WO2012041918A3 - Process for the manufacture of hydrogen peroxide - Google Patents

Process for the manufacture of hydrogen peroxide Download PDF

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Publication number
WO2012041918A3
WO2012041918A3 PCT/EP2011/066893 EP2011066893W WO2012041918A3 WO 2012041918 A3 WO2012041918 A3 WO 2012041918A3 EP 2011066893 W EP2011066893 W EP 2011066893W WO 2012041918 A3 WO2012041918 A3 WO 2012041918A3
Authority
WO
WIPO (PCT)
Prior art keywords
hydrogen peroxide
radical
manufacture
different
alkylanthraquinone
Prior art date
Application number
PCT/EP2011/066893
Other languages
French (fr)
Other versions
WO2012041918A2 (en
Inventor
Frédérique Jacqueline DESMEDT
Philip Hodge
Francine Janssens
Original Assignee
Solvay Sa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Solvay Sa filed Critical Solvay Sa
Publication of WO2012041918A2 publication Critical patent/WO2012041918A2/en
Publication of WO2012041918A3 publication Critical patent/WO2012041918A3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C01B15/01—Hydrogen peroxide
    • C01B15/022—Preparation from organic compounds
    • C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C07C45/68—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
    • C07C45/69—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by addition to carbon-to-carbon double or triple bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C46/00—Preparation of quinones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C46/00—Preparation of quinones
    • C07C46/02—Preparation of quinones by oxidation giving rise to quinoid structures
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/02—Ortho- or ortho- and peri-condensed systems
    • C07C2603/04—Ortho- or ortho- and peri-condensed systems containing three rings
    • C07C2603/22—Ortho- or ortho- and peri-condensed systems containing three rings containing only six-membered rings
    • C07C2603/24—Anthracenes; Hydrogenated anthracenes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/56—Ring systems containing bridged rings
    • C07C2603/86—Ring systems containing bridged rings containing four rings
    • C07C2603/88—Ethanoanthracenes; Hydrogenated ethanoanthracenes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The present invention relates to a process for the preparation of aqueous hydrogen peroxide from the anthraquinone (AO) loop process, comprising using at least one alkylanthraquinone of formula (I) wherein -R1, R2 and R3 are chosen from H, methyl radical, isopropyl radical, n-propyl radical, and tert-amyl radical, and -at least two of the three groups R1, R2 and R3 are different from H and are different from each other.
PCT/EP2011/066893 2010-09-28 2011-09-28 Process for the manufacture of hydrogen peroxide WO2012041918A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP10181367.3 2010-09-28
EP10181367 2010-09-28

Publications (2)

Publication Number Publication Date
WO2012041918A2 WO2012041918A2 (en) 2012-04-05
WO2012041918A3 true WO2012041918A3 (en) 2012-06-21

Family

ID=43558281

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2011/066893 WO2012041918A2 (en) 2010-09-28 2011-09-28 Process for the manufacture of hydrogen peroxide

Country Status (1)

Country Link
WO (1) WO2012041918A2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106810430A (en) * 2016-11-30 2017-06-09 浙江师范大学 A kind of preparation method of the naphthoquinone derivatives of 2 trifluoromethyl 1,4

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3543208A1 (en) * 2018-03-19 2019-09-25 Solvay Sa Process for manufacturing an aqueous hydrogen peroxide solution
CN114702012B (en) * 2022-04-06 2024-05-03 山东华鲁恒升化工股份有限公司 Working solution, preparation method thereof and application thereof in producing hydrogen peroxide by anthraquinone process

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB943683A (en) * 1959-12-16 1963-12-04 John Martin Taylor Improvements in or relating to the cyclic process for the production of hydrogen peroxide
US6127580A (en) * 1995-09-06 2000-10-03 Basf Aktiengesellschaft Process for the preparation of substituted anthraquinones
US6224845B1 (en) * 1998-06-18 2001-05-01 Solvay S.A. Process for manufacturing an aqueous hydrogen peroxide solution

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3041143A (en) 1959-06-18 1962-06-26 Lynn H Dawsey Production of hydrogen peroxide
US4428923A (en) 1982-11-09 1984-01-31 Degussa Aktiengesellschaft Continuous process for the production of hydrogen peroxide according to the anthraquinone process
DE3732015A1 (en) 1987-09-23 1989-04-06 Basf Ag 2-NEOPENTYLANTHRACHINONE, METHOD FOR PRODUCING 2-NEOPENTYLANTHRACHINONE AND THE USE THEREOF AS A CATALYST FOR H (ARROW DOWN) 2 (ARROW DOWN) O (ARROW DOWN) 2 (ARROW DOWN) MANUFACTURER
DE10038101A1 (en) 2000-08-04 2002-02-14 Degussa Process for the preparation of 2- (4-methyl-3-pentenyl) anthraquinone

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB943683A (en) * 1959-12-16 1963-12-04 John Martin Taylor Improvements in or relating to the cyclic process for the production of hydrogen peroxide
US6127580A (en) * 1995-09-06 2000-10-03 Basf Aktiengesellschaft Process for the preparation of substituted anthraquinones
US6224845B1 (en) * 1998-06-18 2001-05-01 Solvay S.A. Process for manufacturing an aqueous hydrogen peroxide solution

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
EUL W ET AL: "Hydrogen Peroxyde", KIRK OTHMER ENCYCLOPEDIA OF CHEMICAL TECHNOLOGY, XX, XX, 1 January 2001 (2001-01-01), pages 1 - 9, XP002211258 *
GOOR G ET AL: "Ullmann's Encyclopedia of Industrial Chemistry, Fifth Edition", 1 January 1989, ULLMANN'S ENCYCLOPEDIA OF INDUSTRIAL CHEMISTRY. HIGH PERFORMANCE FIBERS TO IMIDAZOLE AND DERIVATIVES; [ULLMANN'S ENCYCLOPEDIA OF INDUSTRIAL CHEMISTRY], WEINHEIM, VCH VERLAG, DE, PAGE(S) 447 - 457, XP002233848 *
LEO A. PAQUETTE ET AL: "Electronic control of stereoselectivity. 6. Directionality of singlet oxygen addition to 1,4-dimethoxynaphthalenes laterally fused to bridged bicyclic systems", THE JOURNAL OF ORGANIC CHEMISTRY, vol. 45, no. 24, 1 November 1980 (1980-11-01), pages 4913 - 4921, XP055002737, ISSN: 0022-3263, DOI: 10.1021/jo01312a019 *
STRUBELL, W. AND BAUMGÄRTEL, H.: "Über p-Cymol und seine Derivate, XXXV. FRIEDEL-CRAFTS-Acylierung mit p-Cymol und Umsetzungen mit 1-Methyl-4-isopropyl-zimtsäure-2", JOURNAL FÜR PRAKTISCHE CHEMIE, vol. 17, 1962, online, pages 326 - 330, XP002666728, DOI: 10.1002/prac.19620170509 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106810430A (en) * 2016-11-30 2017-06-09 浙江师范大学 A kind of preparation method of the naphthoquinone derivatives of 2 trifluoromethyl 1,4
CN106810430B (en) * 2016-11-30 2019-07-30 浙江师范大学 A kind of 2- Trifluoromethyl-1, the preparation method of 4- naphthoquinone derivatives

Also Published As

Publication number Publication date
WO2012041918A2 (en) 2012-04-05

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