WO2014006153A1 - Improved control of permeate flow in a filter - Google Patents

Improved control of permeate flow in a filter Download PDF

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Publication number
WO2014006153A1
WO2014006153A1 PCT/EP2013/064181 EP2013064181W WO2014006153A1 WO 2014006153 A1 WO2014006153 A1 WO 2014006153A1 EP 2013064181 W EP2013064181 W EP 2013064181W WO 2014006153 A1 WO2014006153 A1 WO 2014006153A1
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WO
WIPO (PCT)
Prior art keywords
flow
connecting rod
filter
filter unit
speed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2013/064181
Other languages
French (fr)
Inventor
Tomas Skoglund
Fredrik Innings
Jeanette Lindau
Jan Vos
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tetra Laval Holdings and Finance SA
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Tetra Laval Holdings and Finance SA
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Filing date
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Publication of WO2014006153A1 publication Critical patent/WO2014006153A1/en
Anticipated expiration legal-status Critical
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14Ultrafiltration; Microfiltration
    • B01D61/147Microfiltration
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14Ultrafiltration; Microfiltration
    • B01D61/18Apparatus therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14Ultrafiltration; Microfiltration
    • B01D61/20Accessories; Auxiliary operations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D63/00Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/08Flat membrane modules
    • B01D63/082Flat membrane modules comprising a stack of flat membranes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D65/00Accessories or auxiliary operations, in general, for separation processes or apparatus using semi-permeable membranes
    • B01D65/02Membrane cleaning or sterilisation ; Membrane regeneration
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2321/00Details relating to membrane cleaning, regeneration, sterilization or to the prevention of fouling
    • B01D2321/02Forward flushing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2321/00Details relating to membrane cleaning, regeneration, sterilization or to the prevention of fouling
    • B01D2321/04Backflushing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2321/00Details relating to membrane cleaning, regeneration, sterilization or to the prevention of fouling
    • B01D2321/20By influencing the flow
    • B01D2321/2066Pulsated flow
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2321/00Details relating to membrane cleaning, regeneration, sterilization or to the prevention of fouling
    • B01D2321/20By influencing the flow
    • B01D2321/2083By reversing the flow
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D65/00Accessories or auxiliary operations, in general, for separation processes or apparatus using semi-permeable membranes
    • B01D65/02Membrane cleaning or sterilisation ; Membrane regeneration
    • B01D65/04Membrane cleaning or sterilisation ; Membrane regeneration with movable bodies, e.g. foam balls

Definitions

  • This application relates to an apparatus and a method for controlling microfilters and particularly for controlling microfilters in food procesing for preventing clogging of microfilters.
  • Cross flow membrane filtration technology has been used widely and globally in industry.
  • a feed F is supplied to the cross flow membrane unit, wherein a permeate P exits the unit on the other side of the filter while a retentate R exits the unit on the same side of the filter as the feed F enters.
  • Filtration membranes can be organic, such as polymeric, or inorganic, such as ceramic, depending upon the application.
  • the principles of cross-flow filtration are used in reverse osmosis, i.e. concentration of solutions by removing water, nanofiltration, i.e. concentration of organic components by removal of ions like sodium and chlorine, ultrafiltration, i.e. concentration of large and macromolecules, for example proteins, and microfiltration, i.e. removal of bacteria.
  • reverse osmosis is performed on a plate and frame design, tubular design with polymers, and spiral-wound; nanofiltration is performed in spiral wound; ultrafiltration is performed on plate and frame design, tubular design with polymers, tubular design with ceramics, spiral-wound, and hollow- fibre; and
  • Filters in cross flow membrane filtration are periodically cleaned/washed through backwashing.
  • backwashing the transmembrane pressure is periodically inverted by the use of a secondary pump, so that permeate flows back into the feed, lifting the fouling layer from the surface of the membrane, which is disclosed in Figure. 2.
  • Backwashing results in a pressure increase on the feed/retentate side of the filter, which affects the system negatively.
  • Microfiltration is a membrane technical filtration process which removes contaminants from a fluid (liquid or gas) by passage through a microporous membrane.
  • a typical microfiltration membrane pore size range is 0.1 to 10 micrometres ( ⁇ ).
  • the use of micro filters is widespread in food procesing where the pore size is ideal for separating unwanted dissolved solids, such as pores for example.
  • One technique is to periodically block the forward feed short times periodically allowing the pores to be unclogged as the blocking of the permeate flow will cause a backwards flow that rinses the pores. However, it is difficult to ascertain that the backwards flow will actually occur and it is also hard to control it.
  • Another technique is to periodically push the permeate flow backwards for a short time period for example using a piston
  • the inventors of the present invention have realized, after inventive and insightful reasoning, that by generating a backpulse or a backwards flow (or reverse flow) through a membrane of a filter at a higher speed for a short time, the filter can effectively be rinsed. It is also possible to control the forwards flow through the membrane ensuring that the permeate flow does not stop.
  • the flow can be controlled precisely through a cam that is connected to a connecting rod driving a piston based pumping device.
  • the piston based pumping device may be a piston-pump, or a simple piston in a cylinder, which piston is movable in the cylinder thus creating a two-way flow.
  • Figure 1 illustrates schematic view of a filter unit according to the prior art
  • Figure 2 illustrates schematic view of a filter unit according to the prior art during backwashing
  • Figure 3 illustrates schematic view of a filter unit according to one embodiment of the invention
  • Figure 4 illustrates schematic view of a filter unit according to one embodiment of the invention during backwashing
  • Figure 5 a illustrates a perspective view of a filter unit according to one embodiment of the invention
  • Figure 5b illustrates a cross-sectional view of a filter unit according to one embodiment of the invention
  • Figure 6 shows a schematic view of a filter apparatus according to one embodiment of the teachings of this application.
  • Figure 7 shows a schematic, cross-sectional view of the general structure of a filter apparatus according to one embodiment of the teachings of this application.
  • Figure 8 shows a partial view of a connecting rod arrangement according to one embodiment of the teachings of this application.
  • the present invention relates to an arrangement in a cross flow filtration unit, such as a micro filtration unit, having a feed inlet, a permeate outlet and retentate outlet, for improving performance/washing action of the filter.
  • the filter is preferably inorganic, such as ceramic or silica-based, since organic, such as polymeric, membranes tend to delaminate during backwashing.
  • the present invention pertains to an arrangement in a cross flow filtration unit 30, such as a microfiltration unit, having a feed inlet stream F, a permeate outlet stream P and retentate outlet stream R, in accordance with Figures. 3 and 4, in a dairy system.
  • the filtration unit 30 is positioned in the dairy system for removal of microorganisms and bacteria.
  • the filter unit 30 comprises at least one feed/retentate channel, extending from the inlet to the retentate outlet, through which feed F gradually turns into retentate R, exiting the filter unit 30.
  • the feed/retentate channel extends adjacent a filter 31, such as a microfiltration filter, such that the feed/retentate channel not has to cross the filter 31 on its way from the feed inlet to the retentate outlet.
  • the filter unit 30 further comprises at least one permeate channel, extending from the filter 31 to the permeate outlet. Liquid passing from the feed F over the filter 31 will enter the permeate channel to become permeate P, which in turn exits the filter unit 30 at the permeate outlet.
  • a pressure volume adjusting body 37 is positioned in the feed/retentate channel.
  • the pressure volume adjusting body 37 may in one embodiment be a flexible membrane with hollow inner volume, such as a balloon or balloon-like body. Suitable materials for the balloon or balloon-like body 37 are thus plastics and rubbers. The plastics and rubbers are preferably of food-grade, due to the requirements on food production facilities.
  • the balloon or balloon like body 37 is inflated, such that the balloon or balloon like body 37, in production mode of the dairy system, has a first volume.
  • the first volume may be kept by inflating the balloon or balloon-like body 37 with a suitable gas or liquid, such as air, through a conduit outside the filter unit 30.
  • a suitable gas or liquid such as air
  • the balloon or balloon-like body 37 When the pressure on the feed/retentate side of the filter 31 in the filter unit 30 wants to increase, the balloon or balloon-like body 37 will decrease in volume into a second volume to compensate for the pressure derivate, such that the backflow through the filter 31 and on the feed retentate side not is adversely affected by an increase in pressure. Thus, the liquid volume on the feed F/retentate R side of the filter will effectively be increased. In this way, the pressure on the feed/retentate side of the filter 31 in the filter unit 30 may be kept substantially constant.
  • the pressure volume adjusting body 37 may be a coated sponge-like body with a first volume.
  • the coating of the coated sponge-like body 37 is not permeable to the dairy product. Suitable materials for the coated spongelike body 37 are thus plastics and rubbers. The plastics and rubbers are preferably of food-grade, due to the requirements on food production facilities. Due to the spongelike and compressible core of the sponge-like body 37, the first volume may be kept without application of a pressure through a separate conduit, connected to a pressure supply outside the filter unit 30.
  • the sponge-like body will be compressed during backwash in the same manner as the balloon or balloon-like body described above into a second volume, to compensate for the positive pressure derivate on the feed/retentate side of the filter 31 in the filter unit 30.
  • the structure of the core sponge should be selected such that it - under the circumstances - substantially holds the first volume during production mode, while it during backwashing is compressed into the second volume as a result of positive pressure derivate on the feed/retentate side.
  • a filtration unit 50 in a dairy system comprises several membranes 51 sandwiched between membrane support plates 52, which are arranged in stacks.
  • the membranes may be microfiltration membranes.
  • the feed F is forced through narrow channels 53.
  • the narrow channels 53 may be configured for parallel flow or as a combination of parallel and serial channels.
  • the filter unit 50 comprises at least one feed/retentate channel, extending from the inlet to the retentate outlet, through which feed F gradually turns into retentate R when exiting the filter unit 50.
  • the feed/retentate channel extends adjacent the filter membrane 51, such as a micro filtration filter, such that the feed/retentate channel not has to cross the filter on its way from the feed inlet to the retentate outlet.
  • the filter unit 50 further comprises at least one permeate channel, extending from the filter to the permeate outlet. Liquid passing from the feed F over the filter will enter the permeate channel to become permeate P, which in turn exits the filter unit 50 at the permeate outlet.
  • the filtration unit 50 may be divided into sections, in each of which the flow between pairs of membranes 51 is parallel. The sections are separated by a special membrane support plate 52 in which one hole is closed with a stop disc to reverse the direction of flow, giving serial flow between successive sections.
  • the sizes of the modules may vary, depending on the size and capacity of the dairy system using the filtration unit 50.
  • Retentate channels 54 extend into the filtration unit 50 to intersect with the planes in which the membranes 51 are arranged, sandwiched between membrane support plates 52.
  • the retentate channels 54 may extend perpendicularly to the planes in which the membranes 51 are arranged. These retentate channels 54 provide close proximity to the membranes 51 , while simultaneously providing good volume for the retentate R on its way to leave the filter unit 50.
  • a top support plate 55 and a bottom support plate 56 are arranged. In at least one of these, but also possibly in both, feed inlets and retentate outlets are arranged.
  • a pressure volume adjusting body 57 is positioned.
  • the pressure volume adjusting body 57 may in be a flexible membrane with hollow inner volume, such as the balloon or balloon-like body described above, or the pressure volume adjusting body 57 may be a coated sponge-like body in accordance with above. Suitable materials for the balloon or balloon-like body 31 and/or the coated sponge-like body are plastics and rubbers.
  • the pressure volume adjusting body 57 extends into the filtration unit 50, in said feed/retentate channel 54 to intersect with the planes in which the membranes 51 are arranged, sandwiched between membrane support plates 52.
  • the pressure volume adjusting body 57 may - just as the retentate channels 54 - extend
  • the pressure volume adjusting body 57 is then provided in close proximity to the membranes 51 , whereby it can adjust in volume in fast response and in good correlation with the increased pressure derivate caused by the backwashing.
  • the pressure volume adjusting body 57 is inflated, such that the pressure volume adjusting body 57, in production mode of the dairy system, has a first volume.
  • the first volume may be kept by inflating the pressure volume adjusting body 57 with a suitable gas or liquid, such as air, through a conduit outside the filter unit 50.
  • a suitable gas or liquid such as air
  • the pressure volume adjusting body 57 When the pressure on the feed/retentate side of the filter in the filter unit 50 wants to increase, the pressure volume adjusting body 57 will decrease in volume into a second volume to compensate for the pressure derivate, such that the backflow through the filter membrane 51 and on the feed retentate side not is adversely affected by an increase in pressure. In this way, the pressure on the feed/retentate side of the filter in the filter unit 50 may be kept substantially constant.
  • the present invention relates to a filter
  • volume adjusting body according to the embodiments above can be combined with the embodiments of the filter arrangement for generating a back-pulse of a flow through a membrane of said filter according to the embodiments disclosed below.
  • FIG. 6 shows a filtration system 1 according to the teachings herein.
  • a filter unit 2 comprises a piston based pumping device which is controlled by a connecting rod 3.
  • the connecting rod 3 is driven by a motor 4 to move back and forth (up or down in the figure).
  • the connecting rod 3 moves back and forth (up or down in the figure)
  • the flow through the filter unit 2 is pushed or pumped backwards and forwards correspondingly through the filter membranes of the filter unit 2.
  • TMP Trans Membrane Pressure
  • the filter is preferably a non-polymeric filter, even though traditional polymeric filter membranes commonly used in devices for ultra filtration, nano filtration or reverse osmosis will also work within the context of the invention.
  • non-polymeric filters are less prone to be delaminated by the two-way flow of the device according to embodiments of the invention.
  • the connecting rod 3 is arranged to allow a level of flow in a direction in relation to the distance of the connecting rod 3 from a midpoint of the connecting rod 3.
  • the connecting rod 3 controls the flow so that when the piston is in the bottom-most position the flow is at a maximum forwards flow. When the connecting rod 3 is in its top-most position the flow is at a maximum backwards flow.
  • the connecting rod 3 is controlled to cause a slow forward flow being interrupted with a fast, periodical backward flow or backpulse for a repeated rinsing effect.
  • Figure 7 shows a cutout view of the piston arrangement of figure 6.
  • the arrangement is adapted to provide an improved control of a flow.
  • the connecting rod 3 of figure 6 is springloaded by a spring 5 to push against a cam 6. This causes the movement of the connecting rod 3 to be controlled by the shape of the cam 6.
  • the spring 5 is adapted to be suitable for a 15 to 30 Hz
  • the cam 6 is drivingly connected to the motor 4 of figure 6 through a spindle 7. As the spindle 7 revolves so does the cam 6 and based on the shape or profile of the cam 6 the connecting rod 3 is moved up and down (up and down directions refer to the directions in the figures) causing the forwards and backwards flow accordingly.
  • the cam 6 is shaped to have low profile for most of its circumference enabling a slow forward flow.
  • the low profile is interrupted by a short peak.
  • the low profile causes the connecting rod 3 to drive the piston based pumping device slowly in a forwards direction, while the peak will cause the connecting rod 3 to be raised thereby causing the piston based pumping device to pump the flow backwards for a short time period.
  • the piston based pumping device is solely arranged to generate the backpulse.
  • the piston based pumping device When the piston is moved from a low position the raising the piston, the piston based pumping device causes a reverse or backwards flow. If the peak is short and rises quickly enough the reverse flow will be in the form of a short backpulse.
  • the uppermost (in the figure) surface portion of the cam 6 has a peak, whereas the bottommost (in the figure) surface portion of the cam 6 has a lower profile.
  • the speed and direction of the flow - in either direction - can be precisely controlled.
  • the period of the backward flow is determined by the length of the peak.
  • the speed of the flow is controlled by the height of the cam profile. The lower, the faster the forwards flow, the higher, the faster the backwards flow.
  • cam 6 which has a profile that enables a precise control of the connecting rod 3 and the piston based pumping device so that the flow through the filter membranes of the filter unit 2 can be precisely controlled. This allows for rinsing the pores of the filters of the filter unit 2 and thereby extends the effective life time of the filter unit 2, which extends overall production time. This also leads to a decreased need for cleaning-in-place (CIP) and a decreased need for cleaning chemicals during operation.
  • CIP cleaning-in-place
  • the connecting rod 3 is supported by a first support 8 and a second support 9.
  • the connecting rod 3 is connected to the supports 8 and 9 by bearings 11, 12, 13.
  • the bearings 11, 12, 13 supporting the connecting rod 3 are adapted to cancel side forces, prevent rotation and limit bending forces on the connecting rod 3,
  • the spindle 7 is attached to a casing 10 by pendel bearings 14 (in one specific embodiment the bending of the pendel bearing is 0.3) and to the cam 6 by axial angle contact bearings 15.
  • the system comprising the connecting rod 3 and its drive system can be implemented as a micro-electromechanical system, as in figure 7.
  • the system comprising the connecting rod 3 and its drive system can also be implemented as a pneumatic system.
  • the connecting rod 3 is further arranged with a cam follower 16, see figure 8, which is adapted to operate being subjected to forces up to about 20 kN.
  • the force in the tube (not shown) enclosing the connecting rod 3 is limited to 7 kN to prevent bending of the connecting rod 3.
  • the connecting rod 3 is arranged to drive a piston based pumping device to only cause a backpulse in the transmembrane flow.
  • the flow through the membrane of the filter would also be controlled by other, conventional filter components (not shown).
  • the connecting rod 3 is controllably driven by a hydraulics system. Be regulating the pressure in a hydraulic system operably connected to the connecting rod 3, the connecting rod 3 can be caused to move up and down according to the pressure changes. As the pressure increases in the hydraulic system, the connecting rod 3 is forced upwards and as the pressure decreases, the connecting rod 3 is allowed to retreat downwards, possibly biased by a spring 5.
  • the pressure in the hydraulic system can be affected with a pump or by other means and such means can be controlled by a Programmable Logic Circuit or other control means to increase and decrease the pressure at specific intervals and at specific rates, thereby enabling an accurate and precise control of the movement of the connecting rod 3.
  • a piston based pumping device based filter system is connected to a pipe system for providing the filter unit 2 with feed and for transporting the permeate from the filter unit 2.
  • the small volume of the flow from the piston based pumping device does not significantly affect the overall permeate flow. Simulations have shown that when the pipes transporting the permeate are long, the piston displacement in the piston based pumping device is superimposed on the flow through a filter membrane in the filter unit 2 without affecting the downstream flow in the permeate. This enables a steady delivery of the permeate even though a backwards flow through the membrane is generated for short time periods.
  • the cam 6 is designed to cause a fall time for the TMP of 44 ms and a wait time of 17 ms.
  • the rise time is 6 ms.
  • the fall time is 61 ms and the wait time is 0 ms.
  • the rinsing caused by the backwards or reverse flow depends on at least two factors.
  • the first factor is the maximum negative flow length (s neg ) through the pores.
  • the second factor is the maximum negative flow velocity (v neg ) through the pores.
  • a pore s is the area of the pores
  • Q' r is the negative flow through the membrane
  • V' r is the negative volume of flow through the membrane.
  • V' r V r * (1 - 1/T) - t r * Qaveperm (4)
  • V r Ap Um p * Spump (5)
  • V r A pump is the area of the piston based pumping device
  • S pU mp is the amplitude for the piston based pumping device.
  • a pump is 13 cm 2 and the stroke of the piston is about 0.15 cm.
  • One benefit of the teachings herein is that a precise control of the reverse flow causing the rinsing effect can be achieved.
  • the control is provided through the use of a cam which is simple to design.
  • the lifespan of a filter is thereby effectively increased in a predictable manner.
  • a filtration unit such as the filtration unit 30, 50 having been disclosed with reference to figures 1 to 5, can beneficially be arranged in a filter unit such as the filter unit 2 in the filter apparatus 1 having been disclosed with reference to figures 6 to 8.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Water Supply & Treatment (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)

Description

IMPROVED CONTROL OF PERMEATE FLOW IN A FILTER
TECHNICAL FIELD
This application relates to an apparatus and a method for controlling microfilters and particularly for controlling microfilters in food procesing for preventing clogging of microfilters.
BACKGROUND
Cross flow membrane filtration technology has been used widely and globally in industry. A feed F is supplied to the cross flow membrane unit, wherein a permeate P exits the unit on the other side of the filter while a retentate R exits the unit on the same side of the filter as the feed F enters. Filtration membranes can be organic, such as polymeric, or inorganic, such as ceramic, depending upon the application. The principles of cross-flow filtration are used in reverse osmosis, i.e. concentration of solutions by removing water, nanofiltration, i.e. concentration of organic components by removal of ions like sodium and chlorine, ultrafiltration, i.e. concentration of large and macromolecules, for example proteins, and microfiltration, i.e. removal of bacteria.
Up to this point, reverse osmosis is performed on a plate and frame design, tubular design with polymers, and spiral-wound; nanofiltration is performed in spiral wound; ultrafiltration is performed on plate and frame design, tubular design with polymers, tubular design with ceramics, spiral-wound, and hollow- fibre; and
microfiltration on tubular design with ceramics.
In the field of dairy industry, it has thus been common practice to remove bacteria through microfiltration on tubular design with ceramics. Normally, skim milk is treated in microfiltration, since otherwise also fat would be removed with bacteria.
Filters in cross flow membrane filtration are periodically cleaned/washed through backwashing. In backwashing, the transmembrane pressure is periodically inverted by the use of a secondary pump, so that permeate flows back into the feed, lifting the fouling layer from the surface of the membrane, which is disclosed in Figure. 2. Backwashing results in a pressure increase on the feed/retentate side of the filter, which affects the system negatively.
It would thus be advantageous if maintenance of a microfiltration system could be improved, while simultaneously obtaining higher cost efficiency. It would additionally be advantageous if these positives could be obtained simultaneously as providing a system wherein backwashing is improved.
Microfiltration is a membrane technical filtration process which removes contaminants from a fluid (liquid or gas) by passage through a microporous membrane. A typical microfiltration membrane pore size range is 0.1 to 10 micrometres (μιη). The use of micro filters is widespread in food procesing where the pore size is ideal for separating unwanted dissolved solids, such as pores for example.
In crossflow filtration, the feed is passed across the filter membrane
(tangentially) at positive pressure relative to the permeate side. A proportion of the material which is smaller than the membrane pore size passes through the membrane as permeate or filtrate; everything else is retained on the feed side of the membrane as retentate.
Over time deposition of various components in the feed will build up and accumulate on, within and around the pores. The pores will then become clogged which will cause the flux through the filter to decline and eventually the filter will become blocked. Such membrane fouling thus shortens the time a filter can be actively used.
To prevent, or at least delay, such clogging and thereby increase the time a filter can actively be used, various techniques have been proposed. One technique is to periodically block the forward feed short times periodically allowing the pores to be unclogged as the blocking of the permeate flow will cause a backwards flow that rinses the pores. However, it is difficult to ascertain that the backwards flow will actually occur and it is also hard to control it. Another technique is to periodically push the permeate flow backwards for a short time period for example using a piston
basedpumping device. This will aid in unclogging the pores by causing a rinsing effect. However, such back- flow is difficult to control.
These problems are also present in Ultrafiltration, Nano filtration and Reverse
Osmosis. SUMMARY
It is an object of the teachings of this application to overcome the problems listed above by providing an apparatus to be attached to a filter for generating a back- pulse of a flow through a membrane of said filter, said apparatus comprising means for causing a flow through said membrane in a first direction at a first speed and in a second direction at a second speed, wherein the second speed is not the same as the first speed.
It is also an object of the teachings of this application to overcome the problems listed above by providing a method for controlling a back-pulse generation of a flow through a membrane of said filter comprising causing a flow through said membrane in a first direction at a first speed and in a second direction at a second speed, wherein the second speed is not the same as the first speed. Put in other words, the first speed is different from the second speed.
It is also an object of the teachings of this application to overcome the problems listed above by providing an apparatus to be attached to a filter for generating a back-pulse of a flow through a membrane of said filter, said apparatus comprising a connecting rod wherein the connecting rod is arranged to move in a first direction at a first speed and in a second direction at a second speed, wherein the second speed is not the same as the first speed.
The inventors of the present invention have realized, after inventive and insightful reasoning, that by generating a backpulse or a backwards flow (or reverse flow) through a membrane of a filter at a higher speed for a short time, the filter can effectively be rinsed. It is also possible to control the forwards flow through the membrane ensuring that the permeate flow does not stop. The flow can be controlled precisely through a cam that is connected to a connecting rod driving a piston based pumping device. The piston based pumping device may be a piston-pump, or a simple piston in a cylinder, which piston is movable in the cylinder thus creating a two-way flow.
Other features and advantages of the disclosed embodiments will appear from the following detailed disclosure, from the attached dependent claims as well as from the drawings. Generally, all terms used in the claims are to be interpreted according to their ordinary meaning in the technical field, unless explicitly defined otherwise herein.
All references to "a/an/the [element, device, component, means, step, etc]" are to be interpreted openly as referring to at least one instance of the element, device, component, means, step, etc., unless explicitly stated otherwise. The steps of any method disclosed herein do not have to be performed in the exact order disclosed, unless explicitly stated.
BRIEF DESCRIPTION OF DRAWINGS
The invention will be described in further detail under reference to the accompanying drawings in which:
Figure 1 illustrates schematic view of a filter unit according to the prior art;
Figure 2 illustrates schematic view of a filter unit according to the prior art during backwashing;
Figure 3 illustrates schematic view of a filter unit according to one embodiment of the invention;
Figure 4 illustrates schematic view of a filter unit according to one embodiment of the invention during backwashing;
Figure 5 a illustrates a perspective view of a filter unit according to one embodiment of the invention;
Figure 5b illustrates a cross-sectional view of a filter unit according to one embodiment of the invention;
Figure 6 shows a schematic view of a filter apparatus according to one embodiment of the teachings of this application;
Figure 7 shows a schematic, cross-sectional view of the general structure of a filter apparatus according to one embodiment of the teachings of this application; and
Figure 8 shows a partial view of a connecting rod arrangement according to one embodiment of the teachings of this application.
DETAILED DESCRIPTION The disclosed embodiments will now be described more fully hereinafter with reference to the accompanying drawings, in which certain embodiments of the invention are shown. This invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein; rather, these embodiments are provided by way of example so that this disclosure will be thorough and complete, and will fully convey the scope of the invention to those skilled in the art. Like numbers refer to like elements throughout.
According to one aspect, the present invention relates to an arrangement in a cross flow filtration unit, such as a micro filtration unit, having a feed inlet, a permeate outlet and retentate outlet, for improving performance/washing action of the filter. The filter is preferably inorganic, such as ceramic or silica-based, since organic, such as polymeric, membranes tend to delaminate during backwashing.
More specifically, the present invention pertains to an arrangement in a cross flow filtration unit 30, such as a microfiltration unit, having a feed inlet stream F, a permeate outlet stream P and retentate outlet stream R, in accordance with Figures. 3 and 4, in a dairy system. The filtration unit 30 is positioned in the dairy system for removal of microorganisms and bacteria.
The filter unit 30 comprises at least one feed/retentate channel, extending from the inlet to the retentate outlet, through which feed F gradually turns into retentate R, exiting the filter unit 30. The feed/retentate channel extends adjacent a filter 31, such as a microfiltration filter, such that the feed/retentate channel not has to cross the filter 31 on its way from the feed inlet to the retentate outlet. The filter unit 30 further comprises at least one permeate channel, extending from the filter 31 to the permeate outlet. Liquid passing from the feed F over the filter 31 will enter the permeate channel to become permeate P, which in turn exits the filter unit 30 at the permeate outlet. In the feed/retentate channel a pressure volume adjusting body 37 is positioned.
The pressure volume adjusting body 37 may in one embodiment be a flexible membrane with hollow inner volume, such as a balloon or balloon-like body. Suitable materials for the balloon or balloon-like body 37 are thus plastics and rubbers. The plastics and rubbers are preferably of food-grade, due to the requirements on food production facilities. In use, the balloon or balloon like body 37 is inflated, such that the balloon or balloon like body 37, in production mode of the dairy system, has a first volume. The first volume may be kept by inflating the balloon or balloon-like body 37 with a suitable gas or liquid, such as air, through a conduit outside the filter unit 30. When backwashing of the dairy filter unit 30 of the dairy system is performed, the pressure on the feed/retentate side of the filter unit 30 wants to increase. When the pressure on the feed/retentate side of the filter 31 in the filter unit 30 wants to increase, the balloon or balloon-like body 37 will decrease in volume into a second volume to compensate for the pressure derivate, such that the backflow through the filter 31 and on the feed retentate side not is adversely affected by an increase in pressure. Thus, the liquid volume on the feed F/retentate R side of the filter will effectively be increased. In this way, the pressure on the feed/retentate side of the filter 31 in the filter unit 30 may be kept substantially constant.
In another embodiment, the pressure volume adjusting body 37 may be a coated sponge-like body with a first volume. The coating of the coated sponge-like body 37 is not permeable to the dairy product. Suitable materials for the coated spongelike body 37 are thus plastics and rubbers. The plastics and rubbers are preferably of food-grade, due to the requirements on food production facilities. Due to the spongelike and compressible core of the sponge-like body 37, the first volume may be kept without application of a pressure through a separate conduit, connected to a pressure supply outside the filter unit 30. Simultaneously, the sponge-like body will be compressed during backwash in the same manner as the balloon or balloon-like body described above into a second volume, to compensate for the positive pressure derivate on the feed/retentate side of the filter 31 in the filter unit 30. Thus, the structure of the core sponge should be selected such that it - under the circumstances - substantially holds the first volume during production mode, while it during backwashing is compressed into the second volume as a result of positive pressure derivate on the feed/retentate side.
In Figures. 5a and 5b a filtration unit 50 in a dairy system is disclosed. The filtration unit 50 comprises several membranes 51 sandwiched between membrane support plates 52, which are arranged in stacks. The membranes may be microfiltration membranes. The feed F is forced through narrow channels 53. The narrow channels 53 may be configured for parallel flow or as a combination of parallel and serial channels.
The filter unit 50 comprises at least one feed/retentate channel, extending from the inlet to the retentate outlet, through which feed F gradually turns into retentate R when exiting the filter unit 50. The feed/retentate channel extends adjacent the filter membrane 51, such as a micro filtration filter, such that the feed/retentate channel not has to cross the filter on its way from the feed inlet to the retentate outlet. The filter unit 50 further comprises at least one permeate channel, extending from the filter to the permeate outlet. Liquid passing from the feed F over the filter will enter the permeate channel to become permeate P, which in turn exits the filter unit 50 at the permeate outlet.
The filtration unit 50 may be divided into sections, in each of which the flow between pairs of membranes 51 is parallel. The sections are separated by a special membrane support plate 52 in which one hole is closed with a stop disc to reverse the direction of flow, giving serial flow between successive sections. The sizes of the modules may vary, depending on the size and capacity of the dairy system using the filtration unit 50.
Retentate channels 54 extend into the filtration unit 50 to intersect with the planes in which the membranes 51 are arranged, sandwiched between membrane support plates 52. The retentate channels 54 may extend perpendicularly to the planes in which the membranes 51 are arranged. These retentate channels 54 provide close proximity to the membranes 51 , while simultaneously providing good volume for the retentate R on its way to leave the filter unit 50.
At the top and the bottom, respectively, of the filtration unit 50, a top support plate 55 and a bottom support plate 56 are arranged. In at least one of these, but also possibly in both, feed inlets and retentate outlets are arranged.
In at least one, but possibly two of the feed/retentate channels 54 a pressure volume adjusting body 57 is positioned. The pressure volume adjusting body 57 may in be a flexible membrane with hollow inner volume, such as the balloon or balloon-like body described above, or the pressure volume adjusting body 57 may be a coated sponge-like body in accordance with above. Suitable materials for the balloon or balloon-like body 31 and/or the coated sponge-like body are plastics and rubbers.
The pressure volume adjusting body 57 extends into the filtration unit 50, in said feed/retentate channel 54 to intersect with the planes in which the membranes 51 are arranged, sandwiched between membrane support plates 52. Thus, the pressure volume adjusting body 57 may - just as the retentate channels 54 - extend
perpendicularly to the planes in which the membranes 51 are arranged. The pressure volume adjusting body 57 is then provided in close proximity to the membranes 51 , whereby it can adjust in volume in fast response and in good correlation with the increased pressure derivate caused by the backwashing.
In use, the pressure volume adjusting body 57 is inflated, such that the pressure volume adjusting body 57, in production mode of the dairy system, has a first volume. The first volume may be kept by inflating the pressure volume adjusting body 57 with a suitable gas or liquid, such as air, through a conduit outside the filter unit 50. When backwashing of the dairy filter unit 50 of the dairy system is performed, the pressure on the feed/retentate side of the filter unit 50 wants to increase. When the pressure on the feed/retentate side of the filter in the filter unit 50 wants to increase, the pressure volume adjusting body 57 will decrease in volume into a second volume to compensate for the pressure derivate, such that the backflow through the filter membrane 51 and on the feed retentate side not is adversely affected by an increase in pressure. In this way, the pressure on the feed/retentate side of the filter in the filter unit 50 may be kept substantially constant.
According to another aspect the present invention relates to a filter
arrangement for generating a back-pulse of a flow through a membrane of said filter. The volume adjusting body according to the embodiments above can be combined with the embodiments of the filter arrangement for generating a back-pulse of a flow through a membrane of said filter according to the embodiments disclosed below.
Figure 6 shows a filtration system 1 according to the teachings herein. A filter unit 2 comprises a piston based pumping device which is controlled by a connecting rod 3. In the example embodiment of figure 6 there is a plurality of filter membranes in the filter unit 2 all connected to the same connecting rod 3. This enables for controlling a plurality of filter membranes in the filter unit 2 in an efficient manner. The connecting rod 3 is driven by a motor 4 to move back and forth (up or down in the figure). As the connecting rod 3 moves back and forth (up or down in the figure), the flow through the filter unit 2 is pushed or pumped backwards and forwards correspondingly through the filter membranes of the filter unit 2. As the flow is pushed forwards the TMP (Trans Membrane Pressure) is kept at a high level. The level is dependent on the type of filtration as would be apparent to a skilled person. As the flow is pushed backwards the TMP is allowed to fall.
The filter is preferably a non-polymeric filter, even though traditional polymeric filter membranes commonly used in devices for ultra filtration, nano filtration or reverse osmosis will also work within the context of the invention.
However, non-polymeric filters are less prone to be delaminated by the two-way flow of the device according to embodiments of the invention.
In one embodiment the connecting rod 3 is arranged to allow a level of flow in a direction in relation to the distance of the connecting rod 3 from a midpoint of the connecting rod 3. In the exemplifying embodiment of figure 6, the connecting rod 3 controls the flow so that when the piston is in the bottom-most position the flow is at a maximum forwards flow. When the connecting rod 3 is in its top-most position the flow is at a maximum backwards flow.
To enable an improved prevention of clogging the filters of the filter unit 2, the connecting rod 3 is controlled to cause a slow forward flow being interrupted with a fast, periodical backward flow or backpulse for a repeated rinsing effect.
Figure 7 shows a cutout view of the piston arrangement of figure 6. The arrangement is adapted to provide an improved control of a flow. The connecting rod 3 of figure 6 is springloaded by a spring 5 to push against a cam 6. This causes the movement of the connecting rod 3 to be controlled by the shape of the cam 6. In a specific embodiment, the spring 5 is adapted to be suitable for a 15 to 30 Hz
application. The cam 6 is drivingly connected to the motor 4 of figure 6 through a spindle 7. As the spindle 7 revolves so does the cam 6 and based on the shape or profile of the cam 6 the connecting rod 3 is moved up and down (up and down directions refer to the directions in the figures) causing the forwards and backwards flow accordingly. As can be seen in figure 7, the cam 6 is shaped to have low profile for most of its circumference enabling a slow forward flow. The low profile is interrupted by a short peak. The low profile causes the connecting rod 3 to drive the piston based pumping device slowly in a forwards direction, while the peak will cause the connecting rod 3 to be raised thereby causing the piston based pumping device to pump the flow backwards for a short time period. In an alternative embodiment the piston based pumping device is solely arranged to generate the backpulse. When the piston is moved from a low position the raising the piston, the piston based pumping device causes a reverse or backwards flow. If the peak is short and rises quickly enough the reverse flow will be in the form of a short backpulse.
As can be seen in figure 7, the uppermost (in the figure) surface portion of the cam 6 has a peak, whereas the bottommost (in the figure) surface portion of the cam 6 has a lower profile.
By designing the cam profile the speed and direction of the flow - in either direction - can be precisely controlled. The period of the backward flow is determined by the length of the peak. The speed of the flow is controlled by the height of the cam profile. The lower, the faster the forwards flow, the higher, the faster the backwards flow.
It is thereby possible to design a cam 6 which has a profile that enables a precise control of the connecting rod 3 and the piston based pumping device so that the flow through the filter membranes of the filter unit 2 can be precisely controlled. This allows for rinsing the pores of the filters of the filter unit 2 and thereby extends the effective life time of the filter unit 2, which extends overall production time. This also leads to a decreased need for cleaning-in-place (CIP) and a decreased need for cleaning chemicals during operation.
In figure 7 the connecting rod 3 is supported by a first support 8 and a second support 9. The connecting rod 3 is connected to the supports 8 and 9 by bearings 11, 12, 13. The bearings 11, 12, 13 supporting the connecting rod 3 are adapted to cancel side forces, prevent rotation and limit bending forces on the connecting rod 3, The spindle 7 is attached to a casing 10 by pendel bearings 14 (in one specific embodiment the bending of the pendel bearing is 0.3) and to the cam 6 by axial angle contact bearings 15.
The system comprising the connecting rod 3 and its drive system (spindle, motor) can be implemented as a micro-electromechanical system, as in figure 7. The system comprising the connecting rod 3 and its drive system (spindle 7, motor 4) can also be implemented as a pneumatic system.
The connecting rod 3 is further arranged with a cam follower 16, see figure 8, which is adapted to operate being subjected to forces up to about 20 kN. In one embodiment the force in the tube (not shown) enclosing the connecting rod 3 is limited to 7 kN to prevent bending of the connecting rod 3.
In one embodiment, as mentioned above, the connecting rod 3 is arranged to drive a piston based pumping device to only cause a backpulse in the transmembrane flow. In such an embodiment the flow through the membrane of the filter would also be controlled by other, conventional filter components (not shown).
It should be noted that the up/down movement of the connecting rod 3 and corresponding control of the flow can be reversed to down/up by a corresponding change in the shape of the cam 6.
In an alternative embodiment the connecting rod 3 is controllably driven by a hydraulics system. Be regulating the pressure in a hydraulic system operably connected to the connecting rod 3, the connecting rod 3 can be caused to move up and down according to the pressure changes. As the pressure increases in the hydraulic system, the connecting rod 3 is forced upwards and as the pressure decreases, the connecting rod 3 is allowed to retreat downwards, possibly biased by a spring 5. The pressure in the hydraulic system can be affected with a pump or by other means and such means can be controlled by a Programmable Logic Circuit or other control means to increase and decrease the pressure at specific intervals and at specific rates, thereby enabling an accurate and precise control of the movement of the connecting rod 3.
In one embodiment a piston based pumping device based filter system according to herein is connected to a pipe system for providing the filter unit 2 with feed and for transporting the permeate from the filter unit 2. As the permeate flow has an inertia and the time period for the reveres flow is kept short, the small volume of the flow from the piston based pumping device does not significantly affect the overall permeate flow. Simulations have shown that when the pipes transporting the permeate are long, the piston displacement in the piston based pumping device is superimposed on the flow through a filter membrane in the filter unit 2 without affecting the downstream flow in the permeate. This enables a steady delivery of the permeate even though a backwards flow through the membrane is generated for short time periods.
In one particular embodiment designed for a flux of 45 ml/min with a 15 Hz cam cycle, the cam 6 is designed to cause a fall time for the TMP of 44 ms and a wait time of 17 ms. The rise time is 6 ms. In an alternative embodiment the fall time is 61 ms and the wait time is 0 ms.
The rinsing caused by the backwards or reverse flow depends on at least two factors. The first factor is the maximum negative flow length (sneg) through the pores. The second factor is the maximum negative flow velocity (vneg) through the pores. These can be determined through the following equations:
S„eg = V'r / (1)
and
Figure imgf000013_0001
where Apores is the area of the pores, Q'r is the negative flow through the membrane and V'r is the negative volume of flow through the membrane. V'r and Q'r are determined through:
Q'r = Vr * (l/tr - 1/T) - Qaveperm (3)
and
V'r = Vr * (1 - 1/T) - tr * Qaveperm (4)
where Qaveperm is the average flow of the permeate, Vr is the volume flow of the permeate, tr is the fall time and T is the cycle time. Through these equations it is possible to design the piston based pumping device . For the piston based pumping device driven by the connecting rod 3 we have:
Vr = ApUmp * Spump (5)
where Vr =Apump is the area of the piston based pumping device, and SpUmp is the amplitude for the piston based pumping device. In an embodiment, Apump is 13 cm2 and the stroke of the piston is about 0.15 cm.
The necessary setting for the piston and the piston based pumping device can thus be calculated through:
Spump = (V'r + tr * Qavepenil) / (Apump * (1 - tr/T)) (6).
One benefit of the teachings herein is that a precise control of the reverse flow causing the rinsing effect can be achieved. The control is provided through the use of a cam which is simple to design. The lifespan of a filter is thereby effectively increased in a predictable manner.
It should be noted that a filtration unit, such as the filtration unit 30, 50 having been disclosed with reference to figures 1 to 5, can beneficially be arranged in a filter unit such as the filter unit 2 in the filter apparatus 1 having been disclosed with reference to figures 6 to 8.
The invention has mainly been described above with reference to a few embodiments. However, without further elaboration, it is believed that one skilled in the art can, using the preceding description, utilize the present invention to its fullest extent. The preferred specific embodiments described herein are, therefore, to be construed as merely illustrative and not limitative of the remainder of the description in any way whatsoever. Further, although the present invention has been described above with reference to specific embodiments, it is not intended to be limited to the specific form set forth herein.
In the claims, the term "comprises/comprising" does not exclude the presence of other elements or steps. Additionally, although individual features may be included in different claims, these may possibly advantageously be combined, and the inclusion in different claims does not imply that a combination of features is not feasible and/or advantageous. In addition, singular references do not exclude a plurality. The terms "a", "an", "first", "second" etc do not preclude a plurality.

Claims

1. An apparatus (1) to be attached to a filter unit (2) for generating a back-pulse of a flow through a membrane of said filter unit (2), said apparatus comprising means for causing a connecting rod (3) to move in a first forward direction at a first speed and in a second backwards direction at a second speed, wherein the second speed is not the same as the first speed.
2. The apparatus according to claim 1, wherein said connecting rod (3) is arranged to control said means for causing a flow through a membrane of said filter unit (2).
3. The apparatus according to claim 1 or 2, further comprising means for moving said connecting rod (3), wherein the means for moving said connecting rod (3) comprises a cam (6) wherein the cam (6) has a profile that is designed to drive the connecting rod (3).
4. The apparatus according to claim 3, wherein the cam (6) has a profile that is designed to drive the connecting rod (3).
5. The apparatus according to claim 3 or 4, wherein the connecting rod (3) is arranged to control a piston based pumping device for affecting a reverse flow through a filter membrane of said filter unit (2).
6. The apparatus according to any of claims 3 to 5, wherein the connecting rod (3) is arranged to cause a forwards flow through a membrane of said filter unit (2) at a first flow speed when the piston is driven in said first direction and a reverse flow through a filter membrane of said filter unit (2) at a second flow speed where the second flow speed is higher than the first flow speed.
7. The apparatus according to claim 1 or 2, further comprising means for moving said connecting rod (3), wherein the means for moving said connecting rod (3) comprises a hydraulic system.
8. The apparatus according to any of claims 1 to 7, wherein the connecting rod (3) is arranged to cause a forwards flow through a filter membrane of said filter unit (2) at a first flow speed when the piston is driven in a first direction and a reverse flow through a filter membrane of said filter unit (2) at a second flow speed when the piston is driven in a first direction where the second flow speed is higher than the first flow speed.
9. The apparatus according to any of claims 1 to 8, wherein the apparatus (1) is pneumatic.
10. The apparatus according to any of claims 1 to 9, wherein the apparatus (1) is micro-electromechanical.
11. The apparatus according to any of claims 1 to 10, wherein the apparatus (1) comprises a plurality of filter membranes of the filter unit (2) and the connecting rod (3) is arranged to drive a plurality of pistons, each piston being operably connected to a filter unit (2).
12. The apparatus according to any of claims 1 to 11, wherein a distance between the connecting rod (3) and the filter unit (2) is short to allow for creating said back pulse with only a small flow volume.
13. The apparatus of any of claims 1 to 12, wherein said filter unit is a filtration unit (2, 30, 50) for filtration of a liquid food product, said filtration unit (2, 30, 50) comprising:
a feed inlet (F);
a permeate outlet (P), arranged down streams the feed inlet (F); a filter (31, 51), arranged in between the feed inlet (F) and the permeate outlet (P) to divide the filtration unit (2, 30, 50) into at least a feed side and a permeate side; and
a pressure volume adjusting body (37, 57), capable of varying in volume in response to pressure in the liquid food product.
14. A method for controlling a back-pulse generation of a flow through a filter membrane of said filter unit (2) comprising causing a connecting rod (3) to move in a first direction at a first speed and in a second direction at a second speed, wherein the second speed is not the same as the first speed.
15. The method according to claim 14, further comprising controlling said connecting rod (3) through a cam (6) wherein the cam (6) has a profile that is designed to drive the connecting rod (3) for causing said flow.
16. The method according to claim 14 or 15, further comprising causing the back-pulse by controlling a piston based pumping device with the connecting rod (3) for affecting a reverse flow through a filter membrane of said filter unit (2).
17. The method according to any of claims 14 to 16, further comprising causing a forwards flow through a filter membrane of said filter unit (2) at a first flow speed when the piston (3) is driven in said first direction and a reverse flow through a filter membrane of said filter unit (2) at a second flow speed where the second flow speed is higher than the first flow speed.
PCT/EP2013/064181 2012-07-05 2013-07-04 Improved control of permeate flow in a filter Ceased WO2014006153A1 (en)

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Citations (6)

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Publication number Priority date Publication date Assignee Title
US4592848A (en) * 1984-12-11 1986-06-03 Pabst Richard E Flow through filter with backflush clearing capability
WO2000057997A1 (en) * 1999-03-25 2000-10-05 Technology Finance Corporation (Proprietary) Limited Filtration system suitable for microfiltration, ultrafiltration or reverse osmosis
WO2001010540A2 (en) * 1999-08-05 2001-02-15 Microfiltration Technology Aps A method of cross-flow filtration and a cross-flow filtration installation
NL1020180C1 (en) * 2002-03-15 2003-09-16 Aquamarijn Holding B V Improvement of filter membrane performance, especially for cross flow or dead end filtration, comprises generating very short back pulses during filtration
WO2005081627A2 (en) * 2004-02-26 2005-09-09 Boris Podolsky Crossflow filtration system and method for membrane fouling prevention
WO2008127098A1 (en) * 2007-04-11 2008-10-23 Fluxxion B.V. Crossflow filter with backflushing device

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US4592848A (en) * 1984-12-11 1986-06-03 Pabst Richard E Flow through filter with backflush clearing capability
WO2000057997A1 (en) * 1999-03-25 2000-10-05 Technology Finance Corporation (Proprietary) Limited Filtration system suitable for microfiltration, ultrafiltration or reverse osmosis
WO2001010540A2 (en) * 1999-08-05 2001-02-15 Microfiltration Technology Aps A method of cross-flow filtration and a cross-flow filtration installation
NL1020180C1 (en) * 2002-03-15 2003-09-16 Aquamarijn Holding B V Improvement of filter membrane performance, especially for cross flow or dead end filtration, comprises generating very short back pulses during filtration
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