WO2016011596A1 - Bubble solution for highly stable, pattable bubbles and preparation method for bubble solution - Google Patents
Bubble solution for highly stable, pattable bubbles and preparation method for bubble solution Download PDFInfo
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- WO2016011596A1 WO2016011596A1 PCT/CN2014/082681 CN2014082681W WO2016011596A1 WO 2016011596 A1 WO2016011596 A1 WO 2016011596A1 CN 2014082681 W CN2014082681 W CN 2014082681W WO 2016011596 A1 WO2016011596 A1 WO 2016011596A1
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- bubble
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- A—HUMAN NECESSITIES
- A63—SPORTS; GAMES; AMUSEMENTS
- A63H—TOYS, e.g. TOPS, DOLLS, HOOPS OR BUILDING BLOCKS
- A63H33/00—Other toys
- A63H33/28—Soap-bubble toys; Smoke toys
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
Definitions
- the present invention relates to a bubble water, and more particularly to a bubble water having a long-lasting explosion-proof, high stability, and slap-off. Further, the present invention relates to a method of preparing the bubble water.
- BACKGROUND OF THE INVENTION Blowing bubbles is one of the children's favorite games. However, due to the chemical raw materials used, the bubble water currently purchased in the market always has a pungent odor, which has a certain effect on the child's health. Hidden dangers; For safety reasons, some parents also use detergents, shampoos, etc. as raw materials to make bubble water for children. However, the bubbles that are blown out from the market or the homemade bubble water continue to exist.
- An object of the present invention is to overcome the deficiencies of the prior art and to provide a bubble water having a long bubble duration and which is not easily broken. Another object of the present invention is to provide a method for preparing the bubble water.
- a high stability, tapable bubble water, in weight percentage consists of the following components: Foaming agent: 0.6 ⁇ 7.5%; Solvent: 6.5 ⁇ 11% Film former: 0.6 3.5%; preservative: 0.5-1.0%;
- the bubble water is composed of the following components in terms of weight percent: foaming agent: 1.5%; solvent: 10%; film former: 1.6%; preservative: 0.605%; water: balance.
- the foaming agent is lauramide propyl betaine, cocamidopropyl betaine, thioglycoside, ammonium decyl polyoxyethyl ether sulfate, amphoteric imidazoline, dodecyl benzene One or more of sodium sulfonate, sodium dodecyl sulfate, octadecyl dihydroxyethyl amine oxide, and lauramide propyl amine oxide.
- the solvent is glycerol.
- the film former is polyvinylpyrrolidone and/or polyvinyl alcohol.
- the preservative is one of ethylene glycol phenyl ether, 3-iodo-2-propynyl-butyl carbamate, polyhexamethylene biguanide hydrochloride, and imidazolium urea. Or several.
- a method for preparing bubble water as described above comprising the following preparation steps:
- step 2) After mixing the film-forming agent solution in step 1) with the solvent, adding a foaming agent and mixing uniformly;
- step 2) Add the preservative and the remaining amount of water to the mixture in step 2), and stir the mixture at room temperature to obtain the bubble water.
- the invention has the beneficial effects that the invention improves the durability and stability of the bubbles blown out by the bubble water by adjusting the ratio between the film forming agent and the solvent, and at the same time improves the water film of the bubble by controlling the amount of the solvent added.
- Polarity such that when the water film of the bubble comes into contact with the material of the non-polar fiber, the bubble and the non-polar fiber material are incompatible with each other and repel each other, so that the bubble is in the non-polar fiber material.
- the foaming agent is lauramide propyl betaine, cocamidopropyl betaine, thioglycoside, dodecyl polyoxyethyl ether ammonium sulfate, amphoteric imidazoline, dodecyl benzene sulfonic acid One or more of sodium, sodium dodecyl sulfate, octadecyl dihydroxyethyl amine oxide, and lauramide propyl amine oxide;
- the solvent is glycerol;
- the film former is polyethylene Pyrrolidone and/or polyvinyl alcohol;
- the preservatives are ethylene glycol phenyl ether, 3-iodo-2-propynyl-butyl carbamate, polyhexamethylene biguanide hydrochloride and imidazolium One or more of the base ureas.
- Example 1 A high stability, tapable bubble water having a composition by weight: lauric amidopropyl betaine: 1.5%; glycerol: 10%; polyvinylpyrrolidone: 1.6%; Ethylene glycol phenyl ether: 0.3%;
- IPBC-II 3-iodo-2-propynyl-butylcarbamate
- PHMB polyhexamethylene biguanide hydrochloride
- imidazolium urea 0.2%
- Preparing the bubble water composed as described above includes the following steps:
- step 2) after mixing the solution of polyvinylpyrrolidone in step 1) with glycerin, adding lauramide propyl betaine and mixing uniformly;
- step 3 sequentially adding ethylene glycol phenyl ether, 3-iodo-2-propynyl-butyl carbamate, polyhexamethylene biguanide hydrochloride, imidazolium urea to the mixture in step 2) And the balance of water, after stirring at room temperature, the high stability bubble water of the present invention is obtained.
- Example 2 A highly stable, smearable bubble water having a weight percent composition of: Twc-dodecyl polyoxyethyl ether ammonium sulfate: 6.5%; glycerol: 6.5%; polyvinylpyrrolidone: 0.6 %; ethylene glycol phenyl ether: 0.25%; 3-iodo-2-propynyl-butyl carbamate (IPBC-II): 0.075%; Polyhexamethylene biguanide hydrochloride (PHMB): 0.045%; imidazolium urea: 0.3%; water: balance.
- IPBC-II 3-iodo-2-propynyl-butyl carbamate
- IPBC-II 3-iodo-2-propynyl-butyl carbamate
- PHMB Polyhexamethylene biguanide hydrochloride
- imidazolium urea 0.3%
- water balance.
- the preparation method was the same
- the invention is based on the principle that physical and chemical polarity and non-polarity are mutually exclusive, and by adjusting and optimizing the formulation of the bubble water, the bubble forming property and the explosion resistance of the blown bubble are improved, so that the blown bubble has longer durability.
- the specific embodiments described herein are only used in the detailed description of the specific implementation process of the bubble water of the present invention, and are not intended to limit the preparation thereof. Any modification or modification of this product, the substitution and use of similar or similar substances within the scope or scope of patents, is within the scope of the patent protection of the present invention.
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
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Abstract
A bubble solution for highly stable, pattable bubbles, the weight percentage composition of the various components being: a foaming agent: 0.6-7.5%; a solvent: 6.5-11%; a film-forming agent: 0.6-3.5%; a preservative: 0.5-1.0%; water: the remainder. A preparation method for the bubble solution comprises: 1) the film-forming agent is stirred with 90-100oC hot water until completely dissolved to obtain a film-forming agent solution; 2) the film-forming agent solution in step 1) is evenly mixed with the solvent, the foaming agent is added, and even mixing is performed; 3) the preservative and the remaining water are added to the mixture in step 2), and the bubble solution is obtained after even stirring at room temperature. Blown bubbles have high film-formability, burst-resistance and lasting stability.
Description
一种高稳定性、 可拍打泡泡水及其制备方法 High stability, tapable bubble water and preparation method thereof
技术领域 本发明涉及一种泡泡水， 具体涉及一种具有持久耐爆、 高稳定性、 可拍打的泡泡水， 此外， 本发明还涉及一种所述泡泡水的制备方法。 背景技术 吹泡泡是儿童最喜欢的游戏之一， 然而， 由于所采用的化学原料的关系， 目前市场 购买的泡泡水总是有一股刺鼻的异味， 对孩子的身体健康造成了一定的隐患； 出于安全 考虑， 有些家长也会利用洗洁精、 洗发水等为原料给孩子自制泡泡水， 但是， 上述无论是 市场购买还是自制的泡泡水， 吹出来的泡泡都存在持续时间不长、泡泡易破裂的问题， 影 响了孩子们的游戏乐趣。 发明内容 本发明的目的在于克服现有技术的不足， 提供一种泡泡持续时间长、 不易破裂的泡 泡水， 本发明的另一目的在于提供一种该泡泡水的制备方法。 为实现上述目的， 本发明采用以下技术方案： 一种高稳定性、 可拍打泡泡水， 按重量百分比计， 由以下组分组成： 发泡剂： 0.6~7.5%； 溶剂： 6.5~11%； 成膜剂： 0.6 3.5%; 防腐剂: 0.5-1.0%；
优选的是： 按重量百分比计， 所述泡泡水由以下组分组成： 发泡剂： 1.5%; 溶剂： 10%; 成膜剂： 1.6%; 防腐剂： 0.605%; 水： 余量。 优选的是： 所述发泡剂为月桂酰胺丙基甜菜碱、 椰油酰胺丙基甜菜碱、 垸基糖苷、 十二垸基聚氧乙基醚硫酸铵、两性咪唑啉、 十二垸基苯磺酸钠、 十二垸基硫酸钠、 十八垸 基二羟乙基氧化胺和月桂酰胺丙基氧化胺中的一种或几种。 优选的是： 所述溶剂为丙三醇。 优选的是： 所述成膜剂为聚乙烯吡咯垸酮和 /或聚乙烯醇。 优选的是： 所述防腐剂为乙二醇苯醚、 3-碘 -2-丙炔基 -丁基氨基甲酸酯、 聚六亚甲基 双胍盐酸盐和咪唑垸基脲中的一种或几种。 本发明的另一目的， 一种如上所述泡泡水的制备方法， 包括以下制备步骤： BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a bubble water, and more particularly to a bubble water having a long-lasting explosion-proof, high stability, and slap-off. Further, the present invention relates to a method of preparing the bubble water. BACKGROUND OF THE INVENTION Blowing bubbles is one of the children's favorite games. However, due to the chemical raw materials used, the bubble water currently purchased in the market always has a pungent odor, which has a certain effect on the child's health. Hidden dangers; For safety reasons, some parents also use detergents, shampoos, etc. as raw materials to make bubble water for children. However, the bubbles that are blown out from the market or the homemade bubble water continue to exist. The problem is that the time is not long and the bubble is easy to break, which affects the children's fun. SUMMARY OF THE INVENTION An object of the present invention is to overcome the deficiencies of the prior art and to provide a bubble water having a long bubble duration and which is not easily broken. Another object of the present invention is to provide a method for preparing the bubble water. In order to achieve the above object, the present invention adopts the following technical solutions: A high stability, tapable bubble water, in weight percentage, consists of the following components: Foaming agent: 0.6~7.5%; Solvent: 6.5~11% Film former: 0.6 3.5%; preservative: 0.5-1.0%; Preferably, the bubble water is composed of the following components in terms of weight percent: foaming agent: 1.5%; solvent: 10%; film former: 1.6%; preservative: 0.605%; water: balance. Preferably, the foaming agent is lauramide propyl betaine, cocamidopropyl betaine, thioglycoside, ammonium decyl polyoxyethyl ether sulfate, amphoteric imidazoline, dodecyl benzene One or more of sodium sulfonate, sodium dodecyl sulfate, octadecyl dihydroxyethyl amine oxide, and lauramide propyl amine oxide. Preferably, the solvent is glycerol. Preferably, the film former is polyvinylpyrrolidone and/or polyvinyl alcohol. Preferably, the preservative is one of ethylene glycol phenyl ether, 3-iodo-2-propynyl-butyl carbamate, polyhexamethylene biguanide hydrochloride, and imidazolium urea. Or several. Another object of the present invention, a method for preparing bubble water as described above, comprising the following preparation steps:
1 ) 将成膜剂用 90 100 °C热水搅拌至完全溶解得成膜剂溶液； 1) stirring the film former with hot water at 90 100 ° C until completely dissolved to obtain a film former solution;
2) 将步骤 1 ) 中的成膜剂溶液与溶剂混匀后， 加入发泡剂， 混合均匀； 2) After mixing the film-forming agent solution in step 1) with the solvent, adding a foaming agent and mixing uniformly;
3 ) 向步骤 2) 中的混合液中加入防腐剂以及余量的水， 于常温下搅拌均匀后即得所 述的泡泡水。 本发明的有益效果在于， 本发明通过调整成膜剂和溶剂之间的比例来提高泡泡水吹 出来泡泡的持续性和稳定性， 同时通过控制溶剂的添加量来提高泡泡的水膜极性，使得泡 泡的水膜在与非极性的纤维的物料接触时， 泡泡与非极性的纤维物料间不相溶而相互排 斥，从而使得泡泡在与非极性的纤维物料相接触时不会破裂，儿童甚至可以穿戴手套来持
续拍打泡泡水数十次而不破裂，突破了传统泡泡水只能吹泡泡的玩法，增加了游戏的趣味 性。 具体实施方式 下面结合具体实施例对本发明的具体实施方式做进一步说明。 但本发明并不仅限于 下述实施例。 若无特别说明， 本发明所采用的各原料均可通过市场购买可得。 一种高稳定性、 可拍打泡泡水， 其重量百分比组分为： 发泡剂： 0.6~7.5%； 溶剂： 6.5~11%； 成膜剂： 0.6 3.5%; 防腐剂： 0.5~1.0%; 水： 余量。 其中， 所述发泡剂为月桂酰胺丙基甜菜碱、 椰油酰胺丙基甜菜碱、 垸基糖苷、 十二 垸基聚氧乙基醚硫酸铵、两性咪唑啉、 十二垸基苯磺酸钠、 十二垸基硫酸钠、 十八垸基二 羟乙基氧化胺和月桂酰胺丙基氧化胺中的一种或几种；所述溶剂为丙三醇；所述成膜剂为 聚乙烯吡咯垸酮和 /或聚乙烯醇； 所述防腐剂为乙二醇苯醚、 3-碘 -2-丙炔基-丁基氨基甲酸 酯、 聚六亚甲基双胍盐酸盐和咪唑垸基脲中的一种或几种。 实施例 1 一种高稳定性、 可拍打泡泡水， 其重量百分比组成为： 月桂酰胺丙基甜菜碱： 1.5%; 丙三醇: 10%； 聚乙烯吡咯垸酮: 1.6%；
乙二醇苯醚: 0.3%； 3) Add the preservative and the remaining amount of water to the mixture in step 2), and stir the mixture at room temperature to obtain the bubble water. The invention has the beneficial effects that the invention improves the durability and stability of the bubbles blown out by the bubble water by adjusting the ratio between the film forming agent and the solvent, and at the same time improves the water film of the bubble by controlling the amount of the solvent added. Polarity, such that when the water film of the bubble comes into contact with the material of the non-polar fiber, the bubble and the non-polar fiber material are incompatible with each other and repel each other, so that the bubble is in the non-polar fiber material. Does not break when in contact, children can even wear gloves to hold Continue to shoot bubble water dozens of times without breaking, breaking through the traditional bubble water can only blow bubbles, increasing the fun of the game. DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS The specific embodiments of the present invention will be further described below in conjunction with specific embodiments. However, the present invention is not limited to the following embodiments. Unless otherwise stated, the raw materials used in the present invention are commercially available. A high stability, foamable water, the weight percentage components are: foaming agent: 0.6~7.5%; solvent: 6.5~11%; film former: 0.6 3.5%; preservative: 0.5~1.0% ; water: balance. Wherein, the foaming agent is lauramide propyl betaine, cocamidopropyl betaine, thioglycoside, dodecyl polyoxyethyl ether ammonium sulfate, amphoteric imidazoline, dodecyl benzene sulfonic acid One or more of sodium, sodium dodecyl sulfate, octadecyl dihydroxyethyl amine oxide, and lauramide propyl amine oxide; the solvent is glycerol; the film former is polyethylene Pyrrolidone and/or polyvinyl alcohol; the preservatives are ethylene glycol phenyl ether, 3-iodo-2-propynyl-butyl carbamate, polyhexamethylene biguanide hydrochloride and imidazolium One or more of the base ureas. Example 1 A high stability, tapable bubble water having a composition by weight: lauric amidopropyl betaine: 1.5%; glycerol: 10%; polyvinylpyrrolidone: 1.6%; Ethylene glycol phenyl ether: 0.3%;
3-碘 -2-丙炔基-丁基氨基甲酸酯 （IPBC-II): 0.07%； 聚六亚甲基双胍盐酸盐 （PHMB): 0.035%； 咪唑垸基脲: 0.2%；
制备如上所述组成的泡泡水， 包括以下步骤： 3-iodo-2-propynyl-butylcarbamate (IPBC-II): 0.07%; polyhexamethylene biguanide hydrochloride (PHMB): 0.035%; imidazolium urea: 0.2%; Preparing the bubble water composed as described above includes the following steps:
1 ) 将聚乙烯吡咯垸酮用 95°C热水搅拌至完全溶解得聚乙烯吡咯垸酮溶液； 1) The polyvinylpyrrolidone is stirred with 95 ° C hot water to completely dissolve to obtain a polyvinylpyrrolidone solution;
2)将步骤 1 )中的聚乙烯吡咯垸酮溶液与丙三醇混匀后， 加入月桂酰胺丙基甜菜碱， 混合均匀； 2) after mixing the solution of polyvinylpyrrolidone in step 1) with glycerin, adding lauramide propyl betaine and mixing uniformly;
3 ) 向步骤 2) 中的混合液中依次加入乙二醇苯醚、 3-碘 -2-丙炔基 -丁基氨基甲酸酯、 聚六亚甲基双胍盐酸盐、咪唑垸基脲以及余量的水，于常温下搅拌均匀后即得本发明所述 的高稳定性泡泡水。 3) sequentially adding ethylene glycol phenyl ether, 3-iodo-2-propynyl-butyl carbamate, polyhexamethylene biguanide hydrochloride, imidazolium urea to the mixture in step 2) And the balance of water, after stirring at room temperature, the high stability bubble water of the present invention is obtained.
实施例 2 一种高稳定性、 可拍打泡泡水， 其重量百分比组成为: 十二垸基聚氧乙基醚硫酸铵： 6.5%; 丙三醇： 6.5%; 聚乙烯吡咯垸酮： 0.6%; 乙二醇苯醚： 0.25%; 3-碘 -2-丙炔基-丁基氨基甲酸酯 （IPBC-II): 0.075%；
聚六亚甲基双胍盐酸盐 （PHMB): 0.045%； 咪唑垸基脲： 0.3%; 水： 余量。 制备方法同实施例 1。 本发明基于物理化学极性与非极性相互排斥的原理， 通过调整优化泡泡水的配方， 使得吹出来的泡泡成膜性和耐爆性提高，使得吹出来的泡泡具有更持久耐爆的稳定性；儿 童甚至可以穿戴手套来持续拍打泡泡水数十次而不破裂，突破了传统泡泡水只能吹泡泡的 玩法， 增加了趣味性。 本发明所描述的具体实施例只用于本发明的泡泡水的具体实现过程的详细描述，而不 是对其制备方法的限定。任何对此产品进行的修饰与改良，在专利范围或范畴内同类或相 近物质的替代与使用， 均属于本发明专利保护范围。
Example 2 A highly stable, smearable bubble water having a weight percent composition of: Twc-dodecyl polyoxyethyl ether ammonium sulfate: 6.5%; glycerol: 6.5%; polyvinylpyrrolidone: 0.6 %; ethylene glycol phenyl ether: 0.25%; 3-iodo-2-propynyl-butyl carbamate (IPBC-II): 0.075%; Polyhexamethylene biguanide hydrochloride (PHMB): 0.045%; imidazolium urea: 0.3%; water: balance. The preparation method was the same as in Example 1. The invention is based on the principle that physical and chemical polarity and non-polarity are mutually exclusive, and by adjusting and optimizing the formulation of the bubble water, the bubble forming property and the explosion resistance of the blown bubble are improved, so that the blown bubble has longer durability. The stability of the explosion; children can even wear gloves to continue to tap the bubble water dozens of times without breaking, breaking through the traditional bubble water can only blow bubbles, adding fun. The specific embodiments described herein are only used in the detailed description of the specific implementation process of the bubble water of the present invention, and are not intended to limit the preparation thereof. Any modification or modification of this product, the substitution and use of similar or similar substances within the scope or scope of patents, is within the scope of the patent protection of the present invention.
Claims
1、 一种高稳定性、 可拍打泡泡水， 其特征在于： 按重量百分比计， 由以下组分组成: 发泡剂： 0.6~7.5%； 溶剂： 6.5~11%； 成膜剂： 0.6 3.5%; 防腐剂： 0.5~1.0%; 水： 余量。 1. A high-stability, patted bubble water, characterized by: by weight percentage, consisting of the following components: foaming agent: 0.6~7.5%; solvent: 6.5~11%; film forming agent: 0.6 3.5%; preservative: 0.5~1.0% ; water: balance.
2、 根据权利要求 1所述的泡泡水， 其特征在于： 按重量百分比计， 由以下组分组成: 发泡剂： 1.5%; 溶剂： 10%; 成膜剂： 1.6%; 防腐剂： 0.605%; 水： 余量。 2. The bubble water according to claim 1, characterized by: by weight percent, consisting of the following components: a blowing agent: 1.5%; a solvent: 10%; a film former: 1.6%; a preservative: 0.605%; Water: balance.
3、 根据权利要求 1或 2所述的泡泡水， 其特征在于： 所述发泡剂为月桂酰胺丙基甜 菜碱、 椰油酰胺丙基甜菜碱、 垸基糖苷、 十二垸基聚氧乙基醚硫酸铵、 两性咪唑啉、 十二 垸基苯磺酸钠、十二垸基硫酸钠、十八垸基二羟乙基氧化胺和月桂酰胺丙基氧化胺中的一 种或几种。 The bubble water according to claim 1 or 2, wherein the foaming agent is lauramide propyl betaine, cocamidopropyl betaine, thioglycoside, and decyl polyoxyl One or more of ethyl ether sulfate ammonium, amphoteric imidazoline, sodium dodecylbenzenesulfonate, sodium dodecyl sulfate, octadecyl dihydroxyethyl amine oxide and lauramide propyl amine oxide .
4、 根据权利要求 1或 2所述的泡泡水， 其特征在于： 所述溶剂为丙三醇。 The bubble water according to claim 1 or 2, wherein the solvent is glycerin.
5、根据权利要求 1或 2所述的泡泡水， 其特征在于： 所述成膜剂为聚乙烯吡咯垸酮 和 /或聚乙烯醇。 The bubble water according to claim 1 or 2, wherein the film-forming agent is polyvinylpyrrolidone and/or polyvinyl alcohol.
6、 根据权利要求 1或 2所述的泡泡水， 其特征在于： 所述防腐剂为乙二醇苯醚、 3-
碘 -2-丙炔基-丁基氨基甲酸酯、 聚六亚甲基双胍盐酸盐和咪唑垸基脲中的一种或几种。 6. The bubble water according to claim 1 or 2, wherein: the preservative is ethylene glycol phenyl ether, 3- One or more of iodo-2-propynyl-butylcarbamate, polyhexamethylene biguanide hydrochloride, and imidazolium urea.
7、一种如权利要求 1或 2所述泡泡水的制备方法，其特征在于：包括以下制备步骤: A method for preparing bubble water according to claim 1 or 2, which comprises the following preparation steps:
1 ) 将成膜剂用 90 100 °C热水搅拌至完全溶解得成膜剂溶液； 1) stirring the film former with hot water at 90 100 ° C until completely dissolved to obtain a film former solution;
2) 将步骤 1 ) 中的成膜剂溶液与溶剂混匀后， 加入发泡剂， 混合均匀； 2) After mixing the film-forming agent solution in step 1) with the solvent, adding a foaming agent and mixing uniformly;
3 ) 向步骤 2) 中的混合液中加入防腐剂以及余量的水， 于常温下搅拌均匀后即得所 述的泡泡水。
3) Add the preservative and the remaining amount of water to the mixture in step 2), and mix well at room temperature to obtain the bubble water.
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| Application Number | Priority Date | Filing Date | Title |
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| PCT/CN2014/082681 WO2016011596A1 (en) | 2014-07-22 | 2014-07-22 | Bubble solution for highly stable, pattable bubbles and preparation method for bubble solution |
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| Application Number | Priority Date | Filing Date | Title |
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| PCT/CN2014/082681 WO2016011596A1 (en) | 2014-07-22 | 2014-07-22 | Bubble solution for highly stable, pattable bubbles and preparation method for bubble solution |
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| WO2018038823A1 (en) | 2016-08-24 | 2018-03-01 | Tran Dat Q | Formulations for edible bubble solution |
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| CN1787864A (en) * | 2003-06-24 | 2006-06-14 | 尤尼科技投资有限公司 | Device and composition for blowing a soap bubble |
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| US4284534A (en) * | 1979-04-03 | 1981-08-18 | Jack S. Wachtel | Aqueous bubble blowing composition |
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