WO2007034501A3 - A novel process for the manufacture of 5-nonyl salicylaldoxime - Google Patents

A novel process for the manufacture of 5-nonyl salicylaldoxime Download PDF

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Publication number
WO2007034501A3
WO2007034501A3 PCT/IN2006/000003 IN2006000003W WO2007034501A3 WO 2007034501 A3 WO2007034501 A3 WO 2007034501A3 IN 2006000003 W IN2006000003 W IN 2006000003W WO 2007034501 A3 WO2007034501 A3 WO 2007034501A3
Authority
WO
WIPO (PCT)
Prior art keywords
aldehyde
nonyl
manufacture
novel process
catalyst mixture
Prior art date
Application number
PCT/IN2006/000003
Other languages
French (fr)
Other versions
WO2007034501A2 (en
Inventor
Suresh Bhikulal Paliwal
Mathur Vijay Bhagwanswarup Dr
Bhikulal Narsidas Mirani
Original Assignee
Star Orechem Internat Pvt Ltd
Suresh Bhikulal Paliwal
Mathur Vijay Bhagwanswarup Dr
Bhikulal Narsidas Mirani
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Star Orechem Internat Pvt Ltd, Suresh Bhikulal Paliwal, Mathur Vijay Bhagwanswarup Dr, Bhikulal Narsidas Mirani filed Critical Star Orechem Internat Pvt Ltd
Priority to AP2008004424A priority Critical patent/AP2376A/en
Priority to CN2006800434061A priority patent/CN101326148B/en
Publication of WO2007034501A2 publication Critical patent/WO2007034501A2/en
Publication of WO2007034501A3 publication Critical patent/WO2007034501A3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/32—Oximes
    • C07C251/34—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C251/48—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups bound to a carbon atom of a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)

Abstract

The invention relates to a process for producing 5-nonyl salicylaldoxime that comprises of converting nonyl phenol to a 5-nonyl aldehyde in a two-step reaction using a novel catalyst mixture, followed by the oximation of the said aldehyde using hydroxylamine sulphate, and that the said catalytic process of aldehyde production is the main invention, in that the effective use of the catalyst mixture helps the reaction proceed at a faster and controlled rate which leads to a higher yield of aldehyde, as a result of complete conversion of all the reactants to the final products.
PCT/IN2006/000003 2005-09-21 2006-01-02 A novel process for the manufacture of 5-nonyl salicylaldoxime WO2007034501A2 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
AP2008004424A AP2376A (en) 2005-09-21 2006-01-02 A novel process for the manufacture of 5-nonyl salicylaldoxime.
CN2006800434061A CN101326148B (en) 2005-09-21 2006-01-02 A novel process for the manufacture of 5-nonyl salicylaldoxime

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
IN1163/MUM/2005 2005-09-21
IN1163MU2005 2005-09-21

Publications (2)

Publication Number Publication Date
WO2007034501A2 WO2007034501A2 (en) 2007-03-29
WO2007034501A3 true WO2007034501A3 (en) 2007-06-14

Family

ID=37889260

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/IN2006/000003 WO2007034501A2 (en) 2005-09-21 2006-01-02 A novel process for the manufacture of 5-nonyl salicylaldoxime

Country Status (3)

Country Link
CN (1) CN101326148B (en)
AP (1) AP2376A (en)
WO (1) WO2007034501A2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104230748B (en) * 2014-11-04 2017-01-04 洛阳市三诺化工有限公司 A kind of synthesis technique of copper extractant 5-nonyl salicyl aldooxime

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101497576B (en) * 2009-03-12 2012-04-18 常州胜杰化工有限公司 Preparation method of 5-nonyl salicylaldoxime
EP3121161B1 (en) 2015-07-23 2018-03-07 S.P.C.M. Sa A method for the preparation of alkylsalicylaldehyde and alkylsalicylaldoxime, and use thereof
CN108083996A (en) * 2017-12-18 2018-05-29 甘肃省化工研究院 A kind of preparation method of 5- nonyls salicylide

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5763675A (en) * 1993-07-08 1998-06-09 Zeneca Limited Process for the preparation of 2-hydroxyarylaldehydes under reduced pressure

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB9217724D0 (en) * 1992-08-20 1992-09-30 Ici Plc Chemical process

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5763675A (en) * 1993-07-08 1998-06-09 Zeneca Limited Process for the preparation of 2-hydroxyarylaldehydes under reduced pressure

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104230748B (en) * 2014-11-04 2017-01-04 洛阳市三诺化工有限公司 A kind of synthesis technique of copper extractant 5-nonyl salicyl aldooxime

Also Published As

Publication number Publication date
WO2007034501A2 (en) 2007-03-29
CN101326148B (en) 2012-01-04
CN101326148A (en) 2008-12-17
AP2376A (en) 2012-03-07
AP2008004424A0 (en) 2008-04-30

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