WO2017167610A1 - Vaporizing assembly comprising a viewable heating element and liquid delivery device for an aerosol generating system - Google Patents

Vaporizing assembly comprising a viewable heating element and liquid delivery device for an aerosol generating system Download PDF

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Publication number
WO2017167610A1
WO2017167610A1 PCT/EP2017/056741 EP2017056741W WO2017167610A1 WO 2017167610 A1 WO2017167610 A1 WO 2017167610A1 EP 2017056741 W EP2017056741 W EP 2017056741W WO 2017167610 A1 WO2017167610 A1 WO 2017167610A1
Authority
WO
WIPO (PCT)
Prior art keywords
aerosol
forming substrate
substrate
liquid aerosol
heater assembly
Prior art date
Application number
PCT/EP2017/056741
Other languages
French (fr)
Inventor
Laurent Manca
Rui Nuno BATISTA
Original Assignee
Philip Morris Products S.A.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Philip Morris Products S.A. filed Critical Philip Morris Products S.A.
Priority to CA3013263A priority Critical patent/CA3013263A1/en
Priority to JP2018550538A priority patent/JP6937777B2/en
Priority to CN201780018081.XA priority patent/CN109068732B/en
Priority to MX2018011461A priority patent/MX2018011461A/en
Priority to RU2018138197A priority patent/RU2735575C2/en
Priority to KR1020187030018A priority patent/KR102433532B1/en
Priority to EP17710996.4A priority patent/EP3435796B1/en
Priority to US15/475,297 priority patent/US10098387B2/en
Publication of WO2017167610A1 publication Critical patent/WO2017167610A1/en
Priority to IL261508A priority patent/IL261508A/en
Priority to US16/160,160 priority patent/US10506833B2/en
Priority to US16/692,540 priority patent/US10952475B2/en
Priority to US17/181,120 priority patent/US11317475B2/en
Priority to US17/722,599 priority patent/US11771854B2/en
Priority to US18/469,738 priority patent/US20240001057A1/en

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Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40—Constructional details, e.g. connection of cartridges and battery parts
    • A24F40/46—Shape or structure of electric heating means
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F47/00—Smokers' requisites not otherwise provided for
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/10—Devices using liquid inhalable precursors
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40—Constructional details, e.g. connection of cartridges and battery parts
    • A24F40/48—Fluid transfer means, e.g. pumps
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/60—Devices with integrated user interfaces
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61M—DEVICES FOR INTRODUCING MEDIA INTO, OR ONTO, THE BODY; DEVICES FOR TRANSDUCING BODY MEDIA OR FOR TAKING MEDIA FROM THE BODY; DEVICES FOR PRODUCING OR ENDING SLEEP OR STUPOR
    • A61M11/00—Sprayers or atomisers specially adapted for therapeutic purposes
    • A61M11/006—Sprayers or atomisers specially adapted for therapeutic purposes operated by applying mechanical pressure to the liquid to be sprayed or atomised
    • A61M11/008—Sprayers or atomisers specially adapted for therapeutic purposes operated by applying mechanical pressure to the liquid to be sprayed or atomised by squeezing, e.g. using a flexible bottle or a bulb
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61M—DEVICES FOR INTRODUCING MEDIA INTO, OR ONTO, THE BODY; DEVICES FOR TRANSDUCING BODY MEDIA OR FOR TAKING MEDIA FROM THE BODY; DEVICES FOR PRODUCING OR ENDING SLEEP OR STUPOR
    • A61M11/00—Sprayers or atomisers specially adapted for therapeutic purposes
    • A61M11/04—Sprayers or atomisers specially adapted for therapeutic purposes operated by the vapour pressure of the liquid to be sprayed or atomised
    • A61M11/041—Sprayers or atomisers specially adapted for therapeutic purposes operated by the vapour pressure of the liquid to be sprayed or atomised using heaters
    • A61M11/042—Sprayers or atomisers specially adapted for therapeutic purposes operated by the vapour pressure of the liquid to be sprayed or atomised using heaters electrical
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61M—DEVICES FOR INTRODUCING MEDIA INTO, OR ONTO, THE BODY; DEVICES FOR TRANSDUCING BODY MEDIA OR FOR TAKING MEDIA FROM THE BODY; DEVICES FOR PRODUCING OR ENDING SLEEP OR STUPOR
    • A61M15/00—Inhalators
    • A61M15/0065—Inhalators with dosage or measuring devices
    • A61M15/0066—Inhalators with dosage or measuring devices with means for varying the dose size
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61M—DEVICES FOR INTRODUCING MEDIA INTO, OR ONTO, THE BODY; DEVICES FOR TRANSDUCING BODY MEDIA OR FOR TAKING MEDIA FROM THE BODY; DEVICES FOR PRODUCING OR ENDING SLEEP OR STUPOR
    • A61M15/00—Inhalators
    • A61M15/06—Inhaling appliances shaped like cigars, cigarettes or pipes
    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B1/00—Details of electric heating devices
    • H05B1/02—Automatic switching arrangements specially adapted to apparatus ; Control of heating devices
    • H05B1/0227—Applications
    • H05B1/023—Industrial applications
    • H05B1/0244—Heating of fluids
    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B3/00—Ohmic-resistance heating
    • H05B3/20—Heating elements having extended surface area substantially in a two-dimensional plane, e.g. plate-heater
    • H05B3/22—Heating elements having extended surface area substantially in a two-dimensional plane, e.g. plate-heater non-flexible
    • H05B3/26—Heating elements having extended surface area substantially in a two-dimensional plane, e.g. plate-heater non-flexible heating conductor mounted on insulating base
    • H05B3/265—Heating elements having extended surface area substantially in a two-dimensional plane, e.g. plate-heater non-flexible heating conductor mounted on insulating base the insulating base being an inorganic material, e.g. ceramic
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61M—DEVICES FOR INTRODUCING MEDIA INTO, OR ONTO, THE BODY; DEVICES FOR TRANSDUCING BODY MEDIA OR FOR TAKING MEDIA FROM THE BODY; DEVICES FOR PRODUCING OR ENDING SLEEP OR STUPOR
    • A61M15/00—Inhalators
    • A61M15/0001—Details of inhalators; Constructional features thereof
    • A61M15/0013—Details of inhalators; Constructional features thereof with inhalation check valves
    • A61M15/0015—Details of inhalators; Constructional features thereof with inhalation check valves located upstream of the dispenser, i.e. not traversed by the product
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61M—DEVICES FOR INTRODUCING MEDIA INTO, OR ONTO, THE BODY; DEVICES FOR TRANSDUCING BODY MEDIA OR FOR TAKING MEDIA FROM THE BODY; DEVICES FOR PRODUCING OR ENDING SLEEP OR STUPOR
    • A61M2205/00—General characteristics of the apparatus
    • A61M2205/02—General characteristics of the apparatus characterised by a particular materials
    • A61M2205/0238—General characteristics of the apparatus characterised by a particular materials the material being a coating or protective layer
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61M—DEVICES FOR INTRODUCING MEDIA INTO, OR ONTO, THE BODY; DEVICES FOR TRANSDUCING BODY MEDIA OR FOR TAKING MEDIA FROM THE BODY; DEVICES FOR PRODUCING OR ENDING SLEEP OR STUPOR
    • A61M2205/00—General characteristics of the apparatus
    • A61M2205/12—General characteristics of the apparatus with interchangeable cassettes forming partially or totally the fluid circuit
    • A61M2205/123—General characteristics of the apparatus with interchangeable cassettes forming partially or totally the fluid circuit with incorporated reservoirs
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61M—DEVICES FOR INTRODUCING MEDIA INTO, OR ONTO, THE BODY; DEVICES FOR TRANSDUCING BODY MEDIA OR FOR TAKING MEDIA FROM THE BODY; DEVICES FOR PRODUCING OR ENDING SLEEP OR STUPOR
    • A61M2205/00—General characteristics of the apparatus
    • A61M2205/12—General characteristics of the apparatus with interchangeable cassettes forming partially or totally the fluid circuit
    • A61M2205/128—General characteristics of the apparatus with interchangeable cassettes forming partially or totally the fluid circuit with incorporated valves
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61M—DEVICES FOR INTRODUCING MEDIA INTO, OR ONTO, THE BODY; DEVICES FOR TRANSDUCING BODY MEDIA OR FOR TAKING MEDIA FROM THE BODY; DEVICES FOR PRODUCING OR ENDING SLEEP OR STUPOR
    • A61M2205/00—General characteristics of the apparatus
    • A61M2205/36—General characteristics of the apparatus related to heating or cooling
    • A61M2205/3653—General characteristics of the apparatus related to heating or cooling by Joule effect, i.e. electric resistance
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61M—DEVICES FOR INTRODUCING MEDIA INTO, OR ONTO, THE BODY; DEVICES FOR TRANSDUCING BODY MEDIA OR FOR TAKING MEDIA FROM THE BODY; DEVICES FOR PRODUCING OR ENDING SLEEP OR STUPOR
    • A61M2205/00—General characteristics of the apparatus
    • A61M2205/58—Means for facilitating use, e.g. by people with impaired vision
    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B2203/00—Aspects relating to Ohmic resistive heating covered by group H05B3/00
    • H05B2203/013—Heaters using resistive films or coatings
    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B2203/00—Aspects relating to Ohmic resistive heating covered by group H05B3/00
    • H05B2203/021—Heaters specially adapted for heating liquids

Definitions

  • the present invention relates to a vaporizing assembly for an aerosol-generating system, such as a handheld electrically operated aerosol-generating system.
  • Handheld electrically operated aerosol-generating systems consist of a device portion comprising a battery and control electronics, a cartridge portion comprising a supply of aerosol-forming substrate held in a liquid storage portion, and an electrically operated vaporiser.
  • the vaporiser typically comprises a coil of heater wire wound around an elongate wick soaked in the liquid aerosol-forming substrate held in the liquid storage portion.
  • the cartridge portion typically comprises not only the supply of aerosol-forming substrate and an electrically operated vaporiser, but also a mouthpiece, from which the user inhales aerosol.
  • the liquid aerosol-generating medium may not always be completely volatilized. Residues may be created upon transport and heating of the liquid aerosol-forming substrate. Such residues may affect aerosol creation. In particular, residues may impair repeatability of aerosol creation. In order to increase customer satisfaction, it is desirable to offer customers the opportunity to visually inspect cleanliness of functional components of the vaporiser used in aerosol-generating systems.
  • a vaporizing assembly for an aerosol generating system comprising a liquid aerosol-forming substrate delivery device for delivering liquid aerosol-forming substrate, and a heater assembly.
  • the heater assembly comprises a heat resistive substrate and an electric heater element.
  • the liquid aerosol-forming substrate delivery device delivers liquid aerosol-forming substrate to at least a surface of the heater assembly, wherein the heating element is isolated from the liquid aerosol-forming substrate during normal use.
  • the heat resistive substrate of the heater assembly may be transparent or semi- transparent.
  • the heat resistive substrate of the heater assembly may be made from glass, heat resistive glass, ceramics, silicon, semiconductors, metals or metal alloys.
  • the heat resistive substrate may be produced from pure glass or a glass compound, as well as glass with specific crystal orientation to enable optimized thermal transfer effects.
  • the heater assembly may be formed from transparent or semi-transparent materials, the user may easily see and assess the need to clean the surface of the heat resistive substrate. In order to clean the surface, the heater assembly may be rinsed with water or a suitable cleaning liquid.
  • the heat resistive substrate may be substantially flat and may have any desired shape.
  • the heat resistive substrate may have a rectangular, polygonal, circular or oval shape with for example width and length dimensions of between 3 to 10 millimeters.
  • the thickness of the heat resistive substrate may range between 0.2 and 2.5 millimeters.
  • the heat resistive substrate may be have a rectangular shape with a size of about 7 x 6 millimeters or 5 x 5 millimeters (L x W), and a thickness of about 1 to 1.5 millimeters.
  • substantially flat means an arrangement that is in the form of a substantially two dimensional object.
  • the substantially flat heat resistive substrate extends in two dimensions substantially more than in a third dimension.
  • the dimensions of the substantially flat heat resistive substrate in each of the two dimensions is at least 5 times larger than in the third dimension.
  • the two dimensions may define a surface of the heat resistive substrate and third dimension may define a thickness of the heat resistive substrate, normal to the surface.
  • An example of a substantially flat heat resistive substrate is an object between two imaginary and substantially parallel planar surfaces, wherein the distance between the two imaginary surfaces is substantially smaller than the extent of the object parallel to the surfaces.
  • the extent of the object in two orthogonal directions parallel to the surfaces may be at least five times greater than the distance (or thickness) between the two parallel surfaces.
  • the substantially flat heat resistive substrate is planar and the distance between the parallel planar surfaces would be the thickness of the material used for forming the heater.
  • the substantially flat heat resistive substrate is curved along one or more dimensions, for example forming a dome shape or bridge shape.
  • the heating element may be transparent but may also include partially transparent or not transparent materials.
  • the heating element may comprise metallic layers or elements in at least one of the surfaces of the heat resistive substrate for the purpose of creating a resistive element.
  • contact pads for electrical conductivity and connection with other parts of the device may be provided, which are not transparent.
  • the non-transparent parts are used only in such extent that the user may still be able to see and assess the need to clean the surface of the heat resistive substrate.
  • the heating element is isolated from the liquid aerosol-forming substrate during normal use.
  • isolated from the liquid aerosol-forming substrate as used throughout this application is to be understood in the sense that the heating element is provided such that it does not come into direct contact with the liquid aerosol-forming substrate during normal use.
  • the heating element may be provided within the volume of the heat resistive substrate, may be sandwiched between two elements of the heat resistive substrate or may be covered with a protective layer of heat resistive material. With such configuration, contact between the heating element and the liquid aerosol-forming substrate may be completely avoided.
  • isolated from the liquid aerosol-forming substrate is also to be construed in a way that it encompasses embodiments in which the heating element is provided on a surface of the heat resistive substrate onto which the liquid aerosol-forming substrate is not directly delivered.
  • the liquid aerosol-forming substrate may be delivered to a front side of the heat resistive substrate and the heating element may be provided on a backside of the heat resistive substrate.
  • the heating element may be provided as a thin film coating provided to the surface of the heat resistive substrate.
  • the heating element can be impregnated, deposited or printed on the surface of the heat resistive substrate.
  • the material of the thin film heating element can be any suitable material which has convenient electrical properties and a sufficiently high adherence to the heat resistive substrate.
  • the thin film coating of the heating element may extend substantially over the complete surface of the heat resistive substrate.
  • the geometrical shape of the heating element may vary, being any adequate shape to produce the intended electrical resistance and the intended heating capabilities.
  • the heating element assembly may be localized in such configuration in the vaporizing assembly that one of the large surfaces of the heat resistive substrate, also referred to as the front side surface, faces towards the delivery device.
  • the liquid aerosol-forming substrate is substantially dispensed only onto the front side surface of the heat resistive substrate.
  • the heating element is provided to the large surface of the heat resistive substrate which points away from the delivery device. This surface is also referred to as the backside of the heat resistive substrate. The backside does not come into direct contact with the liquid aerosol-forming substrate.
  • the heating element is configured such that the front side of the heat resistive substrate is heated to temperatures of about between 120 degrees Celsius and 250 degrees Celsius.
  • the actual temperature of the heater assembly may be adjusted or chosen for example depending on the type of liquid aerosol-forming substrate that is used.
  • the heating element may be embedded in the heat resistive substrate.
  • embedded as used throughout this application is to be understood in the sense that the heating element is provided within the volume of the heat resistive substrate, is sandwiched between two elements of the heat resistive substrate or is sandwiched between one of the surfaces of the heat resistive substrate and an additional cover layer.
  • the cover layer may be a specific coating of glass or mainly polymeric transparent material with good resistance to temperatures up to the operating temperature of the heating element.
  • the heating element may comprise a metallic wire which is embedded in a heat resistive substrate of glass or any other suitable material.
  • the heat resistive substrate of the heater assembly may be made from a material having low adhesion or anti-adhesion properties with respect to the liquid aerosol-forming substrate. This can reduce the probability of accumulation of residues on the surface of the heater element. Moreover, the heating element may be easier to clean by the consumer.
  • the surface of the heat resistive substrate of the heater assembly may be non-porous. Non-porous means that the surface of the heat resistive substrate does not allow liquid or air to pass through it.
  • the heater assembly may additionally comprise further sensors or components for specific additional purposes.
  • additional sensors may include real-time chemical sensors and temperature sensors. With these sensors, the chemical composition and the temperature on the surface of the heater assembly can be monitored in a fast and geometrically precise way.
  • the heater assembly element may be an all-in-one built-in component such as a semiconductor component, a microchip component or a set of those components, manufactured using semiconductor technologies as a single component comprising nano- sized integrated structures.
  • Such heater assemblies may be more easily connected and disconnected from the man body of the device, and are therefore desirable as replacement parts. However, depending on the material used, specific cleaning procedures may apply.
  • the liquid aerosol-forming substrate preferably only comes into contact with the front side surface of the heat resistive substrate.
  • the liquid aerosol-forming substrate delivery device is connectable to a liquid storage portion and is configured to convey the liquid aerosol-forming substrate onto the heater assembly.
  • the liquid aerosol-forming substrate delivery device may comprise an outlet end for discharging the liquid aerosol-forming substrate onto the heater assembly.
  • the outlet end of the delivery device may be spaced apart from the heater assembly.
  • the distance between the outlet end of the delivery device and the heater assembly may be between 0.1 and 10 millimeters, may be between 0.5 and 5 millimeters and may further be between 0.7 and 2.5 millimeters.
  • Embodiments in which the heater assembly spaced apart from delivery device may offer additional advantages. Reflux of liquid aerosol-forming substrate from the heating element to the delivery device is efficiently prevented. Moreover, as the heating element is mechanically decoupled from the delivery device, handling of the vaporizing assembly, in particular disassembly for replacement purposes or cleaning is facilitated.
  • the heater assembly may be releasably connected to the liquid aerosol-forming substrate delivery device. Releasably connected in this context means that the heater assembly may be disconnected from the liquid aerosol-forming substrate delivery device and reconnected to liquid aerosol- forming substrate delivery device without damaging either the heater assembly or liquid aerosol-forming substrate delivery device.
  • the delivery device may further comprise a pump for delivering the liquid aerosol- forming substrate onto the heater assembly.
  • the pump may be a hand operated, manual pump, an electromechanical pump or a conventional micropump.
  • Micropumps may allow on-demand delivery of liquid aerosol-forming substrate at a low flow rate of for example approximately 0.5 to 4.5 microliters per second for intervals of variable or constant duration.
  • the pump may be carefully tuned in order to deliver the appropriate amount of liquid aerosol-forming substrate to the heating element. Consequently, the amount of deposited liquid aerosol-forming substrate can be determined from the amount of pump cycles.
  • the pumped volume of one complete cycle of a micropump typically is about 0.50 microliters per second.
  • Such micropumps typically are operated at a pump frequency of between 5 to 20 hertz.
  • the pump may be configured to pump liquid aerosol-forming substrates that are characterized by a relatively high viscosity as compared to water.
  • the viscosity of a liquid aerosol-forming substrate may be in the range from about 10 to 500 millipascal seconds, preferably in the range from about 17 to 86 millipascal seconds.
  • the liquid aerosol-forming delivery device may further be configured to deliver a metered amount of liquid aerosol-forming substrate onto the heater assembly.
  • the estimated maximum amount of liquid to be pumped as a dose for a puff is a small volume, as a pumping pulse liquid volume from 0.010 to 0.060 microliters, preferably of around 0.0125 microliters.
  • a nozzle may be provided via which the liquid aerosol-forming substrate may be sprayed onto the heater assembly for volatilization and aerosol creation.
  • the nozzle converts the flow of the liquid aerosol-forming substrate into a plurality of small droplets.
  • the spray pattern of the droplets may be adapted to the shape of the heater assembly.
  • the delivery device may comprise a classic type atomizer spray nozzle, in which case a flow of air is supplied through the nozzle by the action of puffing from the user, creating a pressurized air flow that will mix and act with the liquid creating an atomized spray in the outlet of the nozzle.
  • a classic type atomizer spray nozzle in which case a flow of air is supplied through the nozzle by the action of puffing from the user, creating a pressurized air flow that will mix and act with the liquid creating an atomized spray in the outlet of the nozzle.
  • nozzles that work with small volumes of liquid, in sizes that meet the requirements to fit in small portable devices.
  • Another class of nozzle that may be used is an airless spray nozzle, sometimes referred to as a micro-spray nozzle. Such nozzles create micro spray cones in very small sizes.
  • the airflow management inside the device namely inside the mouth piece, surrounds the nozzle and the heater assembly, flushing the heater assembly surface towards the outlet of the mouthpiece, preferably including a turbulent air flow pattern of the aerosol exiting the mouthpiece.
  • the distance of the air gap between the delivery device and the surface of the heat resistive substrate facing the nozzle is preferably within a range from 2 to 10 millimeters, more preferably from 3 to 7 millimeters. Any type of available spraying nozzles may be used. Airless nozzle 062 Minstac from manufacturer "The Lee Company" is an example of a suitable spray nozzle.
  • the vaporizing assembly may have a longitudinal axis.
  • the delivery device may deliver or spray liquid aerosol-forming substrate along the longitudinal axis.
  • the heat resistive substrate may have a surface that receives the liquid aerosol-forming substrate and the surface may be oblique to the longitudinal axis of the vaporizing assembly.
  • the surface of at least a central portion of the heater assembly that receives liquid aerosol-forming substrate from the delivery device delivered along the longitudinal axis may be oblique to the longitudinal axis of the vaporizing assembly.
  • a coupling unit may be provided in order to connect the delivery device to a liquid storage portion.
  • the coupling unit may include a "luer" type connection. However, any type of leakage free connection system may be used.
  • an aerosol- generating system comprising a vaporizing assembly as disclosed above and a housing in which the vaporizing assembly is located. At least a part of the housing in which the heater assembly of the vaporizing assembly is located, is made from transparent material, such that the heater assembly can be visually inspected by the consumer.
  • the housing of the aerosol-generating system may comprise a mouthpiece through which the consumer may inhale the generated aerosol.
  • the mouthpiece maybe detachably connected to the housing.
  • the heater assembly of the vaporizing assembly may be located in the mouthpiece. At least a portion of the mouthpiece may be transparent, such that the heater assembly can be visually inspected by the consumer.
  • the transparent portion of the housing or the mouthpiece may be made from for example thermal resistant glass, shock resistant glass, polymeric materials, hybrid compounds, carbon compounds, graphite, polysulfone (PSU), polyethersulfone (PES) or polyphenylsulfone (PPSU).
  • thermal resistant glass shock resistant glass
  • polymeric materials hybrid compounds
  • carbon compounds graphite
  • PSU polysulfone
  • PES polyethersulfone
  • PPSU polyphenylsulfone
  • the mouthpiece and the heater assembly may be integrally formed as a single part.
  • the mouthpiece and the heater assembly may be provided as a replaceable part, which can be changed after use.
  • the consumer can visually inspect the heater assembly of the aerosol-generating system. When undesired contaminations are detected, the consumer may disassemble the aerosol-generating system and clean the heater assembly.
  • the design of the vaporizing assembly of the present invention allows the user to easily clean the heating element for example by rinsing it with water.
  • the aerosol-generating system may further comprise a device portion including a power supply and a control unit.
  • the aerosol-generating system may further comprise a replaceable liquid storage portion. When assembled, the liquid storage portion is in fluid connection with the liquid aerosol-forming substrate delivery device.
  • the mouthpiece may be detachable from the device portion and the liquid storage portion.
  • the liquid storage portion may comprise pressurized liquid.
  • the liquid may be stored in the liquid storage portion in a collapsible balloon.
  • a one way valve may be temporarily opened to allow liquid flow out of the liquid storage portion.
  • the liquid storage portion may have a flexible or movable wall.
  • the liquid aerosol-forming substrate may be forced out of the liquid storage portion.
  • the liquid aerosol-forming substrate from the liquid storage portion may then be delivered by the delivery device to the heater assembly.
  • Additional one-way valves may be provided in the delivery device wherever it is desired to avoid reflux of the liquid aerosol-forming substrate.
  • commercially available one-way valves with adequate size and liquid flows may be used, including mini and micro flutter valves, duckbill valves, check valves.
  • the valves may be made of materials resistant to aggressive chemicals or FDA certified materials, which may be used for food industry and medical applications.
  • the aerosol-generating system may further comprise a control unit connected to the vaporiser and to an electrical power source.
  • the control unit may be used to set the temperature and the heating duration of the heating element.
  • the control unit may also be used to activate the pump in order to deliver the liquid aerosol-generating substrate onto the heater assembly.
  • the control unit may be in communication with an air flow sensor, which allows the control unit to detect when a user draws a puff.
  • the control unit may comprise a microprocessor, which may be a programmable microprocessor.
  • the control unit may comprise further electronic components.
  • the control unit may be configured to regulate a supply of power to the vaporizing assembly. Power may be supplied to the vaporizing assembly continuously following activation of the system or may be supplied intermittently, such as on a puff-by-puff basis. The power may be supplied to the vaporizing assembly in the form of pulses of electrical current.
  • the power supply provides the required electric energy to the electric components of the aerosol-generating system.
  • the power supply may be in form of a charge storage device such as a capacitor.
  • the power supply may require recharging and may have a capacity that allows for the storage of enough energy for one or more user experiences; for example, the power supply may have sufficient capacity to allow for the continuous generation of aerosol for a period of around six minutes or for a period that is a multiple of six minutes. In another example, the power supply may have sufficient capacity to allow for a predetermined number of puffs or discrete activations of the heater assembly.
  • a wall of the housing of the aerosol-generating system is provided with at least one semi-open inlet.
  • the semi-open inlet preferably allows air to enter the aerosol-generating system, but no air or liquid to leave the aerosol-generating system through the semi-open inlet.
  • a semi-open inlet may for example be a semi-permeable membrane, permeable in one direction only for air, but is air- and liquid-tight in the opposite direction.
  • a semi-open inlet may for example also be a one-way valve.
  • the semi-open inlets allow air to pass through the inlet only if specific conditions are met, for example a minimum depression in the aerosol-generating system or a volume of air passing through the valve or membrane.
  • the liquid aerosol-forming substrate is a substrate capable of releasing volatile compounds that can form an aerosol.
  • the volatile compounds may be released by heating the liquid aerosol-forming substrate.
  • the liquid aerosol-forming substrate may comprise plant- based material.
  • the liquid aerosol-forming substrate may comprise tobacco.
  • the liquid aerosol-forming substrate may comprise a tobacco-containing material containing volatile tobacco flavour compounds, which are released from the liquid aerosol-forming substrate upon heating.
  • the liquid aerosol-forming substrate may alternatively comprise a non-tobacco- containing material.
  • the liquid aerosol-forming substrate may comprise homogenised plant- based material.
  • the liquid aerosol-forming substrate may comprise homogenised tobacco material.
  • the liquid aerosol-forming substrate may comprise at least one aerosol-former.
  • the liquid aerosol-forming substrate may comprise other additives and ingredients, such as flavourants.
  • the aerosol-generating system may be an electrically operated aerosol-generating system.
  • the aerosol-generating system is portable.
  • the aerosol-generating system may have a size comparable to a conventional cigar or cigarette.
  • the aerosol-generating system may have a total length between approximately 30 millimeters and approximately 150 millimeters.
  • the aerosol-generating system may have an external diameter between approximately 5 millimeters and approximately 30 millimeters.
  • the aerosol-generating system may be elongate and have a longitudinal axis.
  • An outlet may be provided in the mouthpiece at one end of the longitudinal axis.
  • the surface of the heat resistive substrate may be oblique to the longitudinal axis of the aerosol-generating system. This may improve the transport of vapour and liquid from the heater assembly to the outlet.
  • the surface of at least a central portion of the heater assembly may be oblique to the longitudinal axis of the aerosol- generating system.
  • a method for generating aerosol comprising the steps of storing liquid aerosol-forming substrate in a liquid storage portion, providing a heater assembly comprising a heat resistive substrate and an electric heating element, delivering liquid aerosol-forming substrate from the liquid storage portion to the heater assembly via a delivery device, and volatilizing at least a part of the delivered liquid aerosol-forming substrate by activating the heating element of the heater assembly.
  • the heating element is isolated from the liquid aerosol-forming substrate. The heating element therefore does not directly contact the liquid aerosol-forming substrate in normal use.
  • Direct contact between the liquid aerosol-forming substrate and the heating element may be preferably avoided by embedding the heating element in the heat resistive substrate of the heater assembly or by providing the heating element on a surface of the heat resistive substrate which does not come into contact with the liquid aerosol-forming substrate.
  • the method may further comprise the step of providing a housing in which the heater assembly is located, wherein at least the part of the housing in which the heater assembly is located, is made from transparent material, such that the heater assembly can be visually inspected from outside. This allows the consumer to verify whether contaminations or residues have formed on the heater assembly. In case such undesired contaminations have indeed formed, the consumer can take the necessary steps to remove these contaminations.
  • the mouthpiece including the heater assembly is configured to be cleanable, for example rinseable with water.
  • the delivery of the liquid aerosol-forming substrate and the heating element may be triggered by a puff detection system.
  • these elements may be triggered by pressing an on-off button, held for the duration of a puff.
  • the delivery of the liquid aerosol-forming substrate may be delayed to the activation of the heating element.
  • the heating element is pre-heated to a desired operation temperature, before the liquid aerosol-forming substrate is delivered onto the heater assembly.
  • Fig. 1 is an exploded view of an embodiment of an aerosol-generating system
  • Fig. 2 shows the fully assembled aerosol-generating system of Fig. 1 ;
  • Fig. 3 shows an enlarged view of the heater assembly.
  • Fig. 1 shows the components of an aerosol-generating system of the present invention in an exploded view.
  • the aerosol-generating system 10 comprises a device portion 12a, including a housing 14, a power source 16 and a control unit 18.
  • the aerosol-generating system 10 further comprises a vaporizer assembly 12b, including a housing 20, an exchangeable liquid storage portion 22, a delivery device 30, and a heater assembly 40.
  • a transparent mouthpiece 50 portion can be detachably connected to the housing 20 of the vaporizer assembly 12b.
  • the device portion 12a and the vaporizer assembly 12b are connected via any suitable coupling unit, which provides mechanical and electrical connection between the device portion 12a and the vaporizer assembly 12b.
  • the liquid storage portion 22 is connected to the aerosol-forming substrate delivery device 30 via a coupling unit 24.
  • the coupling unit is a "luer" type coupling unit.
  • the liquid storage portion 20 can easily be replaced by the user, by separating the vaporizer assembly 12b from the device portion 12a and removing the liquid storage portion 22 from the open distal end of the vaporizer assembly 12b.
  • the liquid aerosol-forming substrate delivery device 30 is configured to transport the liquid aerosol-forming substrate from the liquid storage portion 22 to the heater assembly 40.
  • the liquid aerosol-forming substrate delivery device 30 comprises a tubing 32 and micropump 34 which are in fluid connection with the liquid storage portion 22.
  • Micropump 34 is configured to pump the liquid aerosol-forming substrate onto the heater assembly 40.
  • Spray nozzle 36 is configured to dispense the liquid aerosol-forming substrate onto the heater assembly 40 in a predetermined spray pattern.
  • nozzle 36 is a conventional airless nozzle, providing a cone like spray pattern. The spray pattern is adapted to the size of the surface of the heater assembly 40.
  • the heater assembly 40 comprises a substantially rectangular substrate 42 made from thermo-resistive glass.
  • the substrate 42 has a size of 5 x 5 square millimetres and a thickness of 1 millimeter.
  • the substrate 42 is mounted on support posts 44, which in turn are fixed to the housing 20 of the vaporizer assembly 12b.
  • the substrate 42 is mounted such that its front side 42a faces the nozzle 36 and is held at a distance of about 7 millimetres from the nozzle 36.
  • the front side of the substrate is at an oblique angle to the longitudinal axis of the system. This improves transport of liquid droplet and vapour from the substrate through the mouthpiece portion 50 when compared to an arrangement in which the front side of the substrate is perpendicular to the longitudinal axis of the system.
  • the heater assembly 40 further comprises a heating element 46 in the form of a conductive thin film coating applied to the backside 42b of the substrate 42.
  • the thin film coating is electrically connected via the support posts 44 to the control unit 18 and the power source 16.
  • the support posts 44 may also provide electrical contacts for establishing the electrical connection between the heater assembly 40 and the power source 16.
  • the heating element 46 is provided on the backside 42b of the substrate 42, the heating element 46 does not come into direct contact with the liquid aerosol-forming substrate under normal operating conditions.
  • the micropump 34 is electrically connected with the power source 16 and controlled by the control unit 18.
  • the micropump 34 can be activated to provide a desired liquid flow through the nozzle 36 provided at the outlet end of the liquid aerosol-forming substrate delivery device 30.
  • the heat resistive substrate 42 is heated up to temperatures of above 120°Celsius, which is sufficient to volatilize the liquid aerosol-forming substrate sprayed on the front side 42a of the heat resistive substrate 42.
  • Fig. 2 the aerosol-generating system 10 is depicted in a fully assembled state.
  • the complete mouthpiece 50 is made from shock resistant transparent glass. Due to the transparency of the mouthpiece 50 and the heater assembly 40 the consumer can at any time visually monitor aerosol-formation in the aerosol-generating system 10, and can monitor cleanliness of the vaporization unit.
  • the aerosol-generating system 10 may be activated by the user by manual operation of a power switch, or may automatically be activated by corresponding detection means when a user draws a puff. Upon detection of such signals, the heater assembly 40 and the liquid aerosol-forming substrate delivery device 30 are activated by the control unit 18. The liquid aerosol-forming substrate delivered to the heater assembly 40 is vaporized and is mixed with the air stream to form an aerosol, which is delivered to the user.
  • the specific design of the aerosol-generating system ensures that the delivered liquid aerosol-forming substrate is substantially completely volatilized and formation of residues within the inner surface of the mouthpiece 50 and on the heater assembly 40 is avoided. Due to transparency of the employed materials, a consumer can at any time verify that no undesired residues have formed. Should a consumer nevertheless notice that such undesired residues have formed, the aerosol-generating system of the present invention allows for easy access to internal parts of the system. By removing the detachable mouthpiece portion the consumer can easily gain access to the heater assembly and rinse the mouthpiece and the heater assembly with tab water or any other suitable cleaning liquid.
  • Fig. 3 shows an enlarged view of the heater assembly 40.
  • the heat resistive substrate 42 is mounted on support posts 44 and is held at a predefined distance from the nozzle 36.
  • the front side 42a of the heat resistive substrate 42 faces towards nozzle 36, such that the liquid aerosol-forming substrate is directly delivered only onto the front side 42a of the heat resistive substrate.
  • the backside 42b of the heat resistive substrate 42 is provided with a heating element in form of an electrically conductive thin film coating 46.
  • the support posts are also used for electrically contacting the conductive thin film coating to the power source of the aerosol-generating system 10. As the heating element is provided on the backside 42b of the heat resistive substrate, it does not come into direct contact with the liquid aerosol-forming substrate delivered via nozzle 36.
  • the heater assembly 40 may be detachable from the nozzle to allow for removal and easy cleaning.
  • the support posts may be received in slots in the nozzle 36.
  • the heater assembly may be fixed to the mouthpiece portion 50.

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Abstract

The vaporizing assembly (12b) for an aerosol generating system (10) comprises a liquid aerosol-forming substrate delivery device (30) for delivering liquid aerosol-forming substrate, and a heater assembly (40). The heater assembly comprises a heat resistive substrate (42) and an electric heater element (46). The liquid aerosol-forming substrate delivery device delivers liquid aerosol-forming substrate to at least a surface of the heat resistive substrate, wherein the heating element is isolated from the liquid aerosol-forming substrate. The invention is also directed to a method for generating an aerosol.

Description

VAPORIZING ASSEMBLY COMPRISING A VIEWABLE HEATING ELEMENT AND LIQUID DELIVERY DEVICE FOR AN AEROSOL GENERATING SYSTEM
The present invention relates to a vaporizing assembly for an aerosol-generating system, such as a handheld electrically operated aerosol-generating system.
Handheld electrically operated aerosol-generating systems are known that consist of a device portion comprising a battery and control electronics, a cartridge portion comprising a supply of aerosol-forming substrate held in a liquid storage portion, and an electrically operated vaporiser. The vaporiser typically comprises a coil of heater wire wound around an elongate wick soaked in the liquid aerosol-forming substrate held in the liquid storage portion. The cartridge portion typically comprises not only the supply of aerosol-forming substrate and an electrically operated vaporiser, but also a mouthpiece, from which the user inhales aerosol.
In conventional aerosol-generating systems the liquid aerosol-generating medium may not always be completely volatilized. Residues may be created upon transport and heating of the liquid aerosol-forming substrate. Such residues may affect aerosol creation. In particular, residues may impair repeatability of aerosol creation. In order to increase customer satisfaction, it is desirable to offer customers the opportunity to visually inspect cleanliness of functional components of the vaporiser used in aerosol-generating systems.
In conventional aerosol-generating systems the vaporiser is usually not easily accessible and the heating elements are mostly very small and fragile. Thus, in these systems cleaning of the vaporiser is very difficult or not possible at all.
It is further desirable in some cases to increase and facilitate product handling and maintenance by designing aerosol-generating systems in a modular fashion, wherein individual components can be easily and reliably cleaned by the users.
According to a first aspect of the present invention there is provided a vaporizing assembly for an aerosol generating system, comprising a liquid aerosol-forming substrate delivery device for delivering liquid aerosol-forming substrate, and a heater assembly. The heater assembly comprises a heat resistive substrate and an electric heater element. The liquid aerosol-forming substrate delivery device delivers liquid aerosol-forming substrate to at least a surface of the heater assembly, wherein the heating element is isolated from the liquid aerosol-forming substrate during normal use.
The heat resistive substrate of the heater assembly may be transparent or semi- transparent. The heat resistive substrate of the heater assembly may be made from glass, heat resistive glass, ceramics, silicon, semiconductors, metals or metal alloys.
The heat resistive substrate may be produced from pure glass or a glass compound, as well as glass with specific crystal orientation to enable optimized thermal transfer effects. By forming the heater assembly from transparent or semi-transparent materials, the user may easily see and assess the need to clean the surface of the heat resistive substrate. In order to clean the surface, the heater assembly may be rinsed with water or a suitable cleaning liquid.
The heat resistive substrate may be substantially flat and may have any desired shape. The heat resistive substrate may have a rectangular, polygonal, circular or oval shape with for example width and length dimensions of between 3 to 10 millimeters. The thickness of the heat resistive substrate may range between 0.2 and 2.5 millimeters. In some embodiments the heat resistive substrate may be have a rectangular shape with a size of about 7 x 6 millimeters or 5 x 5 millimeters (L x W), and a thickness of about 1 to 1.5 millimeters.
As used herein, "substantially flat" means an arrangement that is in the form of a substantially two dimensional object. Thus, the substantially flat heat resistive substrate extends in two dimensions substantially more than in a third dimension. In particular, the dimensions of the substantially flat heat resistive substrate in each of the two dimensions is at least 5 times larger than in the third dimension. The two dimensions may define a surface of the heat resistive substrate and third dimension may define a thickness of the heat resistive substrate, normal to the surface. An example of a substantially flat heat resistive substrate is an object between two imaginary and substantially parallel planar surfaces, wherein the distance between the two imaginary surfaces is substantially smaller than the extent of the object parallel to the surfaces. As described above, the extent of the object in two orthogonal directions parallel to the surfaces may be at least five times greater than the distance (or thickness) between the two parallel surfaces. In some embodiments, the substantially flat heat resistive substrate is planar and the distance between the parallel planar surfaces would be the thickness of the material used for forming the heater. In other embodiments, the substantially flat heat resistive substrate is curved along one or more dimensions, for example forming a dome shape or bridge shape.
The heating element may be transparent but may also include partially transparent or not transparent materials. For example, the heating element may comprise metallic layers or elements in at least one of the surfaces of the heat resistive substrate for the purpose of creating a resistive element. Further, contact pads for electrical conductivity and connection with other parts of the device may be provided, which are not transparent. The non-transparent parts are used only in such extent that the user may still be able to see and assess the need to clean the surface of the heat resistive substrate.
The heating element is isolated from the liquid aerosol-forming substrate during normal use. The expression "isolated from the liquid aerosol-forming substrate" as used throughout this application is to be understood in the sense that the heating element is provided such that it does not come into direct contact with the liquid aerosol-forming substrate during normal use. For example, as disclosed in more detail below, the heating element may be provided within the volume of the heat resistive substrate, may be sandwiched between two elements of the heat resistive substrate or may be covered with a protective layer of heat resistive material. With such configuration, contact between the heating element and the liquid aerosol-forming substrate may be completely avoided.
The expression "isolated from the liquid aerosol-forming substrate" is also to be construed in a way that it encompasses embodiments in which the heating element is provided on a surface of the heat resistive substrate onto which the liquid aerosol-forming substrate is not directly delivered. For example, in some embodiments the liquid aerosol-forming substrate may be delivered to a front side of the heat resistive substrate and the heating element may be provided on a backside of the heat resistive substrate.
In such configurations indirect contact between the heating element and the liquid aerosol-forming substrate might not be avoided. Such indirect contact may occur when residual liquid aerosol-forming substrate creeps over the heat resistive substrate or when vaporized liquid substrate condenses at the heating element.
The heating element may be provided as a thin film coating provided to the surface of the heat resistive substrate. The heating element can be impregnated, deposited or printed on the surface of the heat resistive substrate. The material of the thin film heating element can be any suitable material which has convenient electrical properties and a sufficiently high adherence to the heat resistive substrate.
In order to allow for a homogenous heating of the heat resistive substrate, the thin film coating of the heating element may extend substantially over the complete surface of the heat resistive substrate. The geometrical shape of the heating element may vary, being any adequate shape to produce the intended electrical resistance and the intended heating capabilities.
The heating element assembly may be localized in such configuration in the vaporizing assembly that one of the large surfaces of the heat resistive substrate, also referred to as the front side surface, faces towards the delivery device. In use the liquid aerosol-forming substrate is substantially dispensed only onto the front side surface of the heat resistive substrate.
The heating element is provided to the large surface of the heat resistive substrate which points away from the delivery device. This surface is also referred to as the backside of the heat resistive substrate. The backside does not come into direct contact with the liquid aerosol-forming substrate.
The heating element is configured such that the front side of the heat resistive substrate is heated to temperatures of about between 120 degrees Celsius and 250 degrees Celsius. The actual temperature of the heater assembly may be adjusted or chosen for example depending on the type of liquid aerosol-forming substrate that is used.
The heating element may be embedded in the heat resistive substrate. The expression "embedded" as used throughout this application is to be understood in the sense that the heating element is provided within the volume of the heat resistive substrate, is sandwiched between two elements of the heat resistive substrate or is sandwiched between one of the surfaces of the heat resistive substrate and an additional cover layer. The cover layer may be a specific coating of glass or mainly polymeric transparent material with good resistance to temperatures up to the operating temperature of the heating element. The heating element may comprise a metallic wire which is embedded in a heat resistive substrate of glass or any other suitable material.
The heat resistive substrate of the heater assembly may be made from a material having low adhesion or anti-adhesion properties with respect to the liquid aerosol-forming substrate. This can reduce the probability of accumulation of residues on the surface of the heater element. Moreover, the heating element may be easier to clean by the consumer. The surface of the heat resistive substrate of the heater assembly may be non-porous. Non-porous means that the surface of the heat resistive substrate does not allow liquid or air to pass through it.
The heater assembly may additionally comprise further sensors or components for specific additional purposes. Such additional sensors may include real-time chemical sensors and temperature sensors. With these sensors, the chemical composition and the temperature on the surface of the heater assembly can be monitored in a fast and geometrically precise way.
The heater assembly element may be an all-in-one built-in component such as a semiconductor component, a microchip component or a set of those components, manufactured using semiconductor technologies as a single component comprising nano- sized integrated structures. Such heater assemblies may be more easily connected and disconnected from the man body of the device, and are therefore desirable as replacement parts. However, depending on the material used, specific cleaning procedures may apply.
During vaporization the liquid aerosol-forming substrate preferably only comes into contact with the front side surface of the heat resistive substrate.
The liquid aerosol-forming substrate delivery device is connectable to a liquid storage portion and is configured to convey the liquid aerosol-forming substrate onto the heater assembly. The liquid aerosol-forming substrate delivery device may comprise an outlet end for discharging the liquid aerosol-forming substrate onto the heater assembly. The outlet end of the delivery device may be spaced apart from the heater assembly. The distance between the outlet end of the delivery device and the heater assembly may be between 0.1 and 10 millimeters, may be between 0.5 and 5 millimeters and may further be between 0.7 and 2.5 millimeters.
Embodiments in which the heater assembly spaced apart from delivery device may offer additional advantages. Reflux of liquid aerosol-forming substrate from the heating element to the delivery device is efficiently prevented. Moreover, as the heating element is mechanically decoupled from the delivery device, handling of the vaporizing assembly, in particular disassembly for replacement purposes or cleaning is facilitated. The heater assembly may be releasably connected to the liquid aerosol-forming substrate delivery device. Releasably connected in this context means that the heater assembly may be disconnected from the liquid aerosol-forming substrate delivery device and reconnected to liquid aerosol- forming substrate delivery device without damaging either the heater assembly or liquid aerosol-forming substrate delivery device.
The delivery device may further comprise a pump for delivering the liquid aerosol- forming substrate onto the heater assembly. The pump may be a hand operated, manual pump, an electromechanical pump or a conventional micropump.
Micropumps may allow on-demand delivery of liquid aerosol-forming substrate at a low flow rate of for example approximately 0.5 to 4.5 microliters per second for intervals of variable or constant duration. The pump may be carefully tuned in order to deliver the appropriate amount of liquid aerosol-forming substrate to the heating element. Consequently, the amount of deposited liquid aerosol-forming substrate can be determined from the amount of pump cycles.
The pumped volume of one complete cycle of a micropump typically is about 0.50 microliters per second. Such micropumps typically are operated at a pump frequency of between 5 to 20 hertz.
The pump may be configured to pump liquid aerosol-forming substrates that are characterized by a relatively high viscosity as compared to water. The viscosity of a liquid aerosol-forming substrate may be in the range from about 10 to 500 millipascal seconds, preferably in the range from about 17 to 86 millipascal seconds.
The liquid aerosol-forming delivery device may further be configured to deliver a metered amount of liquid aerosol-forming substrate onto the heater assembly. The estimated maximum amount of liquid to be pumped as a dose for a puff is a small volume, as a pumping pulse liquid volume from 0.010 to 0.060 microliters, preferably of around 0.0125 microliters.
At the outlet end of the liquid aerosol-forming substrate delivery device a nozzle may be provided via which the liquid aerosol-forming substrate may be sprayed onto the heater assembly for volatilization and aerosol creation. The nozzle converts the flow of the liquid aerosol-forming substrate into a plurality of small droplets. The spray pattern of the droplets may be adapted to the shape of the heater assembly.
The delivery device may comprise a classic type atomizer spray nozzle, in which case a flow of air is supplied through the nozzle by the action of puffing from the user, creating a pressurized air flow that will mix and act with the liquid creating an atomized spray in the outlet of the nozzle. Several systems are available on the market including nozzles that work with small volumes of liquid, in sizes that meet the requirements to fit in small portable devices. Another class of nozzle that may be used is an airless spray nozzle, sometimes referred to as a micro-spray nozzle. Such nozzles create micro spray cones in very small sizes. With this class of nozzles, the airflow management inside the device, namely inside the mouth piece, surrounds the nozzle and the heater assembly, flushing the heater assembly surface towards the outlet of the mouthpiece, preferably including a turbulent air flow pattern of the aerosol exiting the mouthpiece.
For either class of nozzle, the distance of the air gap between the delivery device and the surface of the heat resistive substrate facing the nozzle, is preferably within a range from 2 to 10 millimeters, more preferably from 3 to 7 millimeters. Any type of available spraying nozzles may be used. Airless nozzle 062 Minstac from manufacturer "The Lee Company" is an example of a suitable spray nozzle.
The vaporizing assembly may have a longitudinal axis. The delivery device may deliver or spray liquid aerosol-forming substrate along the longitudinal axis. The heat resistive substrate may have a surface that receives the liquid aerosol-forming substrate and the surface may be oblique to the longitudinal axis of the vaporizing assembly. In the case of a non-planar surface of the heat resistive substrate, the surface of at least a central portion of the heater assembly that receives liquid aerosol-forming substrate from the delivery device delivered along the longitudinal axis may be oblique to the longitudinal axis of the vaporizing assembly.
A coupling unit may be provided in order to connect the delivery device to a liquid storage portion. The coupling unit may include a "luer" type connection. However, any type of leakage free connection system may be used.
According to a second aspect of the present invention there is provided an aerosol- generating system comprising a vaporizing assembly as disclosed above and a housing in which the vaporizing assembly is located. At least a part of the housing in which the heater assembly of the vaporizing assembly is located, is made from transparent material, such that the heater assembly can be visually inspected by the consumer.
The housing of the aerosol-generating system may comprise a mouthpiece through which the consumer may inhale the generated aerosol. The mouthpiece maybe detachably connected to the housing. The heater assembly of the vaporizing assembly may be located in the mouthpiece. At least a portion of the mouthpiece may be transparent, such that the heater assembly can be visually inspected by the consumer.
The transparent portion of the housing or the mouthpiece may be made from for example thermal resistant glass, shock resistant glass, polymeric materials, hybrid compounds, carbon compounds, graphite, polysulfone (PSU), polyethersulfone (PES) or polyphenylsulfone (PPSU).
The mouthpiece and the heater assembly may be integrally formed as a single part. The mouthpiece and the heater assembly may be provided as a replaceable part, which can be changed after use.
With the present invention the consumer can visually inspect the heater assembly of the aerosol-generating system. When undesired contaminations are detected, the consumer may disassemble the aerosol-generating system and clean the heater assembly. The design of the vaporizing assembly of the present invention allows the user to easily clean the heating element for example by rinsing it with water.
The aerosol-generating system may further comprise a device portion including a power supply and a control unit. The aerosol-generating system may further comprise a replaceable liquid storage portion. When assembled, the liquid storage portion is in fluid connection with the liquid aerosol-forming substrate delivery device. The mouthpiece may be detachable from the device portion and the liquid storage portion.
In some embodiments the liquid storage portion may comprise pressurized liquid. The liquid may be stored in the liquid storage portion in a collapsible balloon. A one way valve may be temporarily opened to allow liquid flow out of the liquid storage portion.
In some embodiments the liquid storage portion may have a flexible or movable wall. By manual or electromechanical action onto the moveable wall, the liquid aerosol-forming substrate may be forced out of the liquid storage portion. The liquid aerosol-forming substrate from the liquid storage portion may then be delivered by the delivery device to the heater assembly.
Additional one-way valves may be provided in the delivery device wherever it is desired to avoid reflux of the liquid aerosol-forming substrate. To this end, commercially available one-way valves with adequate size and liquid flows may be used, including mini and micro flutter valves, duckbill valves, check valves. The valves may be made of materials resistant to aggressive chemicals or FDA certified materials, which may be used for food industry and medical applications.
The aerosol-generating system according to an embodiment of the present invention may further comprise a control unit connected to the vaporiser and to an electrical power source.
The control unit may be used to set the temperature and the heating duration of the heating element. The control unit may also be used to activate the pump in order to deliver the liquid aerosol-generating substrate onto the heater assembly. To this end the control unit may be in communication with an air flow sensor, which allows the control unit to detect when a user draws a puff.
The control unit may comprise a microprocessor, which may be a programmable microprocessor. The control unit may comprise further electronic components. The control unit may be configured to regulate a supply of power to the vaporizing assembly. Power may be supplied to the vaporizing assembly continuously following activation of the system or may be supplied intermittently, such as on a puff-by-puff basis. The power may be supplied to the vaporizing assembly in the form of pulses of electrical current.
The power supply provides the required electric energy to the electric components of the aerosol-generating system. The power supply may be in form of a charge storage device such as a capacitor. The power supply may require recharging and may have a capacity that allows for the storage of enough energy for one or more user experiences; for example, the power supply may have sufficient capacity to allow for the continuous generation of aerosol for a period of around six minutes or for a period that is a multiple of six minutes. In another example, the power supply may have sufficient capacity to allow for a predetermined number of puffs or discrete activations of the heater assembly.
For allowing air to enter the aerosol-generating system, a wall of the housing of the aerosol-generating system is provided with at least one semi-open inlet. The semi-open inlet preferably allows air to enter the aerosol-generating system, but no air or liquid to leave the aerosol-generating system through the semi-open inlet. A semi-open inlet may for example be a semi-permeable membrane, permeable in one direction only for air, but is air- and liquid-tight in the opposite direction. A semi-open inlet may for example also be a one-way valve. Preferably, the semi-open inlets allow air to pass through the inlet only if specific conditions are met, for example a minimum depression in the aerosol-generating system or a volume of air passing through the valve or membrane.
The liquid aerosol-forming substrate is a substrate capable of releasing volatile compounds that can form an aerosol. The volatile compounds may be released by heating the liquid aerosol-forming substrate. The liquid aerosol-forming substrate may comprise plant- based material. The liquid aerosol-forming substrate may comprise tobacco. The liquid aerosol-forming substrate may comprise a tobacco-containing material containing volatile tobacco flavour compounds, which are released from the liquid aerosol-forming substrate upon heating. The liquid aerosol-forming substrate may alternatively comprise a non-tobacco- containing material. The liquid aerosol-forming substrate may comprise homogenised plant- based material. The liquid aerosol-forming substrate may comprise homogenised tobacco material. The liquid aerosol-forming substrate may comprise at least one aerosol-former. The liquid aerosol-forming substrate may comprise other additives and ingredients, such as flavourants.
The aerosol-generating system may be an electrically operated aerosol-generating system. Preferably, the aerosol-generating system is portable. The aerosol-generating system may have a size comparable to a conventional cigar or cigarette. The aerosol-generating system may have a total length between approximately 30 millimeters and approximately 150 millimeters. The aerosol-generating system may have an external diameter between approximately 5 millimeters and approximately 30 millimeters.
The aerosol-generating system may be elongate and have a longitudinal axis. An outlet may be provided in the mouthpiece at one end of the longitudinal axis. The surface of the heat resistive substrate may be oblique to the longitudinal axis of the aerosol-generating system. This may improve the transport of vapour and liquid from the heater assembly to the outlet. In the case of a non-planar surface of the heat resistive substrate, the surface of at least a central portion of the heater assembly may be oblique to the longitudinal axis of the aerosol- generating system.
According to a third aspect of the present invention there is provided a method for generating aerosol, comprising the steps of storing liquid aerosol-forming substrate in a liquid storage portion, providing a heater assembly comprising a heat resistive substrate and an electric heating element, delivering liquid aerosol-forming substrate from the liquid storage portion to the heater assembly via a delivery device, and volatilizing at least a part of the delivered liquid aerosol-forming substrate by activating the heating element of the heater assembly. The heating element is isolated from the liquid aerosol-forming substrate. The heating element therefore does not directly contact the liquid aerosol-forming substrate in normal use.
Direct contact between the liquid aerosol-forming substrate and the heating element may be preferably avoided by embedding the heating element in the heat resistive substrate of the heater assembly or by providing the heating element on a surface of the heat resistive substrate which does not come into contact with the liquid aerosol-forming substrate.
The method may further comprise the step of providing a housing in which the heater assembly is located, wherein at least the part of the housing in which the heater assembly is located, is made from transparent material, such that the heater assembly can be visually inspected from outside. This allows the consumer to verify whether contaminations or residues have formed on the heater assembly. In case such undesired contaminations have indeed formed, the consumer can take the necessary steps to remove these contaminations. In order to facilitate maintenance of the aerosol-generating system, the mouthpiece including the heater assembly is configured to be cleanable, for example rinseable with water.
During normal operation of the aerosol-generating system, the delivery of the liquid aerosol-forming substrate and the heating element may be triggered by a puff detection system. Alternatively, these elements may be triggered by pressing an on-off button, held for the duration of a puff.
In some embodiments the delivery of the liquid aerosol-forming substrate may be delayed to the activation of the heating element. In these embodiments the heating element is pre-heated to a desired operation temperature, before the liquid aerosol-forming substrate is delivered onto the heater assembly.
Features described in relation to one aspect may equally be applied to other aspects of the invention.
Embodiments of the invention will now be described, by way of example only, with reference to the accompanying drawings, in which:
Fig. 1 is an exploded view of an embodiment of an aerosol-generating system;
Fig. 2 shows the fully assembled aerosol-generating system of Fig. 1 ;
Fig. 3 shows an enlarged view of the heater assembly.
Fig. 1 shows the components of an aerosol-generating system of the present invention in an exploded view. The aerosol-generating system 10 comprises a device portion 12a, including a housing 14, a power source 16 and a control unit 18. The aerosol-generating system 10 further comprises a vaporizer assembly 12b, including a housing 20, an exchangeable liquid storage portion 22, a delivery device 30, and a heater assembly 40. A transparent mouthpiece 50 portion can be detachably connected to the housing 20 of the vaporizer assembly 12b.
The device portion 12a and the vaporizer assembly 12b are connected via any suitable coupling unit, which provides mechanical and electrical connection between the device portion 12a and the vaporizer assembly 12b.
The liquid storage portion 22 is connected to the aerosol-forming substrate delivery device 30 via a coupling unit 24. In this case, the coupling unit is a "luer" type coupling unit. The liquid storage portion 20 can easily be replaced by the user, by separating the vaporizer assembly 12b from the device portion 12a and removing the liquid storage portion 22 from the open distal end of the vaporizer assembly 12b.
In this embodiment the liquid aerosol-forming substrate delivery device 30 is configured to transport the liquid aerosol-forming substrate from the liquid storage portion 22 to the heater assembly 40. To this end the liquid aerosol-forming substrate delivery device 30 comprises a tubing 32 and micropump 34 which are in fluid connection with the liquid storage portion 22. Micropump 34 is configured to pump the liquid aerosol-forming substrate onto the heater assembly 40.
At the outlet end of the liquid aerosol-forming substrate delivery device 30 a spray nozzle 36 is provided. Spray nozzle 36 is configured to dispense the liquid aerosol-forming substrate onto the heater assembly 40 in a predetermined spray pattern. In the depicted embodiment nozzle 36 is a conventional airless nozzle, providing a cone like spray pattern. The spray pattern is adapted to the size of the surface of the heater assembly 40.
The heater assembly 40 comprises a substantially rectangular substrate 42 made from thermo-resistive glass. The substrate 42 has a size of 5 x 5 square millimetres and a thickness of 1 millimeter. The substrate 42 is mounted on support posts 44, which in turn are fixed to the housing 20 of the vaporizer assembly 12b. The substrate 42 is mounted such that its front side 42a faces the nozzle 36 and is held at a distance of about 7 millimetres from the nozzle 36. The front side of the substrate is at an oblique angle to the longitudinal axis of the system. This improves transport of liquid droplet and vapour from the substrate through the mouthpiece portion 50 when compared to an arrangement in which the front side of the substrate is perpendicular to the longitudinal axis of the system.
The heater assembly 40 further comprises a heating element 46 in the form of a conductive thin film coating applied to the backside 42b of the substrate 42. The thin film coating is electrically connected via the support posts 44 to the control unit 18 and the power source 16. To this end the support posts 44 may also provide electrical contacts for establishing the electrical connection between the heater assembly 40 and the power source 16. As the heating element 46 is provided on the backside 42b of the substrate 42, the heating element 46 does not come into direct contact with the liquid aerosol-forming substrate under normal operating conditions.
The micropump 34 is electrically connected with the power source 16 and controlled by the control unit 18. The micropump 34 can be activated to provide a desired liquid flow through the nozzle 36 provided at the outlet end of the liquid aerosol-forming substrate delivery device 30.
By applying electrical current to the thin film coating, the heat resistive substrate 42 is heated up to temperatures of above 120°Celsius, which is sufficient to volatilize the liquid aerosol-forming substrate sprayed on the front side 42a of the heat resistive substrate 42.
In Fig. 2 the aerosol-generating system 10 is depicted in a fully assembled state. In this embodiment the complete mouthpiece 50 is made from shock resistant transparent glass. Due to the transparency of the mouthpiece 50 and the heater assembly 40 the consumer can at any time visually monitor aerosol-formation in the aerosol-generating system 10, and can monitor cleanliness of the vaporization unit.
The aerosol-generating system 10 may be activated by the user by manual operation of a power switch, or may automatically be activated by corresponding detection means when a user draws a puff. Upon detection of such signals, the heater assembly 40 and the liquid aerosol-forming substrate delivery device 30 are activated by the control unit 18. The liquid aerosol-forming substrate delivered to the heater assembly 40 is vaporized and is mixed with the air stream to form an aerosol, which is delivered to the user.
The specific design of the aerosol-generating system ensures that the delivered liquid aerosol-forming substrate is substantially completely volatilized and formation of residues within the inner surface of the mouthpiece 50 and on the heater assembly 40 is avoided. Due to transparency of the employed materials, a consumer can at any time verify that no undesired residues have formed. Should a consumer nevertheless notice that such undesired residues have formed, the aerosol-generating system of the present invention allows for easy access to internal parts of the system. By removing the detachable mouthpiece portion the consumer can easily gain access to the heater assembly and rinse the mouthpiece and the heater assembly with tab water or any other suitable cleaning liquid.
Fig. 3 shows an enlarged view of the heater assembly 40. The heat resistive substrate 42 is mounted on support posts 44 and is held at a predefined distance from the nozzle 36. The front side 42a of the heat resistive substrate 42 faces towards nozzle 36, such that the liquid aerosol-forming substrate is directly delivered only onto the front side 42a of the heat resistive substrate. The backside 42b of the heat resistive substrate 42 is provided with a heating element in form of an electrically conductive thin film coating 46. The support posts are also used for electrically contacting the conductive thin film coating to the power source of the aerosol-generating system 10. As the heating element is provided on the backside 42b of the heat resistive substrate, it does not come into direct contact with the liquid aerosol-forming substrate delivered via nozzle 36. The heater assembly 40 may be detachable from the nozzle to allow for removal and easy cleaning. The support posts may be received in slots in the nozzle 36. The heater assembly may be fixed to the mouthpiece portion 50.
The exemplary embodiments described above illustrate but are not limiting. In view of the above discussed exemplary embodiments, other embodiments consistent with the above exemplary embodiments will now be apparent to one of ordinary skill in the art.

Claims

1 . A vaporizing assembly for an aerosol generating system, comprising a liquid aerosol-forming substrate delivery device for delivering liquid aerosol-forming substrate, and
a heater assembly,
the heater assembly comprising a heat resistive substrate and an electric heater element,
the liquid aerosol-forming substrate delivery device being arranged for delivering liquid aerosol-forming substrate to at least a surface of the heat resistive substrate, wherein the heating element is isolated from the liquid aerosol-forming substrate.
2. A vaporizing assembly according to claim 1 , wherein the heat resistive substrate of the heater assembly is transparent.
3. A vaporizing assembly according to any of claims 1 or 2, wherein the surface of the heat resistive substrate is substantially flat.
4. A vaporizing assembly according to any of the preceding claims, wherein the heating element is embedded in the heat resistive substrate.
5. A vaporizing assembly according to any of the preceding claims, wherein the heater assembly is releasably connected to the liquid aerosol-forming substrate delivery device.
6. A vaporizing assembly according to any of the preceding claims, wherein the heat resistive substrate of the heater assembly is made from a material having low adhesion or anti-adhesion properties with respect to liquid aerosol-forming substrate.
7. A vaporizing assembly according to any of the preceding claims, wherein the heat resistive substrate of the heater assembly is non-porous.
8. A vaporizing assembly according to any of the preceding claims, wherein the liquid aerosol-forming substrate delivery device comprises a pump and a nozzle for spraying the liquid aerosol-forming substrate onto the heater.
9. A vaporizing assembly according to the preceding claim, wherein nozzle is spaced at least 0.1 mm and no more than 2.5 mm from the heater assembly.
10. A vaporizing assembly according to the preceding claim, wherein the vaporising assembly is elongate and has a longitudinal axis, and wherein the surface of the heat resistive substrate is oblique to the longitudinal axis.
1 1 . An aerosol-generating system comprising
a vaporizing assembly according to any of the preceding claims, and
a housing in which the vaporizing assembly is located, wherein
at least the part of the housing is made from transparent material, such that the heater assembly is visible from outside the system.
12. An aerosol-generating system according to claim 1 1 , wherein the housing comprises a mouthpiece, wherein the heater assembly of the vaporizing assembly is located in the mouthpiece, and wherein the mouthpiece is made from transparent material.
13. An aerosol-generating system according to claim12, wherein the mouthpiece and heater assembly are integrally formed as a single part.
14. An aerosol-generating system according to any of claims 12 or 13, comprising:
a device portion, comprising a power supply and a control unit,
a replaceable liquid storage portion, and
wherein the mouthpiece is detachable from the device portion and the liquid storage portion.
15. A method for generating aerosol, comprising:
storing liquid aerosol-forming substrate in a liquid storage portion of an aerosol- generating system;
providing a heater assembly comprising a heat resistive substrate and an electric heating element configured to receive liquid aerosol-forming substrate,
delivering liquid aerosol-forming substrate from the liquid storage portion to the heater assembly via a delivery device, where the delivery device is in fluid communication with the liquid storage,
volatilizing at least a part of the delivered liquid aerosol-forming substrate by activating the heating element of the heater assembly,
whereby the heating element is isolated from the liquid aerosol-forming substrate.
PCT/EP2017/056741 2016-03-31 2017-03-21 Vaporizing assembly comprising a viewable heating element and liquid delivery device for an aerosol generating system WO2017167610A1 (en)

Priority Applications (14)

Application Number Priority Date Filing Date Title
CA3013263A CA3013263A1 (en) 2016-03-31 2017-03-21 Vaporizing assembly comprising a viewable heating element and liquid delivery device for an aerosol generating system
JP2018550538A JP6937777B2 (en) 2016-03-31 2017-03-21 Vaporization assembly for aerosol generation systems with visible heating element and liquid delivery device
CN201780018081.XA CN109068732B (en) 2016-03-31 2017-03-21 Vaporization assembly for an aerosol-generating system comprising a visual heating element and a liquid transfer device
MX2018011461A MX2018011461A (en) 2016-03-31 2017-03-21 Vaporizing assembly comprising a viewable heating element and liquid delivery device for an aerosol generating system.
RU2018138197A RU2735575C2 (en) 2016-03-31 2017-03-21 Evaporation unit comprising a visible heating element and a liquid delivery device for an aerosol generating system
KR1020187030018A KR102433532B1 (en) 2016-03-31 2017-03-21 A vaporization assembly for an aerosol-generating system comprising a visible heating element and a liquid delivery device
EP17710996.4A EP3435796B1 (en) 2016-03-31 2017-03-21 Aerosol generating system with a vaporizing assembly comprising a viewable heating element and liquid delivery device
US15/475,297 US10098387B2 (en) 2016-03-31 2017-03-31 Vaporizing assembly comprising a viewable heating element and delivery device for an aerosol-generating system
IL261508A IL261508A (en) 2016-03-31 2018-09-02 Vaporizing assembly comprising a viewable heating element and liquid delivery device for an aerosol generating system
US16/160,160 US10506833B2 (en) 2016-03-31 2018-10-15 Vaporizer including a heater assembly and delivery device
US16/692,540 US10952475B2 (en) 2016-03-31 2019-11-22 Vaporizer including a heater assembly and delivery device
US17/181,120 US11317475B2 (en) 2016-03-31 2021-02-22 Vaporizer including a heater assembly and delivery device
US17/722,599 US11771854B2 (en) 2016-03-31 2022-04-18 Vaporizer including a heater assembly and delivery device
US18/469,738 US20240001057A1 (en) 2016-03-31 2023-09-19 Vaporizer including a heater assembly and a delivery device

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP16163416.7 2016-03-31
EP16163416 2016-03-31

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US15/475,297 Continuation US10098387B2 (en) 2016-03-31 2017-03-31 Vaporizing assembly comprising a viewable heating element and delivery device for an aerosol-generating system

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EP (1) EP3435796B1 (en)
JP (1) JP6937777B2 (en)
KR (1) KR102433532B1 (en)
CN (1) CN109068732B (en)
CA (1) CA3013263A1 (en)
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MX (1) MX2018011461A (en)
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RU2735575C2 (en) 2020-11-03
CN109068732B (en) 2022-05-13
US20240001057A1 (en) 2024-01-04
EP3435796B1 (en) 2021-01-06
RU2018138197A3 (en) 2020-07-28
KR102433532B1 (en) 2022-08-18
US11317475B2 (en) 2022-04-26
US20220240353A1 (en) 2022-07-28
MX2018011461A (en) 2019-01-10
US11771854B2 (en) 2023-10-03
KR20180122441A (en) 2018-11-12
IL261508A (en) 2018-10-31
JP2019513361A (en) 2019-05-30
US20210176830A1 (en) 2021-06-10
EP3435796A1 (en) 2019-02-06
CN109068732A (en) 2018-12-21
JP6937777B2 (en) 2021-09-22
RU2018138197A (en) 2020-04-30

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