WO2011127238A1 - Multi-well interference testing and in-situ reservoir behavior characterization - Google Patents
Multi-well interference testing and in-situ reservoir behavior characterization Download PDFInfo
- Publication number
- WO2011127238A1 WO2011127238A1 PCT/US2011/031514 US2011031514W WO2011127238A1 WO 2011127238 A1 WO2011127238 A1 WO 2011127238A1 US 2011031514 W US2011031514 W US 2011031514W WO 2011127238 A1 WO2011127238 A1 WO 2011127238A1
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- WIPO (PCT)
- Prior art keywords
- pressure
- reservoir
- impulse
- wells
- responses
- Prior art date
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- 238000012360 testing method Methods 0.000 title claims abstract description 15
- 238000012512 characterization method Methods 0.000 title claims description 8
- 238000011065 in-situ storage Methods 0.000 title abstract description 3
- 230000004044 response Effects 0.000 claims abstract description 89
- 238000004891 communication Methods 0.000 claims abstract description 29
- 238000004519 manufacturing process Methods 0.000 claims abstract description 21
- 230000004888 barrier function Effects 0.000 claims abstract description 14
- 238000009826 distribution Methods 0.000 claims abstract description 6
- 238000000034 method Methods 0.000 claims description 35
- 238000012545 processing Methods 0.000 claims description 34
- 230000015572 biosynthetic process Effects 0.000 claims description 21
- 238000005755 formation reaction Methods 0.000 claims description 21
- 239000012530 fluid Substances 0.000 claims description 17
- 238000005553 drilling Methods 0.000 claims description 10
- 238000009530 blood pressure measurement Methods 0.000 claims description 8
- 230000000149 penetrating effect Effects 0.000 claims description 7
- 238000004088 simulation Methods 0.000 claims description 6
- 230000000977 initiatory effect Effects 0.000 claims 3
- 230000008878 coupling Effects 0.000 claims 1
- 238000010168 coupling process Methods 0.000 claims 1
- 238000005859 coupling reaction Methods 0.000 claims 1
- 238000002347 injection Methods 0.000 abstract description 6
- 239000007924 injection Substances 0.000 abstract description 6
- 238000005259 measurement Methods 0.000 abstract description 5
- 230000005540 biological transmission Effects 0.000 description 5
- 230000008569 process Effects 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 230000006399 behavior Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 238000003384 imaging method Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000001934 delay Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 238000004148 unit process Methods 0.000 description 1
Classifications
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B49/00—Testing the nature of borehole walls; Formation testing; Methods or apparatus for obtaining samples of soil or well fluids, specially adapted to earth drilling or wells
- E21B49/008—Testing the nature of borehole walls; Formation testing; Methods or apparatus for obtaining samples of soil or well fluids, specially adapted to earth drilling or wells by injection test; by analysing pressure variations in an injection or production test, e.g. for estimating the skin factor
Definitions
- Wells are drilled in an earth formation to extract the gas, water, and/or hydrocarbons from a reservoir.
- operators may use seismic data, test wells, well logs, and other techniques available in the art.
- the reservoir can be viewed as a large pressure network. Knowing the distribution of pressure in a reservoir can, therefore, be very beneficial for operators as they plan and perform production operations in various wells in the reservoir.
- One technique for determining reservoir pressure uses a repeat formation tester pressure survey. In such a survey, a well-to-well interference test is conducted between a pulse well and an observation well. Details of this technique are disclosed in Lasseter et al.,
- Methods and systems for reservoir characterization use downhole pressure devices deployed in wells penetrating a reservoir. Initially, the pressure devices obtain reference pressure measurements, which are then used to scale later-obtained pressure responses. The arrangement of pressure devices, depths, wells and proposed pressure impulse can also be verified prior to performing a pressure impulse. For example, processing that performs reservoir simulation based on input data can determine if magnitudes of pressure responses of the downhole pressure devices will fall within acceptable limits.
- At least one pressure impulse is initiated at an impulse time in at least one of the wells penetrating the reservoir.
- This impulse can be initiated by producing a pressure drop in the well, performing production from the well, producing a pressure spike in the well, drilling in the well with drilling fluid, injecting treatment fluid in the well, and performing a test in the well.
- the downhole pressure devices coupled to the formations in the wells obtain pressure responses at response times.
- the data is communicated to a central unit using communication equipment. The communication can be done in real-time using satellite, wireless, wired, or any other known technology. Alternatively, the pressure responses, response times, and other data can be stored in memory of the downhole pressure devices for later retrieval and processing.
- communication of the data can be performed in a number of ways, including real-time transmission, transferring data after recovering downhole memory tools, making a wet connect to downhole memory tools for electronic transmission, downloading data through acoustic or optical data transmission with downhole memory tools, or the like.
- processing equipment at the central unit uses the obtained data to process the pressure responses and the response times and obtained pressure responses and times, the central unit can use other data about the reservoir, including depths of the downhole pressure devices, seismic data of the reservoir, information from formation cores of the wells, locations of the wells having the downhole pressure devices, known fluid types in the wells, previous production data of the wells, previous logging data of the wells, and reservoir simulations.
- the processing can determine or verify a number of features of the reservoir, including the reservoir's extent, boundaries, communication, and reserve estimates. Likewise, the processing can determine the pressure distribution in the reservoir and characterize barriers, faults, pools, permeable zones,
- the processing can determine that at least one of the downhole pressure devices has failed to obtain at least one of the pressure responses, even though this well may be producing. This may be used to characterize an obstruction in the reservoir between the well in which the impulse was initiated and the downhole pressure device in one of the other wells.
- the processing can determine that a first of the downhole pressure devices in a first well has obtained pressure responses while a second downhole pressure device in a second well has failed to obtain pressure responses. From this, the processing can characterize the reservoir as having a first poo! associated with the first well and having a second pool associated with the second well.
- the processing can determine that a downhole pressure device in a first well has obtained a first magnitude of pressure responses within a first time interval and a second magnitude of pressure responses within a second time interval. From this, the processing can characterize the reservoir as having a first
- the downhole pressure devices can be deployed at different depths than the depth at which the pressure impulse is initiated. After obtaining responses and times from the initiated impulse, the processing can calculate speeds of pressure wave propagation for the pressure responses of the downhole pressure devices. Based on the calculated speeds, the processing can
- FIG. 1 illustrates a well having a reservoir pressure system according to certain teachings of the present disclosure.
- FIG. 2A shows several adjacent wells in a reservoir having various arrangements of observer locations and an impulse location for characterizing features of the reservoir.
- FIG. 2B is a process for characterizing features of a reservoir using the disclosed reservoir pressure system.
- FIG. 3A shows a plan view of a first arrangement of adjacent wells in a reservoir having various observer locations and an impulse location for characterizing features of the reservoir.
- FIG. 3B shows an example graph of reservoir pressure versus time from the arrangement in Fig. 3A.
- FIG. 4A shows a plan view of a second arrangement of adjacent welis in a reservoir having various observer and impulse locations as well as a barrier in the reservoir.
- FIG. 4B shows an example graph of reservoir pressure versus time from the arrangement in Fig. 4A.
- FIG. 5A shows a plan view of a third arrangement of adjacent wells in a reservoir having various observer and impulse locations as well as isolated pools.
- FIG. 5B shows an example graph of reservoir pressure versus time from the arrangement in Fig. 5A.
- FIG. 6A shows a plan view of a fourth arrangement of adjacent wells in a reservoir having various observer and impulse locations as well as isolated pools with communication paths therebetween.
- FIG. 6B shows an example graph of reservoir pressure versus time from the arrangement in Fig. 6A.
- FIG. 7A shows a side view of a fifth arrangement of adjacent wells in a reservoir having various observer and impulse locations as well as a dome with layers.
- FIG. 7B shows an example graph of reservoir pressure versus time from the arrangement in Fig. 7A.
- FIG. 8A shows a plan view of a sixth arrangement of adjacent welis in a reservoir having various observer and impulse locations as well as an obstruction with communication paths therearound.
- FIG. 8B shows an example graph of reservoir pressure versus time from the arrangement in Fig. 8A.
- FIG. 9A shows a plan view of a seventh arrangement of adjacent wells in a reservoir having various observer and impulse locations.
- FIG. 9B shows an example graph of reservoir pressure versus time from the arrangement in Fig. 9A.
- FIG. 1 illustrates a well 10 having a reservoir pressure system 100 according to certain teachings of the present disclosure.
- the system 100 has a downhole pressure device or tool 110 that deploys in the well 10 and couples with the adjacent formation.
- the tool 110 can be assisted by a non-gravity assisted conveyance 126. Otherwise, the tool 110 can be conveyed by a wireline 124, which in turn can be used for communication purposes.
- the tool 110 could be deployed in the well 10 and left in place without the wireline 124 connected, in which case memory on the tool 110 may record the desired
- the downhole tool 110 can be a formation pressure
- the tool 110 can be any suitable tool used for wireline formation testing, production logging, Logging While
- the downhole tool 110 can be a CompactTM
- Formation Pressure Tester available from Weatherford that can be set to record pressure measurements using a wireline 124 or the like.
- the too! 110 can be set using a logging unit, and the wireline 124 can be anchored to wellhead.
- the logging unit can be removed, and the well 10 can be sealed off at the surface.
- the wireline 124 can be connected to a remote data unit.
- a cable clamp 120 and seal mechanism 122 can hold the wireline 124.
- communication equipment can communicate with the downhole tools 110 in real-time and can send data in real-time using satellite, wireless, wired, or any other known technology.
- a mobile logging unit 35 can connect by a quick connect 128 to the wireline 124 to obtain formation pressure measurements in real-time.
- a logging skid or remote data unit 130 can connect to the wireline 124.
- the unit 130/135 can send real-time data transmissions of the formation pressure measurements to a centralized location 140 having its own data processing capabilities and equipment, such as processing equipment at the centralized location 140 communicatively couples to the communication equipment 130/135 and receives the data to be processed to characterize the reservoir.
- the received data can generally include the time that the impulse was initiated, the pressure responses and times of the downhole pressure devices 1 10, and other suitable data as detailed herein.
- the tool 1 10 With the tool 1 10 deployed downhole and coupied to the formation, the tool 1 10 can measure perturbations or changes in the formation's pressure. These perturbations are produced in an adjacent well passing through the reservoir. As shown in Figure 2A, for example, several adjacent wells 10A-C may be already drilled into a reservoir.
- the system 100 can be used in these existing wells of the reservoir so that new wells do not need to be drilled.
- Each of these wells 10A-C is equipped with a downhole tool 1 10A-C at an observation location 0 A- c for obtaining formation pressure measurements from the reservoir in their respective wells 10A-C.
- An impulse is induced in the reservoir in at least one of the wells ⁇ i.e., impulse well 10A in this example). Pressure pulses or perturbations from this impulse then travel through the reservoir in the formation, and the downhole tools 1 10A-C detect the formation pressures at their locations in reai-time.
- the impulse can be provided by a variety of activities.
- production in the well 10A can induce an impulse (i.e., pressure drop) in the reservoir to be detected at the tools 100A-C.
- drilling in the well 10A with drilling mud and the like can induce the impulse (i.e., pressure spike), in another example, stimulating the well with a frac operation or an injection operation can also produce the impulse.
- testing in the well 10A such as pore pressure or well production tests, can produce the impulse needed.
- the overall process 150 of producing the impulse and detecting existing wells (10A-C) in a reservoir operators select a cluster of observation locations (0 A -c) and one or more impulse locations (Block 152).
- the observation locations (0 A- c) can be situated at horizontal or vertical points in the given wells (10), and the same well 10 can have one or more observation locations (O A- c)-
- at least one impulse location (I) is used at a given time, although multiple wells (10) could have impulse locations (I) and a given well (10) may have multiple impulse locations (I) that act simultaneously or separately.
- Each consideration of how the observation and impulse locations (I, O) are set up in wells (10) of a reservoir depends on what wells (10) are existing, what expected characteristics the reservoir has, and what information is desired from the characterization, as well as other considerations that depend on the implementation. In selecting locations, operators may use existing seismic information, well logs, and other information that has already been used to model the reservoir and formation. Moreover, the arrangement of wells (10) for observation and impulse are selected for providing the best correlations from a cluster of wells in the reservoir.
- operators perform reservoir simulation to determine if magnitude of possible reservoir responses will be within gauge [0042]
- operators initiate the impulse at the impulse location (I) (Block 158), To do this, operators affect one well (i.e., 10A) in the reservoir with a large pressure impulse during oilfield operations related to drilling, production, exploration, or testing.
- the impulse may be from an injection of material added to the reservoir or may be from production (removal) of materials from the reservoir.
- the downhole pressure devices (110) obtain reservoir pressure data at the
- the impulse preferably continues until a real-time response is obtained at the remote devices (1 10). Once obtained, the responses from the devices (1 10) can be transmitted real-time to a central unit (140) and/or may be recorded in memory of the devices (1 0) for later retrieval.
- Processing can use a numerical simulator to model characteristics of the reservoir and can be based on input data, including well locations, pressure responses, depths, known fluid types, seismic data, previous production or logging data, etc. In general, the processing is based on the measured pressure levels, the type of impulse used, the locations/distances/orientations of the observation wells in reservoir, the time between impulse and responses, and other variables depending on the implementation.
- the pressure responses may need to be normalized based on the reference pressure value initially obtained and based on any time lag related to transmission delays in the system (100).
- the processed data is then interpreted to define or confirm the reservoir's extent, boundaries, communication, and reserve estimates. For example, operators can use the processed data to determine the pressure distribution in the reservoir and characterize barriers, faults, pools, permeable zones, communication paths, obstructions, and other features of the reservoir.
- the system (100) directly monitors and measures actual reservoir behavior for effective and efficient reservoir understanding and optimization. In other words, the system (100) obtains direct pressure measurements that are not inferred from other information. Therefore, the resulting characterization of the reservoir is based directly on the fluid pressure as measured in the reservoir and not just by an inferred model obtained through imaging techniques generally used in the art.
- Figure 3A shows a plan view of a first arrangement 10OA having various observer wells (Oi -4 ) surrounding an impulse well (I) for characterizing features of a reservoir.
- the impulse from the impulse well (I) emanates outward to the observations wells (0 -4 ), where the changes in formation pressure can be detected.
- the observations wells (Oi -4 ) are located at various distances (di- ) from the impulse well (I), and the pressure responses detected at the
- Figure 3B shows an example graph 200A of this graph, a single impulse (Po) is produced in the reservoir using production at the impulse well (I).
- the reservoir pressure dips during the single production impulse.
- injection would produce a pressure spike.
- the pressure impulse emanates from the impulse well (I) and travels the distances (di -4 ) to the observations wells (Oi -4 ).
- the observations wells (O 1 -4 ) record pressure drops at various times (ti- ) and with various magnitudes (P1-4). Processing can then use the magnitudes (Pi-4), times (ti-4), and distances (d-i -4 ) involved to measure reservoir features such as the connectivity of the reservoir, the reservoir's path length, the reservoir's extent, and the reservoir's fluid type based on the time of pressure propagation from impulse to observation.
- the pressure responses from the observation wells (Oi -4 ) can be combined with existing seismic data, information from formation cores of the wells, and reservoir simulations, as well as other information to further enhance the characterization of the reservoir. Additionally, one or more of the observations wells (O1-4) can be selected as the impulse well so that another impulse can be performed and measured from other perspectives in the reservoir to further characterize it.
- Figure 4A shows a plan view of a second arrangement 100B of adjacent wells in a reservoir having various observations wells (Oi- ) and an impulse well (I).
- a barrier 20 exists in the reservoir, and operators may not know of this barrier 20, or operators may not know the full extent of this reservoir or whether any communication paths exist through the barrier 20.
- Information about the barrier 20 may be obtained from seismic imaging or other techniques. Yet, the seismic image may not characterize how the barrier affects the reservoir's connectivity, communications, pressure distribution, etc.
- operators use the disclosed system 100 and techniques to determine information about this reservoir and the barrier (production shown) and observed pressure responses at two of the observation wells (Oicept 2 ). Pressure responses are not observed at the other observations wells (0 3-4 ). Processing this data, operators can determine the connectivity and extent of the reservoir as well as confirm the existence and extent of the barrier 20. In this case, there appears to be no communication across the barrier 20.
- Figure 5A shows a plan view of a third arrangement 100C of adjacent wells in a reservoir having various observations wells ( ⁇ 1 - 2 ) and an impulse well (I).
- the reservoir has isolated pools 30 and 35. Operators may not know these pools 30 and 35 exist, or operators may not know the full extent of the reservoir or whether any communication paths exist between the pools 30 and 35.
- the time difference (t 2 - 1 3 ) between responses (P 2 - P3) can then be used to define the different lengths of the paths 32/34. Knowledge of these paths 32/34 can then be used to plan injection operations or the like to better extract fluid from the reservoir with the existing wells.
- FIG. 7A shows a side view of a fifth arrangement 100E of adjacent welis (Wells A, B, & C) in a reservoir.
- a first well (Wei! A) has an observation location (O a ) at a first depth
- a second well (Well B) has a second observation location (OB) at a second depth
- a third well (Well C) has an observation location (Oc) at a third depth.
- the second well (Well B) also has an impulse location (IB) at a depth in this well.
- the reservoir has a dome 40 containing a lower layer 42 of water, an intermediate layer 44 of oil, and an upper layer 46 of gas.
- the observation locations (OA-C) and impulse location (IB) may be positioned at their different depths in the various layers 42, 44, and 46.
- the graph 200E in Figure 7B shows a single impulse (i.e., production at the impulse location I) and observed pressure responses at observation locations (OA-C)-
- OA-C observed pressure responses at observation locations
- the times observed can be synchronized accurately using GPS or other techniques. Operators processing the data can then determine the extent of fluid types using the different speed of pressure wave propagation in the layers 42, 44, and 46 based on the pressure response lags and the like. From this, operators can identify the effectiveness of injection operations, identify fluid level contacts, and reservoir connectivity.
- a sixth arrangement 10OF of adjacent wells in a reservoir has various observation wells (Oi -3 ) and an impulse well (I) as well as an obstruction 50 with communication paths 52/54 therearound. Operators may not know the obstruction 50 exists, or operators may not know the full extent of the reservoir or whether any communication paths exist around the obstruction.
- Figure 9A shows a plan view of a seventh arrangement 100G of adjacent wells in a reservoir having various observation wells ( ⁇ 1.7) and an impulse well (I).
- Figure 9B shows an example graph 200G of the impulse well (I), some of the observation wells ( ⁇ - ⁇ - ⁇ ) monitor pressure responses at various time lags without much difference. From this, operators may seek to optimize in field drilling to drain reservoir and conclude there are too many welis. For example, operators can determine that most of the wells are unnecessary to drain the reservoir.
- Optimal spacing for the reservoir may be the distance between the impulse well (I) and the farthest observation well (0 7 ) and not the current spacing of all the other wells (O 1-6 ) relative to the impulse well (I).
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Abstract
Description
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Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP11766700A EP2556209A1 (en) | 2010-04-07 | 2011-04-07 | Multi-well interference testing and in-situ reservoir behavior characterization |
CA2781567A CA2781567C (en) | 2010-04-07 | 2011-04-07 | Multi-well interference testing and in-situ reservoir behavior characterization |
AU2011237598A AU2011237598A1 (en) | 2010-04-07 | 2011-04-07 | Multi-well interference testing and in-situ reservoir behavior characterization |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US32176910P | 2010-04-07 | 2010-04-07 | |
US61/321,769 | 2010-04-07 |
Publications (1)
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WO2011127238A1 true WO2011127238A1 (en) | 2011-10-13 |
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ID=44761540
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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PCT/US2011/031514 WO2011127238A1 (en) | 2010-04-07 | 2011-04-07 | Multi-well interference testing and in-situ reservoir behavior characterization |
Country Status (5)
Country | Link |
---|---|
US (1) | US20110251796A1 (en) |
EP (1) | EP2556209A1 (en) |
AU (2) | AU2011237598A1 (en) |
CA (1) | CA2781567C (en) |
WO (1) | WO2011127238A1 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107013208A (en) * | 2016-01-27 | 2017-08-04 | 江西云晖生物芯片技术有限公司 | A kind of NEXT series of products MSP430 telecommunication systems |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2009094064A1 (en) * | 2008-01-22 | 2009-07-30 | Exxonmobil Upstream Research Company | Dynamic connectivity analysis |
US9169726B2 (en) | 2009-10-20 | 2015-10-27 | Exxonmobil Upstream Research Company | Method for quantitatively assessing connectivity for well pairs at varying frequencies |
US8614577B2 (en) * | 2011-05-18 | 2013-12-24 | Halliburton Energy Services, Inc. | Automatic anisotropy, azimuth and dip determination from upscaled image log data |
US9133708B2 (en) * | 2011-08-31 | 2015-09-15 | Schlumberger Technology Corporation | Estimation and compensation of pressure and flow induced distortion in mud-pulse telemetry |
WO2013187890A1 (en) | 2012-06-13 | 2013-12-19 | Halliburton Energy Services, Inc. | Apparatus and method for pulse testing a formation |
JP6986358B2 (en) * | 2017-03-29 | 2021-12-22 | 三菱重工業株式会社 | Information processing equipment, information processing methods and programs |
CN110489892B (en) * | 2019-08-23 | 2022-04-05 | 中国石油天然气股份有限公司 | Three-phase coupling reservoir structure description technical method |
US11624277B2 (en) * | 2020-07-20 | 2023-04-11 | Reveal Energy Services, Inc. | Determining fracture driven interactions between wellbores |
CN114060003B (en) * | 2021-11-18 | 2024-02-23 | 中海石油(中国)有限公司海南分公司 | Characterization method for inter-well connectivity of offshore complex fault block oil reservoir |
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2011
- 2011-04-07 US US13/081,689 patent/US20110251796A1/en not_active Abandoned
- 2011-04-07 EP EP11766700A patent/EP2556209A1/en not_active Withdrawn
- 2011-04-07 AU AU2011237598A patent/AU2011237598A1/en not_active Abandoned
- 2011-04-07 CA CA2781567A patent/CA2781567C/en not_active Expired - Fee Related
- 2011-04-07 WO PCT/US2011/031514 patent/WO2011127238A1/en active Application Filing
-
2015
- 2015-10-13 AU AU2015242983A patent/AU2015242983A1/en not_active Abandoned
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US6208586B1 (en) * | 1991-06-14 | 2001-03-27 | Baker Hughes Incorporated | Method and apparatus for communicating data in a wellbore and for detecting the influx of gas |
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Also Published As
Publication number | Publication date |
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CA2781567C (en) | 2015-06-16 |
EP2556209A1 (en) | 2013-02-13 |
CA2781567A1 (en) | 2011-10-13 |
AU2011237598A1 (en) | 2012-06-21 |
US20110251796A1 (en) | 2011-10-13 |
AU2015242983A1 (en) | 2015-11-05 |
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