WO2011064327A3 - Method for continuously producing tertiary butyl ethers of glycerol - Google Patents

Method for continuously producing tertiary butyl ethers of glycerol Download PDF

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Publication number
WO2011064327A3
WO2011064327A3 PCT/EP2010/068294 EP2010068294W WO2011064327A3 WO 2011064327 A3 WO2011064327 A3 WO 2011064327A3 EP 2010068294 W EP2010068294 W EP 2010068294W WO 2011064327 A3 WO2011064327 A3 WO 2011064327A3
Authority
WO
WIPO (PCT)
Prior art keywords
glycerol
tertiary butyl
continuously producing
butyl ethers
producing tertiary
Prior art date
Application number
PCT/EP2010/068294
Other languages
German (de)
French (fr)
Other versions
WO2011064327A2 (en
Inventor
Arno Behr
Alexander Kleyensteiber
Original Assignee
Technische Universität Dortmund
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Technische Universität Dortmund filed Critical Technische Universität Dortmund
Priority to US13/511,689 priority Critical patent/US20130031829A1/en
Priority to EP10794915A priority patent/EP2504305A2/en
Publication of WO2011064327A2 publication Critical patent/WO2011064327A2/en
Publication of WO2011064327A3 publication Critical patent/WO2011064327A3/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00Liquid carbonaceous fuels
    • C10L1/02Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The invention relates to a method for producing a mixture of substances comprising a higher tertiary butyl ether of glycerol, comprising the steps: acid-catalyzed reaction of isobutene with glycerol to form a reaction mixture, and extraction of at least part of the reaction mixture from step a by means of at least one solvent, wherein the solvent or the mixture of solvents comprises an ET(30) value of ≤ 35.0.
PCT/EP2010/068294 2009-11-27 2010-11-26 Method for continuously producing tertiary butyl ethers of glycerol WO2011064327A2 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
US13/511,689 US20130031829A1 (en) 2009-11-27 2010-11-26 Method for continuously producing tertiary butyl ethers of glycerol
EP10794915A EP2504305A2 (en) 2009-11-27 2010-11-26 Method for continuously producing tertiary butyl ethers of glycerol

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102009055928.0 2009-11-27
DE102009055928A DE102009055928A1 (en) 2009-11-27 2009-11-27 Process for the continuous production of glycerine tertiary butyl ethers

Publications (2)

Publication Number Publication Date
WO2011064327A2 WO2011064327A2 (en) 2011-06-03
WO2011064327A3 true WO2011064327A3 (en) 2012-02-02

Family

ID=43927113

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2010/068294 WO2011064327A2 (en) 2009-11-27 2010-11-26 Method for continuously producing tertiary butyl ethers of glycerol

Country Status (4)

Country Link
US (1) US20130031829A1 (en)
EP (1) EP2504305A2 (en)
DE (1) DE102009055928A1 (en)
WO (1) WO2011064327A2 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5903284B2 (en) * 2012-01-26 2016-04-13 花王株式会社 Process for producing polyglycerin alkyl ether mixture
EP2964599A1 (en) 2013-03-07 2016-01-13 Saudi Basic Industries Corporation Process for the etherification of a polyol
CN107207389A (en) * 2015-01-30 2017-09-26 沙特基础工业全球技术有限公司 Method for preparing glycerine tertbutyl ether
DE102018200520A1 (en) 2018-01-15 2019-07-18 Robert Bosch Gmbh A method for providing a solution of the substance in a microfluidic device

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0718270A2 (en) * 1994-12-21 1996-06-26 Wessendorf, Richard, Dr. Process for the preparation of polyol alkyl ethers
US5731476A (en) * 1995-01-13 1998-03-24 Arco Chemical Technology, L.P. Poly ether preparation

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3878227A (en) * 1973-12-07 1975-04-15 Dow Chemical Co Process for making tert.-butyl glycidyl ether
US5308365A (en) * 1993-08-31 1994-05-03 Arco Chemical Technology, L.P. Diesel fuel
US5476971A (en) * 1995-01-13 1995-12-19 Arco Chemical Technology, L.P. Glycerine ditertiary butyl ether preparation
FR2764301B1 (en) * 1997-06-09 1999-07-30 Elf Antar France FUEL COMPOSITION COMPRISING OXYGENIC COMPOUNDS FOR DIESEL ENGINES
FI107526B (en) * 1999-04-13 2001-08-31 Fortum Oil & Gas Oy A process for etherification of olefins
FI110262B (en) * 2000-04-14 2002-12-31 Fortum Oyj Process for the preparation of ether
US7195656B2 (en) * 2003-07-02 2007-03-27 Procter & Gamble Company Method for combustion of pulverized coal with reduced emissions
BRPI0507963A (en) * 2004-02-24 2007-07-17 Inst Francais Du Petrole biofuel manufacturing process; transformation of triglycerides into at least two biofuel families: fatty acid monoesters and glycerol soluble ethers and / or acetals
DE102005016152A1 (en) * 2005-04-07 2006-10-12 Basf Ag Preparation of (co) surfactants by reaction of polyols with olefins

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0718270A2 (en) * 1994-12-21 1996-06-26 Wessendorf, Richard, Dr. Process for the preparation of polyol alkyl ethers
US5731476A (en) * 1995-01-13 1998-03-24 Arco Chemical Technology, L.P. Poly ether preparation

Also Published As

Publication number Publication date
EP2504305A2 (en) 2012-10-03
DE102009055928A1 (en) 2011-06-01
WO2011064327A2 (en) 2011-06-03
US20130031829A1 (en) 2013-02-07

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