WO2012148529A1 - Sugarcane coating - Google Patents
Sugarcane coating Download PDFInfo
- Publication number
- WO2012148529A1 WO2012148529A1 PCT/US2012/025972 US2012025972W WO2012148529A1 WO 2012148529 A1 WO2012148529 A1 WO 2012148529A1 US 2012025972 W US2012025972 W US 2012025972W WO 2012148529 A1 WO2012148529 A1 WO 2012148529A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- hydrogenated
- oil
- composition
- chosen
- stearine
- Prior art date
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Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01C—PLANTING; SOWING; FERTILISING
- A01C1/00—Apparatus, or methods of use thereof, for testing or treating seed, roots, or the like, prior to sowing or planting
- A01C1/06—Coating or dressing seed
Definitions
- the present inventions relate to the treatment of plant material and in particular the treatment of sugarcane stem sections.
- Sugarcane is a gramineous plant of commercial importance for a variety of reasons. For example, sugarcane is used for the production of sugar, Falernum, molasses, rum, cachaga (the national spirit of Brazil), and ethanol for fuel. Further, the biomass that remains after sugarcane crushing can also be used in furnaces and boilers.
- stem sections also known as cane cuttings or parts of a stalk or culms or carretels or seedlings.
- Stem sections may be produced from the stem of a sugarcane plant in any number of ways. For example, they may be formed manually or by a variety of machines. The resulting stem sections usually include several nodes per stem section.
- node means the part of the stem of a plant from which a leaf, branch, or aerial root grows.
- stem sections After stem sections are planted, buds (or gemmas) may emerge at the position of each node. Buds may then grow to yield the crop plant. However, emergence rate, or the rate at which nodes bud to yield crop plants is sometimes poor in sugarcane.
- stem sections are often planted with multiple nodes, e.g., 3, 4 or 5 nodes per stem section. These multi-node stem sections (or long stem sections) may have lengths of about 37 cm, 40 cm or greater.
- long stem sections require larger areas for processing, which increases cost. Further, once cut, long stem sections require large areas to stock material, creating additional cost for the process. Also, the planting of long stem sections requires a high weight of material per hectare, such as 16-18 ton/ha (by mechanical planting) or 12-16 ton/ha (by conventional planting).
- the disclosure includes a method of coating a sugarcane stem section with a composition comprising a fatty acid component and a trigger-release component.
- the disclosure includes a stem section that has been coated with a composition comprising a fatty acid component and a trigger-release component.
- the disclosure includes a method of growing sugarcane comprising planting a stem section that has been coated with a composition comprising a fatty acid component and a trigger-release component.
- the current technology includes a method of treating a sugarcane stem section.
- Figures 1 a and 1 b illustrate side and end views, respectively, of one example of a stem section 2 before a coating has been applied.
- Stem section 2 was prepared by cutting a sugarcane stem to the desired length. Node 4 of stem section 2 is visible in Figure 1 a.
- Exposed vascular bundles (EVB) 6 on one end are visible in Figure 1 b.
- EVB may include the cross-section of the sugarcane stem, including xylem and phloem of the vascular bundles as well as the pith and the cortex. The opposite end of cane cutting 2 will have similar EVB.
- stem sections may include more nodes.
- Treatment involves coating the stem section, e.g. at least one part of the stem section, with a composition comprising a fatty acid component and a trigger-release component.
- a composition includes 50 to 99.5% of the fatty acid component and 0.5 to 30% of the trigger-release component.
- a composition includes 60 to 95% of the fatty acid component and 1 to 30% of the trigger-release component.
- a composition includes 70 to 95% of the fatty acid component and 1 to 30% of the trigger-release component.
- a composition includes 80 to 95% of the fatty acid component and 1 to 20% of the trigger-release component.
- a composition includes 85 to 95% of the fatty acid component and 5 to 15% of the trigger-release component.
- Applicant has found that a trigger-release component concentration up to about 20%, is able to produce highly desirable coating formulation speed; sprayability and handling; shelf life extension; and coating rigidity.
- fatty acid component as utilized herein is intended to include at least one of fatty acids and salts of fatty acids.
- a fatty acid is composed of a hydrocarbon chain (or tail) and a terminal carboxyl group (or head).
- Common biological fatty acids include lauric acid, myristic acid, plamitic acid, stearic acid, arachidic acid, behenic acid, lignoceric acid, palmitoleic acid, oleic acid, linoleic acid, arachidonic acid, and nervonic acid.
- An exemplary fatty acid component will include a triglyceride (also called triacylglycerol).
- Fatty acid components may include any of animal fats, animal oils, vegetable fat, and a vegetable oil. Any of these components may further be hydrogenated and/or fractionated.
- fatty acid components may also include hydrogenated animal fats, hydrogenated animal oils, hydrogenated
- Fatty acid components may also include stearines, tallows, and butters, and hydrogenated stearines, hydrogenated tallows, and hydrogenated butters.
- Hydrogenated oils, fats, stearines, tallows and butters may be produced by chemical reactions that result in the addition of hydrogen.
- oils and fats for example, are hydrogenated using a catalyst, e.g. some form of platinum or nickel, to facilitate the addition of hydrogen.
- Hydrogenated oils, fats, stearines, tallows and butters may include fully hydrogenated products and partially hydrogenated products.
- Fully hydrogenated products include oils, fats, stearines, tallows and butters that have been hydrogenated to complete saturation.
- Partially hydrogenated products include oils, fats, stearines, tallows and butters that have at least some degree of hydrogenation, but that are not fully hydrogenated.
- Stearines include the solids formed from the fractionation of oils or fats. Fractionation is a physical method using the crystallization properties of triglycerides to separate a mixture into a low melting liquid fraction and a high melting liquid fraction. Fractionation may be performed by a variety of methods including dry fractionation, detergent fractionation, and solvent fractionation. Tallows include solids rendered from animal or plant fats or oils using heat. Butters include solids that have been physically separated, e.g. by churning or pressing, from a liquid or paste derived from a plant or animal. Exemplary butters include milk butter and cocoa butter.
- Trigger-release component includes components that facilitate permeability in a sugarcane coating comprising a fatty acid component. Permeability may be facilitated when that coated sugarcane is placed in a soil environment, for example a soil environment having recently received rain fall or irrigation.
- Permeability may include any disintegration in the coat that allows water intake into the sugarcane stem section, for example, at least one of a pore, a plurality of pores, a crack, a plurality of cracks, partial disintegration of the coating, or complete disintegration of the coating.
- Trigger-release components may formulate readily with the fatty acid component to create a composition that coats a sugarcane stem section. Applicant has found that trigger-release components having a hydrophilic-lipophilic balance (HLB) of about 7 to about 15 are suitable in many examples of the composition. Applicant has found that trigger-release components having a HLB of about 8.7 to about 12 are more suitable in many examples of the composition. Applicant believes that molecules having an affinity for both water and the fatty-acid component allow for sufficient dispersion in the composition formulation, e.g., pre-application. Post- application and pre-planting, the hardened composition is storage-stable. Post- planting, the trigger-release components attract moisture in the soil through the coating and into contact with the cane cutting.
- HLB hydrophilic-lipophilic balance
- the trigger-release components allow at least one of: attracting water molecules inside of the coating, and moving fatty acid components from inside the coating to water either in the form of mechanical disintegration and/or micro-encapsulation of some of the fatty acid components.
- Exemplary trigger-release components may include at least one of a lecithin, a polysorbate, a span, a ceteareth, a stearoyi fumarate, a stearoyi lactylate, and a glyceryl stearate.
- Exemplary lechithins may include at least one of YELKIN® DS lechithin, THERMOLEC WFC lechithin, THERMOLEC 200 lechithin, THERMOLEC 57 lechithin and PERFORMIXTM E lechithin available from Archer Daniels Midland Company.
- Exemplary polysorbates may include at least one of polysorbate 20 (tween 20 or polyoxyethylene (20) sorbitan monolaurate; polysorbate 40 (tween 40 or polyoxyethylene (20) sorbitan monopalmitate; polysorbate 60 (tween 60 or polyoxyethylene (20) sorbitan monostearate; polysorbate 80 (tween 80 or
- Exemplary spans may include at lease one of span 20 (sorbitan monolaurate); span 40 (sorbitan monopalmitate); and Arlacel 165 (Croda).
- Exemplary ceteareths may include at least one of ceteareth-2, ceteareth- 3, ceteareth-4, ceteareth-5, ceteareth-6, ceteareth-7, ceteareth-8, ceteareth-9, ceteareth-10, ceteareth-1 1 , ceteareth-12, ceteareth-13, ceteareth-15, ceteareth-16, ceteareth-17, ceteareth-18, ceteareth-20, ceteareth-22, ceteareth-23, ceteareth-25, ceteareth-27, ceteareth-28, ceteareth-29, ceteareth-30, ceteareth-33, ceteareth-34, ceteareth-40, ceteareth-50, ceteareth-55, ceteareth-60, ceteareth-80 and ceteareth- 100.
- Exemplary stearoyl lactylates include sodium stearoyl lactylate, calcium stearoyl lactylate.
- Other examples may include other trigger-release components.
- Examples include other "oil-in-water" emulsifiers having an HLB from 7 to 15, or 8.7 to 12. Applicant notes, however, that such emulsifiers are being used herein in a unexpected way to provide unexpected results.
- emulsifiers are not being used to emulsify oil in water. Again, the fatty acid components are solid when the trigger-release component is acting.
- the fatty acid component will include hydrogenated vegetable oil as a major component, e.g. at least any of greater than 50%, greater than 55%, greater than 60%, greater than 65%, greater than 70%, greater than 75%, greater than 80%, greater than 85%, greater than 90%, and greater than 95%.
- hydrogenated vegetable oils may be used, including, for example, at least one of hydrogenated soybean oil, hydrogenated coconut oil, hydrogenated canola oil, hydrogenated castor oil, hydrogenated corn oil, hydrogenated cotton seed oil, hydrogenated sunflower oil, hydrogenated palm oil, hydrogenated palm kernel oil, and hydrogenated cocoa oil.
- compositions herein may vary. In one example, compositions will have a T m of at least 24 °C. Because compositions may include, for example, a variety of different fatty acids, e.g., of different length, different origin, different saturation, different cis-trans isomers, etc., compositions may melt over a range.
- T m refers to the temperature at which a composition begins to melt
- compositions may have a variety of T m , for example, T m may be within at least one of the following ranges: 24 to 68 °C, 28 to 66 °C, 28 to 64 °C, 28 to 62 °C, 28 to 60 °C, 30 to 60 °C, 32 to 60 °C, 34 to 58 °C, 34 to 56 °C, 34 to 54 °C, and 34 to 52 °C. Further, T m may be at least any temperature falling within any of the noted ranges.
- compositions may be used to coat stem sections in a variety of ways, e.g., in batches or continuously. Coating may be achieved by any combination of spraying, dipping, brushing, smearing, etc., of the composition onto the stem section. Coatings may be applied to the entire stem section or applied to parts of the stem section. In one example, a coating is applied to EVB located on one end of the stem section. In another example, a coating is applied to EVB located on both ends of the stem section. In some situations, a stem section may be hydrated, e.g. by soaking in water, prior to coating. Further, in some situations, a stem section may be treated with a pesticide prior to coating, e.g., by being sprayed, dipped or soaked in a pesticide or pesticidal solution.
- Application rates may vary as needed depending on the amount of surface area per stem section being covered. For example, if only the ends of the stem section are being coated, compositions may be applied at 0.2 to 5 g per stem section. If more of the stem section is being coated, application rates may be increased.
- Methods may also include heating the composition to at least a softening point temperature prior to coating.
- the composition will be heated until it becomes liquid. Heating may be performed in a variety of ways, e.g. water bath, microwave, heating filament, steam, etc. Heating temperatures may vary depending on the T m of the composition.
- Exemplary temperatures include a temperature within at least one of the following ranges: T m ⁇ 1 °C, T m ⁇ 2 °C, T m ⁇ 3 °C, T m + 4 °C, T m + 5 °C, T m + 6 °C, T m + 7 °C, T m + 8 °C, T m + 9 °C, T m + 10 °C, T m + 1 1 °C, T m + 12 °C, T m + 13 °C, T m + 14 °C, and T m + 15 °C, T m + 20 °C, and T m + 25 °C prior to coating.
- Others examples include higher and lower
- Methods may further include allowing the composition to cool to at least ambient temperature or below after coating.
- Coated stem sections may be planted or stored for shipping or planting at a later time.
- compositions were melted in a water bath having a temperature about 5 °C above the T m of the composition or greater. Compositions were applied to the EVB of the stem section at approximately 0.2 to 0.25 g per cut end. Coatings were allowed to harden by cooling and then left in exposed drying trays for several days. Replicate number was 5. Treatments and percent weight loss results are contained in Table 1 below.
- composition coatings provided good moisture loss relative to the negative control.
- Composition coatings also provided comparable moisture loss relative to the positive control (“Oil").
- compositions were melted in a water bath having a temperature about 5 °C above the T m of the composition or greater.
- Approximately 10 ⁇ _ of water soluble blue dye (FD&C Blue #1 , Sensient Technologies, St. Louis, MO USA) was injected into the EVB of the stem section.
- Injected stem sections were coated with invention composition (Invention Example A above at approximately 0.2 to 0.25 g per cut end) and fatty acid component (Control "Oil” above at approximately 0.2 to 0.25 g per cut end). Coatings were allowed to harden by cooling and were stored for 3 days.
- invention composition allow for a quicker coating breakdown when exposed to water, as illustrated by the release of the entrapped dye relative to the fatty acid component coating.
- Figure 3 is a picture of beakers at several minutes, illustrating dye diffusion from an invention composition relative to a fatty acid component coating.
- compositions were melted in a water bath having a temperature about 5 °C above the T m of the composition or greater.
- Stem sections were coated with invention composition (Invention Example A 0.2 to 0.25 g per cut end) and fatty acid component (Control "Oil” at approximately 0.2 to 0.25 g per cut end). Coatings were allowed to harden by cooling. Coated sections were placed in beakers containing approximately 200 ml of H20. Oil sensitive paper (Syngenta AG, Switzerland) was used to test for the presence of oil in the beaker, with color change indicating the presence of oil.
- Results The invention composition allow for a quicker coating
- Figure 4 is a picture of beakers and oil sensitive strips at 45 minutes, illustrating oil diffusion from an invention composition relative to a fatty acid component coating.
- Stem sections having a diameter of approximately 25-30 mm and a length of approximately 50 mm are generated from sugarcane stalks and placed on a conveyor system shown in Figure 5a.
- a nozzle-based spray system is used to apply Invention Example A to stem sections placed on the conveyer. The distance between nozzle and stem sections ranges from about 2 to about 3 inches.
- the formulation is heated to approximately 150 °F and is applied at about 10 to about 15 psi liquid pressure in combination with about 3 to about 5 psi air pressure.
- the composition forme a coating on the section almost immediately upon contact with the section.
- Example A is believed to perform similarly to the control composition based on similar handling properties.
- Figures 5a, 5b and 5c show a control composition coatings formed on a stem section almost immediately after spraying according to the conditions described above. The control coating integrity was found to be high, with good adherence and rigidity.
- the composition may be entirely fatty acid component and trigger-release component.
- the composition may include other components.
- the composition may include a carrier, such as water or alcohol to facilitate any of storage, transport, or application.
- compositions may include fertilizers, pesticides, stabilizers, etc.
- Fatty acid and trigger-release components may vary as needed to accommodate other components.
- the current disclosure is also directed to methods of growing sugarcane.
- a method includes obtaining a stem section having EVB and at least one node, coating the stem section with a composition disclosed herein, and planting the coated stem section.
- Stem sections may be obtained in a variety of ways, for example, by cutting the stalk of a sugarcane plant to the desired length and having the desired number of nodes.
- An exemplary stem section may have one node and be 3 to 4 cm long.
- Methods of growing may further include heating the composition prior to coating, for example, as described above.
- the current disclosure is also directed to sugarcane propagation systems.
- the system includes a stem section having at least one bud and exposed vascular bundles (EVB).
- EVB exposed vascular bundles
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
Claims
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
BR112013021209A BR112013021209A2 (en) | 2011-02-21 | 2012-02-21 | sugar cane coating |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161444925P | 2011-02-21 | 2011-02-21 | |
US61/444,925 | 2011-02-21 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2012148529A1 true WO2012148529A1 (en) | 2012-11-01 |
Family
ID=47072665
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2012/025972 WO2012148529A1 (en) | 2011-02-21 | 2012-02-21 | Sugarcane coating |
Country Status (2)
Country | Link |
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BR (1) | BR112013021209A2 (en) |
WO (1) | WO2012148529A1 (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9986679B2 (en) | 2013-10-31 | 2018-06-05 | Fmc Corporation | Alginate coating for sett treatment |
WO2020002980A1 (en) * | 2018-06-26 | 2020-01-02 | Arcor S.A.I.C. | Plant material coating and preparation procedure |
CN110692481A (en) * | 2019-11-15 | 2020-01-17 | 崇左绿泰生物科技有限公司 | Novel planting method for sugarcane |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4397681A (en) * | 1981-06-08 | 1983-08-09 | Fats And Proteins Research Foundation, Inc. | Foliar antitranspirant |
US20060162249A1 (en) * | 2001-11-23 | 2006-07-27 | Diane Zimmermann | Product for use in agriculture or horticulture |
US7776928B2 (en) * | 2003-03-17 | 2010-08-17 | Hrd Corp. | Wax emulsion coating applications |
US20100257640A1 (en) * | 2007-06-22 | 2010-10-07 | Syngenta Crop Protection, Inc. | Method for growing sugarcane |
-
2012
- 2012-02-21 BR BR112013021209A patent/BR112013021209A2/en not_active Application Discontinuation
- 2012-02-21 WO PCT/US2012/025972 patent/WO2012148529A1/en active Application Filing
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4397681A (en) * | 1981-06-08 | 1983-08-09 | Fats And Proteins Research Foundation, Inc. | Foliar antitranspirant |
US20060162249A1 (en) * | 2001-11-23 | 2006-07-27 | Diane Zimmermann | Product for use in agriculture or horticulture |
US7776928B2 (en) * | 2003-03-17 | 2010-08-17 | Hrd Corp. | Wax emulsion coating applications |
US20100257640A1 (en) * | 2007-06-22 | 2010-10-07 | Syngenta Crop Protection, Inc. | Method for growing sugarcane |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9986679B2 (en) | 2013-10-31 | 2018-06-05 | Fmc Corporation | Alginate coating for sett treatment |
WO2020002980A1 (en) * | 2018-06-26 | 2020-01-02 | Arcor S.A.I.C. | Plant material coating and preparation procedure |
CN110692481A (en) * | 2019-11-15 | 2020-01-17 | 崇左绿泰生物科技有限公司 | Novel planting method for sugarcane |
Also Published As
Publication number | Publication date |
---|---|
BR112013021209A2 (en) | 2016-08-23 |
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