generated.

Description

焼成カルシウム飽和溶液生成装置Sintered calcium saturated solution generator
　本発明は、焼成カルシウムを無駄なく溶解させて、野菜などの生鮮食品もしくは食器などの除菌・消臭剤として有用な強アルカリ性焼成カルシウム飽和溶液を連続的に製造するための装置に関する。 The present invention relates to an apparatus for continuously producing a strong alkaline calcined calcium saturated solution useful for disinfecting and deodorizing fresh food such as vegetables or tableware by dissolving calcined calcium without waste.
　従来のカルシウム飽和溶液の製造方法としては、焼成カルシウムをそのまま容器の中で溶解させ白濁した溶液を使用したりする方法を採っていた。又、カルシウム飽和溶液の生成装置としては、特許第５２９５８６３号に記載されたアルカリ性焼成カルシウム水溶液製造装置が知られている。 As a conventional method for producing a saturated calcium solution, a method in which calcined calcium is dissolved in a container as it is and a cloudy solution is used is employed. Moreover, as an apparatus for producing a calcium saturated solution, an alkaline calcined calcium aqueous solution production apparatus described in Japanese Patent No. 5295863 is known.
特許第５２９５８６３号公報Japanese Patent No. 5295863
　前述の焼成カルシウムをそのまま容器の中で溶解させ白濁した溶液を使用する方法では、溶解できなかった粉末状の焼成カルシウムの固形物が食材へ混入し消費者のクレームとなる課題があった。又、特許第５２９５８６３号に記載されたアルカリ性焼成カルシウム水溶液製造装置では、焼成カルシウムは通水板上で蓮根固形状の塊となり焼成カルシウムは長時間十分溶解することができず焼成カルシウムの攪拌能力が低く溶解速度が遅いという課題と溶解出来なかった焼成カルシウム溶解槽の外で蓄積し、沈殿する無駄な課題もあった。 In the method of using the above-mentioned solution in which the calcined calcium is dissolved as it is in the container as described above, there is a problem that the powdered calcined calcium solids that could not be dissolved are mixed into the food and become a consumer complaint. Moreover, in the alkaline calcined calcium aqueous solution manufacturing apparatus described in Japanese Patent No. 5295863, calcined calcium becomes a lotus root solid lump on the water flow plate and the calcined calcium cannot be sufficiently dissolved for a long time, and the calcined calcium has a stirring ability. There were also the problem that it was low and the dissolution rate was slow, and there was a wasteful problem of accumulation and precipitation outside the calcined calcium dissolution tank that could not be dissolved.
　本発明は、上記課題を解決するためになされたもので、請求項１に記載の焼成カルシウム飽和溶液生成装置は筒状本体と逆円錐台状底部とからなる装置本体の上方に粒状焼成カルシウム投入口を備え、下方に水導入口が前記装置本体の円周方向に水を導入するように備えられるとともに前記逆円錐台状底部の底には突起物が設けられ、前記円筒状本体の上部にはフィルターを備えた水溶液取出口が設けられたことを特徴とする。
　請求項２に記載の焼成カルシウム飽和溶液生成装置は円筒状本体と逆円錐台状底部とからなる装置本体の上方に粒状焼成カルシウム投入口を備え、下方に水導入手段が前記装置本体の円周方向に水を導入するように備えられるとともに前記逆円錐台状底部の底には突起物が設けられ、前記円筒状本体の上部には水溶液取出口が設けられ、該水溶液取出し口の下流側にフィルターハウジングが設けられたことを特徴とする。 The present invention has been made to solve the above-mentioned problems, and the calcined calcium saturated solution generating device according to claim 1 is charged with granular calcined calcium above an apparatus main body comprising a cylindrical main body and an inverted frustoconical bottom. And a water inlet is provided below to introduce water in the circumferential direction of the apparatus main body, and a protrusion is provided on the bottom of the inverted truncated cone-shaped bottom, Is characterized in that an aqueous solution outlet provided with a filter is provided.
The calcined calcium saturated solution generating apparatus according to claim 2 is provided with a granular calcined calcium inlet at the upper part of the apparatus main body comprising a cylindrical main body and an inverted frustoconical bottom, and a water introducing means below the circumference of the apparatus main body. The bottom of the inverted frustoconical bottom is provided with a protrusion, and an aqueous solution outlet is provided at the top of the cylindrical body, on the downstream side of the aqueous solution outlet. A filter housing is provided.
　本発明は、粒状焼成カルシウムを効率よく省スペースでカルシウム飽和溶液を生成出来る効果を持つ、装置本体は円筒形で成り、底面部の中心部に突起物が有り、下部は逆台形の円錐筒の溶解槽と側面に水流調整板が設けられており、逆台形の円錐筒上部から上部は円筒形から成り下部側面に水導の供給口が円周方向に向けられ、最上部の密閉蓋が有り、蓋に濾過制度：０．５~１０μのフィルターが付フィルターを通過する水出口から成り、又、円筒中央側面に傾斜上向きに粒状焼成カルシウム投入口と密閉蓋で形成している装置。 The present invention has an effect of generating a calcium saturated solution in an efficient and space-saving manner with granular calcined calcium, the apparatus main body has a cylindrical shape, has a protrusion at the center of the bottom portion, and the lower portion has an inverted trapezoidal conical cylinder. A water flow control plate is provided on the dissolution tank and the side, and the upper trapezoidal conical cylinder from the upper part to the upper part is cylindrical, and the water supply supply port is directed in the circumferential direction on the lower side, with the uppermost sealing lid Filtration system on the lid: an apparatus comprising a water outlet through which a filter of 0.5 to 10 μm passes, and formed by a granular calcined calcium inlet and a sealing lid on the central side surface of the cylinder inclined upward.
　高アルカリ焼成カルシウム飽和溶液の原料となる粒状焼成カルシウムは、底面から上面へ水導水を回転吐出させることにより水流調整板にて底面水流になり粒状焼成カルシウムも同じく回転しながら溶解し、逆台形円錐筒は上方に上がる事により回転速度が速くなり焼成カルシウム飽和溶液が速いスピードで、カルシウム飽和溶液が生成され、又、溶解出来なかった粒状焼成カルシウムは筒の中心部より底部へ沈殿後、水流による回転運動を繰り返し連続して飽和溶液が生成出来る装置であり、装置本体内上部のフィルターを通過して透明な高アルカリ焼成カルシウム飽和溶液が効率よく生成できる装置。 The granular calcined calcium, which is the raw material for the highly alkaline calcined calcium saturated solution, turns the water flow from the bottom to the top to rotate the water flow into the bottom flow through the water flow control plate. As the cylinder rises upward, the rotation speed becomes faster, and the calcium saturated solution is generated at a faster speed, and the granular calcined calcium that could not be dissolved settles from the center of the cylinder to the bottom and then flows due to water flow. A device that can generate a saturated solution continuously by repeating rotational movement, and can efficiently generate a transparent highly alkaline calcined calcium saturated solution through a filter in the upper part of the device body.
本発明の第一の実施形態を示す粒状焼成カルシウム飽和溶液生成装置の概念図The conceptual diagram of the granular baking calcium saturated solution production | generation apparatus which shows 1st embodiment of this invention. 第一の実施形態の粒状焼成カルシウム飽和溶液の生成状態を示す図The figure which shows the production | generation state of the granular baking calcium saturated solution of 1st embodiment 図１のＣ−Ｃ矢視断面図CC sectional view of FIG. Ａ　は図１のＡ−Ａ矢視断面図で、ＢはＢ−Ｂ矢視断面図A is a cross-sectional view taken along the line AA in FIG. 1, and B is a cross-sectional view taken along the line BB. 本発明の第二の実施形態を示す粒状焼成カルシウム飽和溶液生成装置の概念図The conceptual diagram of the granular baking calcium saturated solution production | generation apparatus which shows 2nd embodiment of this invention. 図５のａ−ａ矢視断面図Aa arrow sectional view of FIG. 図６のｂ−ｂ矢視断面図Bb arrow sectional view of FIG.
　以下、本発明の第一の実施形態を図１~図４を参照して説明する。装置本体１は筒状本体１ａと逆円錐状底部１ｂとからなり、筒状本体１ａの上部には水溶液取出口５が設けられ、該水溶液取出口５には円筒状のフィルター４が備えられている。前記逆円錐状底部１ｂには突起物１１が前記逆円錐状底部１ｂの底部１７に設けられている。なお、底部１７には雌ネジ１６が螺刻されていて、前記突起物１１の後端側に前記雌ネジ１６に螺合する雄ネジ１８が螺刻されている。前記筒状本体１ａの下方に水導入手段としての水導入ノズル９が備えられていて、該水導入ノズル９の吐出方向は前記筒状本体１ａの円周方向を向いている。さらに、前記筒状本体１ａの略中央部に粒状焼成カルシウム投入孔１９が設けられ、該焼成カルシウム投入孔１９には焼成カルシウム投入パイプ２０が連設しており、該焼成カルシウム投入パイプ２０の先端部が焼成カルシウム投入口２となっていて、蓋２３で塞がれている。前記水溶液取出口５には水溶液取出パイプ２１が連接されており、前記焼成カルシウム投入パイプ２０には圧力計１２が備えられていて、前記水導入ノズル９には水量調整バルブ１０を備えた水導入パイプ３が連設している。また、前記逆円錐状底部１ｂの内周面には水流調整板６が２箇所に設けられている。 Hereinafter, a first embodiment of the present invention will be described with reference to FIGS. The apparatus main body 1 includes a cylindrical main body 1a and an inverted conical bottom 1b. An aqueous solution outlet 5 is provided on the upper portion of the cylindrical main body 1a, and a cylindrical filter 4 is provided in the aqueous solution outlet 5. Yes. A protrusion 11 is provided on the bottom 17 of the inverted conical bottom 1b on the inverted conical bottom 1b. A female screw 16 is screwed into the bottom portion 17, and a male screw 18 that is screwed into the female screw 16 is screwed into the rear end side of the protrusion 11. A water introduction nozzle 9 as water introduction means is provided below the cylindrical main body 1a, and the discharge direction of the water introduction nozzle 9 faces the circumferential direction of the cylindrical main body 1a. Further, a granular calcined calcium charging hole 19 is provided at a substantially central portion of the cylindrical main body 1a, and a calcined calcium charging pipe 20 is connected to the calcined calcium charging hole 19, and a tip of the calcined calcium charging pipe 20 is provided. The part is a calcined calcium inlet 2 and is closed with a lid 23. An aqueous solution take-out pipe 21 is connected to the aqueous solution take-out port 5, a pressure gauge 12 is provided in the calcined calcium input pipe 20, and a water introduction valve 10 is provided with a water amount adjusting valve 10. The pipe 3 is connected continuously. Further, two water flow adjusting plates 6 are provided on the inner peripheral surface of the inverted conical bottom 1b.
　つぎに、本発明の焼成カルシウム飽和溶液生成装置２２による焼成カルシウム飽和溶液の生成法を説明する。
　まず、装置本体１内に水を半分程度貯水した状態で、粒状焼成カルシウム投入口２の蓋２３を開けて、粒状焼成カルシウムを投入し蓋を閉め、水量調整バルブ１０を開けて装置本体１内に水導水ノズル９より水圧のある水を供給する。すると水導入ノズル９から導入された水による回転水流が発生し、同時に粒状焼成カルシウムの回転が始まり、水流調整板６の効果が加わり、粒状焼成カルシウムが溶解しながら上昇し、焼成カルシウム飽和溶液がフィルター４を通過し水溶液取出口５を経由して水溶液取出パイプ２１から放出される。未溶解の粒状焼成カルシウムは筒状本体１ａの中心部を経由して逆円錐状底部１ｂに向かって下降し、突起物１１により円周方向に分散し、導入水の回転水流と水流調整板６により粒状焼成カルシウムは再び上昇し、上昇下降を繰り返す。
　なお、フィルター４の目詰まりを防ぐには装置本体１内の溶液のうちフィルター４に接触する溶液は透明度が高いことが望ましい。
　また、フィルター４の側面に付着した未溶解の粒状焼成カルシウムも剥がれて底部へ下降する。フィルター４の目詰は圧力計１２の交換指針で把握が出来、フィルター交換蓋７を開けて交換できる装置である、そして装置本体１が透明な樹脂で構成されている場合は、粒状焼成カルシウムの残量の確認が容易である。 Below, the production | generation method of the calcination calcium saturated solution by the calcination calcium saturation solution production | generation apparatus 22 of this invention is demonstrated.
First, with about half of the water stored in the apparatus main body 1, the lid 23 of the granular calcined calcium inlet 2 is opened, the granular calcined calcium is introduced, the lid is closed, and the water amount adjustment valve 10 is opened to open the inside of the apparatus main body 1. Water with water pressure is supplied from the water guide nozzle 9. Then, a rotating water flow is generated by the water introduced from the water introduction nozzle 9, and at the same time, the rotation of the granular calcined calcium starts, the effect of the water flow adjusting plate 6 is added, the granular calcined calcium rises while dissolving, and the calcined calcium saturated solution becomes It passes through the filter 4 and is discharged from the aqueous solution take-out pipe 21 via the aqueous solution take-out port 5. Undissolved granular calcined calcium descends toward the inverted conical bottom 1b via the central portion of the cylindrical main body 1a, and is dispersed in the circumferential direction by the protrusions 11, and the rotational water flow of the introduced water and the water flow adjusting plate 6 As a result, the granular calcined calcium rises again and repeats rising and falling.
In order to prevent the filter 4 from being clogged, it is desirable that the solution in contact with the filter 4 among the solutions in the apparatus main body 1 has high transparency.
Moreover, the undissolved granular calcination calcium adhering to the side surface of the filter 4 is also peeled off and descends to the bottom. The clogging of the filter 4 can be grasped by the replacement guideline of the pressure gauge 12 and the apparatus can be replaced by opening the filter replacement lid 7. It is easy to check the remaining amount.
　装置本体の発明は焼成カルシウムの性質上、空気に触れずにカルシウム飽和溶液を製造でき不溶解の粒状焼成カルシウムが溶解装置に戻りカルシウム飽和溶液と成る装置。 The invention of the device body is a device that can produce a calcium saturated solution without touching air due to the properties of calcined calcium, and the insoluble granular calcined calcium returns to the dissolving device to become a calcium saturated solution.
　本発明は、家庭用の小型装置で円筒の外形は直径２０ｃｍ高さ６０ｃｍを採用した。
　粒状焼成カルシウム８が、焼成カルシウム飽和溶液を生成する工程を説明する、水導口より装置本体直径２０ｃｍへ約１ｌの水を入れ、図１より粒状焼成カルシウムを１００ｇ投入した３０分後水導口内径４ｍｍより毎分２ｌ、
　水圧０．３Ｍｐａの水を入れると、容器の底へ沈殿し蓄積した粒状焼成カルシウムが水と同じく円周回転運動で溶解を始め、装置本体１の上部へ回転しながら上部のフィルター４でろ過され、カルシウム飽和溶液、水溶液出口５内径６ｍｍより水溶液取出しパイプ２１ペーハー値１２，７の強アルカリ溶液が連続生成された。 The present invention employs a small household device with a cylindrical outer diameter of 20 cm and a height of 60 cm.
The granulated calcined calcium 8 explains the process of producing a calcined calcium saturated solution. About 1 liter of water is introduced into the apparatus body diameter 20 cm from the water inlet, and 100 g of granular calcined calcium is introduced from FIG. 2 l per minute from an inner diameter of 4 mm,
When water with a water pressure of 0.3 Mpa is added, the granular calcined calcium that settles and accumulates at the bottom of the container starts to dissolve in the same rotational motion as water, and is filtered by the upper filter 4 while rotating to the top of the device body 1. Then, a strong alkaline solution having a pH value of 12 and 7 of an aqueous solution take-out pipe 21 was continuously generated from a calcium saturated solution and an aqueous solution outlet 5 inner diameter of 6 mm.
　フィルター：濾過精度：１ミクロンの使用では、粒状焼成カルシウム１００ｇに対して９０ｌの無色透明なｐｈ１２．３~１２．７飽和溶液を確認。 Filter: Filtration accuracy: In the case of use of 1 micron, 90 l of a colorless transparent ph12.3 to 12.7 saturated solution is confirmed with respect to 100 g of granular calcined calcium.
　フィルター：濾過精度：１０ミクロンの使用では、粒状焼成カルシウム１００ｇに対し半透明な飽和溶液が確認され、洗浄目的で真水にて洗い流しが必要であり、スプレー式ボトルの使用では溶解してない粒状焼成カルシウムの目詰まりが起きやすい、砂場等の散布など目的にあった使用ができる。 Filter: Filtration accuracy: When using 10 microns, a translucent saturated solution is confirmed for 100 g of granular calcined calcium, and it is necessary to wash away with fresh water for cleaning purposes. Can be used for purposes such as sandbox spraying, where calcium clogging is likely to occur.
　次に、本発明の第二の実施形態を図５~図７を参照して説明する。装置本体１０１は逆円錐状本体１０１ａと筒状底部１０１ｂとからなり、逆円錐本体１０１ａの上部には水溶液取出口５及び粒状焼成カルシウム投入口１０７が設けられ、該水溶液取出口５には水溶液取出パイプ２１が備えられている。前記水溶液取出パイプ２１の下流側にはサイクロンフィルター１０２が接続されている。該サイクロンフィルター１０２の上部には焼成カルシウム溶液取出パイプ１０４が接続されている。前記焼成カルシウム溶液取出パイプ１０４には圧力計１１２が取り付けられている。前記焼成カルシウム溶液取出パイプ１０４の下流側にはフィルターハウジング１０３が接続されている。前記フィルターハウジング１０３の出口側にはｐｈ電極ハウジング１０５が接続されていて水溶液取出し口１１３から焼成カルシウム溶液が放出されるように構成されている。筒状底部１０１ｂには円錐状の突起物１１９が前記筒状底部１０１ｂの底部１７に設けられている。前記筒状底部１０１ｂの側壁に水導入手段としての高速流量ノズル１２０が図５おいて左側に３個取り付けられていて、右側に２個取り付けられていて、右側に２個は左側の高速流量ノズル１２０に対向するように取り付けられている。なお、前記高速流量ノズル１２０の吐出方向は前記筒状底部１０１ｂの円周方向を向いている。さらに、前記逆円錐状本体１０１ａの略中央部に粒状焼成カルシウム投入口１０７が設けられていて、蓋２３で塞がれている。白濁水溶液取出口１１１には白濁水溶液取出パイプ２１が連接されている。前記高速流量ノズル１２０には水量調整バルブ１１５を備えた水導入分岐パイプ１１８が連設している。なお、該水導入分岐パイプ１１８は水量調整バルブ１１５を介して水導入パイプ１０９に連接している。前記サイクロンフィルター１０２下部に不溶解カルシウム回収パイプ１２２が接続されている。該不溶解カルシウム回収パイプ１２２はカルシウムミキシングパイプ１２３に組み込まれたエジェクター１１０に接続されている。前記筒状底部１０１ｂの内側には高速流量ノズル１２０の取付位置と高速流量ノズル１２０の取付位置との間に流量調整板１０６が設けられている。なお、該流量調整板１０６は水導入方法向けて下方に傾斜した状態で設けられている。前記流量調整板１０６はパンチング板が用いられているが、必ずしもパンチング板である必要はない。 Next, a second embodiment of the present invention will be described with reference to FIGS. The apparatus main body 101 includes an inverted conical main body 101a and a cylindrical bottom 101b, and an aqueous solution outlet 5 and a granular calcined calcium inlet 107 are provided on the upper portion of the inverted conical main body 101a. A pipe 21 is provided. A cyclone filter 102 is connected to the downstream side of the aqueous solution extraction pipe 21. A calcined calcium solution extraction pipe 104 is connected to the upper part of the cyclone filter 102. A pressure gauge 112 is attached to the calcined calcium solution extraction pipe 104. A filter housing 103 is connected to the downstream side of the calcined calcium solution extraction pipe 104. A ph electrode housing 105 is connected to the outlet side of the filter housing 103 so that the calcined calcium solution is discharged from the aqueous solution outlet 113. The cylindrical bottom 101b is provided with a conical protrusion 119 on the bottom 17 of the cylindrical bottom 101b. Three high-speed flow nozzles 120 as water introduction means are attached to the left side in FIG. 5 on the side wall of the cylindrical bottom portion 101b, two on the right side, and two on the right side are two high-speed flow rate nozzles on the left side. It is attached to face 120. The discharge direction of the high-speed flow rate nozzle 120 faces the circumferential direction of the cylindrical bottom portion 101b. Further, a granular calcined calcium inlet 107 is provided at a substantially central portion of the inverted conical main body 101 a and is closed with a lid 23. The cloudy aqueous solution outlet pipe 111 is connected to the cloudy aqueous solution outlet 111. A water introduction branch pipe 118 having a water amount adjustment valve 115 is connected to the high-speed flow rate nozzle 120. The water introduction branch pipe 118 is connected to the water introduction pipe 109 via a water amount adjustment valve 115. An insoluble calcium recovery pipe 122 is connected to the lower part of the cyclone filter 102. The insoluble calcium recovery pipe 122 is connected to an ejector 110 incorporated in a calcium mixing pipe 123. A flow rate adjusting plate 106 is provided between the mounting position of the high-speed flow nozzle 120 and the mounting position of the high-speed flow nozzle 120 inside the cylindrical bottom 101b. The flow rate adjusting plate 106 is provided in a state of being inclined downward toward the water introduction method. The flow rate adjusting plate 106 is a punching plate, but is not necessarily a punching plate.
　本発明の装置は省スペースで効率よく高アルカリ焼成カルシウム飽和溶液は無色、透明な溶液が生成されるため、装置のサイズを変えることにより、一般家庭から幼稚園の砂場など学校・ホテル・食品工場・公共施設などの細菌・ウイルス・カビから汚染される食品・厨房・トイレなどに洗浄や噴霧によって環境改善の利用が可能となる。 The device of the present invention is a space-saving and efficient high-calcin calcium-saturated calcium saturated solution that produces a colorless and transparent solution. By changing the size of the device, you can change the size of the device from a general home to a kindergarten sandbox, school, hotel, food factory, The environment can be improved by washing and spraying food, kitchens, and toilets contaminated with bacteria, viruses, and mold in public facilities.
　本発明の装置は密閉容器のであり空気の接触が極めて少なく高アルカリ溶液が生成でき高アルカリの維持で必要なとき必要なだけ使える。 The device of the present invention is a sealed container, and it can generate a highly alkaline solution with very little contact with air, and can be used only when necessary to maintain a high alkali.
　本発明の応用で粒状焼成カルシウム８の容積を深くし水流調整板１１を増設する事により安定したカルシウム飽和溶液の増産生成が可能となる。 By increasing the volume of the granular calcined calcium 8 and adding the water flow adjusting plate 11 by applying the present invention, it is possible to increase production of a stable calcium saturated solution.
　有機野菜の洗浄を次亜塩素酸ナトリウム溶液で洗浄除菌すれば有機野菜と表示出来ないが焼成カルシウム溶液の洗浄除菌は表示義務違反にならない。
　次亜塩素酸ナトリウム溶液の１５０ｐｐｍと同等の除菌効果があり、大学や各研究機関の文献発表「ホタテ貝殻焼成カルシウム文献」で確認できる。
無色透明な焼成カルシウムのｐｈ１２．７のアルカリ溶液を超音波霧化器にて　噴霧することにより浮遊菌を除菌出来るため食品は減菌できる。 If organic vegetables are washed and sterilized with sodium hypochlorite solution, they cannot be labeled as organic vegetables, but cleaning and sterilization of calcined calcium solutions does not violate the labeling obligation.
There is a sterilization effect equivalent to 150 ppm of sodium hypochlorite solution, which can be confirmed in the published literature “Calculated scallop shell calcium calcium” by universities and research institutions.
Since the floating bacteria can be sterilized by spraying an alkaline solution of colorless and transparent calcined calcium ph12.7 with an ultrasonic atomizer, food can be sterilized.
１装置本体
２粒状焼成カルシウム投入
３水導入パイプ
４フィルター
５水溶液取出口
６水流調整板
７フィルター交換蓋
８粒状焼成カルシウム
９水導入ノズル
１０水量調整バルブ
１１突起物
１２圧力計
１３円筒内の飽和溶液の水流と飽和状態
１４飽和溶液上昇
１５飽和溶液生成後過溶解カルシウム粒
１６雌ネジ
１７底部
１８雄ネジ
１９粒状焼成カルシウム投入孔
２０粒状焼成カルシウム投入パイプ
２１水溶液取出パイプ
２２粒状焼成カルシウム飽和溶液生成装置
２３蓋
２４雌ネジ
２５雄ネジ
２６回転水流
１０１装置本体
１０２サイクロンフィルター
１０３フィルターハウジング
１０４焼成カルシウム溶液取出パイプ
１０５ｐｈ電極ハウジング
１０６水流調整板
１０７粒状焼成カルシウム投入口
１０８ＰＨ電極
１０９水導入パイプ
１１０エジェクター
１１１白濁水溶液取出口
１１２圧力計
１１３水溶液取出口
１１４粒状カルシウム溶剤確認窓
１１５水量調整バルブ
１１６突起物
１１７粒状カルシウム溶解タンク返却パイプ
１１８水導入分岐パイプ
１１９円錐状突起物
１２０高速流量ノズル
１２１エアーベント
１２２不溶解カルシウム回収パイプ
１２３カルシウムミキシングパイプ 1 apparatus main body 2 granular calcined calcium input 3 water introduction pipe 4 filter 5 aqueous solution outlet 6 water flow adjusting plate 7 filter replacement lid 8 granular calcined calcium 9 water introduction nozzle 10 water amount adjustment valve 11 protrusion 12 pressure gauge 13 saturated solution in cylinder Water flow and saturation state 14 Saturated solution rise 15 Saturated solution after generation Over-dissolved calcium grains 16 Female thread 17 Bottom 18 Male thread 19 Granular calcined calcium inlet 20 Granular calcium input pipe 21 Aqueous solution extraction pipe 22 Granular calcined calcium saturated solution generator 23 Lid 24 Female Thread 25 Male Thread 26 Rotating Water Flow 101 Device Body 102 Cyclone Filter 103 Filter Housing 104 Calcium Calcium Solution Extraction Pipe 105ph Electrode Housing 106 Water Flow Adjusting Plate 107 Granular Calcium Calcium Input 108 PH Electrode 109 Water Introducing Pipe 110 Ejector 111 White cloudy aqueous solution outlet 112 Pressure gauge 113 Aqueous solution outlet 114 Granular calcium solvent confirmation window 115 Water amount adjustment valve 116 Protrusion 117 Granular calcium dissolution tank return pipe 118 Water introduction branch pipe 119 Conical protrusion 120 High speed flow nozzle 121 Air vent 122 Insoluble calcium recovery pipe 123 calcium mixing pipe

Claims (2)

  1. 　円筒状本体と逆円錐台状底部とからなる装置本体の上方に粒状焼成カルシウム投入口を備え、下方に水導入手段が前記装置本体の円周方向に水を導入するように備えられるとともに前記逆円錐台状底部の底には突起物が設けられ、前記円筒状本体の上部にはフィルターを備えた水溶液取出口が設けられたことを特徴とする焼成カルシウム飽和溶液生成装置。 A granular calcined calcium inlet is provided above the apparatus main body composed of a cylindrical main body and an inverted frustoconical bottom, and a water introduction means is provided below to introduce water in the circumferential direction of the apparatus main body and the reverse A calcined calcium saturated solution generating apparatus, characterized in that a protrusion is provided on the bottom of the truncated cone-shaped bottom part, and an aqueous solution outlet provided with a filter is provided on the upper part of the cylindrical main body.
  2. 　円筒状本体と逆円錐台状底部とからなる装置本体の上方に粒状焼成カルシウム投入口を備え、下方に水導入手段が前記装置本体の円周方向に水を導入するように備えられるとともに前記逆円錐台状底部の底には突起物が設けられ、前記円筒状本体の上部には水溶液取出口が設けられ、該水溶液取出し口の下流側にフィルターハウジングが設けられたことを特徴とする焼成カルシウム飽和溶液生成装置。 A granular calcined calcium inlet is provided above the apparatus main body composed of a cylindrical main body and an inverted frustoconical bottom, and a water introduction means is provided below to introduce water in the circumferential direction of the apparatus main body and the reverse A calcined calcium characterized in that a projection is provided at the bottom of the truncated cone-shaped bottom, an aqueous solution outlet is provided at the top of the cylindrical body, and a filter housing is provided downstream of the aqueous solution outlet. Saturated solution generator.
PCT/JP2017/018757 2016-05-06 2017-05-08 Device for generating saturated solution of calcined calcium WO2017191851A1 (en)

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JP2016-257902 2016-12-15
JP2016257902A JP6354113B2 (en) 2016-05-06 2016-12-15 Sintered calcium saturated solution generator

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10328542A (en) * 1997-06-03 1998-12-15 Nippon Steel Corp Method for dissolving quick line and device therefor
WO2004076042A1 (en) * 2003-02-28 2004-09-10 Okutama Kogyo Co., Ltd. Mixing device and slurrying device
JP2010270082A (en) * 2009-05-25 2010-12-02 Natural Japan Co Ltd Production ejection method of alkaline calcium aqueous solution
JP3199107U (en) * 2015-05-26 2015-08-06 日本富升環保開発 有限会社 Solution preparation equipment
JP3199108U (en) * 2015-05-26 2015-08-06 日本富升環保開発 有限会社 Solution preparation equipment

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10328542A (en) * 1997-06-03 1998-12-15 Nippon Steel Corp Method for dissolving quick line and device therefor
WO2004076042A1 (en) * 2003-02-28 2004-09-10 Okutama Kogyo Co., Ltd. Mixing device and slurrying device
JP2010270082A (en) * 2009-05-25 2010-12-02 Natural Japan Co Ltd Production ejection method of alkaline calcium aqueous solution
JP3199107U (en) * 2015-05-26 2015-08-06 日本富升環保開発 有限会社 Solution preparation equipment
JP3199108U (en) * 2015-05-26 2015-08-06 日本富升環保開発 有限会社 Solution preparation equipment

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