WO2009100165A3 - High-purity fractionation of anthocyanins from fruits and vegetables - Google Patents
High-purity fractionation of anthocyanins from fruits and vegetables Download PDFInfo
- Publication number
- WO2009100165A3 WO2009100165A3 PCT/US2009/033127 US2009033127W WO2009100165A3 WO 2009100165 A3 WO2009100165 A3 WO 2009100165A3 US 2009033127 W US2009033127 W US 2009033127W WO 2009100165 A3 WO2009100165 A3 WO 2009100165A3
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- anthocyanins
- resin
- fruits
- vegetables
- recovery
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H17/00—Compounds containing heterocyclic radicals directly attached to hetero atoms of saccharide radicals
- C07H17/04—Heterocyclic radicals containing only oxygen as ring hetero atoms
- C07H17/06—Benzopyran radicals
- C07H17/065—Benzo[b]pyrans
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Saccharide Compounds (AREA)
Abstract
Disclosed is a method for separating anthocyanins depleted in phenolic mixture content from fruits or vegetables feedstock containing anthocyanins and phenolic mixtures. The first step is to contact the feedstock with a cation-exchange resin at low pH for a time period effective for the resin to selectively bind with the anthocyanins. Next, the non-bound phenolic mixture is separated from the resin for recovery. The bound resin is subjected to solvent wash to release the anthocyanins for recovery.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CA2714084A CA2714084C (en) | 2008-02-06 | 2009-02-05 | High-purity fractionation of anthocyanins from fruits and vegetables |
US12/847,106 US8575334B2 (en) | 2008-02-06 | 2010-07-30 | High-purity fractionation of anthocyanins from fruits and vegetables |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US6376308P | 2008-02-06 | 2008-02-06 | |
US61/063,763 | 2008-02-06 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US12/847,106 Continuation US8575334B2 (en) | 2008-02-06 | 2010-07-30 | High-purity fractionation of anthocyanins from fruits and vegetables |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2009100165A2 WO2009100165A2 (en) | 2009-08-13 |
WO2009100165A3 true WO2009100165A3 (en) | 2009-12-30 |
Family
ID=40952675
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2009/033127 WO2009100165A2 (en) | 2008-02-06 | 2009-02-05 | High-purity fractionation of anthocyanins from fruits and vegetables |
Country Status (2)
Country | Link |
---|---|
CA (1) | CA2714084C (en) |
WO (1) | WO2009100165A2 (en) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102443029A (en) * | 2010-10-01 | 2012-05-09 | 华中农业大学 | Column chromatography method for high-efficiency separation and purification of blood orange anthocyanins |
CN102321062A (en) * | 2011-06-08 | 2012-01-18 | 吉林市新科奇保健食品有限公司 | Separating, purifying and inspecting method of anthocyanin in blueberry wine dregs |
CN102875514B (en) * | 2012-09-25 | 2014-12-17 | 凯里学院 | Method for extracting and purifying anthocyanins from blueberry red leaves |
JP5981675B2 (en) | 2013-03-15 | 2016-08-31 | マース インコーポレーテッドMars Incorporated | Isolation method of blue anthocyanin fraction |
BR112015021395B1 (en) * | 2013-03-15 | 2021-10-26 | Mars, Incorporated | NATURAL BLUE DYES CONTAINING ANTHICIANINE |
CN103435589A (en) * | 2013-09-17 | 2013-12-11 | 北京林业大学 | Treatment method for enhancing stability of blueberry cyanidin |
CN104592326A (en) * | 2015-01-30 | 2015-05-06 | 南开大学 | Method for preparing high-purity anthocyanin from huckleberry crude extract by adopting absorption resin method |
CN108026382B (en) | 2015-06-30 | 2020-08-11 | Wm.雷格利 Jr.公司 | Acylated anthocyanin-based colorant compositions and methods of use thereof |
CN105175463B (en) * | 2015-08-31 | 2018-07-17 | 桂林茗兴生物科技有限公司 | The extraction process of Anthocyanin from Blueberry |
CN105153253B (en) * | 2015-08-31 | 2018-07-20 | 桂林茗兴生物科技有限公司 | The extraction process of anthocyanins pigment from purple sweet potato |
CN105061530B (en) * | 2015-08-31 | 2018-07-20 | 桂林茗兴生物科技有限公司 | The extraction process of red bayberry anthocyanin |
CN107973826B (en) * | 2017-12-07 | 2021-07-16 | 河南省林业科学研究院 | Method for separating and purifying plant leaf anthocyanin by adopting mixed adsorption resin |
DE102020214647A1 (en) * | 2020-11-20 | 2022-05-25 | DIL Deutsches Institut für Lebensmitteltechnik e.V. | Anthocyanin-containing extract powder and method of manufacture |
CN114380875B (en) * | 2021-07-31 | 2023-12-12 | 暨南大学 | Extraction and separation method of plant anthocyanin |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3963700A (en) * | 1974-07-01 | 1976-06-15 | University Patents, Inc. | Recovery of anthocyanin from plant sources |
US4452822A (en) * | 1982-05-17 | 1984-06-05 | United Vintners, Inc. | Extraction and intensification of anthocyanins from grape pomace and other material |
US4500556A (en) * | 1982-03-31 | 1985-02-19 | General Foods Corporation | Anthocyanin colorant from grape pomace |
US6180154B1 (en) * | 1999-04-28 | 2001-01-30 | The State Of Oregon Acting By And Through The State Board Of Higher Education On Behalf Of Oregon State University | Natural colorant from potato extract |
US6322695B1 (en) * | 1998-06-12 | 2001-11-27 | Waters Investments Limited | Ion exchange porous resins for solid phase extraction and chromatography |
-
2009
- 2009-02-05 CA CA2714084A patent/CA2714084C/en not_active Expired - Fee Related
- 2009-02-05 WO PCT/US2009/033127 patent/WO2009100165A2/en active Application Filing
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3963700A (en) * | 1974-07-01 | 1976-06-15 | University Patents, Inc. | Recovery of anthocyanin from plant sources |
US4500556A (en) * | 1982-03-31 | 1985-02-19 | General Foods Corporation | Anthocyanin colorant from grape pomace |
US4452822A (en) * | 1982-05-17 | 1984-06-05 | United Vintners, Inc. | Extraction and intensification of anthocyanins from grape pomace and other material |
US6322695B1 (en) * | 1998-06-12 | 2001-11-27 | Waters Investments Limited | Ion exchange porous resins for solid phase extraction and chromatography |
US6180154B1 (en) * | 1999-04-28 | 2001-01-30 | The State Of Oregon Acting By And Through The State Board Of Higher Education On Behalf Of Oregon State University | Natural colorant from potato extract |
Non-Patent Citations (1)
Title |
---|
MCCALLUM ET AL.: "Improved high performance liquid chromatographic separation of anthocyanin compounds from grapes using a novel mixed-mode ion-exchange reversed-phase column.", JOUMAL OF CHROMATOGRAPHY A, vol. 1148, 27 April 2007 (2007-04-27), pages 38 - 45 * |
Also Published As
Publication number | Publication date |
---|---|
WO2009100165A2 (en) | 2009-08-13 |
CA2714084A1 (en) | 2009-08-13 |
CA2714084C (en) | 2015-09-29 |
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