WO2009100165A3 - High-purity fractionation of anthocyanins from fruits and vegetables - Google Patents

High-purity fractionation of anthocyanins from fruits and vegetables Download PDF

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Publication number
WO2009100165A3
WO2009100165A3 PCT/US2009/033127 US2009033127W WO2009100165A3 WO 2009100165 A3 WO2009100165 A3 WO 2009100165A3 US 2009033127 W US2009033127 W US 2009033127W WO 2009100165 A3 WO2009100165 A3 WO 2009100165A3
Authority
WO
WIPO (PCT)
Prior art keywords
anthocyanins
resin
fruits
vegetables
recovery
Prior art date
Application number
PCT/US2009/033127
Other languages
French (fr)
Other versions
WO2009100165A2 (en
Inventor
Jian He
Maria Monica Giusti
Original Assignee
The Ohio State University Research Foundation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by The Ohio State University Research Foundation filed Critical The Ohio State University Research Foundation
Priority to CA2714084A priority Critical patent/CA2714084C/en
Publication of WO2009100165A2 publication Critical patent/WO2009100165A2/en
Publication of WO2009100165A3 publication Critical patent/WO2009100165A3/en
Priority to US12/847,106 priority patent/US8575334B2/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H17/00—Compounds containing heterocyclic radicals directly attached to hetero atoms of saccharide radicals
    • C07H17/04—Heterocyclic radicals containing only oxygen as ring hetero atoms
    • C07H17/06—Benzopyran radicals
    • C07H17/065—Benzo[b]pyrans

Abstract

Disclosed is a method for separating anthocyanins depleted in phenolic mixture content from fruits or vegetables feedstock containing anthocyanins and phenolic mixtures. The first step is to contact the feedstock with a cation-exchange resin at low pH for a time period effective for the resin to selectively bind with the anthocyanins. Next, the non-bound phenolic mixture is separated from the resin for recovery. The bound resin is subjected to solvent wash to release the anthocyanins for recovery.
PCT/US2009/033127 2008-02-06 2009-02-05 High-purity fractionation of anthocyanins from fruits and vegetables WO2009100165A2 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CA2714084A CA2714084C (en) 2008-02-06 2009-02-05 High-purity fractionation of anthocyanins from fruits and vegetables
US12/847,106 US8575334B2 (en) 2008-02-06 2010-07-30 High-purity fractionation of anthocyanins from fruits and vegetables

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US6376308P 2008-02-06 2008-02-06
US61/063,763 2008-02-06

Related Child Applications (1)

Application Number Title Priority Date Filing Date
US12/847,106 Continuation US8575334B2 (en) 2008-02-06 2010-07-30 High-purity fractionation of anthocyanins from fruits and vegetables

Publications (2)

Publication Number Publication Date
WO2009100165A2 WO2009100165A2 (en) 2009-08-13
WO2009100165A3 true WO2009100165A3 (en) 2009-12-30

Family

ID=40952675

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2009/033127 WO2009100165A2 (en) 2008-02-06 2009-02-05 High-purity fractionation of anthocyanins from fruits and vegetables

Country Status (2)

Country Link
CA (1) CA2714084C (en)
WO (1) WO2009100165A2 (en)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102443029A (en) * 2010-10-01 2012-05-09 华中农业大学 Column chromatography method for high-efficiency separation and purification of blood orange anthocyanins
CN102321062A (en) * 2011-06-08 2012-01-18 吉林市新科奇保健食品有限公司 Separating, purifying and inspecting method of anthocyanin in blueberry wine dregs
CN102875514B (en) * 2012-09-25 2014-12-17 凯里学院 Method for extracting and purifying anthocyanins from blueberry red leaves
CN105339437A (en) * 2013-03-15 2016-02-17 马斯公司 Natural blue anthocyanin-containing colorants
WO2014152417A2 (en) 2013-03-15 2014-09-25 Mars, Incorporated Method of isolating blue anthocyanin fractions
CN103435589A (en) * 2013-09-17 2013-12-11 北京林业大学 Treatment method for enhancing stability of blueberry cyanidin
CN104592326A (en) * 2015-01-30 2015-05-06 南开大学 Method for preparing high-purity anthocyanin from huckleberry crude extract by adopting absorption resin method
CA2990818C (en) 2015-06-30 2020-06-02 Mars, Incorporated Acylated anthocyanin based colourant composition and methods of use thereof
CN105175463B (en) * 2015-08-31 2018-07-17 桂林茗兴生物科技有限公司 The extraction process of Anthocyanin from Blueberry
CN105153253B (en) * 2015-08-31 2018-07-20 桂林茗兴生物科技有限公司 The extraction process of anthocyanins pigment from purple sweet potato
CN105061530B (en) * 2015-08-31 2018-07-20 桂林茗兴生物科技有限公司 The extraction process of red bayberry anthocyanin
CN107973826B (en) * 2017-12-07 2021-07-16 河南省林业科学研究院 Method for separating and purifying plant leaf anthocyanin by adopting mixed adsorption resin
DE102020214647A1 (en) * 2020-11-20 2022-05-25 DIL Deutsches Institut für Lebensmitteltechnik e.V. Anthocyanin-containing extract powder and method of manufacture
CN114380875B (en) * 2021-07-31 2023-12-12 暨南大学 Extraction and separation method of plant anthocyanin

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3963700A (en) * 1974-07-01 1976-06-15 University Patents, Inc. Recovery of anthocyanin from plant sources
US4452822A (en) * 1982-05-17 1984-06-05 United Vintners, Inc. Extraction and intensification of anthocyanins from grape pomace and other material
US4500556A (en) * 1982-03-31 1985-02-19 General Foods Corporation Anthocyanin colorant from grape pomace
US6180154B1 (en) * 1999-04-28 2001-01-30 The State Of Oregon Acting By And Through The State Board Of Higher Education On Behalf Of Oregon State University Natural colorant from potato extract
US6322695B1 (en) * 1998-06-12 2001-11-27 Waters Investments Limited Ion exchange porous resins for solid phase extraction and chromatography

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3963700A (en) * 1974-07-01 1976-06-15 University Patents, Inc. Recovery of anthocyanin from plant sources
US4500556A (en) * 1982-03-31 1985-02-19 General Foods Corporation Anthocyanin colorant from grape pomace
US4452822A (en) * 1982-05-17 1984-06-05 United Vintners, Inc. Extraction and intensification of anthocyanins from grape pomace and other material
US6322695B1 (en) * 1998-06-12 2001-11-27 Waters Investments Limited Ion exchange porous resins for solid phase extraction and chromatography
US6180154B1 (en) * 1999-04-28 2001-01-30 The State Of Oregon Acting By And Through The State Board Of Higher Education On Behalf Of Oregon State University Natural colorant from potato extract

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
MCCALLUM ET AL.: "Improved high performance liquid chromatographic separation of anthocyanin compounds from grapes using a novel mixed-mode ion-exchange reversed-phase column.", JOUMAL OF CHROMATOGRAPHY A, vol. 1148, 27 April 2007 (2007-04-27), pages 38 - 45 *

Also Published As

Publication number Publication date
CA2714084C (en) 2015-09-29
CA2714084A1 (en) 2009-08-13
WO2009100165A2 (en) 2009-08-13

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