WO2013045799A3 - Procédé d'extraction a partir de graines de lesquerella - Google Patents

Procédé d'extraction a partir de graines de lesquerella Download PDF

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Publication number
WO2013045799A3
WO2013045799A3 PCT/FR2012/052124 FR2012052124W WO2013045799A3 WO 2013045799 A3 WO2013045799 A3 WO 2013045799A3 FR 2012052124 W FR2012052124 W FR 2012052124W WO 2013045799 A3 WO2013045799 A3 WO 2013045799A3
Authority
WO
WIPO (PCT)
Prior art keywords
seeds
extraction
lesquerella
lesquerella seeds
gums
Prior art date
Application number
PCT/FR2012/052124
Other languages
English (en)
Other versions
WO2013045799A2 (fr
Inventor
Jean-Luc Dubois
Antoine Piccirilli
Julien Magne
Original Assignee
Arkema France
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema France filed Critical Arkema France
Priority to US14/348,491 priority Critical patent/US9220287B2/en
Priority to CN201280058369.7A priority patent/CN103945702B/zh
Priority to EP12775762.3A priority patent/EP2760292A2/fr
Publication of WO2013045799A2 publication Critical patent/WO2013045799A2/fr
Publication of WO2013045799A3 publication Critical patent/WO2013045799A3/fr

Links

Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
    • A23D9/013—Other fatty acid esters, e.g. phosphatides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/007—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids using organic solvents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/02—Pretreatment
    • C11B1/04—Pretreatment of vegetable raw material
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K10/00—Animal feeding-stuffs
    • A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K10/00—Animal feeding-stuffs
    • A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
    • A23K10/37—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/10—Production of fats or fatty oils from raw materials by extracting
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/02—Refining fats or fatty oils by chemical reaction
    • C11B3/04—Refining fats or fatty oils by chemical reaction with acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/10—Refining fats or fatty oils by adsorption
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/12—Refining fats or fatty oils by distillation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/12—Refining fats or fatty oils by distillation
    • C11B3/14—Refining fats or fatty oils by distillation with the use of indifferent gases or vapours, e.g. steam
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/16—Refining fats or fatty oils by mechanical means
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436—Fatty acid esters
    • C12P7/6445—Glycerides
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
    • Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
    • Y02P60/87—Re-use of by-products of food processing for fodder production

Abstract

La présente invention concerne un procédé d'extraction à partir de graines de lesquerella ayant un taux d'acidité inférieur à 6 mg KOH/g, ledit procédé comprenant les étapes suivantes : - une étape i) de conditionnement des graines comprenant une seule opération d'aplatissage et au moins une opération de séchage des graines; - une étape ii) de mise en contact des graines conditionnées avec un mélange d'alcool léger anhydre et de co-solvant dans des conditions de température et de durée suffisantes pour extraire une huile brute comprenant des phospholipides et des gommes d'une part et obtenir un tourteau déshuilé d'autre part.
PCT/FR2012/052124 2011-09-30 2012-09-24 Procédé d'extraction a partir de graines de lesquerella WO2013045799A2 (fr)

Priority Applications (3)

Application Number Priority Date Filing Date Title
US14/348,491 US9220287B2 (en) 2011-09-30 2012-09-24 Lesquerella seed products and method and device for producing same
CN201280058369.7A CN103945702B (zh) 2011-09-30 2012-09-24 用于从雷斯克勒种子中提取的方法
EP12775762.3A EP2760292A2 (fr) 2011-09-30 2012-09-24 Procédé d'extraction a partir de graines de lesquerella

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1158783 2011-09-30
FR1158783A FR2980669B1 (fr) 2011-09-30 2011-09-30 Procede d'extraction a partir de graines de lesquerella

Publications (2)

Publication Number Publication Date
WO2013045799A2 WO2013045799A2 (fr) 2013-04-04
WO2013045799A3 true WO2013045799A3 (fr) 2013-08-15

Family

ID=47071347

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/FR2012/052124 WO2013045799A2 (fr) 2011-09-30 2012-09-24 Procédé d'extraction a partir de graines de lesquerella

Country Status (5)

Country Link
US (1) US9220287B2 (fr)
EP (1) EP2760292A2 (fr)
CN (2) CN107779253A (fr)
FR (1) FR2980669B1 (fr)
WO (1) WO2013045799A2 (fr)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2015023783A1 (fr) 2013-08-13 2015-02-19 Darling Ingredients Inc. Extraction de lipides
CN105176671B (zh) * 2014-06-18 2018-11-30 中国石油化工股份有限公司 一种含油微藻的破壁及助剂辅助提取油脂的方法
WO2016065280A1 (fr) * 2014-10-24 2016-04-28 Darling Ingredients Inc. Extraction de lipides

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010084276A1 (fr) * 2009-01-20 2010-07-29 Arkema France Procede d'obtention d'une fraction enrichie en esters d'acides gras fonctionnalises a partir de graines de plantes oleagineuses
WO2010122265A1 (fr) * 2009-04-24 2010-10-28 Arkema France Biocarburant constitue d'un melange d'esters d'acides gras d'origine naturelle, et procede de fabrication dudit biocarburant
WO2011048339A1 (fr) * 2009-10-23 2011-04-28 Valagro Carbone Renouvelable Poitou-Charentes Procede d'extraction des insaponifiables de matieres premieres renouvelables

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005030911A2 (fr) 2003-09-29 2005-04-07 Petroleo Brasileiro S.A.-Petrobras Procede de production de biogazole
FR2919303B1 (fr) 2007-07-24 2012-11-30 Jean Pierre Esterez Procede de preparation d'esters d'acides gras a partir de flocon de graines oleagineuses.
FR2940804B1 (fr) 2009-01-05 2011-02-25 Arkema France Procede de trituration reactive des graines de ricin
UA111708C2 (uk) * 2009-10-16 2016-06-10 Бандж Ойлз, Інк. Спосіб рафінування олії
FR2955589B1 (fr) 2010-01-26 2013-03-29 Arkema France Procede de trituration reactive des graines de jatropha

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010084276A1 (fr) * 2009-01-20 2010-07-29 Arkema France Procede d'obtention d'une fraction enrichie en esters d'acides gras fonctionnalises a partir de graines de plantes oleagineuses
WO2010122265A1 (fr) * 2009-04-24 2010-10-28 Arkema France Biocarburant constitue d'un melange d'esters d'acides gras d'origine naturelle, et procede de fabrication dudit biocarburant
WO2011048339A1 (fr) * 2009-10-23 2011-04-28 Valagro Carbone Renouvelable Poitou-Charentes Procede d'extraction des insaponifiables de matieres premieres renouvelables

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
CARLSON K D ET AL: "DEGUMMING AND BLEACHING OF LESQUERELLA FENDLERI SEED OIL", JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY, SPRINGER, BERLIN, DE, vol. 70, no. 6, 1 June 1993 (1993-06-01), pages 579 - 582, XP000372555, ISSN: 0003-021X, DOI: 10.1007/BF02545323 *
GOODRUM J W ET AL: "Influence of fatty acid methyl esters from hydroxylated vegetable oils on diesel fuel lubricity", BIORESOURCE TECHNOLOGY, ELSEVIER BV, GB, vol. 96, no. 7, 1 May 2005 (2005-05-01), pages 851 - 855, XP025313252, ISSN: 0960-8524, [retrieved on 20050501], DOI: 10.1016/J.BIORTECH.2004.07.006 *
K. D. CARLSON ET AL: "Analysis of oil and meal fromLesquerella fendleri seed", JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY, vol. 67, no. 7, 1 July 1990 (1990-07-01), pages 438 - 442, XP055010313, ISSN: 0003-021X, DOI: 10.1007/BF02638957 *

Also Published As

Publication number Publication date
CN103945702A (zh) 2014-07-23
CN103945702B (zh) 2018-01-19
EP2760292A2 (fr) 2014-08-06
FR2980669B1 (fr) 2013-09-27
FR2980669A1 (fr) 2013-04-05
US9220287B2 (en) 2015-12-29
WO2013045799A2 (fr) 2013-04-04
US20140242252A1 (en) 2014-08-28
CN107779253A (zh) 2018-03-09

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