WO2007035380A3 - An integrated lubricant upgrading process using once-through, hydrogen-containing treat gas - Google Patents

An integrated lubricant upgrading process using once-through, hydrogen-containing treat gas Download PDF

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Publication number
WO2007035380A3
WO2007035380A3 PCT/US2006/035724 US2006035724W WO2007035380A3 WO 2007035380 A3 WO2007035380 A3 WO 2007035380A3 US 2006035724 W US2006035724 W US 2006035724W WO 2007035380 A3 WO2007035380 A3 WO 2007035380A3
Authority
WO
WIPO (PCT)
Prior art keywords
hydrogen
once
treat gas
upgrading process
containing treat
Prior art date
Application number
PCT/US2006/035724
Other languages
French (fr)
Other versions
WO2007035380A2 (en
Inventor
Evan P Hyde
Ronald M Gould
Original Assignee
Exxonmobil Res & Eng Co
Evan P Hyde
Ronald M Gould
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Exxonmobil Res & Eng Co, Evan P Hyde, Ronald M Gould filed Critical Exxonmobil Res & Eng Co
Priority to CA002621476A priority Critical patent/CA2621476A1/en
Priority to AU2006292645A priority patent/AU2006292645A1/en
Priority to CN2006800341442A priority patent/CN101268171B/en
Priority to EP06803537A priority patent/EP1941007A2/en
Priority to JP2008531298A priority patent/JP5011300B2/en
Publication of WO2007035380A2 publication Critical patent/WO2007035380A2/en
Publication of WO2007035380A3 publication Critical patent/WO2007035380A3/en

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G65/00—Treatment of hydrocarbon oils by two or more hydrotreatment processes only
    • C10G65/02—Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only
    • C10G65/04—Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only including only refining steps
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G21/00—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • C10G45/04—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used
    • C10G45/06—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used containing nickel or cobalt metal, or compounds thereof
    • C10G45/08—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used containing nickel or cobalt metal, or compounds thereof in combination with chromium, molybdenum, or tungsten metals, or compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/58—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins
    • C10G45/60—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins characterised by the catalyst used
    • C10G45/64—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins characterised by the catalyst used containing crystalline alumino-silicates, e.g. molecular sieves
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G65/00—Treatment of hydrocarbon oils by two or more hydrotreatment processes only
    • C10G65/02—Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only
    • C10G65/04—Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only including only refining steps
    • C10G65/043—Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only including only refining steps at least one step being a change in the structural skeleton
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G67/00—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only
    • C10G67/02—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only plural serial stages only
    • C10G67/04—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only plural serial stages only including solvent extraction as the refining step in the absence of hydrogen
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G67/00—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only
    • C10G67/02—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only plural serial stages only
    • C10G67/04—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only plural serial stages only including solvent extraction as the refining step in the absence of hydrogen
    • C10G67/0409—Extraction of unsaturated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M177/00—Special methods of preparation of lubricating compositions; Chemical modification by after-treatment of components or of the whole of a lubricating composition, not covered by other classes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1022—Fischer-Tropsch products
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1074—Vacuum distillates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • C10G2300/202—Heteroatoms content, i.e. S, N, O, P
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/4018—Spatial velocity, e.g. LHSV, WHSV
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/4093—Catalyst stripping
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/44—Solvents
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/80—Additives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/10—Lubricating oil

Abstract

The invention relates to a process for producing lube oil basestocks involving solvent extracting a waxy feed to produce at least a lube oil boiling- range raffinate. The lube oil raffinate is hydrotreated to produce a hydrotreated raffÊnate, which is dewaxed and hydrofinished.
PCT/US2006/035724 2005-09-16 2006-09-13 An integrated lubricant upgrading process using once-through, hydrogen-containing treat gas WO2007035380A2 (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
CA002621476A CA2621476A1 (en) 2005-09-16 2006-09-13 An integrated lubricant upgrading process using once-through, hydrogen-containing treat gas
AU2006292645A AU2006292645A1 (en) 2005-09-16 2006-09-13 An integrated lubricant upgrading process using once-through, hydrogen-containing treat gas
CN2006800341442A CN101268171B (en) 2005-09-16 2006-09-13 An integrated lubricant upgrading process using once-through, hydrogen-containing treat gas
EP06803537A EP1941007A2 (en) 2005-09-16 2006-09-13 An integrated lubricant upgrading process using once-through, hydrogen-containing treat gas
JP2008531298A JP5011300B2 (en) 2005-09-16 2006-09-13 Integrated Lubricant Quality Improvement Method Using Once-through Hydrogen-Containing Treatment Gas

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US11/228,104 US20070062847A1 (en) 2005-09-16 2005-09-16 Integrated lubricant upgrading process using once-through, hydrogen-containing treat gas
US11/228,104 2005-09-16

Publications (2)

Publication Number Publication Date
WO2007035380A2 WO2007035380A2 (en) 2007-03-29
WO2007035380A3 true WO2007035380A3 (en) 2007-05-31

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ID=37758653

Family Applications (1)

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PCT/US2006/035724 WO2007035380A2 (en) 2005-09-16 2006-09-13 An integrated lubricant upgrading process using once-through, hydrogen-containing treat gas

Country Status (9)

Country Link
US (1) US20070062847A1 (en)
EP (1) EP1941007A2 (en)
JP (1) JP5011300B2 (en)
KR (1) KR20080048539A (en)
CN (1) CN101268171B (en)
AU (1) AU2006292645A1 (en)
CA (1) CA2621476A1 (en)
MY (1) MY143410A (en)
WO (1) WO2007035380A2 (en)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20110024328A1 (en) * 2009-07-31 2011-02-03 Chevron U.S.A. Inc. Distillate production in a hydrocarbon synthesis process.
KR101779605B1 (en) 2010-06-04 2017-09-19 에스케이이노베이션 주식회사 Method for producing base oil using deasphalt oil from reduced pressure distillation
US9074159B2 (en) 2010-10-06 2015-07-07 Uop Llc Process for improving a re-refined lube oil stream
US20120261307A1 (en) * 2011-04-13 2012-10-18 Exxonmobil Research And Engineering Company Integrated hydrotreating hydrodewaxing hydrofinishing process
EP2835418B1 (en) * 2012-03-30 2019-10-09 JX Nippon Oil & Energy Corporation Lubricant base oil
EP2835417B1 (en) * 2012-03-30 2018-10-17 JX Nippon Oil & Energy Corporation Lubricant base oil
CN104611056B (en) * 2015-02-11 2017-03-08 武汉凯迪工程技术研究总院有限公司 A kind of hydrotreating method of Low Temperature Fischer Tropsch synthetic product
CN106994365A (en) * 2016-01-26 2017-08-01 中国石油化工股份有限公司 A kind of catalyst for hydrogenation de-waxing preparation method and catalyst obtained by this method and its application

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WO1998001515A1 (en) * 1996-07-05 1998-01-15 Shell Internationale Research Maatschappij B.V. Process for the preparation of lubricating base oils
US5976354A (en) * 1997-08-19 1999-11-02 Shell Oil Company Integrated lube oil hydrorefining process
WO2004033597A2 (en) * 2002-10-08 2004-04-22 Exxonmobil Research And Engineering Company Process for preparing basestocks having high vi

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US3779897A (en) * 1971-12-29 1973-12-18 Texaco Inc Hydrotreating-hydrocracking process for manufacturing gasoline range hydrocarbons
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CN1225113A (en) * 1996-07-15 1999-08-04 切夫里昂美国公司 Layered catalyst system for lube oil hydroconversion
CA2374501A1 (en) * 1999-05-24 2000-11-30 The Lubrizol Corporation Mineral gear oils and transmission fluids
WO2003033630A1 (en) * 2001-10-16 2003-04-24 Shell Internationale Research Maatschappij B.V. Upgrading of pre-processed used oils
US6951605B2 (en) * 2002-10-08 2005-10-04 Exxonmobil Research And Engineering Company Method for making lube basestocks
US6787026B2 (en) * 2002-10-28 2004-09-07 Chevron U.S.A. Inc. Process for the production of high quality base oils
US20040154957A1 (en) * 2002-12-11 2004-08-12 Keeney Angela J. High viscosity index wide-temperature functional fluid compositions and methods for their making and use
US7597795B2 (en) * 2003-11-10 2009-10-06 Exxonmobil Research And Engineering Company Process for making lube oil basestocks
CN1317368C (en) * 2004-03-31 2007-05-23 中国石油化工股份有限公司 Method for preparing lubricating oil base oil

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WO1998001515A1 (en) * 1996-07-05 1998-01-15 Shell Internationale Research Maatschappij B.V. Process for the preparation of lubricating base oils
US5976354A (en) * 1997-08-19 1999-11-02 Shell Oil Company Integrated lube oil hydrorefining process
WO2004033597A2 (en) * 2002-10-08 2004-04-22 Exxonmobil Research And Engineering Company Process for preparing basestocks having high vi

Also Published As

Publication number Publication date
CN101268171B (en) 2012-02-01
EP1941007A2 (en) 2008-07-09
MY143410A (en) 2011-05-13
WO2007035380A2 (en) 2007-03-29
JP2009508993A (en) 2009-03-05
CN101268171A (en) 2008-09-17
JP5011300B2 (en) 2012-08-29
AU2006292645A1 (en) 2007-03-29
CA2621476A1 (en) 2007-03-29
US20070062847A1 (en) 2007-03-22
KR20080048539A (en) 2008-06-02

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