WO2014015342A1 - Lightweight closure and container package - Google Patents
Lightweight closure and container package Download PDFInfo
- Publication number
- WO2014015342A1 WO2014015342A1 PCT/US2013/051524 US2013051524W WO2014015342A1 WO 2014015342 A1 WO2014015342 A1 WO 2014015342A1 US 2013051524 W US2013051524 W US 2013051524W WO 2014015342 A1 WO2014015342 A1 WO 2014015342A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- closure
- seal element
- top wall
- skirt portion
- wall portion
- Prior art date
Links
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D41/00—Caps, e.g. crown caps or crown seals, i.e. members having parts arranged for engagement with the external periphery of a neck or wall defining a pouring opening or discharge aperture; Protective cap-like covers for closure members, e.g. decorative covers of metal foil or paper
- B65D41/32—Caps or cap-like covers with lines of weakness, tearing-strips, tags, or like opening or removal devices, e.g. to facilitate formation of pouring openings
- B65D41/34—Threaded or like caps or cap-like covers provided with tamper elements formed in, or attached to, the closure skirt
- B65D41/3423—Threaded or like caps or cap-like covers provided with tamper elements formed in, or attached to, the closure skirt with flexible tabs, or elements rotated from a non-engaging to an engaging position, formed on the tamper element or in the closure skirt
- B65D41/3428—Threaded or like caps or cap-like covers provided with tamper elements formed in, or attached to, the closure skirt with flexible tabs, or elements rotated from a non-engaging to an engaging position, formed on the tamper element or in the closure skirt the tamper element being integrally connected to the closure by means of bridges
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D41/00—Caps, e.g. crown caps or crown seals, i.e. members having parts arranged for engagement with the external periphery of a neck or wall defining a pouring opening or discharge aperture; Protective cap-like covers for closure members, e.g. decorative covers of metal foil or paper
- B65D41/02—Caps or cap-like covers without lines of weakness, tearing strips, tags, or like opening or removal devices
- B65D41/04—Threaded or like caps or cap-like covers secured by rotation
- B65D41/0407—Threaded or like caps or cap-like covers secured by rotation with integral sealing means
- B65D41/0414—Threaded or like caps or cap-like covers secured by rotation with integral sealing means formed by a plug, collar, flange, rib or the like contacting the internal surface of a container neck
- B65D41/0421—Threaded or like caps or cap-like covers secured by rotation with integral sealing means formed by a plug, collar, flange, rib or the like contacting the internal surface of a container neck and combined with integral sealing means contacting other surfaces of a container neck
Definitions
- the present invention relates generally to a closure and container package for carbonated beverages and the like, wherein the closure has been specifically configured for reduced use of polymeric material, while at the same time providing the required sealing performance for the carbonated contents of the package.
- Closures of this nature typically formed by compression molding or injection molding, have proven to be especially effective for use on containers having carbonated or otherwise pressurized contents.
- closures of this nature typically include tamper-evident features, such as a tamper-indicating pilfer band, to assure consumers of product freshness quality.
- closures a significant cost associated with closures of this nature is the polymeric material from which the closures are molded.
- Polypropylene, polyethylene, copolymers, and like polymeric materials are typically employed for manufacture of these types of closures.
- any reduction in the amount of polymeric material for closure manufacture can desirably result in significant cost savings.
- the present invention is directed to a closure and container package, including a light-weight closure which has been specifically configured for reduced use of polymeric material, while still providing the requisite closure performance, including sealing performance, while at the same time providing a tamper-evidence function for ensuring package integrity.
- a closure and container package embodying the principles of the present invention has been specifically configured for packaging carbonated products, such as carbonated beverages, or other pressurized products.
- the closure of the package has been specifically configured to require relatively reduced quantities of polymeric material, while at the same time providing the necessary sealing performance, and desired tamper-indication function.
- a lightweight closure embodying the principles of the present invention can be configured as a unitary, one- piece closure molded from polymeric material.
- the closure comprises a closure cap having a top wall portion, and an annular skirt portion depending from the top wall portion.
- the skirt portion includes an external knurl pattern, and an internal thread formation for threaded engagement with an external thread formation of an associated container.
- the present lightweight closure includes a tamper-evident band at least partially detachably connected to the skirt portion of the closure cap.
- the tamper-evident band is detachably connected to the skirt portion by a plurality of circumferentially spaced frangible bridges, each of which is defined between circumferentially spaced scores that extend into the closure between the skirt portion and the tamper-evident band.
- the development of the present closure has found that use of certain polymeric formulations, having a certain density, can be most cost-effective, while providing the desired level of closure performance.
- the present closure if preferably formed from high-density polyethylene polymer having a density of about 0.945 g/cm to about 0.97 g/cm.
- high-density polyethylene having a density of 0.955 g/cm has been successfully employed.
- the polymer formulation preferably include a nucleator when a colorant is provided in the polymer, to thereby minimize dimensional variations of the closure.
- the polymer also preferably includes approximately 0.2 to 0.3% lubricant, by weight.
- the present closure can be configured as a unitary, one-piece constructions, and to this end, preferably includes integral sealing features for sealing cooperation with the associated container.
- the closure includes a substantially continuous, annular sealing element depending from the top wall portion inwardly of the annular skirt portion of the closure cap.
- the outer seal element is generally annular, and defines a generally inwardly facing sealing surface for engagement with a generally outwardly facing sealing surface of the associated container.
- the sealing performance of the outer seal element is enhanced by provision of a plurality of circumferentially spaced, seal reinforcement elements on the inside surface of the skirt portion radially outwardly of the outer seal element, adjacent the top wall portion of the closure cap.
- the reinforcement elements are engageable by the outer seal element to limit outward deflection of the outer seal element, to thereby enhance sealing cooperation of the outer seal element with the associated container, and improve the impact resistance of the closure.
- the present closure further includes an inner plug seal element depending from the top wall portion of the closure cap.
- the plug seal element is generally cylindrical, and defines an outwardly facing sealing surface for sealing engagement with a generally inwardly facing, inside surface of the associated container.
- the internal thread formation of the closure cap is specifically configured to promote closure performance, while minimizing use of polymeric material.
- the internal thread formation is preferably configured to provide a variation in retention force which decreases in a direction away from the top wall portion of the closure cap. Generally speaking, this is achieved by providing a varying thread geometry for the internal thread formation, with the internal thread formation having a larger cross-section toward the top wall portion of the closure cap to provide more resistive force.
- the present closure has been specifically configured to provide a tamper-indication function, with the tamper-evident band of the closure being detachably connected to the annular skirt portion of the closure cap.
- the tamper-evident band includes an annular band portion depending from the skirt portion that is detachably connected thereto, and an annular inner flange portion extending inwardly from a lower margin of the annular band portion.
- the inner flange portion defines a plurality of circumferentially spaced openings, spaced from a free edge thereof.
- the closure pilfer band has been specifically configured to provide the desired tamper-indication performance, while minimizing the quantity of polymeric material from which the band is formed.
- the tamper-evident band has a maximum outside dimension which is substantially aligned with a maximum outside dimension of the skirt portion at the external knurl portion thereof.
- a closure embodying the principles of the present invention has been found to provide all necessary performance characteristics, with a current embodiment thereof weighing approximately 1 .95g, and having an Aggregate Lightweight Performance Index of at least about 40.
- FIGURE 1 is an exploded, side elevational view, partially cutaway, showing a closure and container package for carbonated products embodying the principles of the present invention
- FIGURE 2 is a cross-sectional view of the closure shown in Figure 1 ;
- FIGURE 3 is a cross-sectional view similar to Figure 2 showing the closure in its configuration after ejection from an associated mold, wherein a tamper- evident band of the closure is unscored, and in an orientation in which it is molded.
- a closure and container package 10 for carbonated or otherwise pressurized contents including a lightweight closure 12 embodying the principles of the present invention, and a container 14 having a threaded neck portion that includes an external, helical thread formation 16.
- the thread formation terminates at an annular locking ring 18, which cooperates with closure 12 for tamper-indication.
- providing effective sealing performance for a closure and container package having carbonated contents can be demanding. Retention of carbonization for extended periods, and under varying temperature conditions, requires careful engineering of the closure 12 to provide the desired performance.
- product quality assurance requires that the package provide reliable tamper-indication, with the closure 12 specifically configured to cooperate with the associated container to provide reliable tamper-evidence.
- closure must be convenient for consumers to use, without requiring excessive application of torque during closure manipulation to effect removal from the associated container.
- the closure must lend itself to high-speed application to the container with automated capping equipment, with very low rates of misapplication.
- closure 12 has been specifically configured to provide the necessary performance characteristics, including sealing performance, while at the same time desirably minimizing the use of polymeric material from which the closure is formed, and the cost associated therewith.
- the closure is specifically configured for reliable tamper-indication attendant to partial or complete removal from the associated container, thus providing the desired quality assurance for consumers.
- closure 12 comprises a unitary, one-piece closure cap 12 having a top wall portion 20, and an annular skirt portion 22 depending from the top wall portion.
- the skirt portion 22 is provided with internal thread formation 24 in the form of a plurality of thread segments which collectively define the internal thread formation.
- the internal thread formation 24 is preferably configured to provide a variable retention force, that is, provide a retention force which decreases in a direction away from the top wall portion 20.
- the thread formation can be configured in accordance with U.S. Patent Publication No. 2012/0091 138, published April 19, 2012, the disclosure of which is hereby incorporated by reference.
- this variation in retention force is achieved by providing portions of the internal thread formation 24 which are further from the top wall portion 20 with a reduced thread profile, as illustrated.
- This preferred configuration of the internal thread formation 24 has desirably been found to improve the strip torque performance of the closure.
- Closure 12 is configured for cooperative, sealing engagement with an associated container 14 of the closure and container package 10.
- the container 14 is shown as having a so-called "CSD finish", that is, a configuration in accordance with industry standards for carbonated soft drinks (this is sometimes designated as an "1881 finish").
- the closure 12 is configured for rotatable, threaded application to and removal from, container 14 by inter-engagement of internal thread formation 24 with external thread formation 16. Convenient manipulation of the closure 12 by consumers is facilitated by the provision of a plurality of axially extending external gripping knurls 26 on the exterior surface of the skirt portion 22.
- the closure is of a unitary construction, and does not include a separate sealing liner element. While a closure configured in accordance with the present invention can include such a separate sealing liner, in the illustrated embodiment, the closure cap is provided with integral sealing features for providing the desired sealing cooperation with the associated container 14.
- the closure 12 includes an inner plug seal element 30 which depends integrally from top wall portion 20.
- the inner plug seal element 30 is generally cylindrical, and defines an outwardly facing sealing surface for sealing engagement with a generally inwardly facing, inside surface of the associated container 14.
- the sealing performance of the closure 12 is achieved by the further provision of an outer seal element 32 depending from top wall portion 20 inwardly of annular skirt portion 22.
- the outer seal element 32 which in the illustrated embodiment has an axial dimension less than the axial dimension of inner plug seal element 30, defines a generally inwardly facing sealing surface for engagement with the generally outwardly facing surface of the associated container 14.
- enhanced sealing performance for the closure 12 is achieved by the provision of a plurality of circumferentially spaced, seal reinforcement elements 34 on the inside surface of skirt portion 22 radially outwardly of outer seal element 32.
- the reinforcement elements 34 are positioned adjacent the top wall portion 22, with the individual reinforcement elements being circumferentially spaced about the interior of the closure 12.
- the reinforcement elements can be configured in accordance with U.S. Patent Publication No. 2013/0175285, and are configured so that the reinforcement elements are engageable by the outer seal element 32 to limit outward deflection of the outer seal element, thus enhancing sealing cooperation of the outer seal element with the associated container 14. Impact resistance is also desirably enhanced.
- closure 12 includes a tamper-evident band 40 which is at least partially detachably connected to the annular skirt portion 22.
- a tamper-evident band 40 includes annular band portion 42 depending from skirt portion 22 to which the band portion is detachably connected.
- the tamper-evident band further includes an annular inner flange portion 44 extending inwardly from the lower margin of the annular band portion 42.
- the inner flange portion 44 defines a plurality of circumferentially spaced openings or windows of 46 which are spaced from an inner free edge of the inner flange portion 44.
- the provision of these openings 46 desirably facilitates folding and inversion of the inner flange portion 44 while the orientation in which it is molded, shown in Figure 3, to its in-use orientation, shown in Figure 2.
- the provision of openings 46 has also been found to desirably enhance the tamper-resistance of the tamper-evident band construction, and facilitates inversion or reorientation of the Flange portion 44 from its molded orientation ( Figure 3) to its orientation ( Figure 2) when the closure is applied to a container.
- the tamper-evident band 40 has a maximum outside dimension which is substantially aligned with a maximum outside dimension of skirt portion 22 at the external knurl pattern 26.
- This arrangement has been found to desirably spread the load during any side impact that can occur during transportation, or conveyance in the closure application line, over as much of the side length of the closure as possible.
- This desirably acts to reduce the stress on the frangible connection between the skirt portion and the tamper-evident band, which desirably limits unintended fracture of the closure, prior to closure removal by consumers.
- the desired frangible connection between the tamper-evident band and skirt portion 22 is provided by a plurality of circumferentially spaced frangible bridges 48 (see Figure 2) extending between the lower margin of skirt portion 22 and annular band portion of 42 of tamper-evident band 40.
- Each of the frangible bridges 48 is defined between circumferentially spaced scores 50 that extend into the closure between the skirt portion and the tamper-evident band.
- the scores 50 are formed by the use of an interrupted scoring knife which has been found to desirably produce fewer stress concentrations on edges perpendicular to loads applied to the closure during application to the associated container, and during transportation and conveyance during closure application.
- Partially cut frangible bridges as are sometimes employed, have been found to produce stress concentrations in direct line with typical loading to which closures are subjected. Therefore, the use of an interrupted knife scoring process results in the closure being able to absorb more load without the band breaking away from the skirt portion of the closure.
- This method of formation is preferred in the context of making the closure as light as possible, since the tamper-evident band has relatively less strength. With lower band strength, the frangible bridges need to be relatively weaker longitudinally so that the band still breaks properly during closure removal by consumers. The reduced stress concentrations and the direction of the load allow the bridges to be longitudinally weaker, while still being sufficiently strong in the lateral direction.
- closure 12 is formed from high-density polyethylene polymer having a density in the range of about 0.945 g/cm to about 0.97 g/cm.
- a polymer designated Dow 1250 DMDA-1250 or DMDC-1250
- Dow Chemical has a density of 0.955 g/cm, with a polymer formulated to include approximately 0.2 to 0.3% lubricant (such as erucamide) by weight.
- the polymer includes a colorant in the range of letdown ratios of 0.5 to 2.0 weight percent, in combination with a let-down ratio of nucleator masterbatch of 0.6-1 .6 weight percent (actual nucleator parts per million: 300 to 800), which desirably reduces and minimizes dimensional variations in the closure, as can occur by the use of polymers having colorance.
- the nucleator is a commercially available additive that seeds the material with sites for crystallization (such as calcium carbonate). Different colors nucleate differently, so the nucleator overpowers to the effect of the colorant and the material becomes crystallized very quickly, and therefore changes less once the closure is ejected from the tooling. The end result is that the closure comes out larger, with less dimensional variation both within and between colors. It has been found that this desirably leads to reduced variation in removal torque performance between different colors.
- the illustrated embodiment of the closure 12 has been configured for an industry standard container finish.
- the closure is configured as a 28 mm closure for a carbonated soft drink bottle finish, sometimes referred to as a 1881 finish.
- the closure 12 includes a top wall portion 20 having a nominal thickness of 0.040 inches, and a nominal skirt portion thickness at the root of the thread formation, of 0.035 inches.
- the height of the closure from the top wall portion 22 to scores 50 has a nominal dimension of 0.466 inches, with the tamper-evident band 40 having a nominal dimension of 0.134 inches.
- a closure configured in accordance with these dimensions, as described herein above, has a weight of no more than about 1 .95g. Notably, this compares very favorably to commercially available closures having weights which vary from 2.2g to 2.45g, with the present closure still meeting sealing and impact resistance performance criteria.
- the closure preferably exhibits an Aggregated Lightweight Performance Index of at least about 40, a Sealing Index greater than about 1 .3, and a Strip Torque Index greater than about 15, as discussed below.
- Performance for the present closure and container package including Carbonated Soft Drink sealing performance, can be evaluated in accordance with the test protocols set forth in US Patent Publication No. 201 1/0024423, published February 3, 201 1 , the disclosure of which is hereby incorporated by reference.
- an aspect of the present invention including the lightweight closure of the package, is achieving the desired performance characteristics, including carbonation retention, while minimizing the quantity of the polymeric material from which the closure is formed.
- a closure and container package embodying the present invention exhibit an Aggregate Lightweight Performance Index (ALPI) of at least about 40.
- API Aggregate Lightweight Performance Index
- the ALPI is calculated from specific performance indices, including Sealing Index (SI) and Strip Torque Index (STI).
- SI Sealing Index
- STI Strip Torque Index
- the Sealing Index is weighted by a factor of twenty (20), and combined with the Strip Torque Index (this reflects the relative importance of the Sealing Index.)
- the Sealing Index for a closure can be determined, in accordance with industry protocols, and the performance testing set forth in US Patent Publication No. 201 1/00224423, wherein the Sealing Index equals the sum of (Average Retained CO2 volume/Initial Fill Volume)/total closure mass, at initial carbonation filling of 4.2, 4.5, and 4.7 volumes, after conditioning at 100 degrees F. for 2 weeks. A volume of carbonation is the amount of CO2 that water will absorb at atmospheric pressure and 60 degrees F.
- the Strip Torque Index equals the average strip torque/total closure mass, at conditioning of 100 degrees F. for 24 hours.
- the following comparative data set forth in Table 1 shows the combination of performance criteria provided by the present closure to exhibit an ALPI of at least about 40.
- the measured Sealing Index and Strip Torque Index were used to calculate an ALPI of at least about 40, specifically 42.24. It will be noted that this level of performance, factoring in closure weight, was significantly beyond levels of performance determined for the comparative, commercially available closures.
- closure In connection with these performance criteria, configuring the closure to include a single lead thread formation is presently preferred, for use on a 28mm closure finish (but not necessarily an 1881 finish.)
- Use of polymer of the specified density range (from about 0.9 grams/cubic centimeter to about 0.97 grams/cubic centimeter, and preferably from about 0.945 grams/cubic centimeter to about 0.97 grams/cubic centimeter) generally excludes higher cost polymers that may exhibit a higher density/higher modulus.
- the performance criteria contemplate use of a bottle or container of a specified material, wall thickness and potential volume that represents typical bottle presently found in the field.
- Randomly select 12 performs or filled and capped 12 bottles
- Closure application equipment i.e., Alcoa single head capper or equivalent; Vibrac Torque Tester in application mode, etc.
- Plastic bottle with appropriate finish use largest commonly sold size, i.e., 1 L or 2L for plastic CSD closures, and i.e., 20 fl. oz./600 ml for NCB Pressurized and Non-Pressurized plastic closures)
Abstract
Description
Claims
Priority Applications (9)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2015523304A JP2015526351A (en) | 2012-07-20 | 2013-07-22 | Lightweight closure and container package |
CN201380038441.4A CN104470817A (en) | 2012-07-20 | 2013-07-22 | Lightweight closure and container package |
AU2013292280A AU2013292280A1 (en) | 2012-07-20 | 2013-07-22 | Lightweight closure and container package |
EP13820631.3A EP2874895A4 (en) | 2012-07-20 | 2013-07-22 | Lightweight closure and container package |
RU2015105810A RU2015105810A (en) | 2012-07-20 | 2013-07-22 | LIGHTweight CUTTER AND PACKAGING PAN |
MX2015000833A MX2015000833A (en) | 2012-07-20 | 2013-07-22 | Lightweight closure and container package. |
KR20157001062A KR20150034725A (en) | 2012-07-20 | 2013-07-22 | Lightweight closure and container package |
ZA2015/00236A ZA201500236B (en) | 2012-07-20 | 2015-01-13 | Lightweight closure and container package |
PH12015500098A PH12015500098A1 (en) | 2012-07-20 | 2015-01-14 | Lightweight closure and container package |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201261673942P | 2012-07-20 | 2012-07-20 | |
US61/673,942 | 2012-07-20 |
Publications (1)
Publication Number | Publication Date |
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WO2014015342A1 true WO2014015342A1 (en) | 2014-01-23 |
Family
ID=49945666
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2013/051524 WO2014015342A1 (en) | 2012-07-20 | 2013-07-22 | Lightweight closure and container package |
Country Status (12)
Country | Link |
---|---|
US (1) | US20140021157A1 (en) |
EP (1) | EP2874895A4 (en) |
JP (1) | JP2015526351A (en) |
KR (1) | KR20150034725A (en) |
CN (1) | CN104470817A (en) |
AU (1) | AU2013292280A1 (en) |
CL (1) | CL2015000117A1 (en) |
MX (1) | MX2015000833A (en) |
PH (1) | PH12015500098A1 (en) |
RU (1) | RU2015105810A (en) |
WO (1) | WO2014015342A1 (en) |
ZA (1) | ZA201500236B (en) |
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2013
- 2013-07-22 CN CN201380038441.4A patent/CN104470817A/en active Pending
- 2013-07-22 WO PCT/US2013/051524 patent/WO2014015342A1/en active Application Filing
- 2013-07-22 MX MX2015000833A patent/MX2015000833A/en unknown
- 2013-07-22 RU RU2015105810A patent/RU2015105810A/en not_active Application Discontinuation
- 2013-07-22 EP EP13820631.3A patent/EP2874895A4/en not_active Withdrawn
- 2013-07-22 KR KR20157001062A patent/KR20150034725A/en not_active Application Discontinuation
- 2013-07-22 AU AU2013292280A patent/AU2013292280A1/en not_active Abandoned
- 2013-07-22 JP JP2015523304A patent/JP2015526351A/en not_active Withdrawn
- 2013-07-22 US US13/947,882 patent/US20140021157A1/en not_active Abandoned
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2015
- 2015-01-13 ZA ZA2015/00236A patent/ZA201500236B/en unknown
- 2015-01-14 PH PH12015500098A patent/PH12015500098A1/en unknown
- 2015-01-16 CL CL2015000117A patent/CL2015000117A1/en unknown
Patent Citations (5)
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US5240980A (en) * | 1991-02-08 | 1993-08-31 | Milliken Research Corporation | Colorants for use in opacified thermoplastic resins |
US6913158B1 (en) * | 1999-11-08 | 2005-07-05 | Crown Cork & Seal Technologies Corporation | Closure cap |
US20070213468A1 (en) * | 2004-05-06 | 2007-09-13 | Wilson Debra R | Polymer Molding Compositions |
US20120091134A1 (en) * | 2010-10-15 | 2012-04-19 | Sohail Sadiq | Tamper-evident closure and package |
US20120091138A1 (en) * | 2010-10-15 | 2012-04-19 | Sohail Sadiq | Plastic closure with enhanced performance |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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EP2784985A1 (en) | 2011-12-29 | 2014-10-01 | Huawei Technologies Co., Ltd. | Cloud computing system and method for managing storage resources therein |
Also Published As
Publication number | Publication date |
---|---|
KR20150034725A (en) | 2015-04-03 |
CN104470817A (en) | 2015-03-25 |
ZA201500236B (en) | 2016-01-27 |
RU2015105810A (en) | 2016-09-10 |
MX2015000833A (en) | 2015-04-08 |
EP2874895A4 (en) | 2016-05-11 |
CL2015000117A1 (en) | 2015-06-26 |
US20140021157A1 (en) | 2014-01-23 |
AU2013292280A1 (en) | 2015-01-29 |
JP2015526351A (en) | 2015-09-10 |
PH12015500098A1 (en) | 2015-03-02 |
EP2874895A1 (en) | 2015-05-27 |
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