WO2009099684A3 - Methods and apparatus for catalytic hydrothermal gasification of biomass - Google Patents
Methods and apparatus for catalytic hydrothermal gasification of biomass Download PDFInfo
- Publication number
- WO2009099684A3 WO2009099684A3 PCT/US2009/030099 US2009030099W WO2009099684A3 WO 2009099684 A3 WO2009099684 A3 WO 2009099684A3 US 2009030099 W US2009030099 W US 2009030099W WO 2009099684 A3 WO2009099684 A3 WO 2009099684A3
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- wet
- feedstock
- sulfur
- gasification
- biomass
- Prior art date
Links
- 238000002309 gasification Methods 0.000 title abstract 3
- 239000002028 Biomass Substances 0.000 title abstract 2
- 230000003197 catalytic effect Effects 0.000 title abstract 2
- 238000000034 method Methods 0.000 title 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 4
- 229910052717 sulfur Inorganic materials 0.000 abstract 4
- 239000011593 sulfur Substances 0.000 abstract 4
- 238000000926 separation method Methods 0.000 abstract 3
- 239000000356 contaminant Substances 0.000 abstract 2
- 239000010805 inorganic waste Substances 0.000 abstract 2
- 231100000572 poisoning Toxicity 0.000 abstract 2
- 230000000607 poisoning effect Effects 0.000 abstract 2
- 239000002244 precipitate Substances 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000000470 constituent Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000002638 heterogeneous catalyst Substances 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
- C10J3/00—Production of combustible gases containing carbon monoxide from solid carbonaceous fuels
- C10J3/72—Other features
- C10J3/78—High-pressure apparatus
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
- B09B—DISPOSAL OF SOLID WASTE NOT OTHERWISE PROVIDED FOR
- B09B3/00—Destroying solid waste or transforming solid waste into something useful or harmless
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
- B09B—DISPOSAL OF SOLID WASTE NOT OTHERWISE PROVIDED FOR
- B09B3/00—Destroying solid waste or transforming solid waste into something useful or harmless
- B09B3/40—Destroying solid waste or transforming solid waste into something useful or harmless involving thermal treatment, e.g. evaporation
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
- C10B53/00—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form
- C10B53/02—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form of cellulose-containing material
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L3/00—Gaseous fuels; Natural gas; Synthetic natural gas obtained by processes not covered by subclass C10G, C10K; Liquefied petroleum gas
- C10L3/06—Natural gas; Synthetic natural gas obtained by processes not covered by C10G, C10K3/02 or C10K3/04
- C10L3/08—Production of synthetic natural gas
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L9/00—Treating solid fuels to improve their combustion
- C10L9/08—Treating solid fuels to improve their combustion by heat treatments, e.g. calcining
- C10L9/086—Hydrothermal carbonization
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/18—Carbon
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
- B01J23/46—Ruthenium, rhodium, osmium or iridium
- B01J23/462—Ruthenium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
- B01J23/75—Cobalt
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/78—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with alkali- or alkaline earth metals
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
- C10J2300/00—Details of gasification processes
- C10J2300/09—Details of the feed, e.g. feeding of spent catalyst, inert gas or halogens
- C10J2300/0913—Carbonaceous raw material
- C10J2300/0916—Biomass
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
- C10J2300/00—Details of gasification processes
- C10J2300/09—Details of the feed, e.g. feeding of spent catalyst, inert gas or halogens
- C10J2300/0913—Carbonaceous raw material
- C10J2300/0916—Biomass
- C10J2300/0923—Sludge, e.g. from water treatment plant
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
- C10J2300/00—Details of gasification processes
- C10J2300/09—Details of the feed, e.g. feeding of spent catalyst, inert gas or halogens
- C10J2300/0953—Gasifying agents
- C10J2300/0973—Water
- C10J2300/0979—Water as supercritical steam
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
- Y02P20/145—Feedstock the feedstock being materials of biological origin
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Combustion & Propulsion (AREA)
- Environmental & Geological Engineering (AREA)
- Thermal Sciences (AREA)
- Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Processing Of Solid Wastes (AREA)
- Treatment Of Sludge (AREA)
- Catalysts (AREA)
Abstract
Continuous processing υf wet bi&upsi,-mass feedstock by catalytic hydrothermal gasification must address catalyst fouling and poisoning. One solution can involve heating (101) the wet bioraass with a h&egr,-atmg unit to a temperature sufficient for organic constituents in the feedstock to decompose, for precipitates of inorganic wastes to form, for preheating the wet feedstock in preparation for subsequent separation of sulfur contaminants, or combinations thereof. Treatment further includes separating (102) the precipitates out of the wet feedstock, removing sulfur contaminants (103), or both using a solids separation unit and a sulfur separation unit, respectiv ely. Having removed much of the inorganic wastes and the sulfur that can cause poisoning and fouling, the wet biomass feedstock can be exposed to the heterogeneous catalyst for gasification (104).
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US2497008P | 2008-01-31 | 2008-01-31 | |
US61/024,970 | 2008-01-31 | ||
US12/339,876 US8241605B2 (en) | 2008-01-31 | 2008-12-19 | Methods and apparatus for catalytic hydrothermal gasification of biomass |
US12/339,876 | 2008-12-19 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2009099684A2 WO2009099684A2 (en) | 2009-08-13 |
WO2009099684A3 true WO2009099684A3 (en) | 2010-01-21 |
Family
ID=40952615
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2009/030099 WO2009099684A2 (en) | 2008-01-31 | 2009-01-05 | Methods and apparatus for catalytic hydrothermal gasification of biomass |
Country Status (2)
Country | Link |
---|---|
US (1) | US8241605B2 (en) |
WO (1) | WO2009099684A2 (en) |
Families Citing this family (36)
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CN101460473A (en) | 2006-04-03 | 2009-06-17 | 药物热化学品公司 | Thermal extraction method and product |
US7905990B2 (en) | 2007-11-20 | 2011-03-15 | Ensyn Renewables, Inc. | Rapid thermal conversion of biomass |
US8608981B2 (en) | 2008-01-31 | 2013-12-17 | Battelle Memorial Institute | Methods for sulfate removal in liquid-phase catalytic hydrothermal gasification of biomass |
US8519203B2 (en) | 2010-02-17 | 2013-08-27 | Uop Llc | Low oxygen biomass-derived pyrolysis oils and methods for producing the same |
US20110284359A1 (en) | 2010-05-20 | 2011-11-24 | Uop Llc | Processes for controlling afterburn in a reheater and for controlling loss of entrained solid particles in combustion product flue gas |
US8499702B2 (en) | 2010-07-15 | 2013-08-06 | Ensyn Renewables, Inc. | Char-handling processes in a pyrolysis system |
CZ2010807A3 (en) * | 2010-11-08 | 2010-12-22 | Key@Group@Holding@@s@r@o | Organic waste treatment process, organic waste treatment device and use of treated products |
MY160306A (en) * | 2010-12-13 | 2017-02-28 | Exxonmobil Res & Eng Co | Phosphorus recovery from hydrothermal treatment of biomass |
US8704019B2 (en) * | 2010-12-13 | 2014-04-22 | Exxonmobil Research And Engineering Company | Catalyst recovery in hydrothermal treatment of biomass |
US8704020B2 (en) * | 2010-12-13 | 2014-04-22 | Exxonmobil Research And Engineering Company | Catalytic hydrothermal treatment of biomass |
US8624070B2 (en) | 2010-12-13 | 2014-01-07 | Exxonmobil Research And Engineering Company | Phosphorus recovery from hydrothermal treatment of biomass |
US8487148B2 (en) | 2010-12-13 | 2013-07-16 | Exxonmobil Research And Engineering Company | Hydrothermal treatment of biomass with heterogeneous catalyst |
US9441887B2 (en) | 2011-02-22 | 2016-09-13 | Ensyn Renewables, Inc. | Heat removal and recovery in biomass pyrolysis |
LT2718404T (en) | 2011-06-10 | 2021-05-10 | Steeper Energy Aps | Process for producing liquid hydrocarbons |
US9902908B2 (en) | 2011-06-10 | 2018-02-27 | Steeper Energy Aps | Process and apparatus for producing liquid hydrocarbon |
US9347005B2 (en) | 2011-09-13 | 2016-05-24 | Ensyn Renewables, Inc. | Methods and apparatuses for rapid thermal processing of carbonaceous material |
US10400175B2 (en) | 2011-09-22 | 2019-09-03 | Ensyn Renewables, Inc. | Apparatuses and methods for controlling heat for rapid thermal processing of carbonaceous material |
US10041667B2 (en) | 2011-09-22 | 2018-08-07 | Ensyn Renewables, Inc. | Apparatuses for controlling heat for rapid thermal processing of carbonaceous material and methods for the same |
US9044727B2 (en) | 2011-09-22 | 2015-06-02 | Ensyn Renewables, Inc. | Apparatuses and methods for controlling heat for rapid thermal processing of carbonaceous material |
US9109177B2 (en) | 2011-12-12 | 2015-08-18 | Ensyn Renewables, Inc. | Systems and methods for renewable fuel |
US9758728B2 (en) | 2012-06-08 | 2017-09-12 | Battelle Memorial Institute | Combined hydrothermal liquefaction and catalytic hydrothermal gasification system and process for conversion of biomass feedstocks |
US9670413B2 (en) | 2012-06-28 | 2017-06-06 | Ensyn Renewables, Inc. | Methods and apparatuses for thermally converting biomass |
IN2014DN09147A (en) * | 2012-07-03 | 2015-05-22 | Battelle Memorial Institute | |
CN102794294A (en) * | 2012-07-17 | 2012-11-28 | 浙江省长三角循环经济技术研究院 | Treatment process for biological wastes |
EP3321345A1 (en) | 2012-08-30 | 2018-05-16 | Steeper Energy ApS | Improved method for controlling cleaning of an apparatus for producing liquid hydrocarbons |
EP3868851A1 (en) | 2012-08-30 | 2021-08-25 | Steeper Energy ApS | Improved method for preparing shut down of process and equipment for producing liquid hydrocarbons |
EP2890768A1 (en) | 2012-08-30 | 2015-07-08 | Steeper Energy ApS | Improved method for preparing start up of process and equipment for producing liquid hydrocarbons |
ITRM20120548A1 (en) * | 2012-11-09 | 2014-05-10 | En E Lo Sviluppo Economico Sostenibile L | "PROCESS OF TREATMENT OF WATERS OF VEGETATION OF FRANTOI OLEARI BY REFORMING REACTIONS, AND ITS RELATION" |
EP3013922A4 (en) | 2013-06-26 | 2017-02-08 | Ensyn Renewables, Inc. | Systems and methods for renewable fuel |
US9404063B2 (en) | 2013-11-06 | 2016-08-02 | Battelle Memorial Institute | System and process for efficient separation of biocrudes and water in a hydrothermal liquefaction system |
AU2015255371B2 (en) | 2014-05-05 | 2019-12-05 | Steeper Energy Aps | Feed mixture for producing hydrocarbons |
DK3337966T3 (en) | 2015-08-21 | 2022-02-28 | Ensyn Renewables Inc | HEATING SYSTEM WITH LIQUID BIOMASS |
US10167430B2 (en) | 2016-06-28 | 2019-01-01 | Battelle Memorial Institute | Catalytic hydrothermal liquefaction for bio-oil production |
EP3565664A4 (en) | 2016-12-29 | 2020-08-05 | Ensyn Renewables, Inc. | Demetallization of liquid biomass |
EP4063470A1 (en) | 2021-03-24 | 2022-09-28 | Paul Scherrer Institut | Process for catalytic supercritical water gasification equipped with several sulfur removal steps |
FR3131922B1 (en) | 2022-01-14 | 2024-01-19 | Commissariat Energie Atomique | BIOMASS GASIFICATION PROCESS |
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- 2008-12-19 US US12/339,876 patent/US8241605B2/en active Active
-
2009
- 2009-01-05 WO PCT/US2009/030099 patent/WO2009099684A2/en active Application Filing
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Also Published As
Publication number | Publication date |
---|---|
WO2009099684A2 (en) | 2009-08-13 |
US8241605B2 (en) | 2012-08-14 |
US20100154305A1 (en) | 2010-06-24 |
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