WO2010144700A2 - Method and apparatus for high resolution sound speed measurements - Google Patents
Method and apparatus for high resolution sound speed measurements Download PDFInfo
- Publication number
- WO2010144700A2 WO2010144700A2 PCT/US2010/038170 US2010038170W WO2010144700A2 WO 2010144700 A2 WO2010144700 A2 WO 2010144700A2 US 2010038170 W US2010038170 W US 2010038170W WO 2010144700 A2 WO2010144700 A2 WO 2010144700A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- acoustic signal
- borehole
- reflector
- path
- round trip
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
Classifications
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B47/00—Survey of boreholes or wells
- E21B47/10—Locating fluid leaks, intrusions or movements
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B47/00—Survey of boreholes or wells
- E21B47/12—Means for transmitting measuring-signals or control signals from the well to the surface, or from the surface to the well, e.g. for logging while drilling
- E21B47/14—Means for transmitting measuring-signals or control signals from the well to the surface, or from the surface to the well, e.g. for logging while drilling using acoustic waves
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01V—GEOPHYSICS; GRAVITATIONAL MEASUREMENTS; DETECTING MASSES OR OBJECTS; TAGS
- G01V1/00—Seismology; Seismic or acoustic prospecting or detecting
- G01V1/40—Seismology; Seismic or acoustic prospecting or detecting specially adapted for well-logging
Definitions
- the present invention relates to performing sound speed measurements of a fluid disposed in a borehole penetrating the earth. More specifically, the present invention relates to estimating a gas influx into a drilling mud.
- Exploration and production of hydrocarbons generally requires drilling a borehole into an earth formation, which may contain a reservoir of the hydrocarbons.
- Drilling mud is typically pumped through a drill string to lubricate a drill bit at the distal end of the drill string. After lubricating the drill bit, the drilling mud fills the borehole.
- the drilling mud is usually kept under pressure to keep any fluids in the pores of the formation from escaping into the borehole. Thus, at a certain depth in the borehole, the pressure equals the pressure imposed at the surface of the borehole plus the weight of the drilling mud at that depth.
- an apparatus for estimating an influx of a formation fluid into a borehole fluid disposed in a borehole penetrating the earth having: a carrier configured for being conveyed in the borehole; an acoustic transducer disposed at the carrier and configured to at least one of transmit an acoustic signal and receive a reflection of the acoustic signal; a first reflector disposed a first distance from the acoustic transducer and defining a first path having a first round trip distance; a second reflector disposed a second distance from the acoustic transducer and defining a second path having a second round trip distance; and a processor in communication with the acoustic transducer and configured to measure a difference between a first travel time for the acoustic signal traveling the first round trip distance in the borehole fluid and a second travel time for the acoustic signal traveling the second round trip distance in the borehole fluid to estimate the influx of the formation
- a method for estimating an influx of a formation fluid into a borehole fluid disposed in a borehole penetrating the earth includes: conveying a carrier through the borehole, the carrier having an acoustic transducer, a first reflector disposed a first distance from the acoustic transducer and defining a first path having a first round trip distance, and a second reflector disposed a second distance from the acoustic transducer and defining a second path having a second round trip distance, wherein the acoustic transducer, the first reflector, and the second reflector are disposed in the borehole fluid that is in the borehole; transmitting an acoustic signal from the acoustic transducer through the borehole fluid to the first reflector and the second reflector; receiving a first reflected acoustic signal traveling the first path and a second reflected acoustic signal traveling the second path using the acoustic transducer
- a machine-readable medium having stored thereon a program having instructions that when executed perform a method for estimating an influx of a formation fluid into a borehole fluid disposed in a borehole penetrating the earth, the method includes: transmitting an acoustic signal from an acoustic transducer through the borehole fluid to a first reflector defining a first path having a first round trip distance and a second reflector defining a second path having a second round trip distance, wherein the acoustic transducer, the first reflector, and the second reflector are disposed in the borehole fluid that is in the borehole; receiving a first reflected acoustic signal traveling the first path and a second reflected acoustic signal traveling the second path using the acoustic transducer; and measuring a difference between a first travel time for the acoustic signal traveling the first round trip distance in the borehole fluid and a second travel time for the acoustic signal traveling the second round
- FIG. 1 illustrates an exemplary embodiment of an acoustic logging tool disposed in a borehole penetrating the earth
- FIGS. 2A and 2B depict aspects of the acoustic logging tool.
- FIG. 3 presents one example of a method for estimating an influx of a formation fluid into a borehole fluid disposed in a borehole penetrating the earth.
- the techniques which include apparatus and method, provide for high resolution acoustic measurements of the speed of an acoustic signal traveling in the borehole fluid. By detecting a change in the speed, the influx of the formation fluid into the borehole fluid can be estimated down to at least twenty-five parts per million.
- the techniques use an acoustic transducer to transmit and receive an acoustic pulse (i.e., the acoustic signal) through the borehole fluid. Because the acoustic pulse generated by the acoustic transducer can vary slightly from one firing to another firing, the techniques disclose directing a portion of the acoustic pulse towards a near reflector and another portion of the same acoustic pulse towards a far reflector. Good correlations between received waveforms of the acoustic pulse reflected from the near and far reflectors are obtained, in part, because there are no variations in the original firing-pulse waveform for the two reflected waveforms. In one embodiment, the acoustic transducer, the near reflector, and the far reflector are disposed in a logging tool that is conveyed through the borehole filled with the borehole fluid.
- a cross correlation between reflected acoustic signals from the near reflector and the far reflector provide the difference in round trip travel time.
- the cross correlation maximum between the two reflected waveforms is the round trip travel time.
- the difference in round trip distance for the two reflected waveforms is twice the distance between the near reflector and the far reflector.
- the speed of the acoustic signal is calculated from the difference in the round trip distance divided by the difference in round trip travel times for the two reflected waveforms.
- speed data can be collected at equally spaced time intervals (or channels) that are very closely spaced in time.
- the closely spaced time intervals provide for higher resolution acoustic speed measurements. Higher time resolution permits detection of correspondingly smaller amounts of gas influx.
- acoustic signal relates to the pressure amplitude versus time of a sound wave or an acoustic wave traveling in a medium that allows propagation of such waves.
- the acoustic signal can be a pulse.
- acoustic transducer relates to a device for transmitting (i.e., generating) an acoustic signal or receiving an acoustic signal. When receiving the acoustic signal in one embodiment, the acoustic transducer converts the energy of the acoustic signal into electrical energy. The electrical energy has a waveform that is related to a waveform of the acoustic signal.
- cross correlation relates to a measure of how closely two signals resemble each other as a function of time shift.
- the cross correlation associated with a particular time shift is the dot product of the first digitized waveform with the time shifted version of the second digitized waveform.
- the maximum cross correlation occurs for that time shift at which the two waveforms most resemble each other, which means that the maximum cross correlation is the time shift that is equal to the travel time associated with the difference in distance (between the near and far reflectors) that was traveled by the two waveforms.
- the maximum cross correlation is used to calculate the speed of the acoustic signal from distance divided by time.
- polynomial fitting such as Savitzky-Golay techniques
- a truer function maximum can be interpolated from the interpolated zero crossing of the first derivative of the polynomial fit to the cross correlation function.
- FIG. 1 illustrates an exemplary embodiment of an acoustic logging tool 10 disposed in a borehole 2 penetrating the earth 3.
- the borehole 2 contains a borehole fluid 4, which is generally drilling mud.
- the earth 3 includes a formation 5 that has pores, which can contain a formation fluid 6.
- the logging tool 10 in the embodiment of FIG. 1 is disposed at a drill string 11 having a drill bit 12.
- the drill string 11 is rotated by a motor 13 for drilling the borehole 2.
- the logging tool 10 includes an acoustic transducer 7 configured to transmit and receive an acoustic signal 8.
- the logging tool 10 also includes a first reflector 14 spaced a first distance Dl from the acoustic transducer 7 and a second reflector 15 spaced a second distance D2 from the transducer 7.
- the second distance D2 is greater than the first distance Dl.
- the acoustic transducer 7, the first reflector 14, and the second reflector 15 are disposed in a groove 16 in the drill string 11.
- the groove 16 allows the borehole fluid 4 to flow between the acoustic transducer 7 and the reflectors 14 and 15 so that measurements of the speed of the acoustic signal 8 can be performed on the borehole fluid 4 at the depth of the logging tool 10.
- the groove 16 also protects the transducer 7 and the reflectors 14 and 15 from contact with the wall of the borehole 2.
- the first reflector 14 reflects a portion of the acoustic signal 8 back to the acoustic transducer 7 such that the portion makes a round trip from the transducer 7 to the first reflector 14 and back to the transducer 7.
- the roundtrip distance of this portion of the acoustic signal 8 defines a first path.
- another portion of the acoustic signal 8 makes a round trip from the transducer 7 to the second reflector 15 and back to the transducer 7.
- the round trip distance of this other portion of the acoustic signal 8 defines a second path.
- the speed of the acoustic signal 8 can be calculated by dividing the difference in round trip distance (2*(D1-D2) for round trip) by the difference in round trip travel time (T2-T1, where Tl and T2 are the travel times for the acoustic signal 8 traveling the first path and the second path respectively).
- the difference in the round trip distance may also be stated as the distance of the second path minus the distance of the first path.
- an electronic unit 9 is coupled to the acoustic transducer 7.
- the electronic unit 9 can be used to operate the logging tool 10 and/or process data associated with measurements of the speed of the acoustic wave 8.
- the data can also be transmitted as a data signal 17 to a processing system 18 at the surface of the earth 3.
- the processed data can be used to determine if an influx of a formation fluid such as a gas is occurring.
- the processed data can be provided to an operator. Based on the processed data, the operator can make drilling decisions that can prevent a kick or blowout from occurring. Communication of the data with processing system 18 can be via wired drilling pipe or pulsed mud as non-limiting examples.
- FIG. 1 teaches a measurement-while-drilling (MWD) application
- the techniques are equally suited for use in wireline applications and in open-borehole and cased borehole applications.
- FIG. 2 depicts aspects of the acoustic logging tool 10. Shown in FIG. 2A are embodiments of a first path 21 that the acoustic signal 8 follows between the acoustic transducer 7 and the first reflector 14 and a second path 22 that the acoustic signal 8 follows between the transducer 7 and the second reflector 15.
- the first path 21 and the second path 22 can be adjusted using an adjustment device 23.
- the adjustment device 23 is coupled to the first reflector 14 and the second reflector 15. These adjustments allow the same apparatus to be used in drilling fluids that have very different acoustic attenuation.
- a shorter first path 21 and second path 22 would be used for more attenuating drilling fluids, which are usually those that have more suspended solids and therefore have higher mass density.
- the higher mass density drilling fluids are generally used in deeper and/or higher pressure wells.
- the distance difference D2-D1 is fixed and known.
- the adjustment device 23 can be coupled to the acoustic transducer 7.
- the adjustment device 23 includes an adjustment screw 24 coupled to a motor 25 for each of the first reflector 14 and the second reflector 15.
- the distance between the transducer 7 and the reflectors 14 and 15 can be reduced when the borehole fluid 4 is highly attenuating to the acoustic signal 8.
- the distance or step between the first reflector 14 and the second reflector 15 can be increased to improve cross correlation of the two reflected acoustic signals for a given borehole drilling fluid attenuation.
- FIG. 2B illustrates a side view of the acoustic logging tool 10. Specifically, FIG. 2B shows the acoustic transducer 7, the first reflector 14 and the second reflector 15 disposed in the groove 16 to protect these components from contact with the wall of the borehole 2.
- the groove 16 is open to the borehole environment to allow the borehole fluid 4 to flow into the groove 16 and between these components.
- FIG. 3 presents one example of a method 30 for estimating an influx of the formation fluid 6 into the borehole fluid 4 disposed in the borehole 2 penetrating the earth 3.
- the method 30 calls for (step 31) conveying the acoustic logging tool 10 through the borehole 2. Further, the method 30 calls for (step 32) transmitting the acoustic signal 8 from the acoustic transducer 7 through the borehole fluid 5 to the first reflector 14 and the second reflector 15. Further, the method 3 calls for (step 33) receiving the acoustic signal 8 traveling the first path 21 and the acoustic signal 8 traveling the second path 22 using the acoustic transducer 7.
- the method 30 calls for (step 34) measuring a difference between a first travel time for the acoustic signal traveling the first round trip distance in the borehole fluid and a second travel time for the acoustic signal traveling the second round trip distance in the borehole fluid to estimate the influx of the formation fluid.
- the method 30 can also include comparing a current measurement of speed of the acoustic signal 8 to a previous measurement of speed of the acoustic signal 8 to determine any sudden change in the speed that will indicate the influx of gas into the borehole 2.
- the cross correlation between the waveforms of the two reflected acoustic signals can be improved further by using Savitzky-Golay interpolation techniques that allow sub-channel time resolution that provides four or more times finer resolution than the nearest whole channel resolution.
- the Savitzky-Golay interpolation techniques perform a local polynomial regression on a distribution of equally spaced points (e.g., the equally spaced channels or time intervals) to determine the smoothed value for each point.
- the Savitzky- Golay method provides interpolations that improve resolution while reducing noise from the acoustic signal 8 received by the acoustic transducer 7.
- the Savitzky-Golay method is presented in detail in Savitzky and Golay, Analytical Chemistry, Vol. 36, No. 8, July 1964.
- Precision in determining the speed of the acoustic wave 8 can be improved in at least two ways.
- One way is to over-sample the waveforms of the reflected acoustic signal 8. In one embodiment, one hundred samples are taken per full wave such that a 250 KHz acoustic signal would be sampled at 25 MHz.
- Another way to improve precision is by "stacking" or averaging received waveform data over the equally spaced channels. In one example, the data is stacked from 16 to 256 channels to remove timing variations from firing one acoustic pulse to another acoustic pulse.
- the acoustic signal 8 is transmitted and received by one acoustic transducer 7.
- one or more acoustic transducers 7 can be used to transmit the acoustic signal 8.
- one or more acoustic transducers 7 can be used to receive the acoustic signal 8 reflected from the reflectors 14 and 15.
- carrier means any device, device component, combination of devices, media and/or member that may be used to convey, house, support or otherwise facilitate the use of another device, device component, combination of devices, media and/or member.
- the logging tool 10 is one non-limiting example of a carrier.
- Other exemplary non-limiting carriers include drill strings of the coiled tube type, of the jointed pipe type and any combination or portion thereof.
- Other carrier examples include casing pipes, wirelines, wireline sondes, slickline sondes, drop shots, bottom-hole-assemblies, drill string inserts, modules, internal housings and substrate portions thereof.
- various analysis components may be used, including a digital and/or an analog system.
- the digital and/or analog system can be included in the electronic unit 9 or the processing system 18.
- the system may have components such as a processor, storage media, memory, input, output, communications link (wired, wireless, pulsed mud, optical or other), user interfaces, software programs, signal processors (digital or analog) and other such components (such as resistors, capacitors, inductors and others) to provide for operation and analyses of the apparatus and methods disclosed herein in any of several manners well-appreciated in the art.
- teachings may be, but need not be, implemented in conjunction with a set of computer executable instructions stored on a computer readable medium, including memory (ROMs, RAMs), optical (CD-ROMs), or magnetic (disks, hard drives), or any other type that when executed causes a computer to implement the method of the present invention.
- These instructions may provide for equipment operation, control, data collection and analysis and other functions deemed relevant by a system designer, owner, user or other such personnel, in addition to the functions described in this disclosure.
- various other components may be included and called upon for providing for aspects of the teachings herein.
- a mounting bracket e.g., at least one of a generator, a remote supply and a battery
- cooling component e.g., at least one of a generator, a remote supply and a battery
- heating component e.g., magnet, electromagnet, sensor, electrode, transmitter, receiver, transceiver, antenna, controller, optical unit, electrical unit or electromechanical unit
- controller e.g., optical unit, electrical unit or electromechanical unit
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- Physics & Mathematics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Geology (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geophysics (AREA)
- Mining & Mineral Resources (AREA)
- Acoustics & Sound (AREA)
- Remote Sensing (AREA)
- General Physics & Mathematics (AREA)
- Fluid Mechanics (AREA)
- Geochemistry & Mineralogy (AREA)
- Geophysics And Detection Of Objects (AREA)
- Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)
- Measurement Of Mechanical Vibrations Or Ultrasonic Waves (AREA)
Abstract
Description
Claims
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201080033624.3A CN102803652B (en) | 2009-06-12 | 2010-06-10 | Method and device for high-resolution sound velocity measurement |
| AU2010258643A AU2010258643B2 (en) | 2009-06-12 | 2010-06-10 | Method and apparatus for estimating an influx of a formation fluid into a borehole fluid. |
| CA2765528A CA2765528A1 (en) | 2009-06-12 | 2010-06-10 | Method and apparatus for high resolution sound speed measurements |
| EA201101697A EA021075B1 (en) | 2009-06-12 | 2010-06-10 | Method and apparatus for high resolution sound speed measurements |
| GB1121973.0A GB2483594B (en) | 2009-06-12 | 2010-06-10 | Method and apparatus for estimating an influx of a formation fluid into a borehole fluid. |
| NO20111728A NO20111728A1 (en) | 2009-06-12 | 2011-12-16 | Method and apparatus for high-resolution sound speed paints |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US18654209P | 2009-06-12 | 2009-06-12 | |
| US61/186,542 | 2009-06-12 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| WO2010144700A2 true WO2010144700A2 (en) | 2010-12-16 |
| WO2010144700A3 WO2010144700A3 (en) | 2011-03-10 |
Family
ID=43306325
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/US2010/038170 Ceased WO2010144700A2 (en) | 2009-06-12 | 2010-06-10 | Method and apparatus for high resolution sound speed measurements |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20100315900A1 (en) |
| CN (1) | CN102803652B (en) |
| AU (1) | AU2010258643B2 (en) |
| CA (1) | CA2765528A1 (en) |
| EA (1) | EA021075B1 (en) |
| GB (1) | GB2483594B (en) |
| NO (1) | NO20111728A1 (en) |
| WO (1) | WO2010144700A2 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103485765A (en) * | 2012-06-12 | 2014-01-01 | 辽宁瑞达石油技术有限公司 | Oil-water distribution tester and oil-water distribution test method |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9109433B2 (en) | 2005-08-01 | 2015-08-18 | Baker Hughes Incorporated | Early kick detection in an oil and gas well |
| EP2724182A4 (en) | 2011-06-22 | 2016-01-13 | Piezotech Llc | System and device for acoustic measuring in a medium |
| US9366133B2 (en) | 2012-02-21 | 2016-06-14 | Baker Hughes Incorporated | Acoustic standoff and mud velocity using a stepped transmitter |
| US9556723B2 (en) * | 2013-12-09 | 2017-01-31 | Baker Hughes Incorporated | Geosteering boreholes using distributed acoustic sensing |
| GB2554216A (en) * | 2015-05-22 | 2018-03-28 | Halliburton Energy Services Inc | Measuring frequency-dependent acoustic attenuation |
| CN105954357B (en) * | 2016-04-25 | 2019-10-11 | 宏大矿业有限公司 | Method that is a kind of while measuring the horizontal rock mass velocity of sound of multi-step |
| EP3469186B1 (en) * | 2016-06-22 | 2021-04-21 | Saudi Arabian Oil Company | Systems and methods for mapping hydrocarbon reservoirs using electromagnetic transmissions |
| RU2658697C1 (en) * | 2017-02-17 | 2018-06-22 | Олег Николаевич Журавлев | Monitoring method for horizontal or directional production or injection boreholes |
| US11359488B2 (en) * | 2019-03-12 | 2022-06-14 | Baker Hughes Oilfield Operations Llc | Self-calibrated method of determining borehole fluid acoustic properties |
| US20210109065A1 (en) * | 2019-10-14 | 2021-04-15 | Halliburton Energy Services, Inc. | Well tool for measuring acoustic velocity |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2598817B1 (en) * | 1986-05-16 | 1988-07-15 | Elf Aquitaine | VERY HIGH RESOLUTION SEISMIC PROSPECTION PROCESS IN HORIZONTAL DRILLING. |
| EP0552048B1 (en) * | 1992-01-16 | 1999-04-21 | Hamamatsu Photonics K.K. | A system for measuring timing relationship between two or more signals |
| US5341345A (en) * | 1993-08-09 | 1994-08-23 | Baker Hughes Incorporated | Ultrasonic stand-off gauge |
| US6988566B2 (en) * | 2002-02-19 | 2006-01-24 | Cdx Gas, Llc | Acoustic position measurement system for well bore formation |
| US6618322B1 (en) * | 2001-08-08 | 2003-09-09 | Baker Hughes Incorporated | Method and apparatus for measuring acoustic mud velocity and acoustic caliper |
| US20040095847A1 (en) * | 2002-11-18 | 2004-05-20 | Baker Hughes Incorporated | Acoustic devices to measure ultrasound velocity in drilling mud |
| WO2004074625A1 (en) * | 2003-02-18 | 2004-09-02 | Baker Hughes Incorporated | Radially adjustable downhhole devices & methods for same |
| US7377169B2 (en) * | 2004-04-09 | 2008-05-27 | Shell Oil Company | Apparatus and methods for acoustically determining fluid properties while sampling |
| US7523640B2 (en) * | 2005-08-01 | 2009-04-28 | Baker Hughes Incorporated | Acoustic fluid analyzer |
| US20080047337A1 (en) * | 2006-08-23 | 2008-02-28 | Baker Hughes Incorporated | Early Kick Detection in an Oil and Gas Well |
| US20090078411A1 (en) * | 2007-09-20 | 2009-03-26 | Kenison Michael H | Downhole Gas Influx Detection |
-
2010
- 2010-06-09 US US12/796,817 patent/US20100315900A1/en not_active Abandoned
- 2010-06-10 CN CN201080033624.3A patent/CN102803652B/en not_active Expired - Fee Related
- 2010-06-10 EA EA201101697A patent/EA021075B1/en not_active IP Right Cessation
- 2010-06-10 GB GB1121973.0A patent/GB2483594B/en not_active Expired - Fee Related
- 2010-06-10 CA CA2765528A patent/CA2765528A1/en not_active Abandoned
- 2010-06-10 WO PCT/US2010/038170 patent/WO2010144700A2/en not_active Ceased
- 2010-06-10 AU AU2010258643A patent/AU2010258643B2/en not_active Ceased
-
2011
- 2011-12-16 NO NO20111728A patent/NO20111728A1/en not_active Application Discontinuation
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103485765A (en) * | 2012-06-12 | 2014-01-01 | 辽宁瑞达石油技术有限公司 | Oil-water distribution tester and oil-water distribution test method |
Also Published As
| Publication number | Publication date |
|---|---|
| EA201101697A1 (en) | 2012-07-30 |
| AU2010258643A1 (en) | 2012-01-19 |
| GB2483594B (en) | 2014-03-19 |
| NO20111728A1 (en) | 2012-01-06 |
| CA2765528A1 (en) | 2010-12-16 |
| CN102803652A (en) | 2012-11-28 |
| AU2010258643B2 (en) | 2016-05-26 |
| EA021075B1 (en) | 2015-03-31 |
| WO2010144700A3 (en) | 2011-03-10 |
| CN102803652B (en) | 2015-11-25 |
| GB2483594A (en) | 2012-03-14 |
| GB201121973D0 (en) | 2012-02-01 |
| US20100315900A1 (en) | 2010-12-16 |
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